CN110975724B - Liquid separation processor - Google Patents

Liquid separation processor Download PDF

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Publication number
CN110975724B
CN110975724B CN201911252906.1A CN201911252906A CN110975724B CN 110975724 B CN110975724 B CN 110975724B CN 201911252906 A CN201911252906 A CN 201911252906A CN 110975724 B CN110975724 B CN 110975724B
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China
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fixed
connecting rod
sliding
hinged
disc
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CN201911252906.1A
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CN110975724A (en
Inventor
周敏
王川丕
章虎
张永志
朱萌萌
赵月钧
郭利攀
钟寒辉
周婷婷
孙文闪
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Greentown Nongke Detection Technology Co ltd
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Greentown Nongke Detection Technology Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/40Mixers using gas or liquid agitation, e.g. with air supply tubes
    • B01F33/403Mixers using gas or liquid agitation, e.g. with air supply tubes for mixing liquids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/40Mixers using gas or liquid agitation, e.g. with air supply tubes
    • B01F33/4094Plants
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/23Mixing of laboratory samples e.g. in preparation of analysing or testing properties of materials

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mixers With Rotating Receptacles And Mixers With Vibration Mechanisms (AREA)

Abstract

The invention discloses a liquid separation processor, which belongs to the field of laboratory instruments and comprises a lower fixed disk, an upper fixed disk, a fixed column and a reagent liquid mixing device, wherein the upper fixed disk and the fixed column are arranged in a vertically sliding manner; the reagent liquid mixing device comprises a connecting rod, a hinged sliding disc, a negative pressure air bag, a hollow upper connecting rod, an air inlet pipe and a sleeve pipe sleeved outside the reagent pipe; one end of the connecting rod is connected with the fixing column in a vertical sliding manner, and the other end of the connecting rod is fixed with the side end of the upper connecting rod; one end of the hinged rod is horizontally and slidably connected with the hinged sliding disc, the other end of the hinged rod is hinged with the side end of the upper connecting rod, and correspondingly, the hinged sliding disc is provided with a sliding groove which is matched with the end part of the hinged rod to slide; one end of the sleeve is fixed with the upper fixed disc, and the other end of the sleeve is fixed with the lower end of the hinged sliding disc; one end of the air inlet pipe is fixed with one end of the negative pressure air bag, which faces away from the connecting rod, and the other end of the air inlet pipe is hermetically connected with the upper end of the sleeve. The invention has the advantages of simple operation and high efficiency.

Description

Liquid separation processor
Technical Field
The invention belongs to the field of laboratory instruments, and particularly relates to a liquid separation processor.
Background
Liquid separation is an operation that separates two immiscible liquids. The apparatus used for separating is a separating funnel, and the operation steps are as follows: the liquid to be separated is poured into a separating funnel by a common funnel and then is plugged. The separatory funnel is then placed on a funnel stand or in an iron ring of an iron stand (if the liquid is to be shaken, it should be shaken well and then placed). After the liquid is separated into two layers, the cock is unscrewed to make the lower layer liquid flow down from the funnel pipe, and before the cock is unscrewed, the groove or the small hole on the piston at the top of the separating funnel is aligned with the small hole at the neck of the upper opening of the funnel, or the piston at the top is taken down to be communicated with the atmosphere. Otherwise, liquid cannot flow out of the lower port through the tap. When the lower layer liquid is drained, the cock is immediately closed, and then the upper layer liquid is poured out from the upper opening of the funnel.
However, in the above operation process, the experimenter needs to hold the separating funnel to shake repeatedly and needs to deflate intermittently, which is troublesome. Meanwhile, in the process of shaking and deflating, reagents are easy to leak or topple over, so that the experiment is influenced.
Disclosure of Invention
The invention aims to provide a liquid separation processor which has the advantages of simplicity in operation and high efficiency.
In order to achieve the purpose, the invention provides the following technical scheme:
a liquid separation processor comprises a lower fixed disk, an upper fixed disk, a fixed column and a reagent liquid mixing device, wherein the upper fixed disk and the fixed column are arranged in a vertically sliding manner; the reagent liquid mixing device comprises a connecting rod, a hinged sliding disc, a negative pressure air bag, a hollow upper connecting rod, an air inlet pipe and a sleeve pipe sleeved outside the reagent pipe; one end of the connecting rod is connected with the fixing column in a vertical sliding mode, and the other end of the connecting rod is fixed to the side end of the upper connecting rod; one end of the hinged rod is horizontally and slidably connected with the hinged sliding disc, the other end of the hinged rod is hinged with the side end of the upper connecting rod, and correspondingly, the hinged sliding disc is provided with a sliding groove which is matched with the end part of the hinged rod to slide; one end of the sleeve is fixed with the upper fixed disc, and the other end of the sleeve is fixed with the lower end of the hinged sliding disc; one end of the air inlet pipe is fixed with one end of the negative pressure air bag, which faces away from the connecting rod, and the other end of the air inlet pipe is connected with the upper end of the sleeve in a sealing manner.
Preferably, the reagent solution mixing device further comprises a first elastic piece and a sliding seat, the sliding seat is arranged in the sliding groove in a sliding mode, one end of the first elastic piece is fixed to the groove wall of the sliding groove, and the other end of the first elastic piece is fixed to the side end of the sliding seat.
Preferably, the side end of the upper connecting rod is provided with a hinge sheet, and the end of the hinge rod is hinged with the hinge sheet.
Preferably, the liquid separation processor further comprises an exhaust device, wherein the exhaust device is fixedly arranged on a thimble inside the air inlet pipe and a sliding exhaust plug arranged at the upper end of the upper connecting rod in a sliding manner.
Preferably, the sliding vent plug comprises a hollow insertion column and an upper fixing part, the insertion column is fixed at the lower end of the upper fixing part, a sliding lug is arranged on the periphery of the insertion column, correspondingly, a sliding groove matched with the sliding lug is arranged on the inner side wall of the upper connecting rod, and a vent gap is formed between the insertion column and the inner side wall of the upper connecting rod.
Preferably, exhaust apparatus still includes lower fixed disk and connecting rod, the thimble is fixed to be set up in the top of lower fixed disk, the one end of connecting rod is fixed mutually with the side of lower fixed disk, and the other end is fixed with the inside wall of intake pipe.
Preferably, the lateral wall of fixed column is equipped with first ring channel, the connecting rod is equipped with solid fixed ring towards the one end of fixed column, gu fix mutually through the second elastic component between fixed ring and the first ring channel.
Preferably, the upper end of the fixing column is provided with a limiting plug for preventing the fixing ring from coming off.
Preferably, the fixed column is provided with a second annular groove, the lower end of the upper fixed disc is fixed with one end of a third elastic piece, and the free end of the third elastic piece is fixed with the bottom of the second annular groove.
Preferably, the lower fixed disk is provided with a fixed cylinder for fixing the test tube.
Compared with the prior art, the invention has the beneficial effects that: the experimenter can place the reagents in the test tubes in advance without transferring them to a separatory funnel. Meanwhile, the experimenter can apply pressure downwards to the connecting rod to compress the negative pressure air bag, and the negative pressure air bag can drive the reagent in the test tube to turn over up and down in the process of contraction and expansion, so that the traditional liquid separation process is replaced, the experimenter holds the liquid separation funnel to shake up and down, and a simpler operation method can achieve the same purpose.
Drawings
FIG. 1 is a schematic structural diagram of a liquid separation processor in this embodiment;
FIG. 2 is an enlarged view of portion A of FIG. 1;
FIG. 3 is a schematic cross-sectional view of a liquid separation processor according to the present embodiment;
fig. 4 is an enlarged view of a portion B in fig. 3.
In the figure: 1. the air inlet pipe comprises a lower fixing disc, 11, a fixing cylinder, 2, an upper fixing disc, 3, a fixing column, 31, a connecting rod, 310, a fixing ring, 32, a second elastic piece, 33, a limiting plug, 34, a third elastic piece, 41, a hinged sliding disc, 42, a first elastic piece, 43, a sliding seat, 44, a hinged rod, 45, a negative pressure air bag, 46, a hinged sheet, 47, a sleeve, 48, an air inlet pipe, 49, a lower fixing disc, 491, an ejector pin, 50, an upper connecting rod, 51, an upper fixing part, 510 and an inserting column.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
As shown in fig. 1-4, a liquid separation processor comprises a lower fixed disk 1, an upper fixed disk 2, a fixed column 3 and a reagent liquid mixing device, wherein the upper fixed disk 2 and the fixed column 3 are arranged in a vertically sliding manner. The reagent liquid mixing device comprises a connecting rod 31, a hinged rod 44, a hinged sliding disk 41, a negative pressure air bag 45, a hollow upper connecting rod 50, an air inlet pipe 48 and a sleeve 47 sleeved outside the reagent pipe. One end of the connecting rod 31 is connected with the fixing column 3 in a vertical sliding manner, and the other end of the connecting rod 31 is fixed with the side end of the upper connecting rod 50. One end of the hinge rod 44 is horizontally slidably connected to the hinge sliding plate 41, and the other end is hinged to the side end of the upper connecting rod 50, and accordingly, the hinge sliding plate 41 is provided with a sliding groove adapted to the end of the hinge rod 44 to slide. One end of the sleeve 47 is fixed with the upper fixed disc 2, and the other end is fixed with the lower end of the hinged sliding disc 41. One end of the air inlet pipe 48 is fixed with one end of the negative pressure air bag 45, which is back to the connecting rod 31, and the other end is connected with the upper end of the sleeve 47 in a sealing way.
As shown in fig. 4, the reagent solution mixing device further includes a first elastic member 42 and a sliding seat 43, the sliding seat 43 is slidably disposed in the sliding groove, one end of the first elastic member 42 is fixed to a groove wall of the sliding groove, and the other end is fixed to a side end of the sliding seat 43. The first elastic member 42 may be compressed during the process of pressing the connection rod 31 by the experimenter, thereby providing an elastic force for the restoration of the hinge rod 44, which may cause the negative pressure air bag 45 to be expanded again.
In this embodiment, the side end of the upper connecting rod 50 is provided with a hinge piece 46, and the end of the hinge rod 44 is hinged with the hinge piece 46.
The present embodiment further includes an exhaust device, which is fixed to the ejector 491 disposed inside the air inlet pipe 48 and a sliding exhaust plug slidably disposed on the upper end of the upper connecting rod 50. When the experimenter presses the connecting rod 31 down, the distance between the ejector 491 and the sliding vent plug is reduced until the sliding vent plug is jacked up upwards, so that the air pressure inside and outside the test tube is the same.
As shown in fig. 4, the sliding vent plug includes a hollow insertion column 510 and an upper fixing portion 51, the insertion column 510 is fixed to the lower end of the upper fixing portion 51, a sliding protrusion is disposed on the periphery of the insertion column 510, correspondingly, a sliding groove adapted to the sliding protrusion is disposed on the inner sidewall of the upper connecting rod 50, and a vent gap is formed between the insertion column 510 and the inner sidewall of the upper connecting rod 50.
As shown in fig. 4, the exhaust device further includes a lower fixed disk 49 and a connecting rod, the thimble 491 is fixedly disposed above the lower fixed disk 49, one end of the connecting rod is fixed to a side end of the lower fixed disk 49, and the other end is fixed to an inner side wall of the intake pipe 48.
In order to make the up-and-down sliding of the connecting rod 31 more convenient, the side wall of the fixing column 3 is provided with a first annular groove, one end of the connecting rod 31 facing the fixing column 3 is provided with a fixing ring 310, and the fixing ring 310 and the first annular groove are fixed together through a second elastic piece 32.
In this embodiment, the upper end of the fixing post 3 is provided with a limiting plug 33 for preventing the fixing ring 310 from coming off.
In this embodiment, the fixed column 3 is provided with a second annular groove, the lower end of the upper fixed disk 2 is fixed to one end of the third elastic element 34, and the free end of the third elastic element 34 is fixed to the bottom of the second annular groove.
In this embodiment, the lower fixed tray 1 is provided with a fixed cylinder 11 for fixing the test tube.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (7)

1. The liquid separation processor is characterized by comprising a lower fixed disk (1), an upper fixed disk (2), a fixed column (3) and a reagent liquid mixing device, wherein the upper fixed disk (2) and the fixed column (3) are arranged in a vertically sliding manner;
the reagent liquid mixing device comprises a connecting rod (31), a hinged rod (44), a hinged sliding disc (41), a negative pressure air bag (45), a hollow upper connecting rod (50), an air inlet pipe (48) and a sleeve (47) sleeved outside the reagent pipe;
one end of the connecting rod (31) is connected with the fixing column (3) in a vertical sliding manner, and the other end of the connecting rod is fixed with the side end of the upper connecting rod (50);
one end of the hinged rod (44) is horizontally and slidably connected with the hinged sliding disc (41), the other end of the hinged rod is hinged with the side end of the upper connecting rod (50), and correspondingly, the hinged sliding disc (41) is provided with a sliding groove which is matched with the end of the hinged rod (44) to slide;
one end of the sleeve (47) is fixed with the upper fixed disc (2), and the other end of the sleeve is fixed with the lower end of the hinged sliding disc (41);
one end of the air inlet pipe (48) is fixed with one end of the negative pressure air bag (45) back to the connecting rod (31), and the other end of the air inlet pipe is hermetically connected with the upper end of the sleeve (47);
the air exhaust device is fixedly arranged on a thimble (491) in the air inlet pipe (48) and a sliding exhaust plug which is arranged at the upper end of the upper connecting rod (50) in a sliding way;
the sliding vent plug comprises a hollow inserting column (510) and an upper fixing part (51), the inserting column (510) is fixed at the lower end of the upper fixing part (51), a sliding lug is arranged on the periphery of the inserting column (510), correspondingly, a sliding groove matched with the sliding lug is arranged on the inner side wall of the upper connecting rod (50), and a vent gap is formed between the inserting column (510) and the inner side wall of the upper connecting rod (50);
the exhaust device further comprises a lower fixed disc (49) and a connecting rod, the ejector pin (491) is fixedly arranged above the lower fixed disc (49), one end of the connecting rod is fixed with the side end of the lower fixed disc (49), and the other end of the connecting rod is fixed with the inner side wall of the air inlet pipe (48).
2. The liquid separation processor according to claim 1, wherein the reagent liquid mixing device further comprises a first elastic member (42) and a sliding seat (43), the sliding seat (43) is slidably disposed in the sliding groove, one end of the first elastic member (42) is fixed to a groove wall of the sliding groove, and the other end of the first elastic member is fixed to a side end of the sliding seat (43).
3. The liquid separation processor as claimed in claim 1, wherein a hinge piece (46) is provided at a side end of the upper connecting rod (50), and an end of the hinge rod (44) is hinged with the hinge piece (46).
4. The liquid separation processor according to claim 1, wherein the side wall of the fixed column (3) is provided with a first annular groove, the end of the connecting rod (31) facing the fixed column (3) is provided with a fixed ring (310), and the fixed ring (310) and the first annular groove are fixed through a second elastic piece (32).
5. The liquid separation processor as claimed in claim 4, wherein the upper end of the fixing column (3) is provided with a limiting plug (33) for preventing the fixing ring (310) from falling out.
6. The liquid separation processor according to claim 4, wherein a second annular groove is formed in the fixed column (3), the lower end of the upper fixed disk (2) is fixed to one end of a third elastic piece (34), and the free end of the third elastic piece (34) is fixed to the bottom of the second annular groove.
7. A liquid separation processor according to claim 4, characterized in that the lower fixing disc (1) is provided with a fixing cylinder (11) for fixing the test tube.
CN201911252906.1A 2019-12-09 2019-12-09 Liquid separation processor Active CN110975724B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201911252906.1A CN110975724B (en) 2019-12-09 2019-12-09 Liquid separation processor

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Application Number Priority Date Filing Date Title
CN201911252906.1A CN110975724B (en) 2019-12-09 2019-12-09 Liquid separation processor

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CN110975724A CN110975724A (en) 2020-04-10
CN110975724B true CN110975724B (en) 2022-03-04

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Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6673316B1 (en) * 1996-10-30 2004-01-06 Sumitomo Chemical Co., Ltd. Synthesis experiment automating system, liquid separating treating apparatus and reaction vessel
JP4610889B2 (en) * 2003-12-19 2011-01-12 株式会社アイラー千野 Shaker separator funnel holder
CN105233527B (en) * 2015-11-06 2017-10-17 青岛顺昕电子科技有限公司 A kind of full-automatic concussion abstraction instrument
CN206746441U (en) * 2017-03-31 2017-12-15 郑雨轩 A kind of chemical reagent sampling and mixing arrangement
CN207627979U (en) * 2017-11-22 2018-07-20 运城学院 A kind of separatory funnel with heating function
CN207567312U (en) * 2017-12-08 2018-07-03 江西自立环保科技有限公司 A kind of extraction equipment for electrolytic nickel production

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