CN110926206A - Low-melting-point metal high-flux smelting device - Google Patents

Low-melting-point metal high-flux smelting device Download PDF

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Publication number
CN110926206A
CN110926206A CN201911223095.2A CN201911223095A CN110926206A CN 110926206 A CN110926206 A CN 110926206A CN 201911223095 A CN201911223095 A CN 201911223095A CN 110926206 A CN110926206 A CN 110926206A
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CN
China
Prior art keywords
crucible
stirring rod
tray
fixing
shaft
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CN201911223095.2A
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Chinese (zh)
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CN110926206B (en
Inventor
李才巨
周广吉
易健宏
高鹏
李宁宇
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Kunming University of Science and Technology
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Kunming University of Science and Technology
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Priority to CN201911223095.2A priority Critical patent/CN110926206B/en
Priority claimed from CN201911223095.2A external-priority patent/CN110926206B/en
Publication of CN110926206A publication Critical patent/CN110926206A/en
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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B14/00Crucible or pot furnaces
    • F27B14/06Crucible or pot furnaces heated electrically, e.g. induction crucible furnaces with or without any other source of heat
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B14/00Crucible or pot furnaces
    • F27B14/08Details peculiar to crucible or pot furnaces
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B14/00Crucible or pot furnaces
    • F27B14/08Details peculiar to crucible or pot furnaces
    • F27B14/10Crucibles
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B14/00Crucible or pot furnaces
    • F27B14/08Details peculiar to crucible or pot furnaces
    • F27B14/14Arrangements of heating devices
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D27/00Stirring devices for molten material
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D7/00Forming, maintaining, or circulating atmospheres in heating chambers
    • F27D7/06Forming or maintaining special atmospheres or vacuum within heating chambers
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D7/00Forming, maintaining, or circulating atmospheres in heating chambers
    • F27D7/06Forming or maintaining special atmospheres or vacuum within heating chambers
    • F27D2007/063Special atmospheres, e.g. high pressure atmospheres
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D7/00Forming, maintaining, or circulating atmospheres in heating chambers
    • F27D7/06Forming or maintaining special atmospheres or vacuum within heating chambers
    • F27D2007/066Vacuum

Abstract

The invention discloses a high-flux smelting device for low-melting-point metal, which is used for a high-flux preparation process of a metal block material. The device comprises a transmission motor, a lifting motor, an outer shell, a stirring rod tray fixing column, a stirring rod tray, a stirring rod, a crucible tray, a heating resistance wire, a crucible I, a crucible fixing groove, a lifting rod fixing device, a furnace door, a gear I, a gear II, a bevel gear I, a bevel gear II, a shaft I, a crucible II, a fixing block I, a shaft II, a furnace body and a fixing block II; the tray in the furnace divides the interior of the hearth into two layers, and a certain number of crucibles are placed in each layer for smelting metal. The device disclosed by the invention is simple in structure, simple and convenient to operate, small in occupied space and low in production cost, and can be used for producing a large number of block metal materials and a large variety of block metal materials in unit time, so that the production efficiency is greatly improved, and the high-flux preparation of the block metal materials is realized.

Description

Low-melting-point metal high-flux smelting device
Technical Field
The invention discloses a high-flux smelting device for low-melting-point metal, and belongs to the technical field of metal smelting.
Background
For the current high throughput preparation techniques and equipment of materials, the more commonly used preparation techniques include: the method comprises a diffusion multicomponent method, a codeposition method, a physical mask method, a spraying synthesis method, a microfluidic synthesis method and the like, but has the defects of extremely limited high-flux preparation technology for block materials, low preparation efficiency, extremely difficult preparation of ternary and above-ternary alloys, less related equipment, difficult realization of large-scale production and certain difficulty for the production of multicomponent alloys. To traditional alloy smelting production, adopt single kind and small-scale production more, to the alloy that is mostly the composition homogeneous of same platform equipment production, be difficult to realize producing quantity and the more alloy of kind in the short time, and need consume a large amount of energy, need a large amount of manual operation, lead to equipment area big, manufacturing cost is high, and production efficiency is low, can't produce more kinds and the number of alloys in the short time.
Disclosure of Invention
The invention aims to provide a high-flux smelting device for low-melting-point metal, which has the advantages of simple structure, low cost, simple and convenient operation, less manpower requirement and low energy consumption, and can produce alloys with different components and types, thereby realizing the high-flux production of block metal materials; the device comprises a transmission motor 1, a lifting motor 2, an outer shell 3, a stirring rod tray fixing column 4, a stirring rod tray 5, a stirring rod 6, a crucible tray 7, a heating resistance wire 8, a crucible I9, a crucible fixing groove 10, a lifting rod fixing device 11, a furnace door 12, a gear I15, a gear II 16, a bevel gear I17, a bevel gear II 18, a shaft I19, a crucible II 20, a fixing block I22, a shaft II 23, a furnace body 24 and a fixing block II 25;
the stirring rod tray 5 is of a rectangular structure and is arranged above the furnace body 24, two fixing blocks I22 are arranged in the stirring rod tray 5, a circular hole is formed in the middle of each fixing block I22, and the shaft I19 penetrates through the circular hole and is supported by the fixing blocks I22; the stirring rod tray is characterized in that a transmission motor 1 is fixed to the top of a stirring rod tray 5, a rotating shaft of the transmission motor 1 is connected with a gear I15, the gear I15 is meshed with a gear II 16, the gear II 16 penetrates through a shaft I19, a plurality of bevel gears I17 are further arranged on the shaft I19, the bevel gears I17 are meshed with bevel gears II 18, the bevel gears II 18 are arranged on the stirring rod tray 5, a stirring rod 6 penetrates through the stirring rod tray 5 and the top of a furnace body 24 and is connected with the bevel gears II 18, the stirring rod 6 is different in length and respectively extends into a crucible II 20 and a crucible I9, and the stirring rod 6 is driven to rotate by the rotation of;
two fixing blocks II 25 are arranged at the top of the outer shell 3, a round hole is formed in the middle of each fixing block II 25, a shaft II 23 penetrates through the round hole and is fixed through the fixing blocks II 25, the lifting motor 2 is connected with the shaft II 23, two steel wires are arranged on the shaft II 23, the tail ends of the steel wires are connected with the stirring rod tray 5, the lifting motor 2 rotates to drive the stirring rod tray 5 to ascend and descend along the stirring rod tray fixing column 4, and the stirring rod tray fixing column 4 is fixed at the top of the outer shell 3;
the furnace body 24 is positioned in the outer shell 3, the top of the furnace body 24 is provided with a hole for the stirring rod 6 to pass through, four side walls of the furnace body 24 are provided with heating resistance wires 8, the inside of the furnace body 24 is provided with a crucible tray 7, the crucible tray 7 is fixed on the inner side wall of the furnace body 24, the crucible tray 7 is correspondingly provided with a hole for the stirring rod 6 to pass through, the crucible tray 7 is provided with a plurality of crucible fixing grooves 10, and the crucible II 20 is arranged in the crucible fixing grooves 10; the bottom of the furnace body 24 is also provided with a crucible fixing groove 10, a crucible I9 is arranged in the crucible fixing groove 10, and crucibles II 20 and the crucible I9 are arranged in a staggered mode.
Preferably, the stirring blade 21 is arranged below the stirring rod 6, the stirring rod 6 corresponding to the crucible I9 is of a two-section structure, and when the stirring blade cannot be used, the stirring rod at the lower section is replaced.
Preferably, 1-4 crucibles with the volume of 100-.
Preferably, the outer shell 3 is provided with a vacuumizing hole 13 and a vent hole 14, and the whole smelting process can be carried out under air, vacuum or protective atmosphere.
Preferably, the top of the crucible tray 7 is provided with a steel wire rope end connecting hole 26.
Preferably, the fixing column 4 of the stirring rod tray is of a cylindrical structure, round holes are formed in two ends of the stirring rod tray 5, and the fixing column 4 of the stirring rod tray passes through the round holes, so that the stirring rod tray 5 can move up and down along the fixing column 4 of the stirring rod tray.
The using process of the invention is as follows:
placing different raw materials in each crucible in the hearth according to requirements, wherein the placed raw materials are either pure metals or alloys, and the melting points of the raw materials in the crucibles are close; all crucibles are heated after the resistance furnace is heated until raw materials in all crucibles are melted, the upper position and the lower position of the stirring device are adjusted on an operation panel outside the furnace body according to requirements to stir the melt, the melt is kept warm according to the requirements, and finally the melt in each crucible is poured after smelting.
The invention has the beneficial effects that:
(1) the device solves the problems of difficult high-throughput preparation, large occupied space, low production efficiency, large labor and energy consumption and high production cost of the multi-element alloy block material; the device has the advantages of simple structure, low cost, simple and convenient operation, little manpower, low energy consumption and capability of producing alloys with different components and types, thereby realizing the high-throughput production of the block metal material.
(2) The device realizes high-throughput preparation of ternary and above alloys, has simple equipment structure, does not need too much manual operation, and has automatic rotation of the stirring device and high process precision; the equipment is simple and convenient to operate, and the occupied area is small; greatly improving the labor productivity.
(3) The device increases the number of samples to be smelted at one time, and the crucible fixing grooves on the tray are different in size, so that crucibles of different sizes can be placed; and a row of crucibles and stirring rods can be added on the basis of the equipment according to actual requirements, so that the number of samples to be smelted simultaneously is increased, and the purpose of high-flux smelting is achieved.
Drawings
FIG. 1 is a schematic structural diagram of the present invention:
fig. 2 is a side view of the present invention:
FIG. 3 is a top view of a stir bar tray of the present invention.
In the figure: 1-a transmission motor; 2-a lifting motor; 3-an outer shell; 4-stirring rod tray fixing column; 5-a stirring rod tray; 6-stirring rod; 7-a crucible tray; 8-heating resistance wires; 9-crucible I; 10-crucible fixing groove, 11-lifting rod fixing device; 12-furnace door; 13-vacuum hole; 14-a vent hole; 15-gear I; 16-gear II; 17-bevel gear I; 18-bevel gear II; 19-axis i; 20-crucible II; 22-fixed block I; 23-axis II; 24-a furnace body; 25-fixed block II; and 26-connecting the tail end of the steel wire rope with a hole.
Detailed Description
The present invention will be described in detail below by way of examples with reference to the accompanying drawings, but the scope of the present invention is not limited to the examples.
Example 1
The device for smelting the low-melting-point metal with high flux has the advantages of simple structure, low cost, simple and convenient operation, less manpower requirement, low energy consumption and capability of producing alloys with different components and types, thereby realizing the high-flux production of block metal materials; the device comprises a transmission motor 1, a lifting motor 2, an outer shell 3, a stirring rod tray fixing column 4, a stirring rod tray 5, a stirring rod 6, a crucible tray 7, a heating resistance wire 8, a crucible I9, a crucible fixing groove 10, a lifting rod fixing device 11, a furnace door 12, a gear I15, a gear II 16, a bevel gear I17, a bevel gear II 18, a shaft I19, a crucible II 20, a fixing block I22, a shaft II 23, a furnace body 24 and a fixing block II 25; the stirring rod tray 5 is of a rectangular structure and is arranged above the furnace body 24, two fixing blocks I22 are arranged in the stirring rod tray 5, a circular hole is formed in the middle of each fixing block I22, and the shaft I19 penetrates through the circular hole and is supported by the fixing blocks I22; the stirring rod tray is characterized in that a transmission motor 1 is fixed to the top of a stirring rod tray 5, a rotating shaft of the transmission motor 1 is connected with a gear I15, the gear I15 is meshed with a gear II 16, the gear II 16 penetrates through a shaft I19, a plurality of bevel gears I17 are further arranged on the shaft I19, the bevel gears I17 are meshed with bevel gears II 18, the bevel gears II 18 are arranged on the stirring rod tray 5, a stirring rod 6 penetrates through the stirring rod tray 5 and the top of a furnace body 24 and is connected with the bevel gears II 18, the stirring rod 6 is different in length and respectively extends into a crucible II 20 and a crucible I9, and the stirring rod 6 is driven to rotate by the rotation of; two fixing blocks II 25 are arranged at the top of the outer shell 3, a round hole is formed in the middle of each fixing block II 25, a shaft II 23 penetrates through the round hole and is fixed through the fixing blocks II 25, the lifting motor 2 is connected with the shaft II 23, two steel wires are arranged on the shaft II 23, the tail ends of the steel wires are connected with the stirring rod tray 5, the lifting motor 2 rotates to drive the stirring rod tray 5 to ascend and descend along the stirring rod tray fixing column 4, and the stirring rod tray fixing column 4 is fixed at the top of the outer shell 3; the stirring rod tray fixing column 4 is of a cylindrical structure, round holes are formed in two ends of the stirring rod tray 5, and the stirring rod tray fixing column 4 penetrates through the round holes, so that the stirring rod tray 5 can move up and down along the stirring rod tray fixing column 4; the furnace body 24 is positioned in the outer shell 3, the top of the furnace body 24 is provided with a hole for the stirring rod 6 to pass through, four side walls of the furnace body 24 are provided with heating resistance wires 8, the inside of the furnace body 24 is provided with a crucible tray 7, the crucible tray 7 is fixed on the inner side wall of the furnace body 24, the crucible tray 7 is correspondingly provided with a hole for the stirring rod 6 to pass through, the crucible tray 7 is provided with a plurality of crucible fixing grooves 10, and the crucible II 20 is arranged in the crucible fixing grooves 10; the bottom of the furnace body 24 is also provided with a crucible fixing groove 10, a crucible I9 is arranged in the crucible fixing groove 10, and crucibles II 20 and the crucible I9 are arranged in a staggered mode.
In this embodiment, be equipped with stirring vane 21 below stirring rod 6, stirring rod 6 that crucible I9 corresponds is two segmentation structures, can change according to actual need.
In this embodiment, 4 crucibles with a volume of 300ml are placed on the crucible tray 7, and four holes are formed on the tray for the lower stirring rod to pass through.
In the embodiment, the outer shell 3 is provided with the vacuumizing hole 13 and the vent hole 14, and the whole smelting process can be carried out in air, vacuum or protective atmosphere.
In this embodiment, the top of the crucible tray 7 is provided with a wire rope end connection hole 26.
The first embodiment is as follows:
the preparation method comprises the steps of completely adding Sn-9Zn-1Bi metal mixed powder into 4 crucibles with 300ml volumes in the first layer, wherein the powder is 200ml, completely adding Sn-9Zn-3Ag metal mixed powder into 4 crucibles with 300ml volumes in the second layer, wherein the powder is 200ml, setting the furnace temperature of a resistance furnace to 400 ℃, keeping the temperature for 25 minutes, controlling an electric stirring device operating disc to adjust the height of a stirring rod, stirring melts of the two layers to ensure uniform components, and then pouring to obtain Sn-9Zn-1Bi alloy block materials and Sn-9Zn-3Ag alloy block materials after smelting is finished, so that the high-flux preparation of the Sn-Zn alloy block materials is realized.
The second embodiment is as follows:
putting Sn-9Zn metal mixed powder into two crucibles in which the 4 crucibles with the volumes of 300ml are arranged in the first layer, putting Sn-9Zn-3Ag metal mixed powder into the other two crucibles, adding Sn-9Zn-3Cu metal mixed powder into the crucibles with the volumes of 300ml in the second layer, putting Sn-9Zn-1Bi metal mixed powder into the other two crucibles with the adding amount of 200ml, setting the furnace temperature of a resistance furnace to 550 ℃, keeping the temperature for 30min, adjusting an operation panel to control the lifting of an electric stirring device during the period, stirring a melt to ensure the components to be uniform, respectively pouring each crucible after the smelting is finished, finally obtaining Sn-Zn alloy blocks, and realizing the high-flux preparation of the Sn-Zn alloy block materials.
The above invention is only a basic description of the present invention, and any equivalent changes made according to the technical scheme of the present invention should belong to the protection scope of the present invention.

Claims (6)

1. A low melting point metal high-flux smelting device is characterized in that: the device comprises a transmission motor (1), a lifting motor (2), an outer shell (3), a stirring rod tray fixing column (4), a stirring rod tray (5), a stirring rod (6), a crucible tray (7), a heating resistance wire (8), a crucible I (9), a crucible fixing groove (10), a lifting rod fixing device (11), a furnace door (12), a gear I (15), a gear II (16), a bevel gear I (17), a bevel gear II (18), a shaft I (19), a crucible II (20), a fixing block I (22), a shaft II (23), a furnace body (24) and a fixing block II (25);
the stirring rod tray (5) is of a rectangular structure and is arranged above the furnace body (24), two fixing blocks I (22) are arranged in the stirring rod tray (5), a round hole is formed in the middle of each fixing block I (22), and the shaft I (19) penetrates through the round hole and is supported by the fixing blocks I (22); the stirring rod tray is characterized in that a transmission motor (1) is fixed to the top of a stirring rod tray (5), a rotating shaft of the transmission motor (1) is connected with a gear I (15), the gear I (15) is meshed with a gear II (16), the gear II (16) penetrates through a shaft I (19), a plurality of bevel gears I (17) are further arranged on the shaft I (19), the bevel gears I (17) are meshed with bevel gears II (18), the bevel gears II (18) are arranged on the stirring rod tray (5), a stirring rod (6) penetrates through the tops of the stirring rod tray (5) and a furnace body (24) and is connected with the bevel gears II (18), the stirring rods (6) are different in length and respectively extend into a crucible II (20) and a crucible I (9), and the rotation of the transmission motor (1) drives the stirring rod (6) to rotate;
two fixing blocks II (25) are arranged at the top of the outer shell (3), a round hole is formed in the middle of each fixing block II (25), the shaft II (23) penetrates through the round hole and is fixed through the fixing blocks II (25), the lifting motor (2) is connected with the shaft II (23), two steel wires are arranged on the shaft II (23), the tail ends of the steel wires are connected with the stirring rod tray (5), the lifting motor (2) rotates to drive the stirring rod tray (5) to ascend and descend along the stirring rod tray fixing columns (4), and the stirring rod tray fixing columns (4) are fixed at the top of the outer shell (3);
the furnace body (24) is positioned inside the outer shell (3), the top of the furnace body (24) is provided with holes for the stirring rods (6) to pass through, four side walls of the furnace body (24) are provided with heating resistance wires (8), the furnace body (24) is internally provided with crucible trays (7), the crucible trays (7) are fixed on the inner side wall of the furnace body (24), the crucible trays (7) are correspondingly provided with holes for the stirring rods (6) to pass through, the crucible trays (7) are provided with a plurality of crucible fixing grooves (10), and the crucibles II (20) are arranged in the crucible fixing grooves (10); the bottom of the furnace body (24) is also provided with a crucible fixing groove (10), a crucible I (9) is arranged in the crucible fixing groove (10), and crucibles II (20) and the crucible I (9) are arranged in a staggered mode.
2. The low-melting-point metal high-throughput melting apparatus according to claim 1, characterized in that: stirring blades (21) are arranged below the stirring rod (6), and the stirring rod (6) corresponding to the crucible I (9) is of a two-section structure.
3. The low-melting-point metal high-throughput melting apparatus according to claim 1, characterized in that: 1-4 crucibles with the volume of 100-.
4. The low-melting-point metal high-throughput melting apparatus according to claim 1, characterized in that: the outer shell (3) is provided with a vacuumizing hole (13) and a vent hole (14), and the whole smelting process can be carried out in air, vacuum or protective atmosphere.
5. The low-melting-point metal high-throughput melting apparatus according to claim 1, characterized in that: the top of the crucible tray (7) is provided with a steel wire rope tail end connecting hole (26).
6. The low-melting-point metal high-throughput melting apparatus according to claim 1, characterized in that: the stirring rod tray fixing column (4) is of a cylindrical structure, round holes are formed in the two ends of the stirring rod tray (5), and the stirring rod tray fixing column (4) penetrates through the round holes.
CN201911223095.2A 2019-12-03 High flux smelting device for low-melting-point metal Active CN110926206B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201911223095.2A CN110926206B (en) 2019-12-03 High flux smelting device for low-melting-point metal

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201911223095.2A CN110926206B (en) 2019-12-03 High flux smelting device for low-melting-point metal

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CN110926206A true CN110926206A (en) 2020-03-27
CN110926206B CN110926206B (en) 2024-05-03

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113970242A (en) * 2021-11-05 2022-01-25 中北大学 High-flux aluminum alloy smelting device and method
CN113983813A (en) * 2021-11-05 2022-01-28 中北大学 High-flux magnesium alloy smelting device and method
CN113983813B (en) * 2021-11-05 2023-11-10 中北大学 High-flux magnesium alloy smelting device and method
CN113970242B (en) * 2021-11-05 2023-11-10 中北大学 High-flux aluminum alloy smelting device and method

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