CN111218325A - Ultralow-temperature ashless anti-wear hydraulic oil and preparation method thereof - Google Patents

Ultralow-temperature ashless anti-wear hydraulic oil and preparation method thereof Download PDF

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Publication number
CN111218325A
CN111218325A CN201911216767.7A CN201911216767A CN111218325A CN 111218325 A CN111218325 A CN 111218325A CN 201911216767 A CN201911216767 A CN 201911216767A CN 111218325 A CN111218325 A CN 111218325A
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CN
China
Prior art keywords
olefin
oil
type oil
additive
hitec543
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Pending
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CN201911216767.7A
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Chinese (zh)
Inventor
李艳国
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Sarlboro Petrochemical Industry Tianjin Co ltd
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Sarlboro Petrochemical Industry Tianjin Co ltd
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Priority to CN201911216767.7A priority Critical patent/CN111218325A/en
Publication of CN111218325A publication Critical patent/CN111218325A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04Mixtures of base-materials and additives
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/0206Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers used as base material
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28Esters
    • C10M2207/2805Esters used as base material

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

α -IV-class oil PAO4 synthesized by olefin, α -IV-class oil PAO10 synthesized by olefin, V-class oil TRS-0812 synthesized by olefin, an additive HiTEC543 and a defoaming agent are added, firstly α -IV-class oil PAO4 synthesized by olefin, α -IV-class oil PAO10 synthesized by olefin and V-class oil TRS-0812 synthesized by olefin are added, secondly, the defoaming agent is added, the mechanical circulation stirring is started during the whole feeding period, then the additive HiTEC543 is slowly added at a constant speed, all raw materials are fully mixed by a mixing kettle, a heating device arranged in the mixing kettle is used for heating to 55+5 ℃, and the circulation stirring is carried out for 30-40min in the kettle.

Description

Ultralow-temperature ashless anti-wear hydraulic oil and preparation method thereof
Technical Field
The invention belongs to the field of ashless anti-wear hydraulic oil, and particularly relates to ultralow-temperature ashless anti-wear hydraulic oil and a preparation method thereof.
Background
The anti-wear hydraulic oil and the hydraulic medium used by the hydraulic system utilizing the hydraulic pressure energy play roles of energy transfer, wear resistance, system lubrication, corrosion resistance, rust resistance, cooling and the like in the hydraulic system. For antiwear hydraulic oil, the requirements of a hydraulic device on the viscosity of liquid at working temperature and starting temperature are firstly met, and the viscosity change of lubricating oil is directly related to hydraulic action, transmission efficiency and transmission precision, so that the viscosity-temperature performance and shear stability of the oil are also required to meet various requirements proposed by different purposes. A great deal of facts show that more than 90% of hydraulic faults are caused by working media, so that the correct selection and use of the hydraulic media have very important significance for improving the working performance, working reliability and safety of a hydraulic system and prolonging the service life.
The conventional antiwear hydraulic oil can ensure normal operation of equipment in a relatively mild working environment, but in areas with large temperature difference between day and night in the field and winter in cold north, the problems of unsmooth oil supply, insufficient pressure, equipment operation jitter, blockage and the like are caused because the low-temperature fluidity cannot meet the harsh external environment.
Disclosure of Invention
α -IV-class oil PAO4 synthesized by olefin, α -IV-class oil PAO10 synthesized by olefin, V-class oil TRS-0812, additive HiTEC543 and defoaming agent are added, firstly the IV-class oil PAO4 synthesized by α -olefin, the IV-class oil PAO10 synthesized by α -olefin and the V-class oil TRS-0812 synthesized by olefin are added, secondly the defoaming agent is added, the mechanical circulation stirring is started during the whole feeding period, then the additive HiTEC is slowly added at a constant speed, all raw materials are fully mixed by a blending kettle, a heating device arranged in the blending kettle is used for heating to 55+ 543 ℃, and the circulation stirring in the kettle is carried out for 2 periods.
Preferably, the oil comprises, by weight, α -olefin synthetic IV-type oil PAO4 of 20%, α -olefin synthetic IV-type oil PAO10 of 69.13%, V-type oil TRS-0812 of 10%, additive HiTEC543 of 0.87% and defoaming agent of 20 ppm.
Preferably, the α -olefin artificially synthesized IV-type oil PAO4 and α -olefin artificially synthesized IV-type oil PAO10 have high viscosity index, excellent lubricating property, high flash point and improved safety, low evaporativity, excellent oxidation resistance and high nonpolar strength, so that the oil has excellent hydrolytic stability.
Preferably, the additive HiTEC543 is an ashless hydraulic oil complexing agent, provides extreme pressure anti-wear performance by using nitrogen-phosphorus-sulfur, does not contain zinc, and can effectively protect silver-containing and copper-containing parts in hydraulic equipment.
The invention has the beneficial effects that: the wear-resistant rubber has excellent performance in a working environment at the ultralow temperature of 50 ℃ below zero and ultrahigh viscosity index, so that the wear-resistant rubber has excellent performance at low temperature and unusual performance at wide working temperature, is fully synthesized, has excellent wear-resistant and wear-reducing performance, and has an overlong service life.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention is further described below:
example (b):
α -IV-class oil PAO4 synthesized by olefin, α -IV-class oil PAO10 synthesized by olefin, V-class oil TRS-0812, additive HiTEC543 and defoaming agent are added, firstly the α -IV-class oil PAO4 synthesized by olefin, the α -IV-class oil PAO10 synthesized by olefin and the V-class oil TRS-0812 synthesized by olefin are added, secondly the defoaming agent is added, mechanical circulation stirring is started during the whole feeding period, then the additive HiTEC543 is added slowly at a constant speed, all the raw materials are fully mixed by a mixing kettle, a heating device arranged in the mixing kettle is used for heating to 55+5 ℃, and circulation stirring in the kettle is carried out for 2 periods.
Specifically, the oil comprises, by weight, α -olefin artificially synthesized IV-type oil PAO4 of 20%, α -olefin artificially synthesized IV-type oil PAO10 of 69.13%, V-type oil TRS-0812 of 10%, additive HiTEC543 of 0.87% and defoaming agent of 20 ppm.
Specifically, the α -olefin artificially synthesized IV-class oil PAO4 and α -olefin artificially synthesized IV-class oil PAO10 have high viscosity index, further have good viscosity-temperature performance and more excellent lubricating performance, have high flash point, improve safety, reduce oil-gas concentration in use or storage environment due to low evaporation performance, reduce damage to long-term contact personnel, provide an ultra-long oil change period due to excellent oxidation resistance, and have excellent hydrolytic stability due to strong non-polarity.
Specifically, the V-type oil TRS-0812 has a chemical solubilization effect due to the addition of the ester oil, the solubility of the additive HiTEC543 is enhanced due to the addition of the ester oil, the compatibility of the α -olefin artificially synthesized IV-type oil PAO and the additive HiTEC543 is improved, and the additive can better exert performance.
Specifically, the additive HiTEC543 is an ashless hydraulic oil complexing agent, provides extreme pressure anti-wear performance by using nitrogen-phosphorus-sulfur, does not contain zinc, and can effectively protect silver and copper-containing parts in hydraulic equipment.
Principle of operation
Firstly adding α -olefin artificially synthesized IV-class oil PAO4, 69.13 percent α -olefin artificially synthesized IV-class oil PAO10 and 10 percent V-class oil TRS-0812, secondly adding 20ppm of defoaming agent, starting mechanical circulation stirring in the whole feeding period, then slowly adding 0.87 percent of additive HiTEC543 at a constant speed, fully mixing the raw materials by using a blending kettle, heating to 55+5 ℃ by using a heating device arranged in the blending kettle, and circulating stirring in the kettle for 2 periods.
It should be noted that, in this document, moreover, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (4)

1.α -olefin artificially synthesized IV-type oil PAO4, α -olefin artificially synthesized IV-type oil PAO10, V-type oil TRS-0812, an additive HiTEC543 and a defoaming agent are added, firstly α -olefin artificially synthesized IV-type oil PAO4, α -olefin artificially synthesized IV-type oil PAO10 and V-type oil TRS-0812 are added, secondly the defoaming agent is added, mechanical circulation stirring is started during the whole feeding period, then the additive HiTEC543 is slowly added at a constant speed, all raw materials are fully mixed by a mixing kettle, a heating device arranged in the mixing kettle is used for heating to 55+5 ℃, and circulation stirring is carried out in the kettle for 2 periods.
2. The ultra-low temperature ashless anti-wear hydraulic oil and the preparation method thereof as claimed in claim 1, characterized in that the hydraulic oil comprises, by weight, α -olefin synthetic IV-type oil PAO4 accounting for 20%, α -olefin synthetic IV-type oil PAO10 accounting for 69.13%, V-type oil TRS-0812 accounting for 10%, additive HiTEC543 accounting for 0.87%, and antifoaming agent 20 ppm.
3. The ultra-low temperature ashless anti-wear hydraulic oil and the preparation method thereof as claimed in claim 1, wherein the α -olefin synthetic IV-type oil PAO4 and α -olefin synthetic IV-type oil PAO10 have high viscosity index, excellent lubricating property, high flash point to improve safety, low evaporation, excellent oxidation resistance and nonpolar strength to enable the oil to have excellent hydrolytic stability.
4. The ultra-low temperature ashless anti-wear hydraulic oil and the preparation method thereof as claimed in claim 1, wherein the additive HiTEC543 is an ashless hydraulic oil complexing agent, provides extreme pressure anti-wear performance by using nitrogen-phosphorus-sulfur, is zinc-free, and can effectively protect silver-containing and copper-containing parts in hydraulic equipment.
CN201911216767.7A 2019-12-03 2019-12-03 Ultralow-temperature ashless anti-wear hydraulic oil and preparation method thereof Pending CN111218325A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201911216767.7A CN111218325A (en) 2019-12-03 2019-12-03 Ultralow-temperature ashless anti-wear hydraulic oil and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201911216767.7A CN111218325A (en) 2019-12-03 2019-12-03 Ultralow-temperature ashless anti-wear hydraulic oil and preparation method thereof

Publications (1)

Publication Number Publication Date
CN111218325A true CN111218325A (en) 2020-06-02

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101724489A (en) * 2008-10-15 2010-06-09 中国石油天然气股份有限公司 Air compressor oil composition
CN107541319A (en) * 2017-09-06 2018-01-05 浙江实美润滑科技有限公司 A kind of ashless hydraulic fluid of high viscosity index (HVI) low pour point and preparation method thereof
CN108102774A (en) * 2017-12-26 2018-06-01 金雪驰科技(马鞍山)有限公司 A kind of lubricating oil and its application

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101724489A (en) * 2008-10-15 2010-06-09 中国石油天然气股份有限公司 Air compressor oil composition
CN107541319A (en) * 2017-09-06 2018-01-05 浙江实美润滑科技有限公司 A kind of ashless hydraulic fluid of high viscosity index (HVI) low pour point and preparation method thereof
CN108102774A (en) * 2017-12-26 2018-06-01 金雪驰科技(马鞍山)有限公司 A kind of lubricating oil and its application

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Application publication date: 20200602

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