CN111110609A - Acidic skin-care spray containing mineral elements and preparation method thereof - Google Patents
Acidic skin-care spray containing mineral elements and preparation method thereof Download PDFInfo
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- CN111110609A CN111110609A CN202010138490.7A CN202010138490A CN111110609A CN 111110609 A CN111110609 A CN 111110609A CN 202010138490 A CN202010138490 A CN 202010138490A CN 111110609 A CN111110609 A CN 111110609A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/83—Electrophoresis; Electrodes; Electrolytic phenomena
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Abstract
The invention discloses an acidic skin-care spray containing mineral elements and a preparation method thereof, wherein the preparation method comprises the following steps: (1) mixing the purified and concentrated deep seawater concentrate with the seawater subjected to reverse osmosis treatment to obtain an electrolyte solution, wherein the addition ratio of the deep seawater concentrate is 1-20 per mill of the volume of the seawater subjected to reverse osmosis treatment; (2) placing the electrolyte solution in an electrolytic cell, carrying out electrolysis treatment by using 10-20V direct current voltage, and taking an anode cell solution; (3) adding rose hydrosol with volume fraction of 0.5-3 per mill into the anode solution; (4) clarifying the solution added with the rose hydrosol, adding trehalose into the obtained solution with the rose fragrance in a mass fraction of 0.1-3.0%, and fully and uniformly mixing. The product is rich in mineral elements and microelements, and has effects of improving metabolism, coordinating endocrine organ activity, and smoothing and refining skin due to penetration of these minerals into skin.
Description
Technical Field
The invention relates to the technical field of beauty and skin care products, in particular to an acidic skin care spray containing mineral elements and a preparation method thereof.
Background
Deep sea water is generally sea water which is not irradiated by sunlight below 200 m of sea level. Because sunlight cannot be directly irradiated, and the sunlight is rarely exchanged with surface seawater, the deep seawater has the characteristics of low temperature constancy, cleanness, rich nutrition and minerals and the like. Because the deep seawater is far away from industrial and artificial pollution, the deep seawater has higher extraction, processing and application advantages, and can produce high-quality deep seawater products compared with land water and surface seawater products by taking the deep seawater as a raw material. The deep seawater can be widely applied to industries of food, medicine, health care, skin care products, planting, aquaculture and the like. The ocean water contains various elements which are or may be necessary for human bodies, including Na, Mg, Al, K, Ca, Mn, Fe, Zn, Se, Mo, Sr and the like, wherein the elements of Zn, Cu, Se and the like are enriched in deep seawater. The ocean water contains abundant mineral elements which can promote skin metabolism and maintain healthy sebum. The cluster size of the water molecules can be represented by the half-peak width in a nuclear magnetic resonance oxygen spectrum, the smaller the half-peak width is, the smaller the cluster size of the water molecules is, the small molecular water has strong permeability and can penetrate through the deep layer of the skin, and the effects of deeply moisturizing and caring the skin can be achieved by adopting the small molecular water as a skin care raw material. The weakly acidic toning lotion has a bactericidal effect, acidic water molecules permeate into pores, and can effectively clean grease waste in the pores, soften waste cutin accumulated around the pores, help the skin to dredge the pores, and condition the pH value of the skin.
In recent years, the addition of mineral elements into skin care products has become a development trend of skin care products, such as dead sea mud rich in minerals for skin care; the soothing cream and the lotion containing the zinc additive are added, so that the product has a certain soothing effect; the spray of the French famous product contains zinc and magnesium.
Disclosure of Invention
The invention aims to provide an acidic skin-care spray containing mineral elements and a preparation method thereof.
In order to achieve the purpose, the invention provides the following technical scheme:
a preparation method of an acidic skin-care spray containing mineral elements comprises the following specific steps:
(1) mixing the purified and concentrated deep seawater concentrate with the seawater subjected to reverse osmosis treatment to obtain an electrolyte solution, wherein the addition ratio of the deep seawater concentrate is 1-20 per mill of the volume of the seawater subjected to reverse osmosis treatment;
(2) the above electrolyte solution was placed in an electrolytic cell at 10～Electrolyzing with 20V DC voltage to obtain anode pool solution;
(3) 0.5 per mill of volume fraction in the anode solution～3 per mill rose hydrosol is added;
(4) clarifying the solution containing rose hydrosol to obtain solution with rose fragrance 0.1%～Trehalose was added to 3.0% and mixed well.
Further, the deep seawater concentrated solution in the step (1) is a solution which is obtained by taking seawater with the depth of less than 200 meters, and carrying out ultrafiltration and electrodialysis treatment on the seawater to obtain the solution rich in mineral elements, wherein the content of Ca, Mg and Zn elements is 1 of that of common seawater～1.8 times.
Further, the specific preparation method of the electrolytic anode solution in the step (2) is to use a mixed solution of the deep seawater concentrated solution and reverse osmosis water as an electrolyte solution, iridium-titanium alloy as a cathode and an anode, and direct current voltage 10 is applied to the two electrodes～20V, and the electrolysis time is not less than 5 minutes; the parameters of the anode solution obtained at the anode of the electrolysis device are characterized in that: 1) the pH value is 2.0～6.5；2)17Half-peak width of O-nuclear magnetic resonance spectrum<65Hz。
Furthermore, the rose hydrosol in the step (3) is prepared by distilling fresh rose and then separating water and oil, and has strong rose fragrance.
Compared with the prior art, the invention has the following beneficial effects:
the pH value of the acidic skin-care spray product containing mineral elements prepared by the method is 1.5～6.5，17Half-peak width of O-nuclear magnetic resonance spectrum<65Hz, magnesium content 0.5～20.1 mu g/mL, zinc content 10～100ng/ml, calcium content 2.2～21.4. mu.g/mL. The product is rich in mineral elements and microelements, and has effects of improving metabolism, coordinating endocrine organ activity, and making skin smooth and delicate.17Half-peak width of O-nuclear magnetic resonance spectrum<65Hz belongs to small molecular cluster water, and is easier to absorb by skin.
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described below with reference to specific embodiments, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1:
(1) drawing and treating technology of deep seawater below 200 m:
the drawing method of deep seawater with depth of below 200 m comprises the following steps: choose PE pipe for use as getting water pipeline, transfer the water pipe along the ship board through the guide roll on the ship, because the PE water pipe will overcome self buoyancy, consequently will set up and pull the pouring weight and come to pull the pipeline and transfer into water, the pouring weight is confirmed according to water pipe buoyancy. When the heavy block pulls the water pipe to be placed at a certain water depth position, a crane is used on the ship to connect the water pump and the water pipe. After the water taking pipeline and the water pump are connected, the water pump is started to discharge the seawater in the pipeline, and the pipeline is continuously flushed for 10 min. And after the flushing is finished, the deep seawater is introduced into the seawater storage equipment. After the water storage equipment is fully stored, the valve and the water pump are closed, the water taking pipeline is lifted to disassemble the water taking pipe and the water pump step by step, and the water taking operation is finished. The extracted deep seawater storage equipment is required to be insulated, protected from light and sealed for storage.
(2) 4ml of deep seawater concentrated solution is selected, mixed with 4L of seawater subjected to reverse osmosis treatment, electrolyzed at a direct current voltage of 10V for 5 minutes, collected, discharged from an anode pool, and uniformly mixed in a storage tank.
(3) And (3) mixing rose hydrosol with the acidic anode pool water obtained in the step (2), adding the rose hydrosol with the volume fraction of 1 per mill to obtain a mixed solution, adding trehalose powder into the mixed solution according to the mass fraction of 2% of trehalose, uniformly mixing and standing to obtain the product.
Example 2:
(1) drawing and treating technology of deep seawater below 200 m:
the specific procedure was the same as in example 1.
(2) Selecting 48ml of deep seawater concentrated solution, mixing with 4.8L of seawater subjected to reverse osmosis treatment, performing electrolysis treatment at 20V DC voltage for 5 minutes, collecting the effluent of the anode tank, and uniformly mixing in a storage tank.
(3) And (3) mixing rose hydrosol with the acidic anode pool water obtained in the step (2), wherein the volume fraction of the added rose hydrosol is 0.5 per mill to obtain a mixed solution, adding trehalose powder into the mixed solution according to the mass fraction of 0.1% of trehalose, mixing and shaking uniformly, and standing to obtain the product.
Example 3:
(1) drawing and treating technology of deep seawater below 200 m:
the specific procedure was the same as in example 1.
(2) Selecting 80ml of deep seawater concentrated solution, mixing with 4L of seawater subjected to reverse osmosis treatment, performing electrolysis treatment for 5 minutes under direct current voltage of 17V, collecting water discharged from an anode pool, and uniformly mixing in a storage tank.
(3) And (3) mixing rose hydrosol with the acidic anode pool water obtained in the step (2), adding 3 per mill of rose hydrosol to obtain a mixed solution, adding trehalose powder into the mixed solution according to the proportion of 3 mass percent of trehalose, uniformly mixing and standing to obtain the product.
pH in examples 1 to 3,17The data of the half-width of the O-nuclear magnetic resonance spectrum are shown in Table 1:
TABLE 1
| Example 1 | Example 2 | Example 3 | |
| pH | 3.05 | 2.80 | 2.57 |
| 17O-NMR | 52.32 | 51.23 | 50.97 |
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.
Claims (5)
1. A preparation method of an acidic skin-care spray containing mineral elements is characterized by comprising the following specific steps:
(1) mixing the purified and concentrated deep seawater concentrate with the seawater subjected to reverse osmosis treatment to obtain an electrolyte solution, wherein the addition ratio of the deep seawater concentrate is 1-20 per mill of the volume of the seawater subjected to reverse osmosis treatment;
(2) placing the electrolyte solution in an electrolytic cell, carrying out electrolysis treatment by using 10-20V direct current voltage, and taking an anode cell solution;
(3) adding rose hydrosol with volume fraction of 0.5-3 per mill into the anode solution;
(4) clarifying the solution added with the rose hydrosol, adding trehalose into the obtained solution with the rose fragrance in a mass fraction of 0.1-3.0%, and fully and uniformly mixing.
2. The method of claim 1 wherein the acidic skin care spray containing mineral elements is prepared by the method of claim 1,
the deep seawater concentrated solution in the step (1) is a solution which is rich in mineral elements and is obtained by taking seawater with the depth of less than 200 meters, and performing ultrafiltration and electrodialysis treatment, wherein the content of Ca, Mg and Zn elements is 1-1.8 times of that of common seawater.
3. The method for preparing the mineral element-containing acidic skin care spray according to claim 1, wherein the specific preparation method of the electrolytic anode solution in the step (2) is to use a mixed solution of deep seawater concentrated solution and reverse osmosis water as an electrolyte solution, iridium-titanium alloy as a negative electrode and a positive electrode, apply a direct current voltage of 10-20V to the two electrodes, and perform electrolysis for not less than 5 minutes; the parameters of the anode solution obtained at the anode of the electrolysis device are characterized in that: 1) the pH value is 2.0-6.5; 2)17half-peak width of O-nuclear magnetic resonance spectrum<65Hz。
4. The method for preparing acidic skin care spray containing mineral elements according to claim 1, wherein the rose hydrosol of step (3) is prepared by distilling fresh rose and separating water and oil, and has strong rose fragrance.
5. A mineral element-containing acidic skin care spray made according to the method of any one of claims 1-4.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010138490.7A CN111110609A (en) | 2020-03-03 | 2020-03-03 | Acidic skin-care spray containing mineral elements and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010138490.7A CN111110609A (en) | 2020-03-03 | 2020-03-03 | Acidic skin-care spray containing mineral elements and preparation method thereof |
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101702880A (en) * | 2007-04-25 | 2010-05-05 | 阿夸特克股份有限公司 | Highly stable electrolytic water with reduced NMR half line width |
| CN103387277A (en) * | 2012-05-11 | 2013-11-13 | 台盐实业股份有限公司 | Acidic electrolyzed water and composition thereof |
| TW201346071A (en) * | 2012-05-11 | 2013-11-16 | Taiyen Biotech Co Ltd | Acidic electrolyzed water and composition containing the same |
| CN105030552A (en) * | 2015-07-01 | 2015-11-11 | 吴杰 | Tear-free metabolism spray and preparation method thereof |
| TW201639794A (en) * | 2015-05-08 | 2016-11-16 | Korea Inst Ocean Sci & Tech | Method for electrolyzing sea water to produce mineral beverage and disinfecting water, and mineral beverage, and disinfecting water manufactured by the same |
| CN108675511A (en) * | 2018-05-03 | 2018-10-19 | 国家海洋局天津海水淡化与综合利用研究所 | A kind of preparation method of deep-sea mineralized liquid |
| CN109893473A (en) * | 2017-12-08 | 2019-06-18 | 罗颖明 | Set group and its application are maintained in bathypelagic concentrate skin nursing |
-
2020
- 2020-03-03 CN CN202010138490.7A patent/CN111110609A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101702880A (en) * | 2007-04-25 | 2010-05-05 | 阿夸特克股份有限公司 | Highly stable electrolytic water with reduced NMR half line width |
| CN103387277A (en) * | 2012-05-11 | 2013-11-13 | 台盐实业股份有限公司 | Acidic electrolyzed water and composition thereof |
| TW201346071A (en) * | 2012-05-11 | 2013-11-16 | Taiyen Biotech Co Ltd | Acidic electrolyzed water and composition containing the same |
| TW201639794A (en) * | 2015-05-08 | 2016-11-16 | Korea Inst Ocean Sci & Tech | Method for electrolyzing sea water to produce mineral beverage and disinfecting water, and mineral beverage, and disinfecting water manufactured by the same |
| CN105030552A (en) * | 2015-07-01 | 2015-11-11 | 吴杰 | Tear-free metabolism spray and preparation method thereof |
| CN109893473A (en) * | 2017-12-08 | 2019-06-18 | 罗颖明 | Set group and its application are maintained in bathypelagic concentrate skin nursing |
| CN108675511A (en) * | 2018-05-03 | 2018-10-19 | 国家海洋局天津海水淡化与综合利用研究所 | A kind of preparation method of deep-sea mineralized liquid |
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Application publication date: 20200508 |