CN111040700A - Epoxy daub for repairing high-strength concrete - Google Patents
Epoxy daub for repairing high-strength concrete Download PDFInfo
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- CN111040700A CN111040700A CN201911381928.8A CN201911381928A CN111040700A CN 111040700 A CN111040700 A CN 111040700A CN 201911381928 A CN201911381928 A CN 201911381928A CN 111040700 A CN111040700 A CN 111040700A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J163/00—Adhesives based on epoxy resins; Adhesives based on derivatives of epoxy resins
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Abstract
The invention discloses epoxy daub for repairing high-strength concrete, which comprises a component A and a component B, wherein the mass ratio of the component A to the component B is (8-12): 1; the component A comprises the following components in parts by weight: 35-50 parts of bisphenol A epoxy resin, 15-25 parts of modified epoxy resin, 10-15 parts of functional diluent, 20-40 parts of filler, 1-5 parts of coupling agent and 1-3 parts of auxiliary agent; the component B comprises the following components in parts by weight: 45-65 parts of hydrophobic amine modifier curing agent, 20-40 parts of filler, 1-5 parts of coupling agent, 1-5 parts of dispersing and wetting agent and 1-5 parts of auxiliary agent. The epoxy daub is a modified-base high-molecular high-strength repairing protective material, and has high adhesion, durability, impermeability, impact resistance, compactness, extremely high adhesion and extremely strong waterproof effect.
Description
Technical Field
The invention relates to the technical field of concrete surface repair, reinforcement, protection and the like in projects such as water conservancy and hydropower, tunnels, bridges, terraces and the like, in particular to epoxy daub for repairing high-strength concrete.
Background
Many of the domestic hydraulic engineering are hydraulic building concrete structures built in the early fifty years, and as capillary pores, air holes and micro cracks in the concrete provide channels for degradation factors such as carbon dioxide, soft water, acid rain, chloride ions and the like, the degradation reaction of all the concrete almost needs the participation of water, and simultaneously the water also serves as a carrier for harmful substances to enter and exit the concrete. In addition, the volume of the steel bar corrosion product is about 2.5-7 times of the original volume, the generated expansion pressure can cause cracking and peeling of concrete, and the cracking can cause more corrosive media to enter, so that more serious corrosion is caused. Therefore, most of the early hydraulic engineering is exposed in the nature for a long time, and is degraded to different degrees under the influence of water soaking or natural environment, and in order to guarantee the service life of concrete, the concrete is generally required to be repaired and protected to meet the use requirement.
At present, the domestic hydraulic engineering restoration technology uses an organic polymer material mixture to protect concrete, the organic polymer material has excellent weather resistance and water resistance, and is easy for field construction and curing forming, and the bonding effect formed between the organic polymer material and the concrete is the key for realizing long-term effective surface protection, but many materials can still be peeled off or easily washed out even reaching more than 3MPa when the materials are tested to be pulled, so how to improve the positive tensile strength and the anti-abrasion performance of the restoration material is an effective means for improving the concrete protection.
Disclosure of Invention
The invention aims to solve the problems of repairing, reinforcing and protecting the surface of a concrete body in the projects of water conservancy and hydropower, tunnels, bridges, terraces and the like, improving the waterproof, impact-resistant and wear-resistant capabilities of the concrete body, and particularly solving the concrete repairing problems of hydraulic buildings in the environments of impact abrasion resistance, cavitation erosion resistance and freeze thawing resistance.
The epoxy daub for repairing the high-strength concrete comprises a component A and a component B, wherein the mass ratio of the component A to the component B is (8-12): 1, preferably 10: 1; the component A comprises the following components in parts by weight: 35-50 parts of bisphenol A epoxy resin, 15-25 parts of modified epoxy resin, 10-15 parts of functional diluent, 20-40 parts of filler, 1-5 parts of coupling agent and 1-3 parts of auxiliary agent; the component B comprises the following components in parts by weight: 45-65 parts of hydrophobic amine modifier curing agent, 20-40 parts of filler, 1-5 parts of coupling agent, 1-5 parts of dispersing and wetting agent and 1-5 parts of auxiliary agent.
Preferably, the modified epoxy resin is at least one selected from polyurethane modified epoxy resin, phenolic aldehyde modified epoxy resin, high-molecular toughened epoxy resin and powdered nano rubber modified epoxy resin.
Preferably, the functional diluent is at least one selected from the group consisting of acetone, furfural, cyclohexanone, toluene, xylene, n-butanol, propylene oxide butyl ether, and glycidyl ether resin.
Preferably, the filler is selected from at least one of heavy calcium carbonate, light calcium carbonate, nano silicon dioxide, fumed silica, talcum powder, titanium dioxide, corundum, quartz powder and glass fiber.
Preferably, the coupling agent is selected from at least one of KH560, KH570, KH550, KH792 and hexamethyldisilazane.
Preferably, the hydrophobic amine modifier curing agent is at least one selected from modified aliphatic amine, modified alicyclic amine, phenolic amine and low molecular polyamide.
Preferably, the auxiliary agent is selected from at least one of penetrating agent, leveling agent, preservative, defoaming agent, ultraviolet resistant agent and pigment.
Preferably, when the modified epoxy resin is composed of a plurality of components, the ratio of the components is arbitrary; when the functional diluent consists of a plurality of components, the proportion of each component is any proportion; when the filler consists of a plurality of components, the proportion of each component is any proportion; when the coupling agent consists of a plurality of components, the proportion of each component is any proportion; when the hydrophobic amine modifier curing agent consists of a plurality of components, the proportion of each component is any proportion; when the modified epoxy resin additive consists of a plurality of components, the proportion of each component is any proportion.
The invention is further illustrated below:
according to the invention, the modified epoxy resin can improve the strength and impact resistance of the product and improve the toughness and scouring resistance of the product. The functional diluent can adjust the fluidity and viscosity of the product to adapt to construction requirements, improve the toughness of the product and the like. The filler can adjust the viscosity and the sag resistance of the product, and improve the strength, the impact resistance and the abrasion resistance of the product. The coupling agent can improve the adhesive property range and adhesive strength of products. The modified amine curing agent can promote the product to be cured, adjust the curing speed and improve the impact resistance and the bonding strength of the product. The assistant can improve the penetration and wettability of the product, corrosion resistance, color mixing, light aging resistance, bubble elimination and the like.
The invention finds that the high strength, the abrasion resistance and the cavitation erosion resistance can be really achieved through the matching of different amine curing agents and the combination of different fillers and auxiliaries. The epoxy daub can form firm bonding on a wet concrete interface with water, has moderate sagging property, does not flow on a vertical surface and a back surface, does not stick to a gluing tool, has high bonding strength after curing, and is scour-resistant.
During preparation, the component A and the component B are respectively stirred and mixed uniformly, then the liquid material and the auxiliary agent are added into the raw materials in the components, the filler is added during slow stirring, the mixture is stirred and mixed for 0.5 to 1 hour, then the powder on the inner wall of the kettle is cleaned by scraping the wall, then the mixture is stirred for 0.5 hour, then the mixed material is ground by a three-roller machine to be uniform and fine, and the mixture is discharged to a packaging barrel, so that the high-strength epoxy daub for repairing concrete is obtained.
In a word, the epoxy daub is a modified-base high-polymer high-strength repairing protective material, and has high adhesive force, durability, impermeability, impact resistance, compactness, extremely high adhesive force and extremely strong waterproof effect.
Detailed Description
Example 1
The epoxy daub for repairing the high-strength concrete comprises a component A and a component B, wherein the mass ratio of the component A to the component B is 10: 1; the component A comprises the following components in parts by weight: 35-50 parts of bisphenol A epoxy resin, 15-25 parts of polyurethane epoxy resin, 10-15 parts of functional diluent (furfural and acetone), 20-40 parts of filler (heavy calcium and nano silicon dioxide), 1-5 parts of coupling agent (KH560) and 1-3 parts of auxiliary agent (flatting agent and defoaming agent); the component B comprises the following components in parts by weight: 45-65 parts of hydrophobic amine modifier curing agent (modified alicyclic amine and phenolic amine), 20-40 parts of filler (heavy calcium and fumed silica), 1-5 parts of coupling agent (KH550), 1-5 parts of dispersing wetting agent and 1-5 parts of auxiliary agent (pigment).
Example 2
The epoxy daub for repairing the high-strength concrete comprises a component A and a component B, wherein the mass ratio of the component A to the component B is 10: 1; the component A comprises the following components in parts by weight: 35-50 parts of bisphenol A epoxy resin, 15-25 parts of powder nano rubber modified epoxy resin, 10-15 parts of functional diluent (epoxypropane butyl ether and acetone), 20-40 parts of filler (light calcium and corundum), 1-5 parts of coupling agent (KH560) and 1-3 parts of auxiliary agent (flatting agent and defoaming agent); the component B comprises the following components in parts by weight: 45-65 parts of hydrophobic amine modifier curing agent (modified alicyclic amine and low molecular polyamide), 20-40 parts of filler (heavy calcium and fumed silica), 1-5 parts of coupling agent (KH550), 1-5 parts of dispersing and wetting agent and 1-5 parts of auxiliary agent (pigment).
Example 3
The epoxy daub for repairing the high-strength concrete comprises a component A and a component B, wherein the mass ratio of the component A to the component B is 10: 1; the component A comprises the following components in parts by weight: 35-50 parts of bisphenol A epoxy resin, 15-25 parts of high-molecular toughened epoxy resin, 10-15 parts of a functional diluent (glycidyl ether resin and acetone), 20-40 parts of nano calcium and glass fiber, 1-5 parts of a coupling agent (KH560) and 1-3 parts of an auxiliary agent (a leveling agent and a defoaming agent); the component B comprises the following components in parts by weight: 45-65 parts of hydrophobic amine modifier curing agent (modified alicyclic amine, phenolic aldehyde amine and low molecular polyamide), 20-40 parts of filler (heavy calcium and fumed silica), 1-5 parts of coupling agent (KH550), 1-5 parts of dispersing wetting agent and 1-5 parts of auxiliary agent (pigment).
Example 4
The control group comprises a component A and a component B, wherein the mass ratio of the component A to the component B is 10: 1; the component A comprises the following components in parts by weight: 45-55 parts of bisphenol A epoxy resin, 10-15 parts of a functional diluent (furfural and acetone), 20-40 parts of a filler (heavy calcium and fumed silica), 1-5 parts of a coupling agent (KH560) and 1-3 parts of an auxiliary agent (a leveling agent and a defoaming agent); the component B comprises the following components in parts by weight: 45-65 parts of hydrophobic amine modifier curing agent (modified fatty amine and phenolic amine), 20-40 parts of filler (heavy calcium and fumed silica), 1-5 parts of coupling agent (KH550), 1-5 parts of dispersing wetting agent and 1-5 parts of auxiliary agent (pigment).
The results of comparing the effects of examples 1 to 4 are shown in table 1:
TABLE 1
Claims (8)
1. The epoxy daub for repairing the high-strength concrete is characterized by comprising a component A and a component B, wherein the mass ratio of the component A to the component B is (8-12): 1; the component A comprises the following components in parts by weight: 35-50 parts of bisphenol A epoxy resin, 15-25 parts of modified epoxy resin, 10-15 parts of functional diluent, 20-40 parts of filler, 1-5 parts of coupling agent and 1-3 parts of auxiliary agent; the component B comprises the following components in parts by weight: 45-65 parts of hydrophobic amine modifier curing agent, 20-40 parts of filler, 1-5 parts of coupling agent, 1-5 parts of dispersing and wetting agent and 1-5 parts of auxiliary agent.
2. The epoxy cement of claim 1, wherein the modified epoxy resin is at least one selected from the group consisting of a urethane-modified epoxy resin, a phenolic-modified epoxy resin, a polymeric toughenable epoxy resin, and a powdered nano rubber-modified epoxy resin.
3. The epoxy cement of claim 1, wherein the functional diluent is at least one selected from the group consisting of acetone, furfural, cyclohexanone, toluene, xylene, n-butanol, propylene oxide butyl ether, glycidyl ether resins.
4. The epoxy mastic of claim 1, wherein the filler is selected from at least one of heavy calcium carbonate, light calcium carbonate, nano silica, fumed silica, talc, titanium dioxide, corundum, quartz powder, and glass fiber.
5. The epoxy mastic of claim 1, wherein the coupling agent is selected from at least one of KH560, KH570, KH550, KH792, and hexamethyldisilazane.
6. The epoxy cement of claim 1, wherein the hydrophobic amine modifier curing agent is at least one selected from the group consisting of modified aliphatic amines, modified alicyclic amines, phenolic amines, and low molecular weight polyamides.
7. The epoxy cement of claim 1, wherein the auxiliary agent is at least one selected from the group consisting of a penetrating agent, a leveling agent, a preservative, a defoaming agent, an ultraviolet ray resistant agent, and a pigment.
8. The epoxy mastic as claimed in any one of claims 1 to 7, wherein when the modified epoxy resin is composed of a plurality of components, the ratio of the components is arbitrary; when the functional diluent consists of a plurality of components, the proportion of each component is any proportion; when the filler consists of a plurality of components, the proportion of each component is any proportion; when the coupling agent consists of a plurality of components, the proportion of each component is any proportion; when the hydrophobic amine modifier curing agent consists of a plurality of components, the proportion of each component is any proportion; when the modified epoxy resin additive consists of a plurality of components, the proportion of each component is any proportion.
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CN201911381928.8A CN111040700A (en) | 2019-12-28 | 2019-12-28 | Epoxy daub for repairing high-strength concrete |
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CN201911381928.8A CN111040700A (en) | 2019-12-28 | 2019-12-28 | Epoxy daub for repairing high-strength concrete |
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Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111646748A (en) * | 2020-05-25 | 2020-09-11 | 广东合胜实业股份有限公司 | High-strength anti-permeability leakage repairing material and preparation method thereof |
CN112160258A (en) * | 2020-10-30 | 2021-01-01 | 中铁四院集团工程建设有限责任公司 | Concrete repairing method for bridge pier body |
CN112625635A (en) * | 2020-12-18 | 2021-04-09 | 厦门虹瑞卫浴有限公司 | High-strength wear-resistant impact-resistant epoxy repair adhesive special for factory floor and preparation method and use method thereof |
CN113563835A (en) * | 2021-08-03 | 2021-10-29 | 宋华杰 | Impervious waterproof adhesive for leakage stoppage on back water surface and preparation method thereof |
KR102351716B1 (en) * | 2020-09-02 | 2022-01-13 | 이상일 | Solvent-free two-part primer composition for concrete |
CN114369436A (en) * | 2022-01-17 | 2022-04-19 | 湛江港石化码头有限责任公司 | Nano modified anti-leakage constant-fire repairing elastic material |
CN114381185A (en) * | 2022-01-17 | 2022-04-22 | 湛江港石化码头有限责任公司 | High-strength anti-oil-leakage tank bottom and pipeline non-fire repairing material and method |
KR102405009B1 (en) * | 2021-01-19 | 2022-06-02 | 이상일 | Eco-friendly finishing method for concrete surface |
CN116933689A (en) * | 2023-07-25 | 2023-10-24 | 水利部交通运输部国家能源局南京水利科学研究院 | Epoxy cement protective coating anti-sagging evaluation method based on rheological parameters |
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Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111646748A (en) * | 2020-05-25 | 2020-09-11 | 广东合胜实业股份有限公司 | High-strength anti-permeability leakage repairing material and preparation method thereof |
KR102351716B1 (en) * | 2020-09-02 | 2022-01-13 | 이상일 | Solvent-free two-part primer composition for concrete |
CN112160258A (en) * | 2020-10-30 | 2021-01-01 | 中铁四院集团工程建设有限责任公司 | Concrete repairing method for bridge pier body |
CN112625635A (en) * | 2020-12-18 | 2021-04-09 | 厦门虹瑞卫浴有限公司 | High-strength wear-resistant impact-resistant epoxy repair adhesive special for factory floor and preparation method and use method thereof |
KR102405009B1 (en) * | 2021-01-19 | 2022-06-02 | 이상일 | Eco-friendly finishing method for concrete surface |
CN113563835A (en) * | 2021-08-03 | 2021-10-29 | 宋华杰 | Impervious waterproof adhesive for leakage stoppage on back water surface and preparation method thereof |
CN114369436A (en) * | 2022-01-17 | 2022-04-19 | 湛江港石化码头有限责任公司 | Nano modified anti-leakage constant-fire repairing elastic material |
CN114381185A (en) * | 2022-01-17 | 2022-04-22 | 湛江港石化码头有限责任公司 | High-strength anti-oil-leakage tank bottom and pipeline non-fire repairing material and method |
CN114381185B (en) * | 2022-01-17 | 2022-11-25 | 湛江港石化码头有限责任公司 | High-strength anti-oil-leakage tank bottom and pipeline non-fire repairing material and method |
CN116933689A (en) * | 2023-07-25 | 2023-10-24 | 水利部交通运输部国家能源局南京水利科学研究院 | Epoxy cement protective coating anti-sagging evaluation method based on rheological parameters |
CN116933689B (en) * | 2023-07-25 | 2024-01-30 | 水利部交通运输部国家能源局南京水利科学研究院 | Epoxy cement protective coating anti-sagging evaluation method based on rheological parameters |
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Application publication date: 20200421 |