CN110937937A - Special tea fertilizer process for improving theanine content - Google Patents

Abstract

The invention discloses a tea leaf special fertilizer process for improving theanine content, which comprises the following steps: s1: preparing raw materials; s2: mixing; s3: micronizing; s4: filling; the invention uses the acoustic resonance technology in the physical method, utilizes the pressure pulse device to make the liquid form the instantaneous high-pressure pulse energy, the excitation energy released instantaneously by a plurality of liquid pulses generates the sound barrier effect, the frequency is similar to the frequency of molecules, the acoustic resonance is generated, the quantum transition force is formed, the amino acid is complexed with the amide ion, the amino acid amide is generated, the glutamine and the asparagine are contained, the instantaneous pressure pulse device can make the liquid with the particle diameter less than 30um generate the instantaneous 200-3500Kg pressure, the instantaneous excitation release generates about 1-tens of thousands of kilograms of sound barrier pulses, the technological parameter control is accurate, the operation is simple, the product yield is high, the quality is stable, and the invention has important practical significance for the plant life research. In organic nitrogen, free nitrogen ions are greatly reduced, and the content of the nitrite in plants can be greatly reduced.

Description

Special tea fertilizer process for improving theanine content

Technical Field

The invention relates to the field of agricultural fertilizers, in particular to a special tea fertilizer process for improving theanine content.

Background

Theanine (Theanine) is a characteristic amino acid in tea leaves and is also one of the flavor developing substances of tea leaves. It was discovered from yulu tea young sprout by jiuhualang, japan in 1950, and named theanine (jiuhualang 1950). To date, theanine has been rarely found in other plants, and has not been found in other plants except for mushroom, sasanqua, mushroom, camellia oleifera, and camellia japonica, which have been detected in trace amounts. Theanine is the highest free amino acid content in tea trees, and about 70% of the free amino acids in young shoots of tea trees are theanine. In fresh tea leaves, it is common toThe content of theazine acid accounts for 1-2% of the dry weight, and the content of some famous tea can exceed 2%. In the tea soup, the extraction rate of theanine can reach 80%, and the theanine has an important effect on green tea. In the research on health-care components of tea in recent years, theanine is a more attractive compound, and the theanine belongs to amides and is chemically named as: N-ethyl-Y-L-glutamine, type L molecular formula: HOOCCHNH₂CH₂CH₂CONHCH₂CH₃The prior art has higher manufacturing cost and lower product yield.

Disclosure of Invention

The invention aims to provide a process for preparing a special tea fertilizer with improved theanine content, which aims to solve the problems in the background technology.

In order to achieve the purpose, the invention provides the following technical scheme: a process for preparing a tea leaf special fertilizer capable of increasing theanine content comprises the following steps:

s1: preparing raw materials:

glutamic acid: 399 g/L;

one of carbamide or ethylamine or a mixture of carbamide and ethylamine: 100 g/L;

ATP：50g/L；

VB：50g/L；

small molecule organic acids (fulvic acid): 1000 g/L;

s2: the mixture is prepared by putting the raw materials prepared in the S1 into a composite energy state emulsifying machine to obtain liquid with the particle size of less than 30 um;

s3: micronizing, namely putting the liquid with the particle size of less than 30um obtained in the step S2 into a molecular micronizing machine to obtain organic nitrogen-glutamine and fulvic acid amine with the particle size of 0.1-200 nm;

s4: and (4) filling, namely putting the organic nitrogen-glutamine with the particle size of 0.1-200nm and the fulvic acid amine obtained in the step (S3) into a liquid filling machine for filling.

Further comprising the steps of:

s1: preparing raw materials:

21 amino acids (containing aspartic acid): 400 g/L;

one of carbamide or ethylamine or a mixture of carbamide and ethylamine: 200 g/L;

ATP：50g/L；

VB：50g/L；

small molecule organic acids (fulvic acid): 1000 g/L;

s2: the mixture is prepared by putting the raw materials prepared in the S1 into a composite energy state emulsifying machine to obtain liquid with the particle size of less than 30 um;

s3: micronizing, namely putting the liquid with the particle size of less than 30um obtained in the step S2 into a molecular micronizing machine to obtain organic nitrogen-amino acid amide (containing asparagine) and fulvic acid amine with the particle size of 0.1-200 nm;

s4: and (4) filling, namely putting the organic nitrogen-amino acid amide (containing asparagine) with the particle size of 0.1-200nm obtained in the step (S3) and the fulvic acid amine into a liquid filling machine for filling.

Further comprising the steps of:

s1: preparing raw materials:

one of acetic acid or oligomeric acid or citric acid or glucose (low molecular weight organic acid): 400 g/L;

potassium iodide: 50 g/L;

iodine: 50 g/L;

water: 1000 g;

one of carbamide or ethylamine or a mixture of carbamide and ethylamine: 200 g/L;

s2: the mixture is prepared by putting the raw materials prepared in the S1 into a composite energy state emulsifying machine to obtain liquid with the particle size of less than 30 um;

s3; micronizing, namely putting the liquid with the particle size smaller than 30um obtained in the step S2 into a molecular micronizing machine to obtain organic amide with the particle size of 0.1-200 nm;

s4: and (4) filling, namely putting the organic amide with the particle size of 0.1-200nm obtained in the step S3 into a liquid filling machine for filling.

Preferably wherein the low molecular weight organic acid has a molecular weight of less than 1000D.

Compared with the prior art, the invention has the beneficial effects that:

the invention uses the acoustic resonance technology in the physical method, utilizes the pressure pulse device to make the liquid form the instantaneous high-pressure pulse energy, the excitation energy released instantaneously by a plurality of liquid pulses generates the sound barrier effect, the frequency is similar to the frequency of molecules, the acoustic resonance is generated, the quantum transition force is formed, the amino acid is complexed with the amide ion, the amino acid amide is generated, the glutamine and the asparagine are contained, the instantaneous pressure pulse device can make the liquid with the particle diameter less than 30um generate the instantaneous 200-3500Kg pressure, the instantaneous excitation release generates about 1-tens of thousands of kilograms of sound barrier pulses, the technological parameter control is accurate, the operation is simple, the product yield is high, the quality is stable, and the invention has important practical significance for the plant life research. In organic nitrogen, free nitrogen ions are greatly reduced, and the content of the nitrite in plants can be greatly reduced.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

A process for preparing a tea leaf special fertilizer capable of increasing theanine content comprises the following steps:

s1: preparing raw materials:

glutamic acid: 399 g/L;

one of carbamide or ethylamine or a mixture of carbamide and ethylamine: 100 g/L;

ATP：50g/L；

VB：50g/L；

small molecule organic acids (fulvic acid): 1000 g/L;

s2: the mixture is prepared by putting the raw materials prepared in the S1 into a composite energy state emulsifying machine to obtain liquid with the particle size of less than 30 um;

s3: micronizing, namely putting the liquid with the particle size of less than 30um obtained in the step S2 into a molecular micronizing machine to obtain organic nitrogen-glutamine and fulvic acid amine with the particle size of 0.1-200 nm;

s4: and (4) filling, namely putting the organic nitrogen-glutamine and fulvic acid amine with the particle size of 0.1-200nm obtained in the step S3 into a liquid filling machine for filling, wherein the yield of the organic nitrogen is 93-99%, and glutamine is obtained.

Further comprising the steps of:

s1: preparing raw materials:

21 amino acids (containing aspartic acid): 400 g/L;

one of carbamide or ethylamine or a mixture of carbamide and ethylamine: 200 g/L;

ATP：50g/L；

VB：50g/L；

small molecule organic acids (fulvic acid): 1000 g/L;

s2: the mixture is prepared by putting the raw materials prepared in the S1 into a composite energy state emulsifying machine to obtain liquid with the particle size of less than 30 um;

s3: micronizing, namely putting the liquid with the particle size of less than 30um obtained in the step S2 into a molecular micronizing machine to obtain organic nitrogen-amino acid amide (containing asparagine) and fulvic acid amine with the particle size of 0.1-200 nm;

s4: and (3) filling, namely putting the organic nitrogen-amino acid amide (containing asparagine) with the particle size of 0.1-200nm obtained in the step S3 and fulvic acid amine into a liquid filling machine for filling, wherein the yield of the organic nitrogen is 93-99%, and thus the amino acid amide is obtained.

Further comprising the steps of:

s1: preparing raw materials:

one of acetic acid or oligomeric acid or citric acid or glucose (low molecular weight organic acid): 400 g/L;

potassium iodide: 50 g/L;

iodine: 50 g/L;

water: 1000 g;

one of carbamide or ethylamine or a mixture of carbamide and ethylamine: 200 g/L;

s2: the mixture is prepared by putting the raw materials prepared in the S1 into a composite energy state emulsifying machine to obtain liquid with the particle size of less than 30 um;

s3; micronizing, namely putting the liquid with the particle size smaller than 30um obtained in the step S2 into a molecular micronizing machine to obtain organic amide with the particle size of 0.1-200 nm;

s4: and (4) filling, namely putting the organic amide with the particle size of 0.1-200nm obtained in the step S3 into a liquid filling machine for filling, wherein the yield of the organic nitrogen is 93-99%, and obtaining the organic acid amide.

Wherein the low molecular weight organic acid has a molecular weight of less than 1000D

Wherein, the molecule micromachine is equipment for disassembling organic macromolecules manufactured by utilizing the sound barrier principle into organic micromolecules and carrying out organic micromolecule resonance complexing.

From the various embodiments above, it is known that: the invention uses the acoustic resonance technology in the physical method, utilizes the pressure pulse device to make the liquid form the instantaneous high-pressure pulse energy, the excitation energy released instantaneously by a plurality of liquid pulses generates the sound barrier effect, the frequency is similar to the frequency of molecules, the acoustic resonance is generated, the quantum transition force is formed, the amino acid is complexed with the amide ion, the amino acid amide is generated, the glutamine and the asparagine are contained, the instantaneous pressure pulse device can make the liquid with the particle diameter less than 30um generate the instantaneous 200-3500Kg pressure, the instantaneous excitation release generates about 1-tens of thousands of kilograms of sound barrier pulses, the technological parameter control is accurate, the operation is simple, the product yield is high, the quality is stable, and the invention has important practical significance for the plant life research. In organic nitrogen, free nitrogen ions are greatly reduced, and the content of the nitrite in plants can be greatly reduced.

It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (4)

1. A special tea fertilizer process for improving theanine content is characterized by comprising the following steps: the method comprises the following steps:

s1: preparing raw materials:

glutamic acid: 399 g/L;

one of carbamide or ethylamine or a mixture of carbamide and ethylamine: 100 g/L;

ATP：50g/L；

VB：50g/L；

small molecule organic acids (fulvic acid): 1000 g/L;

s2: the mixture is prepared by putting the raw materials prepared in the S1 into a composite energy state emulsifying machine to obtain liquid with the particle size of less than 30 um;

s3: micronizing, namely putting the liquid with the particle size of less than 30um obtained in the step S2 into a molecular micronizing machine to obtain organic nitrogen-glutamine and fulvic acid amine with the particle size of 0.1-200 nm;

s4: and (4) filling, namely putting the organic nitrogen-glutamine with the particle size of 0.1-200nm and the fulvic acid amine obtained in the step (S3) into a liquid filling machine for filling.

2. The process of claim 1, wherein the process comprises the following steps: further comprising the steps of:

s1: preparing raw materials:

21 amino acids (containing aspartic acid): 400 g/L;

one of carbamide or ethylamine or a mixture of carbamide and ethylamine: 200 g/L;

ATP：50g/L；

VB：50g/L；

small molecule organic acids (fulvic acid): 1000 g/L;

s2: the mixture is prepared by putting the raw materials prepared in the S1 into a composite energy state emulsifying machine to obtain liquid with the particle size of less than 30 um;

s3: micronizing, namely putting the liquid with the particle size of less than 30um obtained in the step S2 into a molecular micronizing machine to obtain organic nitrogen-amino acid amide (containing asparagine) and fulvic acid amine with the particle size of 0.1-200 nm;

s4: and (4) filling, namely putting the organic nitrogen-amino acid amide (containing asparagine) with the particle size of 0.1-200nm obtained in the step (S3) and the fulvic acid amine into a liquid filling machine for filling.

3. The process of claim 1, wherein the process comprises the following steps: further comprising the steps of:

s1: preparing raw materials:

one of acetic acid or oligomeric acid or citric acid or glucose (low molecular weight organic acid): 400 g/L;

potassium iodide: 50 g/L;

iodine: 50 g/L;

water: 1000 g;

one of carbamide or ethylamine or a mixture of carbamide and ethylamine: 200 g/L;

s2: the mixture is prepared by putting the raw materials prepared in the S1 into a composite energy state emulsifying machine to obtain liquid with the particle size of less than 30 um;

s3; micronizing, namely putting the liquid with the particle size smaller than 30um obtained in the step S2 into a molecular micronizing machine to obtain organic amide with the particle size of 0.1-200 nm;

s4: and (4) filling, namely putting the organic amide with the particle size of 0.1-200nm obtained in the step S3 into a liquid filling machine for filling.

4. The process of claim 3, wherein the process comprises the following steps: wherein the low molecular weight organic acid has a molecular weight of less than 1000D.