CN111175331A - Double-load net clamping device for transmission electron microscope - Google Patents
Double-load net clamping device for transmission electron microscope Download PDFInfo
- Publication number
- CN111175331A CN111175331A CN201811342965.3A CN201811342965A CN111175331A CN 111175331 A CN111175331 A CN 111175331A CN 201811342965 A CN201811342965 A CN 201811342965A CN 111175331 A CN111175331 A CN 111175331A
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- China
- Prior art keywords
- sample stage
- electron microscope
- transmission electron
- objective table
- sliding block
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/22—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
- G01N23/2204—Specimen supports therefor; Sample conveying means therefore
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/22—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
- G01N23/2202—Preparing specimens therefor
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2223/00—Investigating materials by wave or particle radiation
- G01N2223/07—Investigating materials by wave or particle radiation secondary emission
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2223/00—Investigating materials by wave or particle radiation
- G01N2223/30—Accessories, mechanical or electrical features
- G01N2223/309—Accessories, mechanical or electrical features support of sample holder
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- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The utility model provides a pair of year net clamping device for transmission electron microscope, mainly includes sample objective table, folding mechanism, hold-down mechanism, locking mechanism, be equipped with the macropore in the middle of the objective table, objective table one side is equipped with the aperture and communicates with each other with the objective table macropore, and the objective table both sides are equipped with the guide rail groove. The folding mechanism comprises a movable hinge, a folding plate and positioning rings, the folding plate and the objective table are connected together by the movable hinge, the positioning rings are respectively installed on the folding plate, and oblique angles are arranged on the outer sides of the positioning rings on the two sides of the folding plate. The pressing mechanism comprises a limiting ring, a sliding block, a compression spring and a fixed disc, wherein the upper part and the lower part of the inner side of the limiting ring are provided with oblique angles and are connected with the sliding block, the sliding block is arranged in a guide rail groove on the objective table, the compression spring is arranged between the sliding block and the fixed disc, and the fixed disc is arranged on the side surface of the objective table. The locking mechanism comprises a movable hinge, a movable block, a support frame and a roller, wherein the movable hinge connects the movable block with the objective table, the roller is arranged on the support frame, and the support frame is arranged on the movable block.
Description
Technical Field
The invention relates to a range of a transmission electron microscope sample preparation device, in particular to a double-load net clamping device for a transmission electron microscope.
Background
The main function of the carrier net film for the transmission electron microscope is to load a small-scale sample during electron microscope observation, and a common single carrier net is generally used for loading the sample. When the magnetic material is observed by a transmission electron microscope, in order to avoid the magnetic material from being adsorbed on a pole shoe of the transmission electron microscope, a duplex carrier net (two carrier nets) is often used for clamping a sample to form a sandwich structure, so that the fixation of the sample is enhanced. Because the duplex carrying net is small in size, the clamping method for folding the duplex carrying net by using the conventional tweezers has the following problems: 1. the folding is not accurate, so that the grid cannot be placed on the transmission electron microscope sample rod; 2. the net is easy to be damaged by the tweezers in the clamping process; 3. the clamping efficiency is low. In order to solve the above problems more effectively, it is necessary to invent a clamping device for a twin load net for a transmission electron microscope.
Disclosure of Invention
The invention aims to provide a double-load-net clamping device for a transmission electron microscope, which aims to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
the utility model provides a pair of year net clamping device for transmission electron microscope, the device mainly includes base, sample objective table, folding mechanism, hold-down mechanism, locking mechanism, and the sample objective table is installed on the base, is equipped with the macropore in the middle of the sample objective table, and sample objective table one side is equipped with the aperture and communicates with each other with sample objective table macropore, and sample objective table both sides are equipped with the guide rail groove. The folding mechanism comprises a movable hinge, a folding plate and positioning rings, the folding plate and the sample object stage are connected together by the movable hinge, the positioning rings are respectively arranged on the folding plate, and oblique angles are arranged outside the positioning rings on the two sides of the folding plate. The pressing mechanism comprises a limiting ring, a sliding block, a compression spring and a fixed disc, wherein the upper part and the lower part of the inner side of the limiting ring are provided with oblique angles and are connected with the sliding block, the sliding block is arranged in a guide rail groove on the objective table, the compression spring is arranged between the sliding block and the fixed disc, and the fixed disc is arranged on the side surface of the sample objective table. The locking mechanism comprises a movable hinge, a movable block, a support frame and a roller, wherein the movable hinge connects the movable block with the sample stage, the roller is arranged on the support frame, and the support frame is arranged on the movable block.
The invention has the outstanding advantages that:
1. simple structure, stability in use is high, and the pair carries the net folding accuracy, effectively avoids the pair to carry the net at folding in-process damage.
2. The ingenious design of position collar and spacing collar for the pair carries the net and can both keep by the state of being compressed tightly in folding process, has guaranteed the counterpoint precision that folding process carried the net.
3. The locking of the duplex load network is ensured by the ingenious design of the locking mechanism.
Drawings
Fig. 1 is a schematic structural view of a dual-carrier clamping device for a transmission electron microscope.
Fig. 2 is a schematic single-side view of the pressing mechanism of the present invention.
Fig. 3 is a schematic view of the locking mechanism of the present invention.
Labeled as: the device comprises a base 1, a sample objective table 2, a locking mechanism 3, a pressing mechanism 4, a guide rail groove 5, a positioning ring 6, a folding plate 7 and a movable hinge 8.
Detailed Description
The technical solution of the present invention is further illustrated by the accompanying drawings 1, 2 and 3.
Referring to fig. 1, 2 and 3, the clamping device for the duplex grid carrier for the transmission electron microscope mainly comprises a base 1, a sample object stage 2, a folding mechanism, a hold-down mechanism 4 and a locking mechanism 3, wherein the sample object stage 2 is arranged on the base 1, a large hole is arranged in the middle of the sample object stage 2, a small hole is arranged on one side of the sample object stage 2 and is communicated with the large hole of the sample object stage 2, and guide rail grooves 5 are arranged on two sides of the sample object stage 2 and are used for installing the hold-down mechanism. Folding mechanism includes activity hinge 8, folded sheet 7, position circle 6, and activity hinge 8 links together folded sheet 7 and sample objective table 2, and position circle 6 is installed respectively on folded sheet 7, and the position circle 6 outside of the last both sides of folded sheet 7 is equipped with the oblique angle. The pressing mechanism 4 comprises a limiting ring 4-1, a sliding block 4-3, a compression spring 4-5 and a fixed disc 4-4, wherein the upper part and the lower part of the inner side of the limiting ring 4-1 are respectively provided with an oblique angle and are connected with the sliding block 4-3, the sliding block 4-3 is arranged in a guide rail groove 5 on the sample object stage 2, the compression spring 4-5 is arranged between the sliding block 4-3 and the fixed disc 4-4, and the fixed disc 4-4 is arranged on the side surface of the sample object stage 2. The locking mechanism 3 comprises a movable hinge 3-4, a movable block 3-1, a support frame 3-2 and a roller 3-3, wherein the movable hinge 3-4 connects the movable block 3-1 with the sample objective table 2, the roller 3-3 is arranged on the support frame 3-2, and the support frame 3-2 is arranged on the movable block 3-1. In the using process, a pincer is inserted into a loading and unloading hole 4-2 on the limiting ring 4-1, the limiting ring 4-1 is pushed towards the outside, then a carrying net with a locking lug in a duplex carrying net for a transmission electron microscope is placed into the limiting ring 4-1, the other carrying net is placed into the positioning ring 6, and finally a folding mechanism, a pressing mechanism and a locking mechanism in the device are tightly matched so as to realize the clamping function of the device on the duplex carrying net.
Claims (5)
1. A clamping device for a duplex load network for a transmission electron microscope solves the problem that the duplex load network for the transmission electron microscope is not easy to fold in the sample clamping process by utilizing a mechanical mechanism, and mainly comprises a sample object stage, a folding mechanism, a pressing mechanism and a locking mechanism.
2. The clamping device of the dual grid carrier for the transmission electron microscope as claimed in claim 1, wherein the sample stage has a large hole in the middle, one side of the sample stage has a small hole and communicates with the large hole of the sample stage, when preparing the transmission electron microscope sample, the sample stage is prevented from being contaminated by the excessive solvent dropped on the grid carrier, and the sample stage has guide rail grooves on both sides for installing the hold-down mechanism.
3. The dual mesh-carrying clamping device for the transmission electron microscope as claimed in claim 1, wherein the folding mechanism comprises a living hinge, a folding plate, and positioning rings, the living hinge connects the folding plate and the sample stage, the positioning rings are respectively mounted on the folding plate, the outer sides of the positioning rings on both sides of the folding plate are provided with oblique angles, and when the folding plate is attached to the sample stage, the positioning rings push the pressing mechanism outwards, so that the mesh carried in the positioning rings is attached to the mesh carried on the sample stage.
4. The dual grid clamping device for the transmission electron microscope as claimed in claim 1, wherein the pressing mechanism comprises a limiting ring, a sliding block, a compression spring and a fixed disk, wherein the upper and lower parts of the inner side of the limiting ring are provided with oblique angles and connected with the sliding block, the sliding block is arranged in a guide rail groove on the sample stage, the compression spring is arranged between the sliding block and the fixed disk, the fixed disk is arranged on the side surface of the sample stage, and when the folding plate is separated from the sample stage, the compression spring pushes the sliding block and drives the limiting ring to return to the initial position so that the grid placed in the limiting ring is pressed by the pressing mechanism.
5. The dual mesh-carrying clamping device for the transmission electron microscope as claimed in claim 1, wherein the locking mechanism comprises a living hinge, a movable block, a support frame and a roller, the living hinge connects the movable block with the sample stage, the roller is mounted on the support frame, the support frame is mounted on the movable block, and when the movable block approaches the sample stage, the roller pushes the locking lug on the outer side of the mesh to fold inwards to lock the mesh.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201811342965.3A CN111175331A (en) | 2018-11-12 | 2018-11-12 | Double-load net clamping device for transmission electron microscope |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201811342965.3A CN111175331A (en) | 2018-11-12 | 2018-11-12 | Double-load net clamping device for transmission electron microscope |
Publications (1)
Publication Number | Publication Date |
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CN111175331A true CN111175331A (en) | 2020-05-19 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201811342965.3A Pending CN111175331A (en) | 2018-11-12 | 2018-11-12 | Double-load net clamping device for transmission electron microscope |
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CN (1) | CN111175331A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2022242152A1 (en) * | 2021-05-21 | 2022-11-24 | 南方科技大学 | Multi-specification microscope linkage analysis sample table for transmission electron microscope sample |
-
2018
- 2018-11-12 CN CN201811342965.3A patent/CN111175331A/en active Pending
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2022242152A1 (en) * | 2021-05-21 | 2022-11-24 | 南方科技大学 | Multi-specification microscope linkage analysis sample table for transmission electron microscope sample |
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