CN111001386A - Attapulgite adsorbent for indoor air purification and production process thereof - Google Patents
Attapulgite adsorbent for indoor air purification and production process thereof Download PDFInfo
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- CN111001386A CN111001386A CN201911289132.XA CN201911289132A CN111001386A CN 111001386 A CN111001386 A CN 111001386A CN 201911289132 A CN201911289132 A CN 201911289132A CN 111001386 A CN111001386 A CN 111001386A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/12—Naturally occurring clays or bleaching earth
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/16—Alumino-silicates
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/20—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
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- Oil, Petroleum & Natural Gas (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
A attapulgite adsorbent for indoor air purification: the raw materials by mass are: 50-80 parts of attapulgite, 20-30 parts of medical stone, 20-30 parts of activated carbon, 10-20 parts of glutinous rice flour, 3-5 parts of xanthan gum, 3-5 parts of gel and 1-2 parts of lignocellulose; the invention has the beneficial effects that: the product is non-toxic and harmless, and no harmful substances are generated in the production process, so that the product is safe and environment-friendly.
Description
Technical Field
The invention belongs to the technical field of attapulgite adsorbent preparation, and particularly relates to an attapulgite adsorbent for indoor air purification and a production process thereof.
Background
With the rapid development of economy, the living standard of people is gradually improved, people have higher requirements on the quality of the home environment, and home decoration becomes fashionable. However, people often neglect the influence of the decorated living room environment on health and safety. It is well known that indoor environmental pollution seriously affects human health. Various indoor articles can release various harmful substances, and especially in newly decorated rooms, the emission of harmful gases such as benzene, formaldehyde and the like is extremely striking.
Attapulgite, which is called attapulgite for short, is a water-containing magnesium-aluminum-rich silicate mineral with a layer chain structure, and belongs to a natural nano material. The attapulgite has huge specific surface area, and has strong ion exchange capacity, adsorption capacity and decolorizing capacity. Research shows that the nano clay has excellent adsorption effect on various metal ions, dyes, partial organic matters and microorganisms, and has the advantages of low cost, simple regeneration and wide application prospect in indoor air purification.
Disclosure of Invention
In order to meet the requirements, the invention provides the attapulgite adsorbent for indoor air purification and the production process thereof, and the attapulgite adsorbent for indoor air purification and the production process thereof provide the attapulgite adsorbent with excellent adsorption capacity, and the product is non-toxic and harmless, has no harmful substances in the production process, and is safe and environment-friendly.
The technical scheme adopted by the invention for solving the technical problems is as follows: a attapulgite adsorbent for indoor air purification: the raw materials by mass are: 50-80 parts of attapulgite, 20-30 parts of medical stone, 20-30 parts of activated carbon, 10-20 parts of glutinous rice flour, 3-5 parts of xanthan gum, 3-5 parts of gel and 1-2 parts of lignocellulose;
the method comprises the following steps:
(1) mixing attapulgite, medical stone and active carbon, grinding to 130 meshes at 100 meshes, treating at 300 ℃ for 3-5h at 200 meshes, cooling, adding glutinous rice flour, and mixing uniformly to obtain mixed powder;
(2) adding xanthan gum and gel into the mixed powder obtained in the step (1) to obtain a mixed solution;
(3) mixing the mixed solution in the step (2) with lignocellulose, stirring at 60-70 ℃ for 20-30min at 600r/min, freeze-drying at-10 ℃ to-50 ℃ for 8-12h, and finally standing at room temperature for 2-4h to obtain a mixed matrix;
(4) and (4) freeze-drying the mixed matrix obtained in the step (3), crushing the obtained material to be 100-mesh and 130-mesh, and subpackaging the reproduced particles to obtain a finished product.
The active carbon is prepared by pyrolyzing and activating carbon-containing raw materials such as wood, coal, petroleum coke and the like, and has a developed pore structure, a larger specific surface area, abundant surface chemical groups and a carbon material with stronger specific adsorption capacity. The medical stone is a compound mineral or medicinal rock which is nontoxic and harmless to organisms and has certain bioactivity, and can increase the components of adsorbed harmful substances and provide a health-care effect. Lignocellulose increases the strength of the granulation, and all ingredients are non-toxic and harmless.
The invention has the beneficial effects that: the product is non-toxic and harmless, and no harmful substances are generated in the production process, so that the product is safe and environment-friendly.
Detailed Description
Example 1
A attapulgite adsorbent for indoor air purification: the raw materials by mass are: 70 parts of attapulgite, 23 parts of medical stone, 24 parts of activated carbon, 16 parts of glutinous rice flour, 4 parts of xanthan gum, 4 parts of gel and 1.6 parts of lignocellulose;
the method comprises the following steps:
(1) mixing attapulgite, medical stone and active carbon, grinding to 110 meshes together, treating at 230 ℃ for 5h, cooling, adding glutinous rice flour, and mixing uniformly to obtain mixed powder;
(2) adding xanthan gum and gel into the mixed powder obtained in the step (1) to obtain a mixed solution;
(3) mixing the mixed solution in the step (2) with lignocellulose, stirring at 520r/min at 65 ℃ for 25min, freeze-drying at-35 ℃ for 10h, and standing at room temperature for 3h to obtain a mixed matrix;
(4) and (4) freeze-drying the mixed matrix obtained in the step (3), crushing the obtained material to 115 meshes, re-granulating and subpackaging to obtain a finished product.
Example 2
A attapulgite adsorbent for indoor air purification: the raw materials by mass are: 65 parts of attapulgite, 26 parts of medical stone, 24 parts of activated carbon, 16 parts of glutinous rice flour, 4 parts of xanthan gum, 3.8 parts of gel and 1.5 parts of lignocellulose;
the method comprises the following steps:
(1) mixing attapulgite, medical stone and active carbon, grinding to 110 meshes together, treating at 240 ℃ for 5h, cooling, adding glutinous rice flour, and mixing uniformly to obtain mixed powder;
(2) adding xanthan gum and gel into the mixed powder obtained in the step (1) to obtain a mixed solution;
(3) mixing the mixed solution in the step (2) with lignocellulose, stirring at 550r/min at 65 ℃ for 25min, freeze-drying at-25 ℃ for 10h, and standing at room temperature for 3h to obtain a mixed matrix;
(4) and (4) freeze-drying the mixed matrix obtained in the step (3), crushing the obtained material to 120 meshes, and subpackaging the re-granulated material to obtain a finished product.
Claims (3)
1. The attapulgite adsorbent for purifying indoor air is characterized by comprising the following components in parts by weight: the raw materials by mass are: 50-80 parts of attapulgite, 20-30 parts of medical stone, 20-30 parts of activated carbon, 10-20 parts of glutinous rice flour, 3-5 parts of xanthan gum, 3-5 parts of gel and 1-2 parts of lignocellulose;
the attapulgite adsorbent for indoor air purification according to claim 1, wherein: the raw materials by mass are: 55-75 parts of attapulgite, 22-28 parts of medical stone, 22-38 parts of activated carbon, 13-19 parts of glutinous rice flour, 3.3-4.4 parts of xanthan gum, 3.3-4 parts of gel and 1.1-1.7 parts of lignocellulose.
2. A attapulgite adsorbent for purifying indoor air and a preparation method thereof are characterized in that: the method comprises the following steps:
(1) mixing attapulgite, medical stone and active carbon, grinding to 130 meshes at 100 meshes, treating at 300 ℃ for 3-5h at 200 meshes, cooling, adding glutinous rice flour, and mixing uniformly to obtain mixed powder;
(2) adding xanthan gum and gel into the mixed powder obtained in the step (1) to obtain a mixed solution;
(3) mixing the mixed solution in the step (2) with lignocellulose, stirring at 60-70 ℃ for 20-30min at 600r/min, freeze-drying at-10 ℃ to-50 ℃ for 8-12h, and finally standing at room temperature for 2-4h to obtain a mixed matrix;
(4) and (4) freeze-drying the mixed matrix obtained in the step (3), crushing the obtained material to be 100-mesh and 130-mesh, and subpackaging the reproduced particles to obtain a finished product.
3. The attapulgite adsorbent for purifying indoor air and the preparation method thereof according to claim 3, wherein the attapulgite adsorbent comprises the following components: the treatment temperature of the attapulgite, the medical stone and the active carbon in the step 1 is 220-275 DEG C
The attapulgite adsorbent for purifying indoor air and the preparation method thereof according to claim 3, wherein the attapulgite adsorbent comprises the following components: in the step 3, the freeze-drying temperature is-30 ℃ to-40 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911289132.XA CN111001386A (en) | 2019-12-16 | 2019-12-16 | Attapulgite adsorbent for indoor air purification and production process thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911289132.XA CN111001386A (en) | 2019-12-16 | 2019-12-16 | Attapulgite adsorbent for indoor air purification and production process thereof |
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| Publication Number | Publication Date |
|---|---|
| CN111001386A true CN111001386A (en) | 2020-04-14 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201911289132.XA Withdrawn CN111001386A (en) | 2019-12-16 | 2019-12-16 | Attapulgite adsorbent for indoor air purification and production process thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113769706A (en) * | 2021-08-31 | 2021-12-10 | 南京信息工程大学 | Air purification material and preparation method thereof |
| CN113769718A (en) * | 2021-08-31 | 2021-12-10 | 南京信息工程大学 | Adsorption drying agent and preparation method thereof |
-
2019
- 2019-12-16 CN CN201911289132.XA patent/CN111001386A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113769706A (en) * | 2021-08-31 | 2021-12-10 | 南京信息工程大学 | Air purification material and preparation method thereof |
| CN113769718A (en) * | 2021-08-31 | 2021-12-10 | 南京信息工程大学 | Adsorption drying agent and preparation method thereof |
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| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20200414 |
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| WW01 | Invention patent application withdrawn after publication |