CN111005229A - Carbon fiber sizing agent and preparation method thereof - Google Patents
Carbon fiber sizing agent and preparation method thereof Download PDFInfo
- Publication number
- CN111005229A CN111005229A CN201911375205.7A CN201911375205A CN111005229A CN 111005229 A CN111005229 A CN 111005229A CN 201911375205 A CN201911375205 A CN 201911375205A CN 111005229 A CN111005229 A CN 111005229A
- Authority
- CN
- China
- Prior art keywords
- carbon fiber
- sizing agent
- unsaturated acid
- water
- polyether alcohol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920000049 Carbon (fiber) Polymers 0.000 title claims abstract description 159
- 239000004917 carbon fiber Substances 0.000 title claims abstract description 159
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 title claims abstract description 132
- 238000004513 sizing Methods 0.000 title claims abstract description 75
- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 51
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 54
- 239000002131 composite material Substances 0.000 claims abstract description 49
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract description 44
- 229920000570 polyether Polymers 0.000 claims abstract description 44
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 43
- 239000002253 acid Substances 0.000 claims abstract description 40
- 239000004841 bisphenol A epoxy resin Substances 0.000 claims abstract description 17
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims abstract description 14
- 239000013638 trimer Substances 0.000 claims abstract description 13
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims abstract description 10
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 8
- BXGYYDRIMBPOMN-UHFFFAOYSA-N 2-(hydroxymethoxy)ethoxymethanol Chemical compound OCOCCOCO BXGYYDRIMBPOMN-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000853 adhesive Substances 0.000 claims abstract description 4
- 230000001070 adhesive effect Effects 0.000 claims abstract description 4
- 238000000034 method Methods 0.000 claims description 61
- 229920005989 resin Polymers 0.000 claims description 49
- 239000011347 resin Substances 0.000 claims description 49
- 238000003756 stirring Methods 0.000 claims description 37
- 238000004519 manufacturing process Methods 0.000 claims description 24
- 150000002148 esters Chemical class 0.000 claims description 22
- 239000000243 solution Substances 0.000 claims description 18
- 239000000835 fiber Substances 0.000 claims description 16
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 15
- 238000010438 heat treatment Methods 0.000 claims description 13
- 239000011159 matrix material Substances 0.000 claims description 12
- 229920006305 unsaturated polyester Polymers 0.000 claims description 12
- 239000000839 emulsion Substances 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 6
- 239000000725 suspension Substances 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 5
- 229920001567 vinyl ester resin Polymers 0.000 claims description 5
- 238000005507 spraying Methods 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- 239000011259 mixed solution Substances 0.000 claims description 2
- 238000001125 extrusion Methods 0.000 claims 1
- 229920001225 polyester resin Polymers 0.000 abstract description 13
- 239000004645 polyester resin Substances 0.000 abstract description 13
- 239000003365 glass fiber Substances 0.000 abstract description 6
- 239000003822 epoxy resin Substances 0.000 description 32
- 229920000647 polyepoxide Polymers 0.000 description 32
- 230000008569 process Effects 0.000 description 31
- 238000000465 moulding Methods 0.000 description 14
- 229920002239 polyacrylonitrile Polymers 0.000 description 11
- 238000001035 drying Methods 0.000 description 10
- 238000006243 chemical reaction Methods 0.000 description 9
- 238000003763 carbonization Methods 0.000 description 8
- 239000004744 fabric Substances 0.000 description 8
- 239000000463 material Substances 0.000 description 8
- 125000003700 epoxy group Chemical group 0.000 description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 5
- 229910052760 oxygen Inorganic materials 0.000 description 5
- 238000004381 surface treatment Methods 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- 230000004913 activation Effects 0.000 description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 4
- 229920002554 vinyl polymer Polymers 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 3
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 3
- 230000007547 defect Effects 0.000 description 3
- 125000001033 ether group Chemical group 0.000 description 3
- 238000009730 filament winding Methods 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 238000003825 pressing Methods 0.000 description 3
- 238000001721 transfer moulding Methods 0.000 description 3
- -1 and usually Substances 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 239000000805 composite resin Substances 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 238000005520 cutting process Methods 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000007380 fibre production Methods 0.000 description 2
- 238000001879 gelation Methods 0.000 description 2
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 238000001746 injection moulding Methods 0.000 description 2
- JYGBQHPBHZTIAP-UHFFFAOYSA-N methoxymethane 2-methylprop-2-enoic acid Chemical compound C(C(=C)C)(=O)O.COC.C(C(=C)C)(=O)O JYGBQHPBHZTIAP-UHFFFAOYSA-N 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000002791 soaking Methods 0.000 description 2
- 238000003892 spreading Methods 0.000 description 2
- 230000007480 spreading Effects 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 238000009941 weaving Methods 0.000 description 2
- WFUGQJXVXHBTEM-UHFFFAOYSA-N 2-hydroperoxy-2-(2-hydroperoxybutan-2-ylperoxy)butane Chemical group CCC(C)(OO)OOC(C)(CC)OO WFUGQJXVXHBTEM-UHFFFAOYSA-N 0.000 description 1
- 229920002748 Basalt fiber Polymers 0.000 description 1
- 240000004282 Grewia occidentalis Species 0.000 description 1
- 239000004760 aramid Substances 0.000 description 1
- 229920006231 aramid fiber Polymers 0.000 description 1
- 239000011203 carbon fibre reinforced carbon Substances 0.000 description 1
- 239000011304 carbon pitch Substances 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 238000010000 carbonizing Methods 0.000 description 1
- 239000007822 coupling agent Substances 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000007723 die pressing method Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 125000004185 ester group Chemical group 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- GEMHFKXPOCTAIP-UHFFFAOYSA-N n,n-dimethyl-n'-phenylcarbamimidoyl chloride Chemical group CN(C)C(Cl)=NC1=CC=CC=C1 GEMHFKXPOCTAIP-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229920000620 organic polymer Polymers 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- 238000002407 reforming Methods 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 230000033764 rhythmic process Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229920005992 thermoplastic resin Polymers 0.000 description 1
- 229920001187 thermosetting polymer Polymers 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 238000005829 trimerization reaction Methods 0.000 description 1
- 229920006337 unsaturated polyester resin Polymers 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
- 238000004804 winding Methods 0.000 description 1
Images
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/55—Epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
- C08J5/06—Reinforcing macromolecular compounds with loose or coherent fibrous material using pretreated fibrous materials
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/2246—Esters of unsaturated carboxylic acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/40—Fibres of carbon
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing & Machinery (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Reinforced Plastic Materials (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201911375205.7A CN111005229B (en) | 2019-12-27 | 2019-12-27 | Carbon fiber sizing agent and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201911375205.7A CN111005229B (en) | 2019-12-27 | 2019-12-27 | Carbon fiber sizing agent and preparation method thereof |
Publications (2)
Publication Number | Publication Date |
---|---|
CN111005229A true CN111005229A (en) | 2020-04-14 |
CN111005229B CN111005229B (en) | 2021-03-02 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201911375205.7A Active CN111005229B (en) | 2019-12-27 | 2019-12-27 | Carbon fiber sizing agent and preparation method thereof |
Country Status (1)
Country | Link |
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CN (1) | CN111005229B (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113832728A (en) * | 2021-10-27 | 2021-12-24 | 北京化工大学 | Sizing agent for carbon fiber, preparation method thereof and composite material |
CN114182533A (en) * | 2021-12-07 | 2022-03-15 | 陈宗良 | Carbon fiber sizing agent and preparation method thereof, and carbon fiber composite material and preparation method thereof |
CN114960207A (en) * | 2022-06-21 | 2022-08-30 | 浙江巨化新材料研究院有限公司 | Perfluorosulfonic acid carbon fiber composite material and preparation method and application thereof |
Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS60104578A (en) * | 1983-11-05 | 1985-06-08 | 竹本油脂株式会社 | Sizing agent for carbon fiber |
JP2000355883A (en) * | 1999-06-16 | 2000-12-26 | Mitsubishi Rayon Co Ltd | Sizing agent for reinforcing fiber |
JP2002013069A (en) * | 2000-06-29 | 2002-01-18 | Mitsubishi Rayon Co Ltd | Sizing agent for carbon fiber, method for sizing carbon fiber, sizing-treated carbon fiber, and sheet-like material and fiber-reinforced composite material containing the same |
CN103797183A (en) * | 2011-09-22 | 2014-05-14 | 三洋化成工业株式会社 | Fiber sizing agent composition |
CN105378176A (en) * | 2013-09-27 | 2016-03-02 | 松本油脂制药株式会社 | Sizing agent for reinforcing fiber and application therefor |
KR20160055983A (en) * | 2014-11-08 | 2016-05-19 | 주식회사 효성 | Sizing agent for carbon-fiber, and carbon-fiber manufactured by using the same |
KR20160077322A (en) * | 2014-12-22 | 2016-07-04 | 주식회사 효성 | A carbon-fiber for filament winding bundle |
-
2019
- 2019-12-27 CN CN201911375205.7A patent/CN111005229B/en active Active
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS60104578A (en) * | 1983-11-05 | 1985-06-08 | 竹本油脂株式会社 | Sizing agent for carbon fiber |
JP2000355883A (en) * | 1999-06-16 | 2000-12-26 | Mitsubishi Rayon Co Ltd | Sizing agent for reinforcing fiber |
JP2002013069A (en) * | 2000-06-29 | 2002-01-18 | Mitsubishi Rayon Co Ltd | Sizing agent for carbon fiber, method for sizing carbon fiber, sizing-treated carbon fiber, and sheet-like material and fiber-reinforced composite material containing the same |
CN103797183A (en) * | 2011-09-22 | 2014-05-14 | 三洋化成工业株式会社 | Fiber sizing agent composition |
CN105378176A (en) * | 2013-09-27 | 2016-03-02 | 松本油脂制药株式会社 | Sizing agent for reinforcing fiber and application therefor |
KR20160055983A (en) * | 2014-11-08 | 2016-05-19 | 주식회사 효성 | Sizing agent for carbon-fiber, and carbon-fiber manufactured by using the same |
KR20160077322A (en) * | 2014-12-22 | 2016-07-04 | 주식회사 효성 | A carbon-fiber for filament winding bundle |
Non-Patent Citations (1)
Title |
---|
WEIWEI JIAO 等: ""Preparation of carbon fiber unsaturated sizing agent for enhancing interfacial strength of carbon fiber_vinyl ester resin composite"", 《APPLIED SURFACE SCIENCE》 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113832728A (en) * | 2021-10-27 | 2021-12-24 | 北京化工大学 | Sizing agent for carbon fiber, preparation method thereof and composite material |
CN114182533A (en) * | 2021-12-07 | 2022-03-15 | 陈宗良 | Carbon fiber sizing agent and preparation method thereof, and carbon fiber composite material and preparation method thereof |
CN114960207A (en) * | 2022-06-21 | 2022-08-30 | 浙江巨化新材料研究院有限公司 | Perfluorosulfonic acid carbon fiber composite material and preparation method and application thereof |
CN114960207B (en) * | 2022-06-21 | 2023-08-15 | 浙江巨化新材料研究院有限公司 | Perfluorosulfonic acid carbon fiber composite material and preparation method and application thereof |
Also Published As
Publication number | Publication date |
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CN111005229B (en) | 2021-03-02 |
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CB03 | Change of inventor or designer information | ||
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Inventor after: Chen Zongliang Inventor after: Jin Pu Inventor before: Jin Pu Inventor before: Chen Zongliang |
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TA01 | Transfer of patent application right |
Effective date of registration: 20210111 Address after: 102400 no.1-q120, area 1, Guba Road, Chengguan Street, Fangshan District, Beijing Applicant after: Hongyu Tengfeng Material Technology Co.,Ltd. Applicant after: Zhiyue Tengfeng Technology Group Co.,Ltd. Applicant after: Jin Pu Address before: 102400 no.1-q120, area 1, Guba Road, Chengguan Street, Fangshan District, Beijing Applicant before: Hongyu Tengfeng Material Technology Co.,Ltd. Applicant before: Zhiyue Tengfeng Technology Group Co.,Ltd. |
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Effective date of registration: 20210401 Address after: 102400 no.1-q120, area 1, Guba Road, Chengguan Street, Fangshan District, Beijing Patentee after: Hongyu Tengfeng Material Technology Co.,Ltd. Patentee after: Jin Pu Address before: 102400 no.1-q120, area 1, Guba Road, Chengguan Street, Fangshan District, Beijing Patentee before: Hongyu Tengfeng Material Technology Co.,Ltd. Patentee before: Zhiyue Tengfeng Technology Group Co.,Ltd. Patentee before: Jin Pu |
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Effective date of registration: 20230414 Address after: 2402, 24th Floor, Building 9, No.1 Ronghua South Road, Daxing District, Beijing, 100176 (Yizhuang Cluster, High end Industrial Zone, Beijing Pilot Free Trade Zone) Patentee after: Hongyu Tengfeng Material Technology Co.,Ltd. Patentee after: Liu Muhua Address before: 102400 no.1-q120, area 1, Guba Road, Chengguan Street, Fangshan District, Beijing Patentee before: Hongyu Tengfeng Material Technology Co.,Ltd. Patentee before: Jin Pu |