CN207930911U - A kind of 6 black of polyamide fibre slice continuous production device - Google Patents
A kind of 6 black of polyamide fibre slice continuous production device Download PDFInfo
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- CN207930911U CN207930911U CN201820069813.XU CN201820069813U CN207930911U CN 207930911 U CN207930911 U CN 207930911U CN 201820069813 U CN201820069813 U CN 201820069813U CN 207930911 U CN207930911 U CN 207930911U
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Abstract
The utility model provides a kind of 6 black of polyamide fibre slice continuous production device, including:Mixing tank, preceding poly- reactor, rear poly- reactor, pelleter, extraction tower, drying tower, finished product storage tank, evaporator, cracking reaction kettle, feed tank, blend tank; the mixing tank is sequentially connected preceding poly- reactor, rear poly- reactor, pelleter, extraction tower, drying tower, finished product storage tank; the extraction tower is also connected with evaporator end; the cracking reaction kettle is separately connected evaporator outlet end and mixing tank, and the feed tank is separately connected blend tank and preceding poly- reactor.The utility model has the beneficial effect that:1)Continuous production, production efficiency is high, and low energy consumption;2)6 black of polyamide fibre slice can be produced;3)Extra raw material can reuse, non-environmental-pollution.
Description
Technical field
The utility model is related to polyamide fibre field, more particularly to a kind of 6 black of polyamide fibre is sliced continuous production device.
Background technology
The chemico-physical properties and nylon66 fiber of polyamide fibre 6 are much like, however, its fusing point is relatively low, and Process temperature ranges
It is very wide.Its impact resistance and antilysis is got well than nylon-66 plastic, but hygroscopicity is also stronger.
Current chinlon 6 section production technology is various, but generally interval metaplasia is used to produce, low production efficiency, and energy consumption is higher;This
The production technology of 6 black of outer polyamide fibre slice is also more rare at home.
Invention content
The purpose of this utility model is that proposing a kind of 6 black of polyamide fibre slice continuous production device, there is production efficiency
The advantages that height, non-environmental-pollution.
To achieve the goals above, the utility model provides a kind of 6 black of polyamide fibre slice continuous production device, including:
Mixing tank, preceding poly- reactor, rear poly- reactor, pelleter, extraction tower, drying tower, finished product storage tank, evaporator, cracking reaction kettle,
Feed tank, blend tank, the mixing tank be sequentially connected preceding poly- reactor, rear poly- reactor, pelleter, extraction tower, drying tower, at
Product storage tank, the extraction tower are also connected with evaporator end, the cracking reaction kettle be separately connected evaporator outlet end and
Mixing tank, the feed tank are separately connected blend tank and preceding poly- reactor.
Further, the preceding poly- reactor is voltage-resistant reactor.
Further, the evaporator is triple effect evaporator.
Further, the feed tank is equipped with flow controller.
The utility model has the beneficial effect that:1)Continuous production, production efficiency is high, and low energy consumption;2)It is black that polyamide fibre 6 can be produced
Color is sliced;3)Extra raw material can reuse, non-environmental-pollution.
Description of the drawings
Fig. 1 is that 6 black of the utility model polyamide fibre is sliced continuous production device schematic diagram;
Wherein:1 be mixing tank, 2 be preceding poly- reactor, 3 be after poly- reactor, 4 be pelleter, 5 be extraction tower, 6 be dry
Dry tower, 7 be finished product storage tank, 8 be evaporator, 9 be cracking reaction kettle, 10 be feed tank, 11 be blend tank.
Specific implementation mode
The embodiments of the present invention are described below in detail, examples of the embodiments are shown in the accompanying drawings, wherein from beginning
Same or similar element or element with the same or similar functions are indicated to same or similar label eventually.Below by ginseng
The embodiment for examining attached drawing description is exemplary, it is intended to for explaining the utility model, and should not be understood as to the utility model
Limitation.
As shown in Figure 1, the utility model provides a kind of 6 black of polyamide fibre slice continuous production device, a kind of 6 black of polyamide fibre
It is sliced continuous production device, including:Mixing tank 1, preceding poly- reactor 2, rear poly- reactor 3, pelleter 4, extraction tower 5, drying
Tower 6, finished product storage tank 7, evaporator 8, cracking reaction kettle 9, feed tank 10, blend tank 11, the mixing tank 1 are poly- anti-before being sequentially connected
Answer device 2, rear poly- reactor 3, pelleter 4, extraction tower 5, drying tower 6, finished product storage tank 7, the extraction tower 5 also with evaporator 8 into
Mouth end is connected, and the cracking reaction kettle 9 is separately connected 8 outlet end of evaporator and mixing tank 1, and the feed tank 10 is separately connected
Blend tank 11 and preceding poly- reactor 2.
The preceding poly- reactor 2 is voltage-resistant reactor.
The evaporator 8 is triple effect evaporator.
The feed tank 10 is equipped with flow controller.
The utility model realization method is as follows:Prepared add is added in liquid caprolactam after being mixed in proportion with concentrate
Add agent, the Hybrid Heating in mixing tank 1;Meanwhile the mixture of carbon black and ethylene glycol, carbon black being added in blend tank 11:Ethylene glycol=
0.01-0.2 introduces feed tank 10 after being sufficiently stirred.
Poly- reactor 2 before mixing tank 1 and the liquid of feed tank 10 are sent into simultaneously, it is preceding to gather for pressurized operation, the polymerization of generation
Object in the past poly- 2 bottom of reactor after poly- gear discharging is pumped to before menstruation poly- reactor 3, caprolactam it is first in rear poly- reactor 3
Open loop, addition reaction are first carried out, then completes polycondensation reaction, so that polymer chain rises to the required degree of polymerization.
Polymer melt is through note band, cooling, solidification, in 4 inscribe of pelleter at regular cylindrical chips.Contain oligomerization
The slice of object is extracted in extraction tower 5 by the thermal process water of counter current contacting therewith.Extraction water containing oligomer is discharged by tower top, is sent
To evaporator 8, the hot nitrogen that the slice by extraction is successively added in drying tower 6 is constantly dry, one addition of hot nitrogen
6 epimere of drying tower, this strand of hot nitrogen mainly remove the surface water of slice, one hot nitrogen is sent into the hypomere of drying tower 6, the hot nitrogen
Gas is then used for removing the residual moisture in slice, and heats slice, keeps its molecular weight constant.
Slice after drying is aqueous≤0.05%, it is cooling after under nitrogen protection with pulse conveying device by slice send at
Product storage tank 7 is used as international sale after metering packing.
In device in addition containing water caprolactam evaporation after ultimate density reach 50-90%, the caprolactam containing water into
Enter cracking reaction kettle 9, the obtained concentrate after cracking reaction is directly by poly- reactor 2 before being pumped to, in this way, caprolactam can
100% utilization, without the loss of caprolactam and oligomer.The clean water being evaporated is condensed and is sent in water basin, and
Send extraction back to therefrom, such water realizes closed cycle.
The utility model has the beneficial effect that:1)Continuous production, production efficiency is high, and low energy consumption;2)It is black that polyamide fibre 6 can be produced
Color is sliced;3)Extra raw material can reuse, non-environmental-pollution.
The above descriptions are merely preferred embodiments of the present invention, is not intended to limit the utility model, although ginseng
The utility model is described in detail according to previous embodiment, it for those skilled in the art, still can be with
Technical scheme described in the above embodiments is modified or equivalent replacement of some of the technical features.It is all
Within the spirit and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in this practicality
Within novel protection domain.
Claims (4)
1. a kind of 6 black of polyamide fibre is sliced continuous production device, which is characterized in that including:Mixing tank, gathers preceding poly- reactor afterwards
Reactor, pelleter, extraction tower, drying tower, finished product storage tank, evaporator, cracking reaction kettle, feed tank, blend tank, the batch mixing
Tank is sequentially connected preceding poly- reactor, rear poly- reactor, pelleter, extraction tower, drying tower, finished product storage tank, the extraction tower also with
Evaporator end is connected, and the cracking reaction kettle is separately connected evaporator outlet end and mixing tank, the feed tank difference
Connect blend tank and preceding poly- reactor.
2. a kind of 6 black of polyamide fibre is sliced continuous production device according to claim 1, which is characterized in that poly- anti-before described
It is voltage-resistant reactor to answer device.
3. a kind of 6 black of polyamide fibre is sliced continuous production device according to claim 1, which is characterized in that the evaporator
For triple effect evaporator.
4. a kind of 6 black of polyamide fibre is sliced continuous production device according to claim 1, which is characterized in that the feed tank
Equipped with flow controller.
Priority Applications (1)
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CN201820069813.XU CN207930911U (en) | 2018-01-16 | 2018-01-16 | A kind of 6 black of polyamide fibre slice continuous production device |
Applications Claiming Priority (1)
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CN201820069813.XU CN207930911U (en) | 2018-01-16 | 2018-01-16 | A kind of 6 black of polyamide fibre slice continuous production device |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108568920A (en) * | 2018-01-16 | 2018-09-25 | 江苏海阳锦纶新材料有限公司 | A kind of 6 black of polyamide fibre slice continuous production device and production method |
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2018
- 2018-01-16 CN CN201820069813.XU patent/CN207930911U/en active Active
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108568920A (en) * | 2018-01-16 | 2018-09-25 | 江苏海阳锦纶新材料有限公司 | A kind of 6 black of polyamide fibre slice continuous production device and production method |
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