CN207930911U - A kind of 6 black of polyamide fibre slice continuous production device - Google Patents

A kind of 6 black of polyamide fibre slice continuous production device Download PDF

Info

Publication number
CN207930911U
CN207930911U CN201820069813.XU CN201820069813U CN207930911U CN 207930911 U CN207930911 U CN 207930911U CN 201820069813 U CN201820069813 U CN 201820069813U CN 207930911 U CN207930911 U CN 207930911U
Authority
CN
China
Prior art keywords
reactor
tank
poly
black
polyamide fibre
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201820069813.XU
Other languages
Chinese (zh)
Inventor
吉增明
朱维兵
尹彦军
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangsu Haiyang Polyamide New Material Co Ltd
Original Assignee
Jiangsu Haiyang Polyamide New Material Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiangsu Haiyang Polyamide New Material Co Ltd filed Critical Jiangsu Haiyang Polyamide New Material Co Ltd
Priority to CN201820069813.XU priority Critical patent/CN207930911U/en
Application granted granted Critical
Publication of CN207930911U publication Critical patent/CN207930911U/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Polyamides (AREA)
  • Reinforced Plastic Materials (AREA)

Abstract

The utility model provides a kind of 6 black of polyamide fibre slice continuous production device, including:Mixing tank, preceding poly- reactor, rear poly- reactor, pelleter, extraction tower, drying tower, finished product storage tank, evaporator, cracking reaction kettle, feed tank, blend tank; the mixing tank is sequentially connected preceding poly- reactor, rear poly- reactor, pelleter, extraction tower, drying tower, finished product storage tank; the extraction tower is also connected with evaporator end; the cracking reaction kettle is separately connected evaporator outlet end and mixing tank, and the feed tank is separately connected blend tank and preceding poly- reactor.The utility model has the beneficial effect that:1)Continuous production, production efficiency is high, and low energy consumption;2)6 black of polyamide fibre slice can be produced;3)Extra raw material can reuse, non-environmental-pollution.

Description

A kind of 6 black of polyamide fibre slice continuous production device
Technical field
The utility model is related to polyamide fibre field, more particularly to a kind of 6 black of polyamide fibre is sliced continuous production device.
Background technology
The chemico-physical properties and nylon66 fiber of polyamide fibre 6 are much like, however, its fusing point is relatively low, and Process temperature ranges It is very wide.Its impact resistance and antilysis is got well than nylon-66 plastic, but hygroscopicity is also stronger.
Current chinlon 6 section production technology is various, but generally interval metaplasia is used to produce, low production efficiency, and energy consumption is higher;This The production technology of 6 black of outer polyamide fibre slice is also more rare at home.
Invention content
The purpose of this utility model is that proposing a kind of 6 black of polyamide fibre slice continuous production device, there is production efficiency The advantages that height, non-environmental-pollution.
To achieve the goals above, the utility model provides a kind of 6 black of polyamide fibre slice continuous production device, including: Mixing tank, preceding poly- reactor, rear poly- reactor, pelleter, extraction tower, drying tower, finished product storage tank, evaporator, cracking reaction kettle, Feed tank, blend tank, the mixing tank be sequentially connected preceding poly- reactor, rear poly- reactor, pelleter, extraction tower, drying tower, at Product storage tank, the extraction tower are also connected with evaporator end, the cracking reaction kettle be separately connected evaporator outlet end and Mixing tank, the feed tank are separately connected blend tank and preceding poly- reactor.
Further, the preceding poly- reactor is voltage-resistant reactor.
Further, the evaporator is triple effect evaporator.
Further, the feed tank is equipped with flow controller.
The utility model has the beneficial effect that:1)Continuous production, production efficiency is high, and low energy consumption;2)It is black that polyamide fibre 6 can be produced Color is sliced;3)Extra raw material can reuse, non-environmental-pollution.
Description of the drawings
Fig. 1 is that 6 black of the utility model polyamide fibre is sliced continuous production device schematic diagram;
Wherein:1 be mixing tank, 2 be preceding poly- reactor, 3 be after poly- reactor, 4 be pelleter, 5 be extraction tower, 6 be dry Dry tower, 7 be finished product storage tank, 8 be evaporator, 9 be cracking reaction kettle, 10 be feed tank, 11 be blend tank.
Specific implementation mode
The embodiments of the present invention are described below in detail, examples of the embodiments are shown in the accompanying drawings, wherein from beginning Same or similar element or element with the same or similar functions are indicated to same or similar label eventually.Below by ginseng The embodiment for examining attached drawing description is exemplary, it is intended to for explaining the utility model, and should not be understood as to the utility model Limitation.
As shown in Figure 1, the utility model provides a kind of 6 black of polyamide fibre slice continuous production device, a kind of 6 black of polyamide fibre It is sliced continuous production device, including:Mixing tank 1, preceding poly- reactor 2, rear poly- reactor 3, pelleter 4, extraction tower 5, drying Tower 6, finished product storage tank 7, evaporator 8, cracking reaction kettle 9, feed tank 10, blend tank 11, the mixing tank 1 are poly- anti-before being sequentially connected Answer device 2, rear poly- reactor 3, pelleter 4, extraction tower 5, drying tower 6, finished product storage tank 7, the extraction tower 5 also with evaporator 8 into Mouth end is connected, and the cracking reaction kettle 9 is separately connected 8 outlet end of evaporator and mixing tank 1, and the feed tank 10 is separately connected Blend tank 11 and preceding poly- reactor 2.
The preceding poly- reactor 2 is voltage-resistant reactor.
The evaporator 8 is triple effect evaporator.
The feed tank 10 is equipped with flow controller.
The utility model realization method is as follows:Prepared add is added in liquid caprolactam after being mixed in proportion with concentrate Add agent, the Hybrid Heating in mixing tank 1;Meanwhile the mixture of carbon black and ethylene glycol, carbon black being added in blend tank 11:Ethylene glycol= 0.01-0.2 introduces feed tank 10 after being sufficiently stirred.
Poly- reactor 2 before mixing tank 1 and the liquid of feed tank 10 are sent into simultaneously, it is preceding to gather for pressurized operation, the polymerization of generation Object in the past poly- 2 bottom of reactor after poly- gear discharging is pumped to before menstruation poly- reactor 3, caprolactam it is first in rear poly- reactor 3 Open loop, addition reaction are first carried out, then completes polycondensation reaction, so that polymer chain rises to the required degree of polymerization.
Polymer melt is through note band, cooling, solidification, in 4 inscribe of pelleter at regular cylindrical chips.Contain oligomerization The slice of object is extracted in extraction tower 5 by the thermal process water of counter current contacting therewith.Extraction water containing oligomer is discharged by tower top, is sent To evaporator 8, the hot nitrogen that the slice by extraction is successively added in drying tower 6 is constantly dry, one addition of hot nitrogen 6 epimere of drying tower, this strand of hot nitrogen mainly remove the surface water of slice, one hot nitrogen is sent into the hypomere of drying tower 6, the hot nitrogen Gas is then used for removing the residual moisture in slice, and heats slice, keeps its molecular weight constant.
Slice after drying is aqueous≤0.05%, it is cooling after under nitrogen protection with pulse conveying device by slice send at Product storage tank 7 is used as international sale after metering packing.
In device in addition containing water caprolactam evaporation after ultimate density reach 50-90%, the caprolactam containing water into Enter cracking reaction kettle 9, the obtained concentrate after cracking reaction is directly by poly- reactor 2 before being pumped to, in this way, caprolactam can 100% utilization, without the loss of caprolactam and oligomer.The clean water being evaporated is condensed and is sent in water basin, and Send extraction back to therefrom, such water realizes closed cycle.
The utility model has the beneficial effect that:1)Continuous production, production efficiency is high, and low energy consumption;2)It is black that polyamide fibre 6 can be produced Color is sliced;3)Extra raw material can reuse, non-environmental-pollution.
The above descriptions are merely preferred embodiments of the present invention, is not intended to limit the utility model, although ginseng The utility model is described in detail according to previous embodiment, it for those skilled in the art, still can be with Technical scheme described in the above embodiments is modified or equivalent replacement of some of the technical features.It is all Within the spirit and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in this practicality Within novel protection domain.

Claims (4)

1. a kind of 6 black of polyamide fibre is sliced continuous production device, which is characterized in that including:Mixing tank, gathers preceding poly- reactor afterwards Reactor, pelleter, extraction tower, drying tower, finished product storage tank, evaporator, cracking reaction kettle, feed tank, blend tank, the batch mixing Tank is sequentially connected preceding poly- reactor, rear poly- reactor, pelleter, extraction tower, drying tower, finished product storage tank, the extraction tower also with Evaporator end is connected, and the cracking reaction kettle is separately connected evaporator outlet end and mixing tank, the feed tank difference Connect blend tank and preceding poly- reactor.
2. a kind of 6 black of polyamide fibre is sliced continuous production device according to claim 1, which is characterized in that poly- anti-before described It is voltage-resistant reactor to answer device.
3. a kind of 6 black of polyamide fibre is sliced continuous production device according to claim 1, which is characterized in that the evaporator For triple effect evaporator.
4. a kind of 6 black of polyamide fibre is sliced continuous production device according to claim 1, which is characterized in that the feed tank Equipped with flow controller.
CN201820069813.XU 2018-01-16 2018-01-16 A kind of 6 black of polyamide fibre slice continuous production device Active CN207930911U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820069813.XU CN207930911U (en) 2018-01-16 2018-01-16 A kind of 6 black of polyamide fibre slice continuous production device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820069813.XU CN207930911U (en) 2018-01-16 2018-01-16 A kind of 6 black of polyamide fibre slice continuous production device

Publications (1)

Publication Number Publication Date
CN207930911U true CN207930911U (en) 2018-10-02

Family

ID=63648663

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201820069813.XU Active CN207930911U (en) 2018-01-16 2018-01-16 A kind of 6 black of polyamide fibre slice continuous production device

Country Status (1)

Country Link
CN (1) CN207930911U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108568920A (en) * 2018-01-16 2018-09-25 江苏海阳锦纶新材料有限公司 A kind of 6 black of polyamide fibre slice continuous production device and production method

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108568920A (en) * 2018-01-16 2018-09-25 江苏海阳锦纶新材料有限公司 A kind of 6 black of polyamide fibre slice continuous production device and production method

Similar Documents

Publication Publication Date Title
CN102382296B (en) Production process for preparing fiber-grade nylon 6 chips with extracted aqueous concentrated solution and apparatus thereof
CN101885842B (en) Continuous polymerization production technology for polyamide fibre 6
CN101068848B (en) Polyester resin, molded object thereof, and processes for producing the same
CN101880386B (en) Recovery method of hexanolactam in polyamide-6 continuous polymerization production process
CN101899152B (en) Preparation of titanium dioxide additive in nylon-6 continuous polymerization production process
CN101434738B (en) Polyester/polyethylene/phenylethylene-butadiene-phenylethylene block copolymer waste plastic alloy material and preparation thereof
CN103289081B (en) Polymerizing polyamide production technique and equipment used
CN104387580A (en) Nylon-6 slice production method capable of improving polymerization conversion rate
CN109867779B (en) Preparation method of polyesteramide and product thereof
CN108586728A (en) A kind of film level nylon 6 slice and its production method
CN109553944A (en) A kind of polylactic acid terblending modification film and preparation method thereof
CN207930911U (en) A kind of 6 black of polyamide fibre slice continuous production device
CN102675113A (en) Method for preparing diglycol phthalate by performing alcoholysis on polyester (PET)
CN100547012C (en) Production process of novel dimer acid amide nylon
CN102701985A (en) Method for preparing epoxy resin curing agent by performing alcoholysis on PET (Polyethylene Terephthalate) polyester
CN207998575U (en) A kind of 6 coloured slice continuous production device of polyamide fibre
CN108570147A (en) A kind of 6 coloured slice continuous production device of polyamide fibre and production method
CN105131542A (en) Blended composite material prepared from lactide surface grafted bamboo powder and polylactic acid, and preparation method and applications thereof
CN105111423A (en) Polymer waterborne polyester and preparation method thereof
CN100427386C (en) Medium grade insoluble sulphur preparing process and producing apparatus
CN108568920A (en) A kind of 6 black of polyamide fibre slice continuous production device and production method
CN107417907A (en) A kind of preparation method of high crystalline poly (arylene ether nitrile)
CN103539078A (en) Method for preparation of insoluble sulfur
CN108084487B (en) A kind of plastics of polyethylene terephthalate nucleating agent and its rapid crystallization
CN106189284A (en) A kind of preparation method of regenerated cellulose film

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant