CN111036172B - Attapulgite adsorbent and preparation method thereof - Google Patents
Attapulgite adsorbent and preparation method thereof Download PDFInfo
- Publication number
- CN111036172B CN111036172B CN201911385211.0A CN201911385211A CN111036172B CN 111036172 B CN111036172 B CN 111036172B CN 201911385211 A CN201911385211 A CN 201911385211A CN 111036172 B CN111036172 B CN 111036172B
- Authority
- CN
- China
- Prior art keywords
- adsorbent
- adsorbent particles
- powder
- parts
- finished product
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/12—Naturally occurring clays or bleaching earth
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
- B01J20/28016—Particle form
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Dispersion Chemistry (AREA)
- Geochemistry & Mineralogy (AREA)
- Inorganic Chemistry (AREA)
- Cosmetics (AREA)
- Medicinal Preparation (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
A attapulgite adsorbent consisting of adsorbent particles divided into an upper adsorbent particle portion, a bitterant layer and a lower adsorbent particle portion, the bitterant layer being disposed between the upper adsorbent particle portion and the lower adsorbent particle portion, the upper adsorbent particle portion being provided with a dyed tip, the lower adsorbent particle portion also being provided with a dyed tip, the bitterant layer consisting of bitter powder. The attapulgite adsorbent has the advantages that the attapulgite adsorbent is skillfully designed on the basis of product structure and raw materials, and has the function of preventing mistaken eating and excellent adsorption capacity.
Description
Technical Field
The invention belongs to the technical field, and particularly relates to a attapulgite adsorbent and a preparation method thereof.
Background
With the improvement of living standard, the air purification adsorbent is used in more and more families, attapulgite clay, which is called attapulgite clay for short, is a water-containing magnesium-rich aluminosilicate clay mineral with a layer chain structure, the attapulgite clay has the functions of sterilization, deodorization, detoxification and insecticidal property and strong adsorption capacity, the reserves of China are huge, and the raw materials are cheap, so the attapulgite clay is an excellent material for manufacturing the adsorbent.
The existing household attapulgite adsorbent is mainly divided into a powder type and a spherical particle type, wherein the powder type is generally packaged by using an air-permeable bag, the contact area with air is small, the adsorption rate is slow, and the cleaning is difficult if the packaging bag is damaged; the granule type is generally taken out then holds in the container, and is main still the top layer with the air contact, and area of contact is big enough, and the easy condition that takes place children to eat by mistake simultaneously causes the injury accident, in case overturn, spherical granule rolls everywhere and also does not well pick up, consequently designs one kind and has the function of preventing eating by mistake, and has fabulous adsorption efficiency's adsorbent and has important meaning.
Disclosure of Invention
In order to meet the requirements, the attapulgite adsorbent has the function of preventing mistaken feeding, has excellent adsorption capacity and is suitable for daily use in families.
The technical scheme adopted by the invention for solving the technical problems is as follows: a attapulgite adsorbent consisting of adsorbent particles divided into an upper adsorbent particle portion, a bitterant layer and a lower adsorbent particle portion, the bitterant layer being disposed between the upper adsorbent particle portion and the lower adsorbent particle portion, the upper adsorbent particle portion being provided with a dyed tip, the lower adsorbent particle portion also being provided with a dyed tip, the bitterant layer consisting of bitter powder.
The adsorbent block comprises the following raw materials in mass percent: 70-80 parts of attapulgite, 10-20 parts of medical stone powder, 10-20 parts of starch, 10-15 parts of carrageenan, 5-10 parts of lignocellulose, 3-5 parts of pigment powder and 1-3 parts of bitter agent powder;
preferably, the pigment powder is a dark green or black edible pigment.
Preferably, the bitter agent powder is fel-terrae powder or balsam pear powder.
The preparation method comprises the following steps:
(1) mixing attapulgite, medical stone powder, starch, carrageenan and lignocellulose in specified amount, heating in water bath at 60-70 deg.C for 15-25min, stirring continuously during heating process, dividing into two parts, cooling, and standing;
(2) adding pigment powder into one part of the product prepared in the step 1, and uniformly stirring to prepare a dyeing tip raw material;
(3) pouring the dyeing tip raw material prepared in the step 2 into a mould plate, pouring the product prepared in the step 1 to prepare a semi-finished product group at the lower part of the adsorbent particles, and preparing a semi-finished product group at the upper part of the adsorbent particles in the same mould plate by the same method;
(4) coating a layer of bitter agent powder on the semi-finished product group at the lower part of the adsorbent particles, then pressing the two die plates together to connect the semi-finished product group at the lower part of the adsorbent particles and the semi-finished product group at the upper part of the adsorbent particles, and then demoulding and cutting to obtain the semi-finished product of the adsorbent particles;
(5) and (4) putting the semi-finished product of the adsorbent particles prepared in the step (4) into a drying chamber, drying for 20-24h at 50-60 ℃, weighing and packaging to prepare a finished product, and warehousing.
The two ends of the adsorbent are dark green or black, and generate great color contrast with other parts, the colors are disliked by children, the probability of taking by mistake is reduced, the surface part of the adsorbent is in a sharp-pricked shape, the contact area with air can be greatly increased, the effect of enhancing the adsorption capacity is achieved, the product looks not good, the medical stone is nontoxic and rough, the product is uncomfortable to touch, the taking by mistake is further reduced, the product is not hard, the pricking condition cannot occur, in case of mistaken eating, the internal bitter agent is extremely bitter, the adsorbent is not spherical, the adsorbent cannot roll around after being overturned, and the adsorbent is easy to collect.
Lignocellulose is added into the adsorbent part, so that the structural strength of the adsorbent part can be improved, the adsorbent is prevented from being broken, and the starch and the carrageenan which are used as adhesives of the adsorbent are nontoxic and harmless.
According to the product structure, adopt in the production process to be equipped with a plurality of pit mould boards, whole layering is pressed earlier, and the mode of cutting pelletization is high-efficient quick.
The invention has the beneficial effects that: the attapulgite adsorbent with the function of preventing mistaken eating and excellent adsorption capacity is obtained by skillfully designing the product structure and the raw materials.
Drawings
The invention is further illustrated by the following figures and examples
Fig. 1 is a schematic structural view of the present invention.
In the figure: 1. the upper part of the adsorbent particle, 1.1. dyeing tip, 2. bittering agent layer, and 3. lower part of the adsorbent particle.
Detailed Description
The attapulgite adsorbent in figure 1 consists of adsorbent particles, wherein: 1. the upper part of the adsorbent particle, 1.1. dyeing tip, 2. bittering agent layer, and 3. lower part of the adsorbent particle. The adsorbent particles are divided into an upper part of the adsorbent particles, a bittering agent layer and a lower part of the adsorbent particles, the bittering agent layer is arranged between the upper part of the adsorbent particles and the lower part of the adsorbent particles, the upper part of the adsorbent particles is provided with a dyeing tip, the lower part of the adsorbent particles is also provided with one bittering agent layer, and the bittering agent layer is composed of bitter powder.
The adsorbent block comprises the following raw materials in mass percent: 70 parts of attapulgite, 12 parts of medical stone powder, 15 parts of starch, 12 parts of carrageenan, 6 parts of lignocellulose, 4 parts of pigment powder and 2 parts of bitter agent powder;
in this example, the pigment powder is a dark green edible pigment powder.
In this example, the bittering agent powder is a powder of scabrous elephantfoot herb.
The preparation method comprises the following steps:
(1) mixing attapulgite, medical stone powder, starch, carrageenan and lignocellulose in specified amount, heating in water bath at 65 deg.C for 15min, stirring continuously during heating process, dividing into two parts, cooling, and standing for use;
(2) adding pigment powder into one part of the product prepared in the step 1, and uniformly stirring to prepare a dyeing tip raw material;
(3) pouring the dyeing tip raw material prepared in the step 2 into a mould plate, pouring the product prepared in the step 1 to prepare a semi-finished product group at the lower part of the adsorbent particles, and preparing a semi-finished product group at the upper part of the adsorbent particles in the same mould plate by the same method;
(4) coating a layer of bitter agent powder on the semi-finished product group at the lower part of the adsorbent particles, then pressing the two die plates together to connect the semi-finished product group at the lower part of the adsorbent particles and the semi-finished product group at the upper part of the adsorbent particles, and then demoulding and cutting to obtain the semi-finished product of the adsorbent particles;
(5) and (4) putting the semi-finished product of the adsorbent particles prepared in the step (4) into a drying chamber, drying for 23 hours at 55 ℃, weighing and packaging to prepare a finished product, and warehousing.
Example 2
The attapulgite adsorbent in figure 1 consists of adsorbent particles, wherein: 1. the upper part of the adsorbent particle, 1.1. dyeing tip, 2. bittering agent layer, and 3. lower part of the adsorbent particle. The adsorbent particles are divided into an upper part of the adsorbent particles, a bittering agent layer and a lower part of the adsorbent particles, the bittering agent layer is arranged between the upper part of the adsorbent particles and the lower part of the adsorbent particles, the upper part of the adsorbent particles is provided with a dyeing tip, the lower part of the adsorbent particles is also provided with a dyeing tip, and the bittering agent layer is composed of bitter powder.
The adsorbent block comprises the following raw materials in mass percent: 80 parts of attapulgite, 20 parts of medical stone powder, 10 parts of starch, 12 parts of carrageenan, 6 parts of lignocellulose, 4 parts of pigment powder and 2 parts of bitter agent powder;
in this example, the pigment powder is a black edible pigment powder.
In this example, the bittering agent powder is bitter gourd powder.
The preparation method comprises the following steps:
(1) mixing attapulgite, medical stone powder, starch, carrageenan and lignocellulose in specified amount, heating in water bath at 70 deg.C for 15min, stirring continuously during heating process, dividing into two parts, cooling, and standing for use;
(2) adding pigment powder into one part of the product prepared in the step 1, and uniformly stirring to prepare a dyeing tip raw material;
(3) pouring the dyeing tip raw material prepared in the step 2 into a mould plate, pouring the product prepared in the step 1 to prepare a semi-finished product group at the lower part of the adsorbent particles, and preparing a semi-finished product group at the upper part of the adsorbent particles in the same mould plate by the same method;
(4) coating a layer of bitter agent powder on the semi-finished product group at the lower part of the adsorbent particles, then pressing the two die plates together to connect the semi-finished product group at the lower part of the adsorbent particles and the semi-finished product group at the upper part of the adsorbent particles, and then demoulding and cutting to obtain the semi-finished product of the adsorbent particles;
(5) and (4) putting the semi-finished product of the adsorbent particles prepared in the step (4) into a drying chamber, drying for 20 hours at the temperature of 60 ℃, weighing and packaging to prepare a finished product, and warehousing.
Claims (4)
1. The attapulgite adsorbent consists of adsorbent particles and is characterized in that: the adsorbent particles are divided into an upper part of the adsorbent particles, a bittering agent layer and a lower part of the adsorbent particles, the bittering agent layer is arranged between the upper part of the adsorbent particles and the lower part of the adsorbent particles, the upper part of the adsorbent particles is provided with a dyeing tip, the lower part of the adsorbent particles is also provided with a dyeing tip, and the bittering agent layer consists of bitter powder;
the adsorbent comprises the following raw materials in parts by mass: 70-80 parts of attapulgite, 10-20 parts of medical stone powder, 10-20 parts of starch, 10-15 parts of carrageenan, 5-10 parts of lignocellulose, 3-5 parts of pigment powder and 1-3 parts of bitter agent powder.
2. The attapulgite adsorbent according to claim 1, wherein: the pigment powder is dark green or black edible pigment.
3. The attapulgite adsorbent according to claim 1, wherein: the bitter agent powder is herba Swertiae Dilutae powder or fructus Momordicae Charantiae powder.
4. The method for preparing the attapulgite adsorbent according to claim 1, which is characterized in that: the method comprises the following steps:
(1) mixing attapulgite, medical stone powder, starch, carrageenan and lignocellulose in specified amount, heating in water bath at 60-70 deg.C for 15-25min, stirring continuously during heating process, dividing into two parts, cooling, and standing;
(2) adding pigment powder into one part of the product prepared in the step 1, and uniformly stirring to prepare a dyeing tip raw material;
(3) pouring the dyeing tip raw material prepared in the step 2 into a mould plate, pouring the product prepared in the step 1 to prepare a semi-finished product group at the lower part of the adsorbent particles, and preparing a semi-finished product group at the upper part of the adsorbent particles in the same mould plate by the same method;
(4) coating a layer of bitter agent powder on the semi-finished product group at the lower part of the adsorbent particles, then pressing the two die plates together to connect the semi-finished product group at the lower part of the adsorbent particles and the semi-finished product group at the upper part of the adsorbent particles, and then demoulding and cutting to obtain the semi-finished product of the adsorbent particles;
(5) and (4) putting the semi-finished product of the adsorbent particles prepared in the step (4) into a drying chamber, drying for 20-24h at 50-60 ℃, weighing and packaging to prepare a finished product, and warehousing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911385211.0A CN111036172B (en) | 2019-12-28 | 2019-12-28 | Attapulgite adsorbent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911385211.0A CN111036172B (en) | 2019-12-28 | 2019-12-28 | Attapulgite adsorbent and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN111036172A CN111036172A (en) | 2020-04-21 |
| CN111036172B true CN111036172B (en) | 2020-07-07 |
Family
ID=70241020
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201911385211.0A Active CN111036172B (en) | 2019-12-28 | 2019-12-28 | Attapulgite adsorbent and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN111036172B (en) |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5382048A (en) * | 1976-11-18 | 1978-07-20 | Mitsubishi Rayon Co Ltd | Method of treating polyvinyl alchol containing waste water |
| CN103537255A (en) * | 2013-07-28 | 2014-01-29 | 王泽辉 | Nanometer oxide ceramic purification and adsorption material with decomposition and bactericidal performance |
| CN108393063A (en) * | 2018-04-28 | 2018-08-14 | 中国科学院水生生物研究所 | A kind of preparation method and application of eutrophic lake sediment phosphorus adsorbent |
-
2019
- 2019-12-28 CN CN201911385211.0A patent/CN111036172B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN111036172A (en) | 2020-04-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103704483A (en) | Feed fermented by utilizing traditional Chinese medicine drugs and preparation method of feed | |
| CN104286838B (en) | A kind of Cordyceps restructuring rice rich in cordycepin and preparation method thereof | |
| CN106723058A (en) | Prepare the method for having and increasing resistance and property starch easy to digest | |
| CN111036172B (en) | Attapulgite adsorbent and preparation method thereof | |
| CN108813224A (en) | A kind of adult fish special compound feed and its preparation method and application hybridizing mandarin fish | |
| CN105614128A (en) | Chicken feed and preparation method thereof | |
| CN102599288A (en) | Tea blend composed of white tea as base tea and pine pollen | |
| CN102406011A (en) | Preparation method of Paeonia ostii flower tea | |
| CN102630949B (en) | Insoluble dietary fiber and manufacturing method for insoluble dietary fiber | |
| CN111001381B (en) | Household attapulgite adsorbent and preparation method thereof | |
| CN106212771B (en) | Fuzhuan tea capable of reducing blood sugar and blood pressure and production process of Fuzhuan tea | |
| CN103373846A (en) | Medical stone sintering vessel and manufacturing process | |
| CN104542862B (en) | Agropyron dietary-fiber biscuit and preparation method thereof | |
| CN112715278B (en) | Chinese medicinal Coriolus versicolor and its cultivation method | |
| CN106234776A (en) | A kind of Hirudo sucks feedstuff | |
| CN204994493U (en) | Utilize fine dried noodle machine of organic raw and other materials production vermicelli | |
| CN107568308A (en) | A kind of square ham batch mould | |
| CN1129664A (en) | Packging products made from corn-stalks and manufacture thereof | |
| CN206491311U (en) | A kind of full-automatic cake system processed | |
| KR100334952B1 (en) | A method for preparing disposable dishes degrading naturally and a manufacturing apparatus thereof | |
| CN106258433A (en) | A kind of Herba Dendrobii implantation methods | |
| CN111499769A (en) | Process for extracting mulberry leaf polysaccharide | |
| CN2398840Y (en) | Tea products | |
| CN117652620B (en) | Dendrobium officinale noodles and preparation method thereof | |
| CN102311243A (en) | Method for manufacturing flowerpot by utilizing crayfish shells |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |