CN110793933A - Method for detecting quality of moxa cone by utilizing terahertz waves - Google Patents

Method for detecting quality of moxa cone by utilizing terahertz waves Download PDF

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CN110793933A
CN110793933A CN202010000161.6A CN202010000161A CN110793933A CN 110793933 A CN110793933 A CN 110793933A CN 202010000161 A CN202010000161 A CN 202010000161A CN 110793933 A CN110793933 A CN 110793933A
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moxa cone
terahertz
moxa
detecting
wave
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CN110793933B (en
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刘红宁
单思
严小军
许小宇
王祺
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Jiangxi University of Traditional Chinese Medicine
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/3563Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing solids; Preparation of samples therefor
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/3581Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light using far infrared light; using Terahertz radiation

Abstract

The invention relates to the technical field of medical detection, and particularly discloses a method for detecting moxa cone quality by utilizing terahertz waves. The method comprises the following steps: s1 placing a sample to be tested; s2, measuring a background value; s3, measuring the terahertz wave energy of different wave bands of the burning moxa cone; s4, processing data; and S5 determining the quality of the moxa cone: the better the quality is if the stronger the terahertz wave intensity of each band is and the waveform changes slightly. The invention provides a brand-new detection method for the quality control standard of moxa cone manufacturers, and brings convenience to accurate judgment of moxa cone quality by moxa cone users. The method has the advantages of simplicity, sensitivity, accurate and reliable data, short detection time, low detection cost and the like.

Description

Method for detecting quality of moxa cone by utilizing terahertz waves
Technical Field
The invention belongs to the technical field of medical detection, and particularly relates to a method for detecting moxa cone quality by utilizing terahertz waves.
Background
Moxibustion is highly appreciated for its effects of warming and activating meridians, harmonizing qi and blood, coordinating yin and yang, strengthening body resistance and eliminating pathogens. But the quality of moxa cones of various brands on the market is uneven, the beads are mixed with the eyes of the fishes, and the research on the quality and the quality control of the moxa cones is less. In the clinical treatment process, moxibustion mainly stimulates acupuncture points through various effects of acupuncture points, medicines, heat radiation, infrared radiation and the like, so that a treatment method for preventing or treating diseases is achieved. After receiving the electric wave with specific wavelength and intensity based on human body matching, the electric wave generates resonance with the same substances contained in the cells in the human body, thereby enhancing the microcirculation effect, promoting metabolism, generating the repair to the pathological changes of the human body, leading patients to be quickly recovered and leading non-patients to improve the self resistance.
The terahertz electromagnetic wave is composed of protons, has lower energy and is an effective nondestructive detection method. The terahertz wave research is mainly applied to the fields of agriculture, food processing industry and the like, such as communication (broadband communication), radar, electronic countermeasure, electric weapons, astronomy, medical imaging (unmarked gene inspection and imaging at a cell level), nondestructive testing, safety inspection (biochemical inspection), grain seed selection, excellent strain selection and the like.
At present, the detection research on the quality of moxa cones (moxa sticks) mainly comprises the aspects of measuring basic parameters (such as length, diameter, hardness, water content, combustion time and temperature, weight of raw materials and ash and the like) of combustion of the moxa cones, infrared spectrum generated by combustion, analysis of chemical components of moxa smoke, acute toxicity and chronic toxicity experiments and the like, and a method for measuring the energy of terahertz waves generated by combustion of the moxa cones (moxa sticks), namely a method for detecting the quality of the moxa cones by utilizing the terahertz waves, has not been reported yet.
Disclosure of Invention
The technical problem to be solved by the invention is as follows: aiming at the defects and shortcomings of the prior art, the method for detecting the energy of the terahertz wave generated in the burning process of the moxa cone by adopting the terahertz spectrometer is provided, and a brand-new quality detection method is provided for the moxa cone quality control standard by combining waveform change.
The invention adopts the following technical scheme to achieve the purpose of the invention.
A method for detecting the quality of a moxa cone by utilizing terahertz waves comprises the following steps:
s1, placing a sample to be detected;
s2, measuring a background value;
s3, measuring the terahertz wave energy of different wave bands of the burning moxa cone;
s4, processing data;
and S5, judging the quality of the moxa cone.
Terahertz (THZ) waves are electromagnetic waves with a frequency of 0.1-10 THZ and are in a band that transitions from macroscopic electronics to microscopic photonics. The moxa cone can generate heat radiation when reaching a certain temperature in the combustion process, terahertz waves are also in the wavelength range of the radiation, the terahertz wave energy generated by the combustion of different moxa cones in different wave bands has different energy levels, and the quality of the moxa cone is judged through data processing.
Further, the placing of the sample to be tested in step S1 specifically includes: the moxa cone is fixed on a frame, and is positioned in the center of an emission opening of the terahertz spectrometer 16cm away from the center.
Further, the background value in step S2 is an electromagnetic wave radiated from the terahertz waveband background of the earth (universe); the background value of the measurement is specifically as follows: and (5) calibrating equipment, detecting the moxa cone terahertz waves in an unburned state for 3-6 times, and taking the average value of the moxa cone terahertz waves.
Further, the step S3 of measuring the terahertz wave energy of different bands of the burning moxa cone specifically includes: after the moxa cone is ignited for 10 seconds, a terahertz spectrometer is used for starting detection, and terahertz waves of the burnt moxa cone are detected for 50-60 times.
Further, the data processing in step S4 specifically includes: each moxa cone measures 373 wave band terahertz magnetic wave intensity values, each wave band intensity value measures 50-60 times, the average value is taken, and 373 wave band intensity values of each brand (series) are respectively compared with 373 wave band intensity values of a blank control group.
Further, the determination of the quality of the moxa cone in step S5 specifically includes: the method is characterized in that the mass of the moxa cone is judged by combining waveform change based on the fact that the terahertz magnetic wave energy generated in the combustion process of the moxa cone is measured by a terahertz magnetic spectrometer, and if the terahertz wave intensity of each waveband is stronger and the waveform slightly changes, the mass is better. According to the research of the teaching team of Wenchun and Chun from the present school, on the terahertz wave characteristics of human body, the comparison and analysis of terahertz magnetic waves generated by healthy people, general qigong teachers and advanced qigong teachers shows that the human body has the characteristics of terahertz waves, the waveform of the 'gas' emitted by the qigong teachers is almost identical to the terahertz waveform of the earth (universe) heat radiation, the stronger the intensity of the qigong function is, the stronger the terahertz intensity is, and the terahertz waves emitted by the senior qigong famous family are slightly changed in waveform.
Furthermore, the model of the terahertz spectrometer is Brukvertex 80 v. In order to expand the wavelength test range to a terahertz waveband, a detector Bolometer working at the liquid helium temperature (4 DEG K) is additionally arranged, and the detector has a terahertz detection patent technology (technical indexes of a terahertz spectrometer, namely spectral characteristic peak resolution is more than 0.2CM-1, scanning speed is 1.0-100mm/sec opda, beam splitters are Mylar 125 mu m, Mylar 50 mu m, Mylar 25 mu m, Mullayer and KBr beam splitters, light sources are a HeNe laser, a mercury lamp and a MIR, detectors are a Bolometer and a model QNbB/PTC, the luminosity accuracy is less than 0.1% T, the relative vacuum degree is less than 500Pa, and operation software is OPUS7.2.139.1294).
Has the advantages that:
(1) the invention provides a brand new detection method for the quality control standard of moxa cone manufacturers by detecting the moxa cone quality by utilizing terahertz waves.
(2) The detection method adopts the terahertz spectrometer to measure the terahertz wave energy generated in the burning process of the moxa cone, combines the waveform change, establishes the method and the steps for measuring the moxa cone mass, and has the advantages of simple and sensitive method, accurate and reliable data, short detection time, low detection cost and the like.
(3) The accurate judgment of the moxa cone quality by the moxa cone user is facilitated. The moxa cone user can intuitively and accurately judge the mass of the moxa cone according to the terahertz wave detection data of the moxa cone mass.
Drawings
Fig. 1 is a graph of the measurement result of the terahertz wave energy of moxa roll burning 2 times through moxa column (moxa filtering 2 times).
FIG. 2 is a graph showing the comparative analysis result of 373 wave band terahertz wave intensity values generated by eight types of moxa cones burning. Wherein:
a is a wave band 119.578-107.765; b is a wave band 107.524-95.7109;
c is a wave band 95.4698-83.6566; d is a waveband of 83.4155-71.6024;
e is a wave band 71.3613-59.5481; f is a wave band 59.307-47.4938;
g is a waveband 47.2527-35.4396; h is a wave band 35.1985-29.8946.
Detailed Description
The present invention will be further described with reference to specific examples, but the present invention is not limited to the following examples. The method is a conventional method unless otherwise specified. The starting materials are commercially available from the open literature unless otherwise specified.
Example 1:
the experiment aims to obtain terahertz waves generated after burning moxa cones of different brands or different series of the same brand so as to establish a method for measuring the energy of the moxa cones terahertz waves.
1.1 materials and instruments
1.1.1 Experimental materials: moxa sticks of different brands, fixing frames, lighters, candles, timers and rulers
1.1.2 Instrument: terahertz spectrometer (Brookvertex 80 v)
1.2 experimental grouping: grouping moxa cones into 23 groups according to brand and different series of the same brand, and specifically grouping as shown in Table 1 below
Figure 219062DEST_PATH_IMAGE001
Wherein the moxa roll for 2 times, the moxa roll for 3 times, the moxa roll for 4 times, the moxa roll for 5 times and the moxa roll for 6 times are prepared from moxa sticks (Jiangxi moxa Biotechnology Co., Ltd.) by different processing technologies, which is shown in Table 2.
Figure 372963DEST_PATH_IMAGE002
Note: the fluff yield refers to the mass ratio of the raw material moxa to the processed moxa.
And (3) randomly extracting 6 moxa cones from each group of the 23 groups respectively for measuring the terahertz wave energy.
1.3 detection method
1.3.1 the moxa cone was fixed to the frame so that it was centered at the emission port, 16cm therefrom, because too close to the emission port easily damaged the emission port.
1.3.2 detecting the moxa cone terahertz waves in an unburned state for 5 times, and taking the average value of the terahertz waves.
1.3.3 igniting the moxa cone, measuring 373 wave band terahertz magnetic wave intensity values by each moxa cone, measuring 50-60 times of each wave band intensity value, taking the average value, listing moxa cones with the serial number of 1 in the table 1 for 2 times of moxa sticks (2 times of moxa filtration), taking 373 wave band terahertz magnetic wave intensity values measured by parallel samples with the serial numbers of 1-3 respectively, wherein the numerical value represents the number of photons in a certain wave band and has no unit. The results are shown in Table 3 below.
1.3.4 the apparatus is deflated and calibrated for the next sample test.
Figure 255468DEST_PATH_IMAGE003
Figure 139110DEST_PATH_IMAGE004
Figure 81658DEST_PATH_IMAGE005
Figure 660538DEST_PATH_IMAGE006
Figure 612314DEST_PATH_IMAGE007
Figure 84884DEST_PATH_IMAGE008
Figure 401595DEST_PATH_IMAGE009
Figure 326826DEST_PATH_IMAGE010
Figure 783270DEST_PATH_IMAGE012
Figure 67621DEST_PATH_IMAGE013
Figure 89935DEST_PATH_IMAGE014
Figure 383513DEST_PATH_IMAGE015
Figure 565095DEST_PATH_IMAGE016
Figure 161293DEST_PATH_IMAGE017
Figure 762913DEST_PATH_IMAGE018
Figure 302796DEST_PATH_IMAGE020
1.4 data processing
Data to
Figure 194529DEST_PATH_IMAGE021
And +/-S (mean +/-standard deviation) represents that the terahertz wave energy is processed by adopting sps statistics17 statistical software, and the terahertz wave energy of different wave bands generated by the combustion of the moxa cones of different brands is compared and analyzed by adopting single-factor variance. Specifically processing data: each Airy pillar measures 373 wave band terahertz magnetic wave intensity values, each wave band intensity value measures 50-60 times, and the average value is taken. The 373 wave band intensity values of each brand were compared with the corresponding wave band intensity values of the blank control group.
1.5 judging the quality of the moxa cone: the quality of the moxa cone is judged based on the combination of the high and low energy of the terahertz magnetic wave generated in the combustion process of the moxa cone by a terahertz magnetic spectrometer and the change of the waveform. The better the quality of the moxa cone, the stronger the terahertz wave intensity in each waveband is, and the emitted terahertz waves are slightly changed in waveform.
Fig. 1 is a graph showing the measurement results of the terahertz wave energy generated by the combustion of the itang 2 times through the moxa column (moxa filtration 2 times). It is found that Estang can radiate terahertz wave when burning 2 times the moxa cone, the spectrum range is 0.90-3.60THz, the photon number and intensity are both greater than 0, and the peak value is at 3.05 THz.
FIG. 2 is a graph showing the comparative analysis result of 373 wave band terahertz wave intensity values generated by eight types of moxa cones burning. The eight moxa cones specific brands (processes) shown in fig. 2 are: moxa sticks are used for 2 times (moxa filtration is performed for 2 times/ moxa hall), 3 times (moxa filtration is performed for 3 times/ moxa hall), 4 times (moxa filtration is performed for 4 times/ moxa hall), 5 times (moxa filtration is performed for 5 times/ moxa hall), 6 times (moxa filtration is performed for 6 times/ moxa hall), 5:1 (lint ratio is 5: 1), 15:1 (lint ratio is 15: 1) and 25:1 (lint ratio is 25: 1). In order to make the statistical analysis chart clearly show and facilitate the comparison of the results, the comparative analysis results of 373 wave band terahertz wave intensity values generated by the combustion of the other 15 types of moxa cones are not shown in the chart together except the eight types of moxa cones.
From the terahertz wave intensity waveform diagrams of the eight moxa sticks in fig. 2, it can be seen that: the moxa roll 5 times (moxa filtering 5 times) has the highest intensity in each 373 wave bands, and the emitted terahertz waves have slight changes in waveform, so that the quality of the eight moxa rolls is moxa roll 5 times (moxa filtering 5 times) relatively better.
The embodiments of the present invention have been described in detail, but the embodiments are merely examples, and the present invention is not limited to the above-described embodiments. Any equivalent modifications and substitutions to those skilled in the art are also within the scope of the present invention. Accordingly, equivalent alterations and modifications are intended to be included within the scope of the invention, without departing from the spirit and scope of the invention.

Claims (7)

1. A method for detecting the mass of a moxa cone by utilizing terahertz waves is characterized by comprising the following steps:
s1, placing a sample to be detected;
s2, measuring a background value;
s3, measuring the terahertz wave energy of different wave bands of the burning moxa cone;
s4, processing data;
and S5, judging the quality of the moxa cone.
2. The method for detecting the quality of the moxa cone by using the terahertz waves as claimed in claim 1, wherein the sample to be detected in step S1 is placed, specifically: the moxa cone is fixed on a frame, and is positioned in the center of an emission opening of the terahertz spectrometer 16cm away from the center.
3. The method for detecting the mass of an moxa cone by using terahertz waves according to claim 1, wherein: the background value in the step S2 is a terahertz wave band background radiation electromagnetic wave of the earth; the background value of the measurement is specifically as follows: and (5) calibrating equipment, detecting the moxa cone terahertz waves in an unburned state for 3-6 times, and taking the average value of the moxa cone terahertz waves.
4. The method for detecting the mass of the moxa cone by using the terahertz waves as claimed in claim 1, wherein the step S3 of measuring the energy of the terahertz waves of different bands of the burning moxa cone specifically comprises: after the moxa cone is ignited for 10 seconds, a terahertz spectrometer is used for starting detection, and terahertz waves of the burnt moxa cone are detected for 50-60 times.
5. The method for detecting the moxa cone mass by using the terahertz waves as claimed in claim 1, wherein the data processing in step S4 specifically comprises: measuring 373 wave band terahertz magnetic wave intensity values of each moxa cone, measuring 50-60 times of each wave band intensity value, taking the average value, and comparing 373 wave band intensity values of each brand with 373 wave band intensity values of a blank control group respectively.
6. The method for detecting the moxa cone mass by using the terahertz waves as claimed in claim 1, wherein the determination of the moxa cone mass in step S5 specifically comprises: the method is characterized in that the mass of the moxa cone is judged by combining waveform change based on the fact that the terahertz magnetic wave energy generated in the combustion process of the moxa cone is measured by a terahertz magnetic spectrometer, and if the terahertz wave intensity of each waveband is stronger and the waveform slightly changes, the mass is better.
7. The method for detecting the mass of the moxa cone by using the terahertz waves as claimed in claim 4, wherein: the model of the terahertz spectrometer is Brukvertex 80 v.
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