CN111298750A - Continuous polyester preparation system for tensile renewable polyester staple fibers and operation method thereof - Google Patents

Continuous polyester preparation system for tensile renewable polyester staple fibers and operation method thereof Download PDF

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Publication number
CN111298750A
CN111298750A CN202010226653.7A CN202010226653A CN111298750A CN 111298750 A CN111298750 A CN 111298750A CN 202010226653 A CN202010226653 A CN 202010226653A CN 111298750 A CN111298750 A CN 111298750A
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China
Prior art keywords
fixedly connected
pipe
box
tensile
kettle cover
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CN202010226653.7A
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Chinese (zh)
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CN111298750B (en
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徐文学
张士灿
王建江
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Hangzhou Yongxing Plastic Chemical Fiber Co ltd
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Hangzhou Yongxing Plastic Chemical Fiber Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/10Particle separators, e.g. dust precipitators, using filter plates, sheets or pads having plane surfaces
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/88Replacing filter elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25DREFRIGERATORS; COLD ROOMS; ICE-BOXES; COOLING OR FREEZING APPARATUS NOT OTHERWISE PROVIDED FOR
    • F25D1/00Devices using naturally cold air or cold water
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28DHEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D7/00Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
    • F28D7/02Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being helically coiled
    • F28D7/024Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being helically coiled the conduits of only one medium being helically coiled tubes, the coils having a cylindrical configuration
    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05BELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B6/00Heating by electric, magnetic or electromagnetic fields
    • H05B6/64Heating using microwaves
    • H05B6/80Apparatus for specific applications
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00054Controlling or regulating the heat exchange system
    • B01J2219/00056Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058Temperature measurement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00092Tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718Type of compounds synthesised
    • B01J2219/0072Organic compounds
    • B01J2219/00736Non-biologic macromolecules, e.g. polymeric compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50Manufacturing or production processes characterised by the final manufactured product
    • Y02P70/62Manufacturing or production processes characterised by the final manufactured product related technologies for production or treatment of textile or flexible materials or products thereof, including footwear

Abstract

The invention discloses a continuous polyester preparation system for tensile renewable polyester staple fibers and an operation method thereof. This continuous process polyester preparation system of tensile renewable polyester staple fiber and operation method thereof, through set up the spiral condenser pipe in the condensing box, increased the area of contact with the air, make the radiating efficiency higher, the dual structure cooperation of cooling tower and condenser pipe has been saved, set up first fan simultaneously and accelerate the air flow, can further improve cooling rate, the heat that simultaneously still can take away the air is arranged to the inside heat preservation intracavity of kettle cover, make the inlayer keep a higher temperature, the cooling effect of outside air to the kettle cover has been avoided, and then the problem of the steam that has avoided distilling out at the internal surface condensation of kettle cover has improved distillation efficiency.

Description

Continuous polyester preparation system for tensile renewable polyester staple fibers and operation method thereof
Technical Field
The invention relates to the technical field of chemical equipment, in particular to a continuous polyester preparation system for tensile renewable polyester staple fibers and an operation method thereof.
Background
Polyester fiber, commonly known as "polyester", is a synthetic fiber obtained by spinning polyester formed by polycondensation of organic dibasic acid and dihydric alcohol, referred to as PET fiber for short, belongs to a high molecular compound, and is the first major variety of the current synthetic fiber in 1941. The polyester fiber has the advantages of good crease resistance and shape retention, high strength and elastic recovery capability. It is firm and durable, has the functions of resisting wrinkle, preventing ironing and preventing hair from sticking. Polyester (PET) fibers are synthetic fibers spun from a fiber-forming polymer formed by ester-linking of individual links in a macromolecular chain, and polyester is abbreviated to PET. The polyester fiber has a series of excellent properties, such as high breaking strength and elastic modulus, moderate rebound resilience, excellent heat setting effect, and good heat resistance and light resistance. Polyester fibers have a melting point of about 255 ℃ and a glass transition temperature of about 70 ℃, are stable in shape under a wide range of end-use conditions, and are widely used for clothing and industrial purposes because they have excellent resistance (e.g., resistance to organic solvents, soaps, detergents, bleaching solutions, and oxidizing agents) and corrosion resistance, and are stable to weak acids and alkalis.
The polyester staple fibers are manufactured by a continuous method, and the steps of esterification, distillation and the like are generally only carried out by using a simple reaction kettle, but the existing reaction kettles all have the same problem that the whole reaction kettle is generally made of metal and has higher cost, and the kettle cover is exposed in the air, so that the temperature is lower than the internal temperature of the reaction kettle even if the heat preservation effect is good, the problem that a small amount of steam is condensed on the inner surface can be caused, and the extraction efficiency is influenced; meanwhile, the prior art discloses an apparatus for preparing polyester polyol, which is also a reaction kettle for esterification distillation and other steps, as CN208786398U discloses, but the apparatus has the following problems: 1. the double cooling measures of the cooling tower and the condenser pipe are used, so that the steps and the cost are increased, and the condenser pipe is simply exposed in the air, so that the air fluidity is high, and the cooling effect is poor; 2. the device uses infrared electric heating cover, though can solve prior art inhomogeneous problem of heating, whole parcel cauldron body, the cost is higher.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a continuous polyester preparation system for tensile renewable polyester staple fibers and an operation method thereof, which solve the problems that the existing reaction kettle is generally made of metal, the cost is higher, and the kettle cover is exposed in the air, so that a small amount of steam is condensed on the inner surface to influence the extraction efficiency; meanwhile, the equipment for preparing polyester polyol disclosed in the prior art CN208786398U uses a cooling tower and a condenser tube for dual cooling measures, which increases the steps and the cost, and has low cooling efficiency, and the use of an infrared electric heating jacket also increases the cost.
(II) technical scheme
In order to achieve the purpose, the invention is realized by the following technical scheme: a continuous polyester preparation system for tensile renewable polyester staple fibers comprises a kettle body and a kettle cover, wherein the kettle body is fixedly connected with the kettle cover through bolts, the bottom of the kettle body is communicated with a discharge pipe, the discharge pipe is fixedly connected with a valve, the left side of the top of the kettle cover is communicated with a feed pipe in a penetrating manner, the right side of the top of the kettle cover is fixedly connected with a condensation box through a support pipe, the bottom of the condensation box is fixedly connected with an outlet pipe through a fixed sleeve, the bottom end of the outlet pipe penetrates through the kettle cover and extends to the lower part of the kettle cover, a spiral condensation pipe is fixedly connected inside the condensation box, one end of the spiral condensation pipe is fixedly connected with the inner surface of the fixed sleeve, the top of the condensation box is fixedly connected with a first fan, the kettle cover comprises an inner layer and an outer layer, a heat preservation cavity is arranged between the inner layer and the outer layer, the upper end and the, the left side at outer top is provided with the boss, and the top of boss rotates and is connected with the protective cover.
Preferably, the cauldron body is outer including ceramic inlayer and plastics, the outer internal surface spraying of plastics has the metallic coating, and fixedly connected with supporting shoe between metallic coating and the ceramic inlayer, the outer bottom of plastics is provided with the mounting box, and the inside fixedly connected with microwave heating device of mounting box, the part that the metallic coating is located microwave heating device top is seted up jaggedly.
Preferably, the mounting box all is provided with a plurality ofly with microwave heating device, and evenly distributed is in the bottom of the cauldron body, establish ties through the wire between the microwave heating device, the positive middle fixedly connected with control panel of the cauldron body, and control panel's bottom and front side microwave heating device's surperficial electric connection.
Preferably, the positive upper right corner fixedly connected with installation cover of the cauldron body, and the positive fixedly connected with heat dissipation box of installation cover, the intercommunication has the cooling tube between the right side at the heat dissipation box back and the plastics skin, the centre fixedly connected with of cooling tube internal surface keeps off the ring, and keeps off the top fixedly connected with elasticity heat insulation glued membrane of ring rear side, the outer positive upper left corner intercommunication of plastics has the blast pipe.
Preferably, the left side sliding connection of heat dissipation box internal surface has the filter box cover, and the internal surface joint of filter box cover has the filter, the filter is provided with the polylith, and passes through connecting rod fixed connection between the polylith filter, the right side fixedly connected with second fan of heat dissipation box inner chamber, and passes through wire electric connection between second fan and the control panel.
Preferably, the other end of the spiral condenser pipe runs through the lower right corner of the condenser box and extends to the outside of the condenser box, the other end of the spiral condenser pipe is rotatably connected with a bent pipe through a sealing sleeve, a supporting bracket is fixedly connected to the upper portion of the right side of the kettle body, a collecting barrel is arranged on the supporting bracket, and the bottom end of the bent pipe extends to the upper portion of the collecting barrel.
Preferably, the centre fixedly connected with motor at kettle cover top, and the surface of motor passes through wire and control panel's top electric connection, the bottom of motor output shaft runs through the kettle cover and extends to the inside of the cauldron body, shaft coupling fixedly connected with pivot is passed through to motor output shaft's bottom, the bottom of pivot is rotated and is connected with the bearing frame, and the bottom fixed connection of tripod and the internal surface of cauldron is passed through to the side of bearing frame, the surface of pivot is rotated through the hinge and is connected with the swing puddler, two liang of a set of longitudinal distribution are on the surface of pivot to the swing puddler.
Preferably, control panel's back fixedly connected with temperature detector, the rear end of temperature detector probe rod runs through the cauldron body and extends to the inside of the cauldron body, control panel includes treater, data contrast ware and feedback element, the output of treater respectively with the input electric connection of first fan, second fan, motor, microwave heating device and data contrast ware, the output of temperature detector and feedback element all with the input electric connection of treater, the output of data contrast ware and feedback element's input electric connection.
The invention also discloses an operation method of the continuous polyester preparation system for the tensile renewable polyester staple fibers, which specifically comprises the following steps:
the method comprises the following steps: connecting a control panel with a power supply, electrifying the equipment, starting a microwave heating device to emit microwaves to preheat the ceramic inner layer, adding the main raw material into the kettle body through a feeding pipe, starting a motor at the same time, driving a rotating shaft to rotate by the motor, further rotating a swinging stirring rod on the surface of the rotating shaft to stir the raw material, and sequentially and quantitatively adding auxiliary materials at a specified time;
step two: the temperature detector is started automatically in the heating process, the temperature of the materials in the kettle body is detected in real time, data are transmitted into the control panel, the processor in the control panel transmits the data to the data comparator and compares the data with a preset value, if the temperature is higher than the preset value, the temperature of the materials reaches the standard, steam begins to be generated and enters the spiral condenser pipe, a feedback element feeds back a signal to the processor, the processor controls the first fan to be started, air is blown into the condenser box, cold air condenses the steam in the spiral condenser pipe to enable the steam to be condensed into solution, the solution flows into the collecting cylinder through the bent pipe, the bent pipe rotates upwards after the collecting cylinder is fully collected, then the bent pipe is replaced, the bent pipe rotates downwards, the cold air carries away heat in the condensing process and then becomes hot air, and enters the heat preservation cavity in the kettle cover through the supporting pipe, keeping the interior in a high-temperature state, and finally ejecting the protective cover from the boss to discharge;
step three: in the reaction process, if the reaction temperature needs to be reduced, the second fan can be started, the second fan pumps cold air into the outside, the cold air enters the heat dissipation pipe after dust is filtered by the filter plate, the elastic heat insulation adhesive film is pushed away to enter the cavity between the ceramic inner layer and the plastic outer layer, heat in the elastic heat insulation adhesive film is taken away, and the elastic heat insulation adhesive film is discharged into the heat exchanger from the exhaust pipe or is connected to other equipment to be heated.
Preferably, in the third step, the filter box sleeve needs to be drawn out periodically, and the internal filter plate needs to be taken out for cleaning.
(III) advantageous effects
The invention provides a continuous polyester preparation system for tensile renewable polyester staple fibers and an operation method thereof. Compared with the prior art, the method has the following beneficial effects:
(1) the continuous polyester preparation system of the tensile renewable polyester staple fiber and the operation method thereof are characterized in that a condensing box is fixedly connected to the right side of the top of a kettle cover through a supporting tube, an air outlet pipe is fixedly connected to the bottom of the condensing box through a fixing sleeve, the bottom end of the air outlet pipe penetrates through the kettle cover and extends to the lower part of the kettle cover, a spiral condensing tube is fixedly connected to the inside of the condensing box, one end of the spiral condensing tube is fixedly connected with the inner surface of the fixing sleeve, a first fan is fixedly connected to the top of the condensing box, the kettle cover comprises an inner layer and an outer layer, a heat preservation cavity is arranged between the inner layer and the outer layer, the upper end and the lower end of the supporting tube are respectively communicated with the condensing box and the heat preservation cavity, a boss is arranged on the left side of the top of the outer layer, a protective cover is rotatably connected to, the double-structure cooperation of a cooling tower and a condenser pipe is omitted, the first fan is arranged to accelerate air flow, cooling speed can be further improved, meanwhile, heat brought away by air can be discharged into a heat preservation cavity inside the kettle cover, the inner layer is kept at a higher temperature, the cooling effect of external air on the kettle cover is avoided, the problem that distilled steam condenses on the inner surface of the kettle cover is avoided, and distillation efficiency is improved.
(2) The continuous polyester preparation system for the tensile renewable polyester short fibers and the operation method thereof are characterized in that a kettle body comprises a ceramic inner layer and a plastic outer layer, a metal coating is sprayed on the inner surface of the plastic outer layer, a supporting block is fixedly connected between the metal coating and the ceramic inner layer, a mounting box is arranged at the bottom of the plastic outer layer, a microwave heating device is fixedly connected inside the mounting box, a gap is formed in the part, above the microwave heating device, of the metal coating, a plurality of mounting boxes and the microwave heating device are arranged and uniformly distributed at the bottom of the kettle body, the microwave heating devices are connected in series through a lead, a control panel is fixedly connected in the middle of the front side of the kettle body, the bottom of the control panel is electrically connected with the surface of the front side microwave heating device, the kettle body is constructed by arranging the ceramic inner layer and the plastic outer layer as main bodies, the cost is relatively reduced, and the metal coating on the inner side of the plastic outer layer can, the energy loss is few can be better heat, and use three to four less microwave heating device can realize comprehensive heating, and the cost is lower.
(3) The continuous polyester preparation system of the tensile renewable polyester staple fiber and the operation method thereof are characterized in that an installation sleeve is fixedly connected to the right upper corner of the front surface of a kettle body, a heat dissipation box is fixedly connected to the front surface of the installation sleeve, a heat dissipation pipe is communicated between the right side of the back surface of the heat dissipation box and a plastic outer layer, a baffle ring is fixedly connected to the middle of the inner surface of the heat dissipation pipe, an elastic heat insulation adhesive film is fixedly connected to the top of the rear side of the baffle ring, an exhaust pipe is communicated with the left upper corner of the front surface of the plastic outer layer, a filtering box sleeve is slidably connected to the left side of the inner surface of the heat dissipation box, a filter plate is clamped on the inner surface of the filtering box sleeve, a plurality of filter plates are arranged, the plurality of filter plates are fixedly connected through connecting rods, a second fan is fixedly connected to the right side of the inner cavity of the, can dispel the heat fast to the pottery inlayer to internal material rapid cooling, accurate assurance heating temperature is favorable to improving the quality of product, and the second fan is close to in tangential to the cavity in the blow cold wind, makes the air can be spiral flow, dispels the heat more fast more even, the filter that sets up simultaneously still can avoid bringing into the dust to the cavity inside, does not worry the problem of pollution, convenient to use.
(4) This continuous process polyester preparation system of tensile renewable polyester staple fiber and operation method thereof, through passing through shaft coupling fixedly connected with pivot in the bottom of motor output shaft, the bottom of pivot is rotated and is connected with the bearing frame, and the bottom fixed connection of tripod and cauldron internal surface is passed through to the side of bearing frame, the surface of pivot is rotated through the hinge and is connected with the swing puddler, two liang of swing puddlers are a set of longitudinal distribution in the surface of pivot, set up rotatable swing puddler on the pivot surface, under different rotational speeds, the centrifugal force that the swing puddler received is different, and then the range that leads to unfolding is different, can be more comprehensive stir the reactant.
Drawings
FIG. 1 is a front view of the structure of the present invention;
FIG. 2 is a cross-sectional view of the kettle cover and condenser box structure of the present invention;
FIG. 3 is an enlarged view of a portion of the invention at A in FIG. 1;
FIG. 4 is a sectional view of a partial structure of the autoclave body according to the present invention;
FIG. 5 is a bottom view of the kettle structure of the present invention;
FIG. 6 is a top view of the internal structure of the mounting sleeve of the present invention;
FIG. 7 is a cross-sectional view of the heat sink box structure of the present invention;
FIG. 8 is a front view of the shaft and oscillating agitator bar arrangement of the present invention;
FIG. 9 is a side view of the control panel and temperature probe configuration of the present invention;
fig. 10 is a schematic block diagram of the system of the present invention.
In the figure, 1-kettle body, 101-ceramic inner layer, 102-plastic outer layer, 103-metal plating layer, 104-supporting block, 105-mounting box, 2-kettle cover, 201-inner layer, 202-outer layer, 203-heat preservation cavity, 204-boss, 205-protective cover, 3-discharging pipe, 4-feeding pipe, 5-supporting pipe, 6-condensation box, 7-gas outlet pipe, 8-spiral condensation pipe, 9-fixing sleeve, 10-first fan, 11-microwave heating device, 12-control panel, 13-mounting sleeve, 14-heat dissipation box, 15-heat dissipation pipe, 16-baffle ring, 17-elastic heat insulation film, 18-gas outlet pipe, 19-filtering box sleeve, 20-filtering plate, 21-connecting rod, 22-a second fan, 23-a sealing sleeve, 24-a bent pipe, 25-a supporting bracket, 26-a collecting barrel, 27-a motor, 28-a rotating shaft, 29-a bearing seat, 30-a swinging stirring rod, 31-a temperature detector, 32-a processor, 33-a data comparator and 34-a feedback element.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1 to 10, an embodiment of the present invention provides a technical solution: a continuous polyester preparation system of tensile renewable polyester staple fibers comprises a kettle body 1 and a kettle cover 2, wherein the kettle body 1 is fixedly connected with the kettle cover 2 through bolts, the kettle body 1 comprises a ceramic inner layer 101 and a plastic outer layer 102, a metal coating 103 is sprayed on the inner surface of the plastic outer layer 102, a supporting block 104 is fixedly connected between the metal coating 103 and the ceramic inner layer 101, a mounting box 105 is arranged at the bottom of the plastic outer layer 102, a microwave heating device 11 is fixedly connected inside the mounting box 105, a gap is arranged at the part of the metal coating 103 above the microwave heating device 11, the mounting box 105 and the microwave heating device 11 are both provided with a plurality of parts and are uniformly distributed at the bottom of the kettle body 1, the microwave heating devices 11 are connected in series through a wire, a control panel 12 is fixedly connected in the middle of the front of the kettle body 1, and the bottom of the control panel 12 is electrically connected with the surface of the front microwave heating device 11, the kettle body 1 is constructed by arranging the ceramic inner layer 101 and the plastic outer layer 102 as main bodies, the cost is relatively reduced, the metal plating layer 103 on the inner side of the plastic outer layer 102 can prevent the dissipation of microwaves emitted by the microwave heating devices 11, the heating can be better realized with less energy loss, the comprehensive heating can be realized by using three to four smaller microwave heating devices 11, the cost is lower, the back surface of the control panel 12 is fixedly connected with the temperature detector 31, the temperature detector 31 needs to resist high temperature, the rear end of the probe rod of the temperature detector 31 penetrates through the kettle body 1 and extends into the kettle body 1, the control panel 12 comprises a processor 32, a data comparator 33 and a feedback element 34, the processor 32 is an ARM9 series processor, the output end of the processor 32 is respectively electrically connected with the input ends of the first fan 10, the second fan 22, the motor 27, the microwave heating devices 11 and the data comparator 33, the output ends of the temperature detector 31 and the feedback element 34 are electrically connected with the input end of the processor 32, the output end of the data comparator 33 is electrically connected with the input end of the feedback element 34, the right upper corner of the front surface of the kettle body 1 is fixedly connected with the mounting sleeve 13, the front surface of the mounting sleeve 13 is fixedly connected with the heat dissipation box 14, the left side of the inner surface of the heat dissipation box 14 is slidably connected with the filtering box sleeve 19, the inner surface of the filtering box sleeve 19 is clamped with the filtering plate 20, the filtering plate 20 is provided with a plurality of filtering plates 20 which are fixedly connected through the connecting rod 21, the right side of the inner cavity of the heat dissipation box 14 is fixedly connected with the second fan 22, the second fan 22 is electrically connected with the control panel 12 through a conducting wire, and the second fan 22 blows cold air into the cavity between the ceramic inner layer 101 and the plastic outer layer 102, so that the ceramic inner layer, the accurate heating temperature of grasping, help to improve the quality of the products, and the second fan 22 blows the cold wind to the cavity nearly tangentially, make the air present the spiral flow, dispel the heat more rapidly and more evenly, the filter 20 set up at the same time can also avoid bringing the dust into the cavity, does not worry about the problem of polluting, easy to use, there is the radiating pipe 15 between plastic skin 102 and the right side of the back of the radiating box 14, the middle of the internal surface of the radiating pipe 15 is fixedly connected with the retaining ring 16, and the top of the rear side of the retaining ring 16 is fixedly connected with elastic heat insulation jelly membrane 17, the elastic heat insulation jelly membrane 17 is similar to the one-way valve flap, naturally fall under the normal condition, can reduce the heat loss in the cavity between ceramic inner layer 101 and plastic skin 102, the front upper left corner of the plastic skin 102 is communicated with the exhaust pipe 18, the middle fixedly connected with electrical machinery 27 of the top of the kettle cover 2, and the surface of the, the bottom end of an output shaft of a motor 27 penetrates through the kettle cover 2 and extends into the kettle body 1, the bottom end of the output shaft of the motor 27 is fixedly connected with a rotating shaft 28 through a coupler, the bottom end of the rotating shaft 28 is rotatably connected with a bearing seat 29, the side surface of the bearing seat 29 is fixedly connected with the bottom of the inner surface of the kettle body 1 through a tripod, the surface of the rotating shaft 28 is rotatably connected with a swinging stirring rod 30 through a hinge, the swinging stirring rods 30 are longitudinally distributed on the surface of the rotating shaft 28 in pairs, the surface of the rotating shaft 28 is provided with the rotatable swinging stirring rod 30, the swinging stirring rod 30 is subjected to different centrifugal forces at different rotating speeds, and further the unfolding amplitude is different, so that reactants can be more comprehensively stirred, the bottom of the kettle body 1 is communicated with a discharge pipe 3, a valve is fixedly connected on the discharge pipe 3, the left side of the top of the kettle cover 2 is communicated with a, and the bottom of the condensing box 6 is fixedly connected with an air outlet pipe 7 through a fixing sleeve 9, the bottom end of the air outlet pipe 7 penetrates through the kettle cover 2 and extends to the lower part of the kettle cover 2, the inside of the condensing box 6 is fixedly connected with a spiral condensing pipe 8, one end of the spiral condensing pipe 8 is fixedly connected with the inner surface of the fixing sleeve 9, the other end of the spiral condensing pipe 8 penetrates through the lower right corner of the condensing box 6 and extends to the outside of the condensing box 6, the other end of the spiral condensing pipe 8 is rotatably connected with a bent pipe 24 through a sealing sleeve 23, a supporting bracket 25 is fixedly connected above the right side of the kettle body 1, a collecting cylinder 26 is arranged on the supporting bracket 25, the bottom end of the bent pipe 24 extends to the upper part of the collecting cylinder 26, the top of the condensing box 6 is fixedly connected with a first fan 10, the kettle cover 2 comprises an inner layer 201 and an outer layer 202, a heat preservation cavity 203 is arranged between the, the left side at outer 202 top is provided with boss 204, and the top of boss 204 is rotated and is connected with protective cover 205, through set up spiral condenser pipe 8 in condensing box 6, increased the area of contact with the air, it is higher to make the radiating efficiency, the dual structure cooperation of cooling tower and condenser pipe has been saved, set up first fan 10 simultaneously and come the air flow with higher speed, can further improve cooling rate, still can arrange the heat that the air was taken away to the inside heat preservation chamber 203 of kettle cover 2 simultaneously, make inlayer 201 keep a higher temperature, the cooling effect of outside air to kettle cover 2 has been avoided, and then the problem of the steam that has avoided distilling out at the 2 internal surfaces of kettle cover condense, the distillation efficiency is improved.
The invention also discloses an operation method of the continuous polyester preparation system for the tensile renewable polyester staple fibers, which specifically comprises the following steps:
the method comprises the following steps: connecting a control panel 12 with a power supply to electrify the equipment, starting a microwave heating device 11 to emit microwaves to preheat the ceramic inner layer 101, adding the main raw materials into the kettle body 1 through a feeding pipe 4, starting a motor 27 at the same time, driving a rotating shaft 28 to rotate by the motor 27, further rotating a swinging stirring rod 30 on the surface of the rotating shaft to stir the raw materials, and sequentially and quantitatively adding auxiliary materials at a specified time;
step two: the temperature detector 31 is started automatically in the heating process, the temperature of the materials in the kettle body 1 is detected in real time, the data are transmitted into the control panel 12, the processor 32 in the control panel 12 transmits the data to the data comparator 33, the data are compared with preset specified values, if the temperature is higher than the preset specified values, the temperature of the materials reaches the standard, steam starts to be generated and enters the spiral condensation pipe 8, a feedback element 34 feeds back a signal to the processor 32 at the moment, the processor 32 controls the first fan 10 to be started, air is blown into the condensation box 6, cold air condenses the steam in the spiral condensation pipe 8, so that the steam is condensed into solution and flows into the collection cylinder 26 through the bent pipe 24, when the collection cylinder 26 is fully collected, the bent pipe 24 is rotated upwards, then an empty collection cylinder 26 is replaced, the bent pipe 24 is rotated downwards, the cold air carries away heat in the condensation process and then becomes hot air, the mixture enters a heat preservation cavity 203 in the kettle cover 2 through a support pipe 5, the interior is kept in a high-temperature state, and finally the protection cover 205 is jacked from a boss 204 to be discharged;
step three: in the reaction process, if the reaction temperature needs to be reduced, the second fan 22 can be started, the second fan 22 pumps cold air into the outside, the cold air enters the radiating pipe 15 after being filtered by the filter plate 20 to remove dust (the filter box sleeve 19 needs to be periodically pumped out and the internal filter plate 20 needs to be taken out for cleaning), the elastic heat insulation adhesive film 17 can enter the cavity between the ceramic inner layer 101 and the plastic outer layer 102 after being pushed away, the heat in the elastic heat insulation adhesive film is taken away, and the elastic heat insulation adhesive film is discharged into a heat exchanger from the exhaust pipe 18 or is connected to other equipment needing to be heated.
And those not described in detail in this specification are well within the skill of those in the art.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (10)

1. The utility model provides a continuous process polyester preparation system of polyester staple fiber can be regenerated in tensile, includes the cauldron body (1) and kettle cover (2), and through bolt fixed connection between the cauldron body (1) and kettle cover (2), the bottom intercommunication of the cauldron body (1) has discharging pipe (3), and fixedly connected with valve on discharging pipe (3), the left side at kettle cover (2) top is run through the intercommunication and is had inlet pipe (4), its characterized in that: the right side of the top of the kettle cover (2) is fixedly connected with a condensing box (6) through a supporting pipe (5), the bottom of the condensing box (6) is fixedly connected with an air outlet pipe (7) through a fixing sleeve (9), the bottom end of the air outlet pipe (7) penetrates through the kettle cover (2) and extends to the lower part of the kettle cover (2), the inner part of the condensing box (6) is fixedly connected with a spiral condensing pipe (8), one end of the spiral condensing pipe (8) is fixedly connected with the inner surface of the fixing sleeve (9), the top of the condensing box (6) is fixedly connected with a first fan (10), the kettle cover (2) comprises an inner layer (201) and an outer layer (202), a heat preservation cavity (203) is arranged between the inner layer (201) and the outer layer (202), the upper end and the lower end of the supporting pipe (5) are respectively communicated with the condensing box (6) and the heat preservation cavity (203), the left side of the top of the outer layer (, and the top of the boss (204) is rotatably connected with a protective cover (205).
2. The continuous-process polyester production system of tensile renewable polyester staple fibers of claim 1, wherein: the kettle body (1) comprises a ceramic inner layer (101) and a plastic outer layer (102), wherein a metal coating (103) is sprayed on the inner surface of the plastic outer layer (102), a supporting block (104) is fixedly connected between the metal coating (103) and the ceramic inner layer (101), a mounting box (105) is arranged at the bottom of the plastic outer layer (102), a microwave heating device (11) is fixedly connected to the inside of the mounting box (105), and a notch is formed in the part, located above the microwave heating device (11), of the metal coating (103).
3. The continuous-process polyester production system of tensile renewable polyester staple fibers of claim 2, wherein: mounting box (105) and microwave heating device (11) all are provided with a plurality ofly, and evenly distributed is in the bottom of the cauldron body (1), establish ties through the wire between microwave heating device (11), the positive middle fixedly connected with control panel (12) of the cauldron body (1), and the bottom of control panel (12) and the surperficial electric connection of front side microwave heating device (11).
4. The continuous-process polyester production system of tensile renewable polyester staple fibers of claim 2, wherein: cauldron body (1) positive upper right corner fixedly connected with installation cover (13), and the positive fixedly connected with heat dissipation box (14) of installation cover (13), the intercommunication has cooling tube (15) between the right side at the heat dissipation box (14) back and plastics skin (102), the centre fixedly connected with of cooling tube (15) internal surface keeps off ring (16), and keeps off top fixedly connected with elasticity heat insulation glued membrane (17) of ring (16) rear side, the positive upper left corner intercommunication of plastics skin (102) has blast pipe (18).
5. The continuous polyester production system of the tensile renewable polyester staple fibers of claim 4, wherein: the left side sliding connection of heat dissipation box (14) internal surface has filtration box cover (19), and the internal surface joint of filtering box cover (19) has filter (20), filter (20) are provided with the polylith, and pass through connecting rod (21) fixed connection between polylith filter (20), the right side fixedly connected with second fan (22) of heat dissipation box (14) inner chamber, and pass through wire electric connection between second fan (22) and control panel (12).
6. The continuous-process polyester production system of tensile renewable polyester staple fibers of claim 1, wherein: the other end of spiral condenser pipe (8) runs through the lower right corner of condenser box (6) and extends to the outside of condenser box (6), and the other end of spiral condenser pipe (8) rotates through seal cover (23) and is connected with return bend (24), top fixedly connected with support bracket (25) on the cauldron body (1) right side, be provided with on support bracket (25) collecting vessel (26), and the bottom of return bend (24) extends to the top of collecting vessel (26).
7. The continuous-process polyester production system of tensile renewable polyester staple fibers of claim 1, wherein: the middle fixedly connected with motor (27) at kettle cover (2) top, and the surface of motor (27) passes through the top electric connection of wire and control panel (12), the bottom of motor (27) output shaft runs through kettle cover (2) and extends to the inside of the cauldron body (1), shaft coupling fixedly connected with pivot (28) is passed through to the bottom of motor (27) output shaft, the bottom of pivot (28) is rotated and is connected with bearing frame (29), and the bottom fixed connection of tripod and cauldron body (1) internal surface is passed through to the side of bearing frame (29), the surface of pivot (28) is rotated through the hinge and is connected with swing puddler (30), two liang of vertical distributions in the surface of pivot (28) of swing puddler (30).
8. The continuous-process polyester production system of tensile renewable polyester staple fibers of claim 3, wherein: the back fixedly connected with temperature detector (31) of control panel (12), the rear end of temperature detector (31) probe rod runs through the cauldron body (1) and extends to the inside of the cauldron body (1), control panel (12) include treater (32), data contrast ware (33) and feedback element (34), the output of treater (32) respectively with first fan (10), second fan (22), motor (27), microwave heating device (11) and the input electric connection of data contrast ware (33), the output of temperature detector (31) and feedback element (34) all with the input electric connection of treater (32), the output of data contrast ware (33) and the input electric connection of feedback element (34).
9. An operation method of a continuous polyester preparation system for tensile renewable polyester staple fibers is characterized in that: the method specifically comprises the following steps:
the method comprises the following steps: connecting a control panel (12) with a power supply, powering on the equipment, starting a microwave heating device (11) to emit microwaves, preheating a ceramic inner layer (101), adding a main raw material into a kettle body (1) through a feeding pipe (4), starting a motor (27), driving a rotating shaft (28) to rotate by the motor (27), further rotating a swinging stirring rod (30) on the surface of the rotating shaft to stir the raw material, and sequentially and quantitatively adding auxiliary materials at a specified time;
step two: the temperature detector (31) is started automatically in the heating process, the temperature of the materials in the kettle body (1) is detected in real time, data are transmitted into the control panel (12), the processor (32) in the control panel (12) transmits the data to the data comparator (33), the data are compared with preset values, if the temperature is higher than the preset values, the temperature of the materials reaches the standard, steam is generated and enters the spiral condensation pipe (8), a feedback element (34) feeds back a signal to the processor (32), the processor (32) controls the first fan (10) to be started, air is blown into the condensation box (6), cold air condenses the steam in the spiral condensation pipe (8), the steam is condensed into solution and flows into the collection cylinder (26) through the bent pipe (24), and the bent pipe (24) is rotated upwards after the collection cylinder (26) is fully collected, then an empty collecting cylinder (26) is replaced, the elbow (24) is turned down, cold air carries away heat in the condensation process and then becomes hot air, the hot air enters a heat preservation cavity (203) in the kettle cover (2) through the supporting tube (5), the interior is kept in a high-temperature state, and finally the protecting cover (205) is jacked from the boss (204) to be discharged;
step three: in the reaction process, if the reaction temperature needs to be reduced, the second fan (22) can be started, the second fan (22) pumps outside air into the cooling air, the air enters the radiating pipe (15) after being filtered by the filter plate (20), the elastic heat insulation adhesive film (17) is pushed away to enter the cavity between the ceramic inner layer (101) and the plastic outer layer (102), and the heat in the cavity is carried away and is discharged into the heat exchanger from the exhaust pipe (18) or is connected to other equipment to be heated.
10. The method of claim 9 for operating a continuous polyester production system for tensile renewable polyester staple fibers, wherein the method comprises the steps of: in the third step, the filter box sleeve (19) is periodically drawn out and the internal filter plate (20) is taken out for cleaning.
CN202010226653.7A 2020-03-27 2020-03-27 Continuous polyester preparation system for tensile renewable polyester staple fibers and operation method thereof Active CN111298750B (en)

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