CN110801796A - Lamp tube module and multi-sample organic photoelectric synthesis parallel reaction device - Google Patents
Lamp tube module and multi-sample organic photoelectric synthesis parallel reaction device Download PDFInfo
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- CN110801796A CN110801796A CN201911244829.5A CN201911244829A CN110801796A CN 110801796 A CN110801796 A CN 110801796A CN 201911244829 A CN201911244829 A CN 201911244829A CN 110801796 A CN110801796 A CN 110801796A
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- 238000003786 synthesis reaction Methods 0.000 title claims abstract description 39
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- 239000007788 liquid Substances 0.000 claims abstract description 56
- 230000017525 heat dissipation Effects 0.000 claims abstract description 35
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- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
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- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B3/00—Electrolytic production of organic compounds
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- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
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- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
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Abstract
A lamp tube module comprises a tube body assembly, a light source assembly and a glass sheet, wherein the tube body assembly is internally provided with a positioning groove for placing a reaction container; the invention also provides a multi-sample organic photoelectric synthesis parallel reaction device, which comprises a base module and a liquid cooling heat dissipation module, wherein the base module is provided with a plurality of sockets along the circumferential direction; the liquid cooling heat dissipation module is provided with a plurality of cooling grooves along the circumferential direction, and the cooling grooves are provided with side openings communicated with the fixing grooves; the lamp tube module can realize simple switching of the photocatalysis direction aiming at single reaction, and the multi-sample organic photoelectric synthesis parallel reaction device can be freely spliced according to the conditions of photocatalysis, electrolysis and photoelectric organic synthesis reaction, and has high yield stability and excellent parallelism.
Description
Technical Field
The invention relates to the technical field of organic photoelectric catalytic synthesis devices, in particular to a lamp tube module and a multi-sample organic photoelectric synthesis parallel reaction device.
Background
In the field of organic synthesis, in order to meet the requirements of energy conservation and emission reduction on sustainable development, a clean technology of green chemistry is applied to organic synthesis, however, the energy crisis in the current society pushes the green organic synthesis to the development and utilization of clean and renewable energy sources (light and electricity), and the organic synthesis means is gradually changed from the traditional heating mode into visible light catalysis, electrocatalysis, photoelectrocatalysis and the like. In order to improve the organic synthesis efficiency and greatly shorten the development time of a new organic synthesis method, a multi-sample parallel reaction device for organic synthesis chemistry is produced.
However, for the new photoelectric organic (catalytic) synthesis reaction in recent two years, the current commercialized light parallel reaction device and electrochemical parallel synthesis device have the integrated fixed characteristic, and cannot meet the requirement of organic photoelectric synthesis, thereby greatly limiting the research and development speed of the organic photoelectric synthesis reaction and the repeatability of experimental data. In order to meet the requirement of organic photoelectric synthesis reaction, a simple device built in a laboratory cannot realize parallel reaction and has serious potential safety hazard.
Disclosure of Invention
The invention aims to provide a lamp cylinder module and a multi-sample organic photoelectric synthesis parallel reaction device.
The purpose of the invention is realized by adopting the following technical scheme. The lamp tube module provided by the invention comprises a tube body assembly 1, a light source assembly 2 and a glass sheet 3, wherein the tube body assembly 1 is internally provided with a positioning groove 103 for placing a reaction vessel, the light source assembly 2 is detachably arranged at the bottom of the tube body assembly 1 and provides a bottom irradiation light source for the reaction vessel, and the glass sheet 3 is arranged between the tube body assembly 1 and the light source assembly 2 and is used for allowing the bottom irradiation light source to pass through and providing a supporting force for the reaction vessel arranged in the tube body assembly 1.
Preferably, the light source assembly 2 is installed at the bottom of the barrel assembly 1 in a thread fit manner.
Preferably, the side wall of the barrel assembly 1 is provided with a window 101 for providing a light-transmitting window for side irradiation of the reaction vessel.
Preferably, the barrel assembly 1 is further provided with a limiting step 102 for limiting.
Preferably, the barrel assembly 1 is provided with a handheld boss 104, and the outer wall of the handheld boss 104 is provided with a plurality of ribs along the circumferential direction for increasing the friction between the lamp barrel module and the outside so as to drive the lamp barrel module to rotate.
Preferably, the light source assembly 2 includes a lamp sheet 201 providing a bottom irradiation light source for the photocatalytic reaction, two connection sheets 209 electrically connected to two electrodes of the lamp sheet 201, a light source housing 202 detachably mounted at the bottom of the barrel assembly 1, a pressing sheet 206 having a plurality of bolt holes, an insulating base 203 having a first limiting groove 207 for limiting the pressing sheet 206 and a second limiting groove 208 for limiting the lamp sheet 201 and mounted at the bottom of the light source housing 202, a first conductive ring 204 and a second conductive ring 205 mounted at the bottom of the insulating base 203 and not in contact with each other, the pressing sheet 206, the insulating base 203, and the second conductive ring 205 are fixed to form a whole by a first bolt, wherein any one of the connection sheets 209, the insulating base 203, the first connection sheet 204 is fixed to form a whole by a second bolt, and the other one of the connection sheets 209 and the pressing sheet 206 is fixed to form a whole by a third bolt.
The invention also provides a multi-sample organic photoelectric synthesis parallel reaction device, which comprises a stirring and adjusting module, a reaction container suitable for organic photoelectric synthesis, a multifunctional power supply adapting module, a base module 5 provided with a plurality of sockets 501, and a liquid cooling heat dissipation module 4 which is arranged on the base module 5 and is also provided with a fixing groove 402; the liquid cooling heat dissipation module 4 is provided with a plurality of cooling tanks 401 for mounting the lamp cartridge module along the circumferential direction, and the cooling tanks 401 are provided with side openings communicated with the fixing grooves 402.
Preferably, the liquid cooled heat sink module 4 is removably mounted to the base module 5.
Preferably, the top surface of the base module 5 is provided with a plurality of positioning pins 502, and the bottom surface of the liquid cooling heat dissipation module 4 is provided with a plurality of positioning holes matched with the positioning pins 502; the bottom of the base module 5 is also provided with a stirring and adjusting module.
Preferably, the liquid cooling heat dissipation module 4 is further provided with a liquid cooling channel, and a liquid inlet and a liquid outlet which are communicated with the liquid cooling channel.
The lamp tube module and the multi-sample organic photoelectric synthesis parallel reaction device provided by the invention have the following advantages:
1. the lamp tube module of this embodiment is convenient for change the lamp piece, can select the lamp piece of different power, different wavelength as required, and the reaction vessel that lies in the lamp tube module simultaneously can select the light source to single reaction, also can realize the simple switching of photocatalysis direction to single reaction, realizes the switching of bottom irradiation light source or side irradiation light source promptly.
2. In this embodiment, the liquid cooling heat dissipation module can give off the heat that the lamp section of thick bamboo module produced, prevents that the overheated damage that arouses of lamp section of thick bamboo module, prevents that the overheated reaction that is unfavorable for the sample of reaction vessel, has also solved the heat dissipation problem of various light sources self simultaneously.
3. The multi-sample organic photoelectric synthesis parallel reaction device can be used for assembling different modules according to needs, has a good cooling effect, and can be easily connected with various electrochemical workstations sold in the market to realize online detection.
4. The multi-sample organic photoelectric synthesis parallel reaction device can improve the accuracy of the test and has the characteristic of good repeatability.
5. The multi-sample organic photoelectric synthesis parallel reaction device can be assembled automatically according to needs, so that the multi-sample organic photoelectric synthesis parallel reaction device is suitable for organic synthesis reactions such as photocatalytic reactions from ultraviolet to visible light, constant-voltage/constant-current electrolytic reactions, photoelectric synthesis and the like under different conditions (low temperature-room temperature) and different wavelengths.
6. The multi-sample organic photoelectric synthesis parallel reaction device can be spliced freely according to the conditions of photocatalysis, electrolysis and photoelectric organic synthesis reaction, and is high in yield stability and excellent in parallelism.
The foregoing is a summary of the present invention, and for the purpose of making the technical means of the present invention more comprehensible, embodiments thereof are described in detail below with reference to the accompanying drawings.
Drawings
Fig. 1 is a schematic diagram of a combination of a lamp cartridge module, a liquid-cooled heat dissipation module, and a base module in this embodiment.
Fig. 2 is an exploded view of fig. 1.
Fig. 3 is an exploded view of the lamp cartridge module according to the present embodiment.
[ reference numerals ]
1-barrel component, 101-window, 102-limiting step, 103-positioning groove, 104-handheld boss, 2-light source component, 201-lamp piece, 202-light source jacket, 203-insulating base, 204-first conducting ring, 205-second conducting ring, 206-pressing piece, 207-first limiting groove, 208-second limiting groove, 209-connecting piece, 3-glass piece, 4-liquid cooling heat dissipation module, 401-cooling groove, 402-fixing groove, 5-base module, 501-socket and 502-positioning pin.
Detailed Description
To further illustrate the technical means and effects of the present invention for achieving the intended purpose, the following detailed description will be made on a lamp cartridge module and a multi-sample organic photoelectric synthesis parallel reaction apparatus according to the present invention with reference to the accompanying drawings and preferred embodiments.
In the description of the present invention, it should be noted that the terms "upper", "lower", "left", "right", and the like indicate orientations or positional relationships based on the drawings, and are only for convenience of describing the present invention and simplifying the description, but do not indicate or imply that the referred device or element must have a specific orientation, be constructed in a specific orientation, and be operated, and thus, should not be construed as limiting the present invention.
The utility model provides a parallel reaction unit of organic photoelectric synthesis of many samples, including stirring and adjusting module, be applicable to organic photoelectric synthesis's reaction vessel, multifunctional power supply adaptation module, base module 5, detachably installs liquid cooling heat dissipation module 4 on base module 5, install a plurality of lamp section of thick bamboo modules in liquid cooling heat dissipation module 4, install the reaction vessel that is used for carrying out organic photoelectric synthesis reaction in the lamp section of thick bamboo module, this reaction vessel includes the quartz glass pipe of high luminousness, install electrolytic device in the quartz glass pipe, this electrolytic device includes sealing washer and polytetrafluoroethylene stopper, quartz glass pipe and polytetrafluoroethylene stopper are connected for the spiral mode and install between the two and be used for isolated air and oxygen anticorrosive anti-oxidant sealing washer simultaneously, 2-5 cavities of 3-6mm have been seted up on the polytetrafluoroethylene stopper, make it can with market electrode, a, The electrolysis device is electrically connected with an external multifunctional power supply adaptation module, the multifunctional power supply adaptation module can provide a constant-voltage or constant-current power supply for the electrolysis device, and the multifunctional power supply adaptation module can be an adjustable direct-current power supply or an adjustable constant-voltage power supply used by various electrochemical workstations; the electrolysis device is the prior art and is not described in detail herein.
The lamp tube module comprises a tube body assembly 1, a light source assembly 2 detachably mounted at the bottom of the tube body assembly 1, and a glass sheet 3 which is mounted between the tube body assembly 1 and the light source assembly 2 and is used for allowing a bottom irradiation light source for carrying out photocatalytic reaction to penetrate through and providing supporting force for a reaction container mounted in the tube body assembly 1. In this embodiment, the light source module 2 is installed at the bottom of the barrel module 1 by means of screw-fitting, but may be installed on the barrel module 1 by means of plug-in fitting or other fitting in other embodiments of the present invention.
The barrel component 1 is hollow, a positioning groove 103 for placing the reaction vessel is arranged in the barrel component 1, a window 101 is arranged on the side wall of the barrel component 1, the reaction phenomenon in the reaction vessel can be observed through the window 101, and a light-transmitting window can be provided for the side irradiation of the reaction vessel.
Still be equipped with on barrel subassembly 1 and carry out spacing step 102 to the position of this lamp section of thick bamboo module at the photocatalysis reaction, barrel subassembly 1 top is equipped with handheld boss 104, is equipped with a plurality of protruding muscle along circumference on the outer wall of handheld boss 104, thereby this protruding muscle can increase this lamp section of thick bamboo module and outside frictional force drive this lamp section of thick bamboo module and take place to rotate.
The light source assembly 2 includes a lamp sheet 201 for providing a bottom irradiation light source for the photocatalytic reaction, a light source housing 202 detachably mounted at the bottom of the barrel assembly 1, two connecting sheets 209 electrically connected to two electrodes of the lamp sheet 201, a pressing sheet 206 with bolt holes, an insulating base 203 detachably mounted at the bottom of the light source housing 202, a first conductive ring 204, and a second conductive ring 205.
In this embodiment, the light source outer sleeve 202 is installed at the bottom end of the barrel assembly 1 in a threaded manner, but in other embodiments of the present invention, the light source outer sleeve may also be installed at the bottom end of the barrel assembly 1 in a plug-in fit manner or other fitting manners, and the insulating base 203 is also installed at the bottom of the light source outer sleeve in a threaded manner or other fitting manners; in this embodiment, the lamp sheet 201 is an LED lamp bead, and certainly, the lamp sheet 201 can be an LED lamp bead with a light wavelength of 360nm to 700nm (ultraviolet-visible light region) and a power of 1 to 10W; in this embodiment, glass sheet 3 is the high printing opacity quartz glass piece, and this glass sheet 3 can ensure that bottom irradiation light source can also avoid reaction vessel direct mount to the surface of lamp piece 201 from bottom to top when fully shining the reaction vessel bottom, leads to the solution in heat direct transfer to the reaction vessel that LED lamp pearl gived off, influences the reaction effect.
The top surface of the insulating base 203 is provided with a first limiting groove 207 for limiting the pressing sheet 206 and a second limiting groove 208 for limiting the lamp sheet 201, the bottom of the insulating base 203 is provided with a first mounting groove for mounting the first conducting ring 204 and a second mounting groove for mounting the second conducting ring 205, and when the lamp is mounted, the first conducting ring 204 is sleeved outside the second conducting ring 205 and the two are not in contact with each other; the pressing sheet 206 is installed in the first limiting groove 207 through a first bolt, the pressing sheet 206, the insulating base 203 and the second conducting ring 205 are fixedly connected into a whole by the first bolt in sequence, the lamp sheet 201 is installed in the second limiting groove 208, any one connecting sheet 209, the insulating base 203 and the first conducting ring 204 are fixedly connected into a whole by the second bolt in sequence, the other connecting sheet 209 and the pressing sheet 206 are fixedly connected into a whole by the third bolt in sequence, and the two connecting sheets 209 are respectively connected with the positive pole and the negative pole of the lamp sheet 201 and fix the lamp sheet in the second limiting groove 208 of the insulating base 203.
In this embodiment, the first conductive ring 204 and the second conductive ring 205 are arranged in a ring shape, so that the lamp cylinder module can be easily inserted and pulled out, and can be rotated by 360 degrees when the lamp cylinder module is powered on; in addition, when the first conductive ring 204 and the second conductive ring 205 are electrically connected to an external power source, the first conductive ring 204 may be electrically connected to the positive electrode of the power source, and the second conductive ring 205 may be electrically connected to the negative electrode of the power source, or the first conductive ring 204 may be electrically connected to the negative electrode of the power source, and the second conductive ring 205 may be electrically connected to the positive electrode of the power source.
The top surface of the base module 5 is circumferentially provided with a plurality of sockets 501 and positioning pins 502, the socket 501 is a socket matched with the lamp cylinder module light source assembly 2, and the socket is the prior art and is not described in detail herein; each socket 501 is connected with an external multifunctional power adapter module through an independent wire, each socket 501 is provided with an independent power supply control switch, and each socket 501 can work independently without mutual influence. During testing, one socket 501 may be used as needed, or multiple sockets 501 may be used simultaneously; the multifunctional power supply adapting module can provide direct current for the socket 501, and further provides direct current power for the lamp sheet 201 in the lamp tube module, the power of the direct current power supply is adjustable, and the multifunctional power supply adapting module can adapt to the requirements of lamp sheets with various wavelengths of 1W-10W.
Still be equipped with the recess of caving in on base module 5's the bottom surface, this recess can be convenient for with base module direct mount on stirring and adjusting module, should stir and adjusting module mainly used adjusts the rotor speed, survey the reaction liquid temperature in the reaction vessel, the most common is the magnetic stirrers on the market, this stirring and adjusting module are prior art, no longer gives details here.
The liquid cooling heat dissipating module 4 is provided with a fixing groove 402 inside, the liquid cooling heat dissipating module 4 is provided with a plurality of cooling tanks 401 which are distributed annularly with the fixing groove 402 as the center and are used for installing the lamp tube module, the cooling tanks 401 penetrate through the top surface and the bottom surface of the liquid cooling heat dissipating module 4, the cooling channels 401 are positioned to correspond to the sockets 501 on the base module 5, while each cooling channel 401 is provided with side openings in its side walls, and a side of each cooling bath 401, which is provided with a side opening through which the cooling bath 401 communicates with the fixing groove 402, faces the fixing groove 402, and when the lamp cartridge module is mounted in the cooling bath 401, if the reaction vessel in the lamp cylinder module only needs the bottom irradiation light source, the lamp cylinder module is rotated, the side of the lamp cylinder module provided with the window 101 is opposite to the fixing groove 402, when the reaction vessel in the lamp cylinder module only needs a side irradiation light source, the side of the lamp cylinder module provided with the window 101 faces the fixing groove 402; a plurality of positioning holes matched with the positioning pins 502 are formed in the bottom surface of the liquid cooling heat dissipation module 4, and when the liquid cooling heat dissipation module 4 is installed on the base module 5 through the matching of the positioning holes and the positioning pins 502, the cooling tanks 401 correspond to the sockets 501 one by one; install liquid cooling heat dissipation module on base module 5, pack the lamp section of thick bamboo module into cooling bath 401 after, the conducting ring of lamp section of thick bamboo module bottom is pegged graft on socket 501, meanwhile, spacing step 102 card is at the top of cooling bath 401 and with the reliable contact of liquid cooling heat dissipation module, liquid cooling heat dissipation module provides a perpendicular ascending holding power for the lamp section of thick bamboo module, avoids lamp section of thick bamboo module to form pressure to socket 501, also can guarantee the stability of overall structure in the reaction process simultaneously.
The liquid cooling heat radiation module 4 also comprises a liquid cooling channel arranged in the liquid cooling heat radiation module 4, a liquid inlet and a liquid outlet which are arranged on the side wall of the liquid cooling heat radiation module 4 and communicated with the liquid cooling channel; the liquid inlet and the liquid outlet are communicated with an external water storage tank through a circulating pump, the liquid cooling channel adopts an S-shaped liquid loop, a refrigerant is introduced into the liquid cooling channel from the liquid inlet, and then the refrigerant absorbing heat is discharged from the liquid outlet, wherein the refrigerant can be water, ethanol, isopropanol and the like; the liquid cooling heat dissipation module can dissipate heat generated by the lamp tube module for carrying out photocatalytic reaction, prevent the lamp tube module from being damaged due to overheating, prevent a reaction container from being overheated to be not beneficial to the reaction of a sample, and solve the heat dissipation problem of various light sources; when the device is used, a high-power mercury lamp, a xenon lamp, a household bulb, an energy-saving lamp and other heterogeneous light sources can be placed in the fixing groove 402, so that the side part of the reaction vessel arranged in the barrel assembly 1 can be irradiated, and a side irradiation light source is provided for the reaction vessel.
In this embodiment, the liquid-cooled heat dissipation module 4 is detachably mounted on the base module 5, but the liquid-cooled heat dissipation module 4 and the base module 5 may be integrated as needed in other embodiments of the present invention.
During the use, install liquid cooling heat dissipation module 4 on base module 5, install base module 5 on stirring and adjusting module, select the lamp piece 201 of suitable power according to experimental needs, then install this lamp piece in lamp section of thick bamboo module, put into the reaction vessel who holds the sample in lamp section of thick bamboo module, install lamp section of thick bamboo module in cooling bath 401, and make light source subassembly 2 of lamp section of thick bamboo module peg graft on socket 501, then with this socket 501 through the connecting wire with the unanimous multi-functional power supply adaptation module electric connection of outside output power and lamp piece 201 power, lamp piece 201 provides the bottom irradiation light source for the sample in the reaction vessel.
The multifunctional power supply adapting module can provide a direct-current power supply for the socket on the base module 5, and the direct-current power supply can meet the requirement of power adjustability; and can also provide a constant voltage/constant current direct current power supply for an electrolysis device used by the organic photoelectric synthesis reaction container, wherein the direct current power supply can be an adjustable direct current power supply or an adjustable constant voltage power supply used by various commercially available electrochemical workstations.
1. When the sample in the reaction container is subjected to photocatalytic reaction
If the batch of samples need a bottom irradiation light source in the test process, a liquid cooling heat dissipation module 4 is installed on a base module 5, the base module 5 is installed on a stirring and adjusting module, a lamp tube module installed with a reaction container is installed in a cooling tank 401, a light source assembly 2 of the lamp tube module is inserted into a socket 501, then the socket 501 is electrically connected with a multifunctional power supply adaptation module with external output power consistent with the power of a lamp piece 201 through a connecting wire, the lamp tube module is manually rotated, one side of the lamp tube module, which is provided with a window 101, is back to a fixed groove 402, a power supply control switch corresponding to the socket 501 on the multifunctional power supply adaptation module is turned on, and at the moment, the samples in the reaction container only react under the irradiation of the bottom irradiation light source;
if this batch of sample need the side in the process of the test when shining the light source, install liquid cooling heat dissipation module 4 on base module 5, install base module 5 on stirring and adjusting module, install reaction vessel's lamp section of thick bamboo module in cooling bath 401 will be installed, and make the light source subassembly 2 of lamp section of thick bamboo module peg graft on socket 501, socket 501 does not electrify, then rotate this lamp section of thick bamboo module that a batch of sample is located, one side orientation fixed slot 402 that makes the lamp section of thick bamboo module be equipped with window 101, then it can to place external light source in fixed slot 402.
2. When the sample in the reaction vessel is subjected to an electrolytic reaction
If the batch of samples need to be subjected to electrolytic reaction in the test process, the liquid cooling heat dissipation module 4 is installed on the base module 5, the base module 5 is installed on the stirring and adjusting module, the lamp tube module provided with the reaction vessel is installed in the cooling tank 401, the socket 501 is not electrified, and then the multifunctional power supply adaptation module providing a constant voltage/constant current power supply for the electrolytic reaction is started.
3. When the sample in the reaction container is subjected to photoelectric reaction
If this batch of sample both need carry out the photocatalytic reaction in the process of the test, need carry out the electrolytic reaction again, then install liquid cooling heat dissipation module 4 on base module 5, install base module 5 on stirring and adjusting module, install the lamp section of thick bamboo module that will install reaction vessel in cooling bath 401, then select bottom irradiation light source or side irradiation light source according to experimental needs, it can to open the multi-functional power adaptation module that provides the power for electrolytic device and photocatalytic reaction simultaneously.
Of course, in the process of the test, part of the samples in the same batch can be subjected to photocatalytic reaction, electrolytic reaction and photoelectric reaction, so that the contrast of the test is increased; the above is only the best embodiment of the present invention, and it is needless to say that the lamp cartridge module may be directly mounted on the base module 5 without the liquid cooling heat dissipation module.
The above description is only a preferred embodiment of the present invention, and should not be taken as limiting the invention in any way, and any simple modification, equivalent change and modification made by those skilled in the art according to the technical spirit of the present invention are still within the technical scope of the present invention without departing from the technical scope of the present invention.
Claims (10)
1. A lamp cartridge module, characterized in that: including inside barrel subassembly (1) that is equipped with constant head tank (103) that is used for placing reaction vessel, detachably install and provide light source subassembly (2) of bottom irradiation light source for reaction vessel simultaneously in barrel subassembly (1) bottom, install and be used for supplying bottom irradiation light source to pass glass piece (3) that provide the holding power to the reaction vessel of installing in barrel subassembly (1) simultaneously between barrel subassembly (1) and light source subassembly (2).
2. The lamp cartridge module of claim 1, wherein: the light source component (2) is arranged at the bottom of the cylinder component (1) in a thread matching mode.
3. The lamp cartridge module of claim 1, wherein: the side wall of the cylinder component (1) is provided with a window (101) which provides a light-transmitting window for the lateral irradiation of the reaction vessel.
4. The lamp cartridge module of claim 1, wherein: the barrel component (1) is also provided with a limiting step (102) for limiting.
5. The lamp cartridge module of claim 1, wherein: be equipped with handheld boss (104) on barrel subassembly (1), thereby the outer wall of handheld boss (104) is equipped with along circumference and is used for increasing this lamp section of thick bamboo module and outside frictional force and takes place a plurality of protruding muscle of pivoted with this lamp section of thick bamboo module of drive.
6. The lamp cartridge module of claim 1, wherein: the light source assembly (2) comprises a lamp sheet (201) for providing a bottom irradiation light source for photocatalytic reaction, two connecting sheets (209) electrically connected with two electrodes of the lamp sheet (201) respectively, a light source jacket (202) detachably installed at the bottom of the barrel assembly (1), a pressing sheet (206) provided with a plurality of bolt holes, a first limiting groove (207) for limiting the pressing sheet (206) and a second limiting groove (208) for limiting the lamp sheet (201) are installed at the bottom of the light source jacket (202) simultaneously, a first conducting ring (204) and a second conducting ring (205) which are installed at the bottom of the insulating base (203) and are not in contact with each other, the pressing sheet (206), the insulating base (203) and the second conducting ring (205) are fixedly connected into a whole through first bolts, wherein any one of the connecting sheets (209), the insulating base (203) and the first conducting ring (204) are fixedly connected into a whole through second bolts, the other connecting piece (209) and the pressing piece (206) are fixedly connected into a whole through a third bolt.
7. The parallel reaction unit of organic photoelectric synthesis of many samples, its characterized in that: the liquid cooling heat dissipation module comprises a base module (5) provided with a plurality of sockets (501), and a liquid cooling heat dissipation module (4) which is arranged on the base module (5) and is also provided with a fixing groove (402); the liquid cooling heat dissipation module (4) is provided with a plurality of cooling grooves (401) along the circumferential direction for installing the lamp cylinder module according to any one of claims 1 to 6, and the cooling grooves (401) are provided with side openings communicated with the fixing grooves (402).
8. The multi-sample organic photoelectric synthesis parallel reaction device according to claim 7, wherein: the liquid cooling heat dissipation module (4) is detachably installed on the base module (5).
9. The multi-sample organic photoelectric synthesis parallel reaction device according to claim 8, wherein: the top surface of the base module (5) is provided with a plurality of positioning pins (502), and the bottom surface of the liquid cooling heat dissipation module (4) is provided with a plurality of positioning holes matched with the positioning pins (502); the bottom of the base module (5) is also provided with a stirring and adjusting module.
10. The multi-sample organic photoelectric synthesis parallel reaction device according to claim 7, wherein: the liquid cooling heat dissipation module (4) comprises a liquid cooling channel arranged inside the liquid cooling heat dissipation module (4), and a liquid inlet and a liquid outlet which are arranged on the liquid cooling heat dissipation module (4) and are communicated with the liquid cooling channel.
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| CN201911244829.5A CN110801796A (en) | 2019-12-06 | 2019-12-06 | Lamp tube module and multi-sample organic photoelectric synthesis parallel reaction device |
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| CN201911244829.5A CN110801796A (en) | 2019-12-06 | 2019-12-06 | Lamp tube module and multi-sample organic photoelectric synthesis parallel reaction device |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111889050A (en) * | 2020-08-19 | 2020-11-06 | 四川大学 | Photocatalysis reaction appearance |
| CN112138618A (en) * | 2020-10-13 | 2020-12-29 | 湖南洋韬材料科技有限公司 | Airtight light-resistant reaction unit |
| CN113559805A (en) * | 2021-08-24 | 2021-10-29 | 忻州师范学院 | Multi-channel photocatalytic reaction device and reaction method thereof |
| CN114733457A (en) * | 2022-04-14 | 2022-07-12 | 扬州联通医药设备有限公司 | Medicine synthesis reactor |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2011104515A (en) * | 2009-11-17 | 2011-06-02 | Ihi Corp | Photocatalytic reaction apparatus |
| CN104190344A (en) * | 2014-07-25 | 2014-12-10 | 北京泊菲莱科技有限公司 | Light irradiation multi-sample parallel reaction device |
| CN107321281A (en) * | 2017-07-05 | 2017-11-07 | 深圳蓝新科技有限公司 | Light reaction instrument |
| CN211246515U (en) * | 2019-12-06 | 2020-08-14 | 洛阳金峰机电装备有限公司 | Lamp tube module and multi-sample organic photoelectric synthesis parallel reaction device |
-
2019
- 2019-12-06 CN CN201911244829.5A patent/CN110801796A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2011104515A (en) * | 2009-11-17 | 2011-06-02 | Ihi Corp | Photocatalytic reaction apparatus |
| CN104190344A (en) * | 2014-07-25 | 2014-12-10 | 北京泊菲莱科技有限公司 | Light irradiation multi-sample parallel reaction device |
| CN107321281A (en) * | 2017-07-05 | 2017-11-07 | 深圳蓝新科技有限公司 | Light reaction instrument |
| CN211246515U (en) * | 2019-12-06 | 2020-08-14 | 洛阳金峰机电装备有限公司 | Lamp tube module and multi-sample organic photoelectric synthesis parallel reaction device |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111889050A (en) * | 2020-08-19 | 2020-11-06 | 四川大学 | Photocatalysis reaction appearance |
| CN112138618A (en) * | 2020-10-13 | 2020-12-29 | 湖南洋韬材料科技有限公司 | Airtight light-resistant reaction unit |
| CN113559805A (en) * | 2021-08-24 | 2021-10-29 | 忻州师范学院 | Multi-channel photocatalytic reaction device and reaction method thereof |
| CN113559805B (en) * | 2021-08-24 | 2022-08-16 | 忻州师范学院 | Multi-channel photocatalytic reaction device and reaction method thereof |
| CN114733457A (en) * | 2022-04-14 | 2022-07-12 | 扬州联通医药设备有限公司 | Medicine synthesis reactor |
| CN114733457B (en) * | 2022-04-14 | 2023-11-21 | 扬州联通医药设备有限公司 | Medicine synthesis reactor |
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