CN110922796A - Wear-resistant coating for graphite boat plate and preparation process thereof - Google Patents

Wear-resistant coating for graphite boat plate and preparation process thereof Download PDF

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Publication number
CN110922796A
CN110922796A CN201911387462.2A CN201911387462A CN110922796A CN 110922796 A CN110922796 A CN 110922796A CN 201911387462 A CN201911387462 A CN 201911387462A CN 110922796 A CN110922796 A CN 110922796A
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CN
China
Prior art keywords
minutes
heating
preserving heat
resistant coating
graphite
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Pending
Application number
CN201911387462.2A
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Chinese (zh)
Inventor
仇周鹏
谢林祥
施达永
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Zhejiang Mingying Alloy Material Co Ltd
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Zhejiang Mingying Alloy Material Co Ltd
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Publication date
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Priority to CN201911387462.2A priority Critical patent/CN110922796A/en
Publication of CN110922796A publication Critical patent/CN110922796A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D1/00Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/65Additives macromolecular

Abstract

The invention discloses a wear-resistant coating for a graphite boat plate, which comprises the following components in percentage by weight: 30% of alcohol, 5-10% of distilled water, 30-40% of aluminum oxide, 5-10% of boron, 5-10% of lubricant, 2-3% of surfactant, 3-5% of defoaming agent, 5-10% of tween, 0.5-1.0% of graphite and 2-5% of cellulose, and carrying out sintering molding after mixing and ball milling for 60 minutes; its preparing process is also disclosed. The invention has reasonable formula, convenient processing method, strong integral adhesion, strong applicability and good practicability, and is beneficial to improving the processing efficiency, and the hardness and the wear resistance of the product can be greatly improved after the product is used.

Description

Wear-resistant coating for graphite boat plate and preparation process thereof
Technical Field
The invention belongs to the technical field of coating formulas, and particularly relates to a wear-resistant coating for a graphite boat plate and a preparation process thereof.
Background
The coating is required to be used on the graphite boat plate to improve hardness and abrasion resistance of the graphite boat plate, but the prior art coating has limited abrasion resistance and adhesion, thereby affecting the practicality thereof to a certain extent.
Disclosure of Invention
The invention aims to provide a wear-resistant coating for a graphite boat plate and a preparation process thereof.
The technical scheme for realizing the aim of the invention is that the wear-resistant coating for the graphite boat plate comprises the following components in percentage by weight: 30% of alcohol, 5-10% of distilled water, 30-40% of aluminum oxide, 5-10% of boron, 5-10% of lubricant, 2-3% of surfactant, 3-5% of defoaming agent, 5-10% of tween, 0.5-1.0% of graphite and 2-5% of cellulose, and the components are mixed, ball-milled for 60 minutes and then sintered and molded.
2. The process of the abrasion resistant coating for graphite boat plate of claim 1, wherein: the method comprises the following steps:
step A, adding 30 percent of alcohol, 5 to 10 percent of distilled water and 30 to 40 percent of alumina into a ball mill for mixing,
step B, then adding 5-10% of lubricant, 2-3% of surfactant, 3-5% of defoaming agent, 5-10% of tween, 0.5-1.0% of graphite and 2-5% of cellulose into the ball mill, ball-milling for 60 minutes to uniformly ball-mill,
c, molding the mixture obtained in the step B under high pressure or low pressure;
and D, adding 5-10% of boron into the molding material obtained in the step C, and then sintering to obtain a finished product.
In the step D, the sintering treatment comprises firstly heating and sintering within 0-350 ℃ for 150 minutes, then preserving heat at 350 ℃ for 30 minutes, then heating 350 ℃ to 450 ℃ for 60 minutes, preserving heat at 450 ℃ for 30 minutes, then heating 450 ℃ to 550 ℃ for 60 minutes, preserving heat at 550 ℃ for 30 minutes, then heating 550 ℃ to 910 ℃ for 180 minutes, preserving heat at 910 ℃ for 20 minutes, then heating 910 ℃ to 1350 ℃ for 120 minutes, preserving heat at 1350 ℃ for 60 minutes, preferably heating 1350 ℃ to 1420 ℃ for 120 minutes, and finally preserving heat for 60 minutes.
The invention has the positive effects that: the invention has reasonable formula, convenient processing method, strong integral adhesion, strong applicability and good practicability, and is beneficial to improving the processing efficiency, and the hardness and the wear resistance of the product can be greatly improved after the product is used.
Detailed Description
(example 1)
The wear-resistant coating for the graphite boat plate comprises the following components in percentage by weight: 30% of alcohol, 5-10% of distilled water, 30-40% of aluminum oxide, 5-10% of boron, 5-10% of lubricant, 2-3% of surfactant, 3-5% of defoaming agent, 5-10% of tween, 0.5-1.0% of graphite and 2-5% of cellulose, and the components are mixed, ball-milled for 60 minutes and then sintered and molded.
2. The process of the abrasion resistant coating for graphite boat plate of claim 1, wherein: the method comprises the following steps:
step A, adding 30 percent of alcohol, 5 to 10 percent of distilled water and 30 to 40 percent of alumina into a ball mill for mixing,
step B, then adding 5-10% of lubricant, 2-3% of surfactant, 3-5% of defoaming agent, 5-10% of tween, 0.5-1.0% of graphite and 2-5% of cellulose into the ball mill, ball-milling for 60 minutes to uniformly ball-mill,
c, molding the mixture obtained in the step B under high pressure or low pressure;
and D, adding 5-10% of boron into the molding material obtained in the step C, and then sintering to obtain a finished product.
In the step D, the sintering treatment comprises firstly heating and sintering within 0-350 ℃ for 150 minutes, then preserving heat at 350 ℃ for 30 minutes, then heating 350 ℃ to 450 ℃ for 60 minutes, preserving heat at 450 ℃ for 30 minutes, then heating 450 ℃ to 550 ℃ for 60 minutes, preserving heat at 550 ℃ for 30 minutes, then heating 550 ℃ to 910 ℃ for 180 minutes, preserving heat at 910 ℃ for 20 minutes, then heating 910 ℃ to 1350 ℃ for 120 minutes, preserving heat at 1350 ℃ for 60 minutes, preferably heating 1350 ℃ to 1420 ℃ for 120 minutes, and finally preserving heat for 60 minutes.
The invention has reasonable formula, convenient processing method, strong integral adhesion, strong applicability and good practicability, and is beneficial to improving the processing efficiency, and the hardness and the wear resistance of the product can be greatly improved after the product is used.
The standard parts used in the present embodiment can be purchased directly from the market, and the non-standard structural parts described in the specification can also be obtained by processing without any doubt according to the common general knowledge in the prior art, and the connection mode of the parts adopts the conventional means matured in the prior art, and the machines, parts and equipment adopt the conventional models in the prior art, so that the detailed description is not given here.
It should be understood that the above-described embodiments of the present invention are merely examples for clearly illustrating the present invention, and are not intended to limit the embodiments of the present invention. Other variations and modifications will be apparent to persons skilled in the art in light of the above description. And are neither required nor exhaustive of all embodiments. And such obvious changes and modifications which fall within the spirit of the invention are deemed to be covered by the present invention.

Claims (3)

1. The wear-resistant coating for the graphite boat plate is characterized by comprising the following components in parts by weight: comprises the following components in percentage by weight: 30% of alcohol, 5-10% of distilled water, 30-40% of aluminum oxide, 5-10% of boron, 5-10% of lubricant, 2-3% of surfactant, 3-5% of defoaming agent, 5-10% of tween, 0.5-1.0% of graphite and 2-5% of cellulose, and the components are mixed, ball-milled for 60 minutes and then sintered and molded.
2. The process of the abrasion resistant coating for graphite boat plate of claim 1, wherein: the method comprises the following steps:
step A, adding 30 percent of alcohol, 5 to 10 percent of distilled water and 30 to 40 percent of alumina into a ball mill for mixing,
step B, then adding 5-10% of lubricant, 2-3% of surfactant, 3-5% of defoaming agent, 5-10% of tween, 0.5-1.0% of graphite and 2-5% of cellulose into the ball mill, ball-milling for 60 minutes to uniformly ball-mill,
c, molding the mixture obtained in the step B under high pressure or low pressure;
and D, adding 5-10% of boron into the molding material obtained in the step C, and then sintering to obtain a finished product.
3. The process of the abrasion resistant coating for graphite boat plate of claim 2, wherein: in the step D, the sintering treatment comprises firstly heating and sintering within 0-350 ℃ for 150 minutes, then preserving heat at 350 ℃ for 30 minutes, then heating 350 ℃ to 450 ℃ for 60 minutes, preserving heat at 450 ℃ for 30 minutes, then heating 450 ℃ to 550 ℃ for 60 minutes, preserving heat at 550 ℃ for 30 minutes, then heating 550 ℃ to 910 ℃ for 180 minutes, preserving heat at 910 ℃ for 20 minutes, then heating 910 ℃ to 1350 ℃ for 120 minutes, preserving heat at 1350 ℃ for 60 minutes, preferably heating 1350 ℃ to 1420 ℃ for 120 minutes, and finally preserving heat for 60 minutes.
CN201911387462.2A 2019-12-16 2019-12-16 Wear-resistant coating for graphite boat plate and preparation process thereof Pending CN110922796A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201911387462.2A CN110922796A (en) 2019-12-16 2019-12-16 Wear-resistant coating for graphite boat plate and preparation process thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201911387462.2A CN110922796A (en) 2019-12-16 2019-12-16 Wear-resistant coating for graphite boat plate and preparation process thereof

Publications (1)

Publication Number Publication Date
CN110922796A true CN110922796A (en) 2020-03-27

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CN (1) CN110922796A (en)

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1948779A (en) * 2006-07-06 2007-04-18 北京航空航天大学 Method of preparing C/C composite material anti oxidation prtective coating for aeroplane brake disk
CN101104902A (en) * 2007-08-17 2008-01-16 株洲钻石切削刀具股份有限公司 Hard alloy added with boron element and preparation method thereof
CN102585569A (en) * 2011-12-23 2012-07-18 江西稀有稀土金属钨业集团有限公司 Coating for sintering hard alloy, preparation method and using method
CN102876094A (en) * 2012-10-19 2013-01-16 广西梧州港德硬质合金制造有限公司 Hard alloy sintered antisticking coating
CN104498749A (en) * 2014-12-15 2015-04-08 技锋精密刀具(马鞍山)有限公司 Production process of hard alloy
CN105419408A (en) * 2015-07-24 2016-03-23 洛阳新巨能高热技术有限公司 Hard alloy substrate sintering anti-adhesion coating
CN106833035A (en) * 2016-12-21 2017-06-13 潜江新锐硬质合金工具有限公司 For the release coating of sintering cemented carbide
CN107033644A (en) * 2017-06-12 2017-08-11 合肥铭佑高温技术有限公司 A kind of high-temperature resistant coating and preparation method thereof

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1948779A (en) * 2006-07-06 2007-04-18 北京航空航天大学 Method of preparing C/C composite material anti oxidation prtective coating for aeroplane brake disk
CN101104902A (en) * 2007-08-17 2008-01-16 株洲钻石切削刀具股份有限公司 Hard alloy added with boron element and preparation method thereof
CN102585569A (en) * 2011-12-23 2012-07-18 江西稀有稀土金属钨业集团有限公司 Coating for sintering hard alloy, preparation method and using method
CN102876094A (en) * 2012-10-19 2013-01-16 广西梧州港德硬质合金制造有限公司 Hard alloy sintered antisticking coating
CN104498749A (en) * 2014-12-15 2015-04-08 技锋精密刀具(马鞍山)有限公司 Production process of hard alloy
CN105419408A (en) * 2015-07-24 2016-03-23 洛阳新巨能高热技术有限公司 Hard alloy substrate sintering anti-adhesion coating
CN106833035A (en) * 2016-12-21 2017-06-13 潜江新锐硬质合金工具有限公司 For the release coating of sintering cemented carbide
CN107033644A (en) * 2017-06-12 2017-08-11 合肥铭佑高温技术有限公司 A kind of high-temperature resistant coating and preparation method thereof

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