CN110819453A - Malic acid milk flavor essence for cigarette case paperboard and gold card glue and preparation method thereof - Google Patents
Malic acid milk flavor essence for cigarette case paperboard and gold card glue and preparation method thereof Download PDFInfo
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- CN110819453A CN110819453A CN201911098291.1A CN201911098291A CN110819453A CN 110819453 A CN110819453 A CN 110819453A CN 201911098291 A CN201911098291 A CN 201911098291A CN 110819453 A CN110819453 A CN 110819453A
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- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 title claims abstract description 129
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 127
- 239000010931 gold Substances 0.000 title claims abstract description 123
- 229910052737 gold Inorganic materials 0.000 title claims abstract description 123
- 239000003292 glue Substances 0.000 title claims abstract description 98
- 239000008267 milk Substances 0.000 title claims abstract description 84
- 210000004080 milk Anatomy 0.000 title claims abstract description 84
- 235000013336 milk Nutrition 0.000 title claims abstract description 84
- 239000000796 flavoring agent Substances 0.000 title claims abstract description 73
- 235000019634 flavors Nutrition 0.000 title claims abstract description 73
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 title claims abstract description 71
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 title claims abstract description 71
- 239000001630 malic acid Substances 0.000 title claims abstract description 71
- 235000011090 malic acid Nutrition 0.000 title claims abstract description 71
- 239000011087 paperboard Substances 0.000 title claims description 33
- 238000002360 preparation method Methods 0.000 title abstract description 21
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 117
- GHBSPIPJMLAMEP-UHFFFAOYSA-N 6-pentyloxan-2-one Chemical compound CCCCCC1CCCC(=O)O1 GHBSPIPJMLAMEP-UHFFFAOYSA-N 0.000 claims abstract description 52
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 claims abstract description 52
- UFLHIIWVXFIJGU-ARJAWSKDSA-N (Z)-hex-3-en-1-ol Chemical compound CC\C=C/CCO UFLHIIWVXFIJGU-ARJAWSKDSA-N 0.000 claims abstract description 41
- QMMFVYPAHWMCMS-UHFFFAOYSA-N Dimethyl sulfide Chemical compound CSC QMMFVYPAHWMCMS-UHFFFAOYSA-N 0.000 claims abstract description 39
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 39
- XYHKNCXZYYTLRG-UHFFFAOYSA-N 1h-imidazole-2-carbaldehyde Chemical compound O=CC1=NC=CN1 XYHKNCXZYYTLRG-UHFFFAOYSA-N 0.000 claims abstract description 26
- WLAMNBDJUVNPJU-UHFFFAOYSA-N 2-methylbutyric acid Chemical compound CCC(C)C(O)=O WLAMNBDJUVNPJU-UHFFFAOYSA-N 0.000 claims abstract description 26
- GWYFCOCPABKNJV-UHFFFAOYSA-M 3-Methylbutanoic acid Natural products CC(C)CC([O-])=O GWYFCOCPABKNJV-UHFFFAOYSA-M 0.000 claims abstract description 26
- XPCTZQVDEJYUGT-UHFFFAOYSA-N 3-hydroxy-2-methyl-4-pyrone Chemical compound CC=1OC=CC(=O)C=1O XPCTZQVDEJYUGT-UHFFFAOYSA-N 0.000 claims abstract description 26
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 claims abstract description 26
- QUKGYYKBILRGFE-UHFFFAOYSA-N benzyl acetate Chemical compound CC(=O)OCC1=CC=CC=C1 QUKGYYKBILRGFE-UHFFFAOYSA-N 0.000 claims abstract description 26
- GWYFCOCPABKNJV-UHFFFAOYSA-N beta-methyl-butyric acid Natural products CC(C)CC(O)=O GWYFCOCPABKNJV-UHFFFAOYSA-N 0.000 claims abstract description 26
- XUPYJHCZDLZNFP-UHFFFAOYSA-N butyl butanoate Chemical compound CCCCOC(=O)CCC XUPYJHCZDLZNFP-UHFFFAOYSA-N 0.000 claims abstract description 26
- HCRBXQFHJMCTLF-ZCFIWIBFSA-N ethyl (2r)-2-methylbutanoate Chemical compound CCOC(=O)[C@H](C)CC HCRBXQFHJMCTLF-ZCFIWIBFSA-N 0.000 claims abstract description 26
- LZCLXQDLBQLTDK-UHFFFAOYSA-N ethyl 2-hydroxypropanoate Chemical compound CCOC(=O)C(C)O LZCLXQDLBQLTDK-UHFFFAOYSA-N 0.000 claims abstract description 26
- WDAXFOBOLVPGLV-UHFFFAOYSA-N ethyl isobutyrate Chemical compound CCOC(=O)C(C)C WDAXFOBOLVPGLV-UHFFFAOYSA-N 0.000 claims abstract description 26
- CBOQJANXLMLOSS-UHFFFAOYSA-N ethyl vanillin Chemical compound CCOC1=CC(C=O)=CC=C1O CBOQJANXLMLOSS-UHFFFAOYSA-N 0.000 claims abstract description 26
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 claims abstract description 26
- AOGQPLXWSUTHQB-UHFFFAOYSA-N hexyl acetate Chemical compound CCCCCCOC(C)=O AOGQPLXWSUTHQB-UHFFFAOYSA-N 0.000 claims abstract description 26
- UAXOELSVPTZZQG-UHFFFAOYSA-N tiglic acid Natural products CC(C)=C(C)C(O)=O UAXOELSVPTZZQG-UHFFFAOYSA-N 0.000 claims abstract description 26
- MBDOYVRWFFCFHM-SNAWJCMRSA-N (2E)-hexenal Chemical compound CCC\C=C\C=O MBDOYVRWFFCFHM-SNAWJCMRSA-N 0.000 claims abstract description 24
- HNAGHMKIPMKKBB-UHFFFAOYSA-N 1-benzylpyrrolidine-3-carboxamide Chemical compound C1C(C(=O)N)CCN1CC1=CC=CC=C1 HNAGHMKIPMKKBB-UHFFFAOYSA-N 0.000 claims abstract description 13
- OALYTRUKMRCXNH-UHFFFAOYSA-N 5-pentyloxolan-2-one Chemical compound CCCCCC1CCC(=O)O1 OALYTRUKMRCXNH-UHFFFAOYSA-N 0.000 claims abstract description 13
- YIKYNHJUKRTCJL-UHFFFAOYSA-N Ethyl maltol Chemical compound CCC=1OC=CC(=O)C=1O YIKYNHJUKRTCJL-UHFFFAOYSA-N 0.000 claims abstract description 13
- HYMLWHLQFGRFIY-UHFFFAOYSA-N Maltol Natural products CC1OC=CC(=O)C1=O HYMLWHLQFGRFIY-UHFFFAOYSA-N 0.000 claims abstract description 13
- GLZPCOQZEFWAFX-JXMROGBWSA-N Nerol Natural products CC(C)=CCC\C(C)=C\CO GLZPCOQZEFWAFX-JXMROGBWSA-N 0.000 claims abstract description 13
- 229940022663 acetate Drugs 0.000 claims abstract description 13
- 229940007550 benzyl acetate Drugs 0.000 claims abstract description 13
- OBNCKNCVKJNDBV-UHFFFAOYSA-N butanoic acid ethyl ester Natural products CCCC(=O)OCC OBNCKNCVKJNDBV-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000001813 ethyl (2R)-2-methylbutanoate Substances 0.000 claims abstract description 13
- 229940090910 ethyl 2-methylbutyrate Drugs 0.000 claims abstract description 13
- 229940116333 ethyl lactate Drugs 0.000 claims abstract description 13
- 229940093503 ethyl maltol Drugs 0.000 claims abstract description 13
- 229940073505 ethyl vanillin Drugs 0.000 claims abstract description 13
- HIGQPQRQIQDZMP-UHFFFAOYSA-N geranil acetate Natural products CC(C)=CCCC(C)=CCOC(C)=O HIGQPQRQIQDZMP-UHFFFAOYSA-N 0.000 claims abstract description 13
- HIGQPQRQIQDZMP-DHZHZOJOSA-N geranyl acetate Chemical compound CC(C)=CCC\C(C)=C\COC(C)=O HIGQPQRQIQDZMP-DHZHZOJOSA-N 0.000 claims abstract description 13
- 150000002596 lactones Chemical class 0.000 claims abstract description 13
- 229940043353 maltol Drugs 0.000 claims abstract description 13
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 claims abstract description 13
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims abstract description 13
- PHXATPHONSXBIL-UHFFFAOYSA-N xi-gamma-Undecalactone Chemical compound CCCCCCCC1CCC(=O)O1 PHXATPHONSXBIL-UHFFFAOYSA-N 0.000 claims abstract description 13
- MBDOYVRWFFCFHM-UHFFFAOYSA-N trans-2-hexenal Natural products CCCC=CC=O MBDOYVRWFFCFHM-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000000853 adhesive Substances 0.000 claims description 54
- 230000001070 adhesive effect Effects 0.000 claims description 54
- 238000003756 stirring Methods 0.000 claims description 42
- 239000011111 cardboard Substances 0.000 claims description 40
- 238000000034 method Methods 0.000 claims description 21
- 239000000123 paper Substances 0.000 claims description 14
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 12
- JVTAAEKCZFNVCJ-UHFFFAOYSA-M Lactate Chemical compound CC(O)C([O-])=O JVTAAEKCZFNVCJ-UHFFFAOYSA-M 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- 230000000391 smoking effect Effects 0.000 abstract description 9
- 230000014759 maintenance of location Effects 0.000 abstract description 5
- 239000000463 material Substances 0.000 abstract description 4
- 238000004513 sizing Methods 0.000 abstract description 3
- -1 ester lactate Chemical class 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 description 13
- 238000004806 packaging method and process Methods 0.000 description 7
- 238000011156 evaluation Methods 0.000 description 6
- 239000003205 fragrance Substances 0.000 description 6
- 230000001953 sensory effect Effects 0.000 description 4
- 244000061176 Nicotiana tabacum Species 0.000 description 2
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000004026 adhesive bonding Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000013441 quality evaluation Methods 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D85/00—Containers, packaging elements or packages, specially adapted for particular articles or materials
- B65D85/07—Containers, packaging elements or packages, specially adapted for particular articles or materials for compressible or flexible articles
- B65D85/08—Containers, packaging elements or packages, specially adapted for particular articles or materials for compressible or flexible articles rod-shaped or tubular
- B65D85/10—Containers, packaging elements or packages, specially adapted for particular articles or materials for compressible or flexible articles rod-shaped or tubular for cigarettes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0069—Heterocyclic compounds
- C11B9/0073—Heterocyclic compounds containing only O or S as heteroatoms
- C11B9/0076—Heterocyclic compounds containing only O or S as heteroatoms the hetero rings containing less than six atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Paper (AREA)
Abstract
The invention discloses malic acid milk flavor essence for cigarette case card paper gold card glue, gold card glue and a preparation method, comprising A, B and C; the component A comprises: butyric acid, ethyl 2-methylbutyrate, ethyl isobutyrate, folic ester lactate, trans-2-hexenal, folic ester acetate, benzyl acetate, folic alcohol, geranyl acetate, ethyl lactate, delta decalactone, ethyl butyrate, hexyl acetate, hexanol, 2-methylbutyric acid, isovaleric acid, butyl butyrate, and the balance propylene glycol; the component B comprises: maltol, peach aldehyde, coconut aldehyde, milk lactone, ethyl maltol, propyl dodecalactone, ethyl vanillin, butyric acid, 2-methyl butyric acid, isovaleric acid and the balance of propylene glycol; the component C comprises: nerol, benzyl alcohol, dimethyl sulfide, leaf alcohol, ethyl acetate, delta-decalactone, and the balance of propylene glycol. The invention not only can reduce the taste of the sizing material, but also has the advantages of long aroma retention time and high strength of the opening aroma, improves the smoking quality and meets the individual requirements of consumers.
Description
Technical Field
The invention relates to the technical field of essence and spice for cigarettes, in particular to malic acid milk flavor essence and gold card glue for cigarette case paperboard gold card glue and a preparation method thereof.
Background
The cigarette case paperboard is a paper sheet packaged between the inner lining paper and the cigarette case, plays a role in fixing the shape of cigarettes and supporting the stacking of the cigarettes, and is one of indispensable procedures of cigarette packaging.
The current cardboard in the cigarette case package needs to be coated with sizing materials such as gold card glue and the like during production, and the existing sizing materials have some peculiar smell, so that the cardboard has little gluing taste, the taste is easy to gather in the cigarette case after the package, and discomfort is brought to customers at the moment of opening the cigarette case; this gummy taste is particularly intense, especially for packets of cigarettes of low odour type.
As a core technology of the tobacco industry, the tobacco flavor and fragrance technology has become one of the keys of the key technology for building Chinese cigarette quality characteristics. The cigarette unpacking aroma becomes an important index for evaluating cigarettes for cigarette consumers, most of the cigarette unpacking aroma in the market belongs to the herbal aroma, the personalized demand of the consumers is continuously increased, and the current cigarette unpacking aroma still has certain defects in the aspects of aroma retention time, aroma intensity and the like, so that the development of novel essence is urgently needed to prolong the aroma retention time, increase the aroma intensity of the cigarette unpacking aroma, improve the smoking quality of the cigarettes and meet the personalized demand of the consumers on the aroma.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide the malic acid milk flavor essence for cigarette case paperboard gold card glue, which can reduce the taste of the glue, has the advantages of long fragrance retention time and high fragrance intensity of opening the package, and improves the smoking quality of cigarettes.
In order to achieve the above purposes, the technical scheme adopted by the invention is as follows: the malic acid milk flavor essence for cigarette case paperboard gold card glue comprises the following components in parts by mass: 2-4: a, B and C of 1;
each 1000 parts of the component A comprises the following components in parts by weight: 5-10 parts of butyric acid, 8-20 parts of ethyl 2-methylbutyrate, 10-30 parts of ethyl isobutyrate, 5-15 parts of phyllyl lactate, 6-30 parts of trans-2-hexenal, 10-30 parts of phyllyl acetate, 20-40 parts of benzyl acetate, 5-10 parts of phyllyl alcohol, 3-15 parts of geranyl acetate, 5-15 parts of ethyl lactate, 2-10 parts of delta decalactone, 15-25 parts of ethyl butyrate, 5-20 parts of hexyl acetate, 8-20 parts of hexanol, 3-5 parts of 2-methylbutyric acid, 8-25 parts of isovaleric acid, 4-15 parts of butyl butyrate and the balance of propylene glycol;
each 1000 parts of the component B comprises the following components in parts by weight: 2-8 parts of maltol, 5-18 parts of peach aldehyde, 2-20 parts of coconut aldehyde, 6-15 parts of milk lactone, 3-15 parts of ethyl maltol, 8-20 parts of propyl dodecalactone, 4-25 parts of ethyl vanillin, 5-10 parts of butyric acid, 3-15 parts of 2-methyl butyric acid, 5-10 parts of isovaleric acid and the balance of propylene glycol;
each 1000 parts of the component C comprises the following components in parts by weight: 15-20 parts of nerol, 20-30 parts of benzyl alcohol, 0.8-2.2 parts of dimethyl sulfide, 3-5 parts of leaf alcohol, 30-50 parts of ethyl acetate, 1-2 parts of delta-decalactone and the balance of propylene glycol.
Further, the method comprises the following steps of (by mass ratio) 7:2: a, B and C of 1;
each 1000 parts of the component A comprises the following components in parts by weight: 8 parts of butyric acid, 10 parts of ethyl 2-methylbutyrate, 30 parts of ethyl isobutyrate, 15 parts of leaf alcohol lactate, 30 parts of trans-2-hexenal, 15 parts of leaf alcohol acetate, 30 parts of benzyl acetate, 5 parts of leaf alcohol, 3 parts of geranyl acetate, 10 parts of ethyl lactate, 5 parts of delta decalactone, 15 parts of ethyl butyrate, 10 parts of hexyl acetate, 15 parts of hexanol, 3 parts of 2-methylbutyric acid, 8 parts of isovaleric acid, 15 parts of butyl butyrate and the balance of propylene glycol;
each 1000 parts of the component B comprises the following components in parts by weight: 8 parts of maltol, 18 parts of peach aldehyde, 2 parts of coconut aldehyde, 6 parts of milk lactone, 10 parts of ethyl maltol, 10 parts of propyl dodecalactone, 10 parts of ethyl vanillin, 5 parts of butyric acid, 10 parts of 2-methyl butyric acid, 5 parts of isovaleric acid and the balance of propylene glycol;
each 1000 parts of the component C comprises the following components in parts by weight: 18 parts of nerol, 20 parts of benzyl alcohol, 1.5 parts of dimethyl sulfide, 3 parts of leaf alcohol, 50 parts of ethyl acetate, 2 parts of delta-decalactone and the balance of propylene glycol.
The invention also provides a preparation method of the malic acid milk flavor essence for cigarette case paperboard gold card glue, which comprises the following steps:
uniformly mixing all components contained in the component A to obtain a component A;
uniformly mixing all components contained in the component B to obtain the component B;
uniformly mixing all components contained in the component C to obtain a component C;
and uniformly mixing the component A, the component B and the component C to obtain the malic acid milk flavor essence for the cigarette case paperboard colloidal gold.
The invention also provides a gold card adhesive for cigarette case cardboard, which comprises gold card adhesive base glue and malic acid milk flavor essence for cigarette case cardboard gold card adhesive, wherein the malic acid milk flavor essence for cigarette case cardboard gold card adhesive accounts for 2-4% of the weight of the gold card adhesive base glue.
Furthermore, the malic acid milk flavor essence for the cigarette case card paper gold card glue accounts for 3% of the weight of the gold card glue base glue.
The invention also provides a preparation method of the gold card adhesive for cigarette case paperboard, which comprises the following steps:
under the condition of stirring, adding malic acid milk flavor essence for cigarette case paperboard and gold card glue into the gold card glue primer;
and stirring uniformly to obtain the cigarette case paperboard gold card glue.
Further, the stirring speed is 120-200 rpm, and the stirring temperature is 22-30 ℃.
Further, the relative humidity during stirring is 42% -50%.
Further, the stirring time of the box card paper gold card adhesive after the malic acid milk flavor essence is added is 2.5-4 h.
The invention also provides application of the gold card adhesive for cigarette case paperboard in cigarette case paperboard.
Compared with the prior art, the invention has the advantages that:
the malic acid milk flavor essence for cigarette case cardboard gold card glue provided by the invention can reduce the taste of glue material, has the advantages of long fragrance retention time and high fragrance intensity of opening package fragrance by being applied to the cigarette case cardboard gold card glue, improves the smoking quality of cigarettes, and meets the individual requirements of consumers.
The preparation method is simple and convenient, has low cost, can be used for large-scale industrial production, and has strong practicability.
Detailed Description
The present invention will be described in further detail with reference to examples.
The embodiment of the invention provides a malic acid milk flavor essence for cigarette case paperboard gold card glue, which comprises the following components in percentage by mass: 2-4: a, B and C of 1;
each 1000 parts of the component A comprises the following components in parts by weight: 5-10 parts of butyric acid, 8-20 parts of ethyl 2-methylbutyrate, 10-30 parts of ethyl isobutyrate, 5-15 parts of phyllyl lactate, 6-30 parts of trans-2-hexenal, 10-30 parts of phyllyl acetate, 20-40 parts of benzyl acetate, 5-10 parts of phyllyl alcohol, 3-15 parts of geranyl acetate, 5-15 parts of ethyl lactate, 2-10 parts of delta decalactone, 15-25 parts of ethyl butyrate, 5-20 parts of hexyl acetate, 8-20 parts of hexanol, 3-5 parts of 2-methylbutyric acid, 8-25 parts of isovaleric acid, 4-15 parts of butyl butyrate and the balance of propylene glycol;
each 1000 parts of the component B comprises the following components in parts by weight: 2-8 parts of maltol, 5-18 parts of peach aldehyde, 2-20 parts of coconut aldehyde, 6-15 parts of milk lactone, 3-15 parts of ethyl maltol, 8-20 parts of propyl dodecalactone, 4-25 parts of ethyl vanillin, 5-10 parts of butyric acid, 3-15 parts of 2-methyl butyric acid, 5-10 parts of isovaleric acid and the balance of propylene glycol;
each 1000 parts of the component C comprises the following components in parts by weight: 15-20 parts of nerol, 20-30 parts of benzyl alcohol, 0.8-2.2 parts of dimethyl sulfide, 3-5 parts of leaf alcohol, 30-50 parts of ethyl acetate, 1-2 parts of delta-decalactone and the balance of propylene glycol.
Preferably, it comprises a mass ratio of 7:2: a, B and C of 1;
each 1000 parts of the component A comprises the following components in parts by weight: 8 parts of butyric acid, 10 parts of ethyl 2-methylbutyrate, 30 parts of ethyl isobutyrate, 15 parts of leaf alcohol lactate, 30 parts of trans-2-hexenal, 15 parts of leaf alcohol acetate, 30 parts of benzyl acetate, 5 parts of leaf alcohol, 3 parts of geranyl acetate, 10 parts of ethyl lactate, 5 parts of delta decalactone, 15 parts of ethyl butyrate, 10 parts of hexyl acetate, 15 parts of hexanol, 3 parts of 2-methylbutyric acid, 8 parts of isovaleric acid, 15 parts of butyl butyrate and the balance of propylene glycol;
each 1000 parts of the component B comprises the following components in parts by weight: 8 parts of maltol, 18 parts of peach aldehyde, 2 parts of coconut aldehyde, 6 parts of milk lactone, 10 parts of ethyl maltol, 10 parts of propyl dodecalactone, 10 parts of ethyl vanillin, 5 parts of butyric acid, 10 parts of 2-methyl butyric acid, 5 parts of isovaleric acid and the balance of propylene glycol;
each 1000 parts of the component C comprises the following components in parts by weight: 18 parts of nerol, 20 parts of benzyl alcohol, 1.5 parts of dimethyl sulfide, 3 parts of leaf alcohol, 50 parts of ethyl acetate, 2 parts of delta-decalactone and the balance of propylene glycol.
The embodiment of the invention also provides a preparation method of the malic acid milk flavor essence for cigarette case cardboard gold card glue, which comprises the following steps: uniformly mixing all components contained in the component A to obtain a component A; uniformly mixing all components contained in the component B to obtain the component B; uniformly mixing all components contained in the component C to obtain a component C; and uniformly mixing the component A, the component B and the component C to obtain the malic acid milk flavor essence for the cigarette case paperboard colloidal gold.
The embodiment of the invention also provides the gold card adhesive for the cigarette case paperboard, which comprises gold card adhesive base glue and malic acid milk flavor essence for the cigarette case paperboard gold card adhesive, wherein the malic acid milk flavor essence for the cigarette case paperboard gold card adhesive accounts for 2-4% of the weight of the gold card adhesive base glue. Preferably 3%.
The embodiment of the invention also provides a preparation method of the gold card adhesive for cigarette case paperboard, which comprises the following steps: under the condition of stirring, adding malic acid milk flavor essence for cigarette case paperboard and gold card glue into the gold card glue primer; and stirring uniformly to obtain the cigarette case paperboard gold card glue.
Specifically, the stirring speed is 120-200 rpm, and the stirring temperature is 22-30 ℃. The relative humidity during stirring is 42% -50%. The stirring time after the malic acid milk flavor essence is added to the gold card glue of the box card paper is 2.5-4 h.
The embodiment of the invention also provides application of the gold card adhesive for cigarette case paper in the cigarette case paper.
The present invention is explained in detail below by way of specific examples.
Example 1
A malic acid milk flavor essence for cigarette case cardboard gold card glue comprises A, B and C, and the mass ratio is 5:4: 1;
each 1000 parts of the component A comprises the following components in parts by weight: 5 parts of butyric acid, 20 parts of ethyl 2-methylbutyrate, 10 parts of ethyl isobutyrate, 5 parts of leaf alcohol lactate, 6 parts of trans-2-hexenal, 30 parts of leaf alcohol acetate, 40 parts of benzyl acetate, 5 parts of leaf alcohol, 10 parts of geranyl acetate, 15 parts of ethyl lactate, 2 parts of delta decalactone, 15 parts of ethyl butyrate, 5 parts of hexyl acetate, 8 parts of hexanol, 5 parts of 2-methylbutyric acid, 8 parts of isovaleric acid, 15 parts of butyl butyrate and the balance of propylene glycol;
each 1000 parts of the component B comprises the following components in parts by weight: 2 parts of maltol, 5 parts of peach aldehyde, 2 parts of coconut aldehyde, 6 parts of milk lactone, 15 parts of ethyl maltol, 8 parts of propyl dodecalactone, 4 parts of ethyl vanillin, 5 parts of butyric acid, 3 parts of 2-methyl butyric acid, 5 parts of isovaleric acid and the balance of propylene glycol;
each 1000 parts of the component C comprises the following components in parts by weight: 15 parts of nerol, 20 parts of benzyl alcohol, 0.8 part of dimethyl sulfide, 3 parts of leaf alcohol, 30 parts of ethyl acetate, 1 part of delta-decalactone and the balance of propylene glycol.
The preparation method comprises the following steps: uniformly mixing all components contained in the component A to obtain a component A; uniformly mixing all components contained in the component B to obtain the component B; uniformly mixing all components contained in the component C to obtain a component C; uniformly mixing the component A, the component B and the component C in a mass ratio of 5:4:1 to obtain the malic acid milk flavor essence for the cigarette case card paper gold card glue.
Example 2
A malic acid milk flavor essence for cigarette case cardboard gold card glue comprises A, B and C, and the mass ratio is 5:4: 1;
each 1000 parts of the component A comprises the following components in parts by weight: 10 parts of butyric acid, 8 parts of ethyl 2-methylbutyrate, 20 parts of ethyl isobutyrate, 15 parts of leaf alcohol lactate, 6 parts of formula-2-hexenal, 10 parts of leaf alcohol acetate, 20 parts of benzyl acetate, 10 parts of leaf alcohol, 15 parts of geranyl acetate, 15 parts of ethyl lactate, 10 parts of delta decalactone, 25 parts of ethyl butyrate, 10 parts of hexyl acetate, 20 parts of hexanol, 5 parts of 2-methylbutyric acid, 8 parts of isovaleric acid, 15 parts of butyl butyrate and the balance of propylene glycol;
each 1000 parts of the component B comprises the following components in parts by weight: 2 parts of maltol, 58 parts of peach aldehyde, 10 parts of coconut aldehyde, 10 parts of milk lactone, 10 parts of ethyl maltol, 20 parts of propyl dodecalactone, 25 parts of ethyl vanillin, 10 parts of butyric acid, 10 parts of 2-methyl butyric acid, 8 parts of isovaleric acid and the balance of propylene glycol;
each 1000 parts of the component C comprises the following components in parts by weight: 20 parts of nerol, 30 parts of benzyl alcohol, 2.2 parts of dimethyl sulfide, 5 parts of leaf alcohol, 50 parts of ethyl acetate, 2 parts of delta-decalactone and the balance of propylene glycol.
The preparation method comprises the following steps: uniformly mixing all components contained in the component A to obtain a component A; uniformly mixing all components contained in the component B to obtain the component B; uniformly mixing all components contained in the component C to obtain a component C; uniformly mixing the component A, the component B and the component C in a mass ratio of 5:4:1 to obtain the malic acid milk flavor essence for the cigarette case card paper gold card glue.
Example 3
A malic acid milk flavor essence for cigarette case cardboard gold card glue comprises A, B and C, and the mass ratio is 6:3: 1;
each 1000 parts of the component A comprises the following components in parts by weight: 10 parts of butyric acid, 20 parts of ethyl 2-methylbutyrate, 30 parts of ethyl isobutyrate, 15 parts of leaf alcohol lactate, 30 parts of trans-2-hexenal, 30 parts of leaf alcohol acetate, 40 parts of benzyl acetate, 10 parts of leaf alcohol, 15 parts of geranyl acetate, 5 parts of ethyl lactate, 2 parts of delta decalactone, 15 parts of ethyl butyrate, 10 parts of hexyl acetate, 10 parts of hexanol, 4 parts of 2-methylbutyric acid, 10 parts of isovaleric acid, 10 parts of butyl butyrate and the balance of propylene glycol;
each 1000 parts of the component B comprises the following components in parts by weight: 5 parts of maltol, 10 parts of peach aldehyde, 10 parts of coconut aldehyde, 10 parts of milk lactone, 5 parts of ethyl maltol, 15 parts of propyl dodecalactone, 20 parts of ethyl vanillin, 8 parts of butyric acid, 10 parts of 2-methyl butyric acid, 7 parts of isovaleric acid and the balance of propylene glycol;
each 1000 parts of the component C comprises the following components in parts by weight: 15 parts of nerol, 25 parts of benzyl alcohol, 1 part of dimethyl sulfide, 4 parts of leaf alcohol, 40 parts of ethyl acetate, 1.5 parts of delta-decalactone and the balance of propylene glycol.
The preparation method comprises the following steps: uniformly mixing all components contained in the component A to obtain a component A; uniformly mixing all components contained in the component B to obtain the component B; uniformly mixing all components contained in the component C to obtain a component C; uniformly mixing the component A, the component B and the component C in a mass ratio of 6:3:1 to obtain the malic acid milk flavor essence for the cigarette case paperboard colloidal gold.
Example 4
A malic acid milk flavor essence for cigarette case cardboard gold card glue comprises A, B and C, and the mass ratio is 6:3: 1;
each 1000 parts of the component A comprises the following components in parts by weight: 8 parts of butyric acid, 10 parts of ethyl 2-methylbutyrate, 30 parts of ethyl isobutyrate, 15 parts of leaf alcohol lactate, 30 parts of trans-2-hexenal, 15 parts of leaf alcohol acetate, 30 parts of benzyl acetate, 5 parts of leaf alcohol, 3 parts of geranyl acetate, 10 parts of ethyl lactate, 5 parts of delta decalactone, 15 parts of ethyl butyrate, 10 parts of hexyl acetate, 15 parts of hexanol, 3 parts of 2-methylbutyric acid, 8 parts of isovaleric acid, 15 parts of butyl butyrate and the balance of propylene glycol;
each 1000 parts of the component B comprises the following components in parts by weight: 8 parts of maltol, 18 parts of peach aldehyde, 2 parts of coconut aldehyde, 6 parts of milk lactone, 10 parts of ethyl maltol, 10 parts of propyl dodecalactone, 10 parts of ethyl vanillin, 5 parts of butyric acid, 10 parts of 2-methyl butyric acid, 5 parts of isovaleric acid and the balance of propylene glycol;
each 1000 parts of the component C comprises the following components in parts by weight: 18 parts of nerol, 20 parts of benzyl alcohol, 1.5 parts of dimethyl sulfide, 3 parts of leaf alcohol, 50 parts of ethyl acetate, 2 parts of delta-decalactone and the balance of propylene glycol.
The preparation method comprises the following steps: uniformly mixing all components contained in the component A to obtain a component A; uniformly mixing all components contained in the component B to obtain the component B; uniformly mixing all components contained in the component C to obtain a component C; uniformly mixing the component A, the component B and the component C in a mass ratio of 6:3:1 to obtain the malic acid milk flavor essence for the cigarette case paperboard colloidal gold.
Example 5
A malic acid milk flavor essence for cigarette case cardboard gold card glue comprises A, B and C, and the mass ratio is 7:2: 1;
each 1000 parts of the component A comprises the following components in parts by weight: 8 parts of butyric acid, 10 parts of ethyl 2-methylbutyrate, 30 parts of ethyl isobutyrate, 15 parts of leaf alcohol lactate, 30 parts of trans-2-hexenal, 15 parts of leaf alcohol acetate, 30 parts of benzyl acetate, 5 parts of leaf alcohol, 3 parts of geranyl acetate, 10 parts of ethyl lactate, 5 parts of delta decalactone, 15 parts of ethyl butyrate, 10 parts of hexyl acetate, 15 parts of hexanol, 3 parts of 2-methylbutyric acid, 8 parts of isovaleric acid, 15 parts of butyl butyrate and the balance of propylene glycol;
each 1000 parts of the component B comprises the following components in parts by weight: 8 parts of maltol, 18 parts of peach aldehyde, 2 parts of coconut aldehyde, 6 parts of milk lactone, 10 parts of ethyl maltol, 10 parts of propyl dodecalactone, 10 parts of ethyl vanillin, 5 parts of butyric acid, 10 parts of 2-methyl butyric acid, 5 parts of isovaleric acid and the balance of propylene glycol;
each 1000 parts of the component C comprises the following components in parts by weight: 18 parts of nerol, 20 parts of benzyl alcohol, 1.5 parts of dimethyl sulfide, 3 parts of leaf alcohol, 50 parts of ethyl acetate, 2 parts of delta-decalactone and the balance of propylene glycol.
The preparation method comprises the following steps: uniformly mixing all components contained in the component A to obtain a component A; uniformly mixing all components contained in the component B to obtain the component B; uniformly mixing all components contained in the component C to obtain a component C; uniformly mixing the component A, the component B and the component C in a mass ratio of 7:2:1 to obtain the malic acid milk flavor essence for the cigarette case card paper gold card glue.
Example 6
A malic acid milk flavor essence for cigarette case cardboard gold card glue comprises A, B and C, and the mass ratio is 7:2: 1;
each 1000 parts of the component A comprises the following components in parts by weight: 10 parts of butyric acid, 8 parts of ethyl 2-methylbutyrate, 20 parts of ethyl isobutyrate, 15 parts of leaf alcohol lactate, 6 parts of trans-2-hexenal, 10 parts of leaf alcohol acetate, 20 parts of benzyl acetate, 10 parts of leaf alcohol, 15 parts of geranyl acetate, 15 parts of ethyl lactate, 10 parts of delta decalactone, 25 parts of ethyl butyrate, 10 parts of hexyl acetate, 20 parts of hexanol, 5 parts of 2-methylbutyric acid, 8 parts of isovaleric acid, 15 parts of butyl butyrate and the balance of propylene glycol;
each 1000 parts of the component B comprises the following components in parts by weight: 2 parts of maltol, 58 parts of peach aldehyde, 10 parts of coconut aldehyde, 10 parts of milk lactone, 10 parts of ethyl maltol, 20 parts of propyl dodecalactone, 25 parts of ethyl vanillin, 10 parts of butyric acid, 10 parts of 2-methyl butyric acid, 8 parts of isovaleric acid and the balance of propylene glycol;
each 1000 parts of the component C comprises the following components in parts by weight: 20 parts of nerol, 30 parts of benzyl alcohol, 2.2 parts of dimethyl sulfide, 5 parts of leaf alcohol, 50 parts of ethyl acetate, 2 parts of delta-decalactone and the balance of propylene glycol.
The preparation method comprises the following steps: uniformly mixing all components contained in the component A to obtain a component A; uniformly mixing all components contained in the component B to obtain the component B; uniformly mixing all components contained in the component C to obtain a component C; uniformly mixing the component A, the component B and the component C in a mass ratio of 7:2:1 to obtain the malic acid milk flavor essence for the cigarette case card paper gold card glue.
Example 7
A cigarette case cardboard gold card adhesive comprises gold card adhesive base glue and malic acid milk flavor essence for cigarette case cardboard gold card adhesive prepared in example 1, wherein the malic acid milk flavor essence for cigarette case cardboard gold card adhesive is 2% of the weight of the gold card adhesive base glue.
The preparation method comprises the following steps: slowly adding malic acid milk flavor essence for cigarette case paperboard gold card glue, wherein the weight of the malic acid milk flavor essence is 2% of that of the gold card glue base glue, stirring at the rotating speed of 120rpm in the process of adding the essence, wherein the stirring temperature is 23 ℃, the relative humidity is 43%, and continuously stirring for 2.6h under the stirring condition after the essence is completely added to prepare the gold card glue a containing the malic acid milk flavor essence.
The gold card adhesive a is utilized to prepare a cigarette product a according to the normal procedures of cigarette box sheet bonding production and cigarette packaging production.
Example 8
A cigarette case cardboard gold card adhesive comprises gold card adhesive base glue and malic acid milk flavor essence for cigarette case cardboard gold card adhesive prepared in example 2, wherein the malic acid milk flavor essence for cigarette case cardboard gold card adhesive is 2% of the weight of the gold card adhesive base glue.
The preparation method comprises the following steps: slowly adding malic acid milk flavor essence for cigarette case paperboard gold card glue, wherein the weight of the malic acid milk flavor essence is 2% of that of the gold card glue base glue, stirring at the rotating speed of 120rpm in the process of adding the essence, wherein the stirring temperature is 23 ℃, the relative humidity is 43%, and continuously stirring for 2.6h under the stirring condition after the essence is completely added to prepare the gold card glue a1 containing the malic acid milk flavor essence.
The gold card adhesive a1 is used for preparing a cigarette product a1 according to the normal procedures of cigarette case sheet bonding production and cigarette packaging production.
Example 9
A cigarette case cardboard gold card adhesive comprises gold card adhesive base glue and malic acid milk flavor essence for cigarette case cardboard gold card adhesive prepared in example 3, wherein the malic acid milk flavor essence for cigarette case cardboard gold card adhesive is 4% of the weight of the gold card adhesive base glue.
The preparation method comprises the following steps: slowly adding malic acid milk flavor essence for cigarette case paperboard gold card glue 4% of the weight of the gold card glue base glue into the gold card glue base glue, stirring at the rotation speed of 180rpm in the process of adding the essence, wherein the stirring temperature is 28 ℃, the relative humidity is 48%, and continuously stirring for 3.8h under the stirring condition after the essence is completely added to prepare the gold card glue b containing the malic acid milk flavor essence.
And (4) preparing a cigarette product b by using the gold card adhesive b according to the normal procedures of cigarette box sheet bonding production and cigarette packaging production.
Example 10
A cigarette case cardboard gold card adhesive comprises gold card adhesive base glue and malic acid milk flavor essence for cigarette case cardboard gold card adhesive prepared in example 4, wherein the malic acid milk flavor essence for cigarette case cardboard gold card adhesive is 4% of the weight of the gold card adhesive base glue.
The preparation method comprises the following steps: slowly adding malic acid milk flavor essence for cigarette case paperboard gold card glue 4% of the weight of the gold card glue base glue into the gold card glue base glue, stirring at the rotation speed of 180rpm in the process of adding the essence, wherein the stirring temperature is 28 ℃, the relative humidity is 48%, and continuously stirring for 3.8h under the stirring condition after the essence is completely added to prepare the gold card glue b1 containing the malic acid milk flavor essence.
The gold card adhesive b1 is utilized to prepare a cigarette product b1 according to the normal procedures of cigarette case sheet bonding production and cigarette packaging production.
Example 11
A cigarette case cardboard gold card adhesive comprises gold card adhesive base glue and the malic acid milk flavor essence for cigarette case cardboard gold card adhesive prepared in example 5, wherein the malic acid milk flavor essence for cigarette case cardboard gold card adhesive is 3% of the weight of the gold card adhesive base glue.
The preparation method comprises the following steps: slowly adding malic acid milk flavor essence for cigarette case paperboard gold card glue, wherein the weight of the malic acid milk flavor essence is 3% of that of the gold card glue base glue, stirring at the speed of 160rpm in the process of adding the essence, wherein the stirring temperature is 26 ℃, the relative humidity is 46%, and continuously stirring for 3.2h under the stirring condition after the essence is completely added to prepare the gold card glue c containing the malic acid milk flavor essence.
And (3) preparing a cigarette product c by using the gold card adhesive c according to the normal procedures of cigarette box sheet bonding production and cigarette packaging production.
Example 12
A cigarette case cardboard gold card adhesive comprises gold card adhesive base glue and the malic acid milk flavor essence for cigarette case cardboard gold card adhesive prepared in example 6, wherein the malic acid milk flavor essence for cigarette case cardboard gold card adhesive is 3% of the weight of the gold card adhesive base glue.
The preparation method comprises the following steps: slowly adding malic acid milk flavor essence for cigarette case paperboard gold card glue, wherein the weight of the malic acid milk flavor essence is 3% of that of the gold card glue base glue, stirring at the speed of 160rpm in the process of adding the essence, wherein the stirring temperature is 26 ℃, the relative humidity is 46%, and continuously stirring for 3.2h under the stirring condition after the essence is completely added to prepare the gold card glue c1 containing the malic acid milk flavor essence.
The gold card adhesive c1 is utilized to prepare a cigarette product c1 according to the normal procedures of cigarette case sheet bonding production and cigarette packaging production.
The method is characterized in that a blank gold card adhesive is prepared by adopting the same method as that in example 12 without adding malic acid milk flavor, then the blank gold card adhesive is prepared into a blank cigarette product comparison d, the cigarette products a, a1, b1, c and c1 in application examples 7, 8, 9, 10, 11 and 12 are subjected to comparative smoking evaluation according to national bureau smoking evaluation standards, a smoking panel consists of 7 cigarette sensory evaluation experts according to the cigarette sensory quality evaluation standards in national standard GB 5606.5-2005, sensory evaluation is carried out in a dark evaluation mode, 100 parts of questionnaires are issued, 100 parts of the questionnaires are withdrawn, meanwhile, smoking is carried out on the opened package incense at certain intervals, and the aroma remaining time is detected.
The sensory evaluation score table is shown in table 1, and the questionnaire survey results are shown in table 2:
as can be seen from tables 1 and 2, the malic acid milk flavor essence is added into the cigarette case card gold card glue to prepare the cigarette product, so that the cigarette can be endowed with a new aroma type, the aroma is comfortable, the strength is high, the taste of the glue is reduced or even eliminated, the aroma retaining time can reach 96h, the smoking quality of the cigarette is improved, and the personalized requirements of consumers are met.
The present invention is not limited to the above-described embodiments, and it will be apparent to those skilled in the art that various modifications and improvements can be made without departing from the principle of the present invention, and such modifications and improvements are also considered to be within the scope of the present invention. Those not described in detail in this specification are within the skill of the art.
Claims (10)
1. The malic acid milk flavor essence for cigarette case paperboard colloidal gold is characterized in that: the weight ratio of the components is 5-7: 2-4: a, B and C of 1;
each 1000 parts of the component A comprises the following components in parts by weight: 5-10 parts of butyric acid, 8-20 parts of ethyl 2-methylbutyrate, 10-30 parts of ethyl isobutyrate, 5-15 parts of phyllyl lactate, 6-30 parts of trans-2-hexenal, 10-30 parts of phyllyl acetate, 20-40 parts of benzyl acetate, 5-10 parts of phyllyl alcohol, 3-15 parts of geranyl acetate, 5-15 parts of ethyl lactate, 2-10 parts of delta decalactone, 15-25 parts of ethyl butyrate, 5-20 parts of hexyl acetate, 8-20 parts of hexanol, 3-5 parts of 2-methylbutyric acid, 8-25 parts of isovaleric acid, 4-15 parts of butyl butyrate and the balance of propylene glycol;
each 1000 parts of the component B comprises the following components in parts by weight: 2-8 parts of maltol, 5-18 parts of peach aldehyde, 2-20 parts of coconut aldehyde, 6-15 parts of milk lactone, 3-15 parts of ethyl maltol, 8-20 parts of propyl dodecalactone, 4-25 parts of ethyl vanillin, 5-10 parts of butyric acid, 3-15 parts of 2-methyl butyric acid, 5-10 parts of isovaleric acid and the balance of propylene glycol;
each 1000 parts of the component C comprises the following components in parts by weight: 15-20 parts of nerol, 20-30 parts of benzyl alcohol, 0.8-2.2 parts of dimethyl sulfide, 3-5 parts of leaf alcohol, 30-50 parts of ethyl acetate, 1-2 parts of delta-decalactone and the balance of propylene glycol.
2. The malic acid milk flavor essence for cigarette case cardboard gold card glue of claim 1, which is characterized in that: the weight ratio of the components is 7:2: a, B and C of 1;
each 1000 parts of the component A comprises the following components in parts by weight: 8 parts of butyric acid, 10 parts of ethyl 2-methylbutyrate, 30 parts of ethyl isobutyrate, 15 parts of leaf alcohol lactate, 30 parts of trans-2-hexenal, 15 parts of leaf alcohol acetate, 30 parts of benzyl acetate, 5 parts of leaf alcohol, 3 parts of geranyl acetate, 10 parts of ethyl lactate, 5 parts of delta decalactone, 15 parts of ethyl butyrate, 10 parts of hexyl acetate, 15 parts of hexanol, 3 parts of 2-methylbutyric acid, 8 parts of isovaleric acid, 15 parts of butyl butyrate and the balance of propylene glycol;
each 1000 parts of the component B comprises the following components in parts by weight: 8 parts of maltol, 18 parts of peach aldehyde, 2 parts of coconut aldehyde, 6 parts of milk lactone, 10 parts of ethyl maltol, 10 parts of propyl dodecalactone, 10 parts of ethyl vanillin, 5 parts of butyric acid, 10 parts of 2-methyl butyric acid, 5 parts of isovaleric acid and the balance of propylene glycol;
each 1000 parts of the component C comprises the following components in parts by weight: 18 parts of nerol, 20 parts of benzyl alcohol, 1.5 parts of dimethyl sulfide, 3 parts of leaf alcohol, 50 parts of ethyl acetate, 2 parts of delta-decalactone and the balance of propylene glycol.
3. A method for preparing the malolactic flavor for the cigarette case cardboard gold card glue according to claim 1 or 2, which comprises the following steps:
uniformly mixing all components contained in the component A to obtain a component A;
uniformly mixing all components contained in the component B to obtain the component B;
uniformly mixing all components contained in the component C to obtain a component C;
and uniformly mixing the component A, the component B and the component C to obtain the malic acid milk flavor essence for the cigarette case paperboard colloidal gold.
4. The utility model provides a cigarette case is gold card glue for card paper which characterized in that: the cigarette case cardboard contains gold card base glue and malic acid milk flavor essence for the gold card glue of the cigarette case cardboard according to claim 1 or 2, wherein the malic acid milk flavor essence for the gold card glue of the cigarette case cardboard accounts for 2-4% of the weight of the gold card base glue.
5. The cigarette pack gold card adhesive as claimed in claim 4, wherein: the malic acid milk flavor essence for the cigarette case card paper gold card glue accounts for 3 percent of the weight of the gold card glue base glue.
6. A method for preparing gold card glue for cigarette case cardboard according to claim 4, characterized by comprising the following steps:
under the condition of stirring, adding malic acid milk flavor essence for cigarette case paperboard and gold card glue into the gold card glue primer;
and stirring uniformly to obtain the cigarette case paperboard gold card glue.
7. The method of claim 6, wherein: the stirring speed is 120-200 rpm, and the stirring temperature is 22-30 ℃.
8. The method of claim 6, wherein: the relative humidity during stirring is 42% -50%.
9. The method of claim 6, wherein: the stirring time after the malic acid milk flavor essence is added to the gold card glue of the box card paper is 2.5-4 h.
10. Use of the gold card glue for cigarette pack cardboard according to claim 4 in cigarette pack cardboard.
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| CN203450574U (en) * | 2013-09-11 | 2014-02-26 | 湖北淡雅香生物科技股份有限公司 | Damp-proof moistening perfumed lining paper |
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