CN110746893A - Production and use method of hot melt belt - Google Patents
Production and use method of hot melt belt Download PDFInfo
- Publication number
- CN110746893A CN110746893A CN201911047012.9A CN201911047012A CN110746893A CN 110746893 A CN110746893 A CN 110746893A CN 201911047012 A CN201911047012 A CN 201911047012A CN 110746893 A CN110746893 A CN 110746893A
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- hot
- hot melt
- parts
- melt adhesive
- fabric
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/20—Adhesives in the form of films or foils characterised by their carriers
- C09J7/21—Paper; Textile fabrics
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
- C09J175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J5/00—Adhesive processes in general; Adhesive processes not provided for elsewhere, e.g. relating to primers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/30—Adhesives in the form of films or foils characterised by the adhesive composition
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/10—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet
- C09J2301/12—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers
- C09J2301/122—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers the adhesive layer being present only on one side of the carrier, e.g. single-sided adhesive tape
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/30—Additional features of adhesives in the form of films or foils characterized by the chemical, physicochemical or physical properties of the adhesive or the carrier
- C09J2301/304—Additional features of adhesives in the form of films or foils characterized by the chemical, physicochemical or physical properties of the adhesive or the carrier the adhesive being heat-activatable, i.e. not tacky at temperatures inferior to 30°C
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2400/00—Presence of inorganic and organic materials
- C09J2400/20—Presence of organic materials
- C09J2400/26—Presence of textile or fabric
- C09J2400/263—Presence of textile or fabric in the substrate
Abstract
The invention provides a production and use method of a hot-melt belt, which relates to the field of fabric processing technology and comprises the following steps: soaking a nylon fabric or a polyester fabric in liquid ammonium polyphosphate and then drying; the raw materials comprise the following components in parts by weight: the preparation method comprises the following steps of (1) primarily mixing PU glue, ceramic powder, difluoromethane, methanol, chloroform, potassium permanganate and a flame retardant, putting the PU glue and the ceramic powder into a heating container, and putting the difluoromethane, the methanol, the chloroform, the potassium permanganate and the flame retardant into the heating container for continuous stirring; uniformly solidifying to obtain a sheet hot melt adhesive; laying a layer of flaky hot melt adhesive on the upper surface of the base fabric, carrying out hot press molding, and carrying out hot press molding for multiple times according to the method to obtain a hot melt strip; cutting the hot-melt strip by using a cutting machine; laying a hot-melting belt at an opening on the surface of the rubber fabric, and matching with a hot-melting compound machine for use; the fusion site was again heat-fused using a high-frequency machine. The invention has good bonding effect and high safety.
Description
Technical Field
The invention belongs to the field of fabric processing technology, and particularly relates to a production and use method of a hot-melt belt.
Background
The hot melt adhesive is a plastic adhesive, the physical state of which changes along with the change of temperature within a certain temperature range, and the chemical property of which is unchanged, is nontoxic and tasteless, and belongs to an environment-friendly chemical product. The product is solid, so the product is convenient to package, transport and store, and has no solvent, pollution and toxicity; and the production process is simple, the added value is high, the bonding strength is high, the speed is high, and the like. In the production process of rubber clothes, the hot melt belt is widely used, the hot melt belt manufactured by the existing production method of the hot melt belt is generally poor in waterproofness, and when the clothes are used for underwater operation, the water leakage condition is easily caused.
Therefore, it is urgently needed to provide a method for producing and using a hot-melt tape with good adhesion effect and high safety.
Disclosure of Invention
The invention aims to provide a method for producing and using a hot melt strip, aiming at the defects of the prior art.
The invention provides the following technical scheme:
a method of making and using a hot melt strip comprising the steps of:
s1, preparing primary backing: soaking a nylon fabric or a polyester fabric in liquid ammonium polyphosphate for 1-3h, and placing the soaked fabric at the temperature of 100-200 ℃ for high-temperature drying for 30min to obtain a primary fabric;
s2: preparing a hot melt adhesive: the raw materials comprise the following components in parts by weight: 45-65 parts of PU adhesive, 20-25 parts of ceramic powder, 2-4 parts of difluoromethane, 5-10 parts of methanol, 5-7 parts of chloroform, 5-7 parts of potassium permanganate and 2-6 parts of flame retardant, the PU adhesive and the ceramic powder are initially mixed and then put into a heating container, the temperature is increased to 200-250 ℃, the stirring of a stirring device in the container is continued for 30-60min, the difluoromethane, the methanol, the chloroform, the potassium permanganate and the flame retardant are put into the heating container, the temperature is increased to 250-300 ℃, the stirring of the stirring device in the container is continued for 30-40min, and the prepared mixture is the hot melt adhesive;
s3: preparing a hot melt adhesive layer: collecting hot melt adhesive into a glue tank, drying the hot melt adhesive by using a dryer, and uniformly solidifying to obtain sheet hot melt adhesive with the thickness of 0.1-0.3 mm;
s3: and (3) combining the hot melt adhesive layer with the primary backing: laying a layer of flaky hot melt adhesive on the upper surface of the base fabric, performing hot-press molding, cooling, laying a layer of flaky hot melt adhesive above the flaky hot melt adhesive again, and performing hot-press molding for multiple times according to the method to obtain a hot-melt strip;
s4: cutting the hot-melt strip into a width of 1-2cm and a length of 100-200m by using a cutting machine;
s5: laying a hot-melting strip on an opening on the surface of the rubber fabric, and fusing the hot-melting strip and the rubber fabric under the action of 300 ℃ in cooperation with a hot-melting compound machine;
s6: the fusion site was again heat-fused using a high-frequency machine.
Preferably, in step S1, the nylon fabric or the polyester fabric is soaked in liquid ammonium polyphosphate for 2 hours, and the soaked fabric is placed at 150 ℃ for high-temperature drying for 30 min.
Preferably, in step S2, the raw materials comprise the following components in parts by weight: 55 parts of PU glue, 23 parts of ceramic powder, 3 parts of difluoromethane, 8 parts of methanol, 6 parts of chloroform, 6 parts of potassium permanganate and 4 parts of flame retardant.
Preferably, the flame retardant in step S2 is one of tributyl phosphate, triphenyl phosphate, or dibromomethane.
Preferably, in step S2, the PU glue and the ceramic powder are primarily mixed and then put into a heating container, the temperature is raised to 230 ℃, the stirring device in the container continuously stirs for 45min, the difluoromethane, the methanol, the chloroform, the potassium permanganate and the flame retardant are put into the heating container, the temperature is raised to 280 ℃, and the stirring device in the container continuously stirs for 35 min.
Preferably, in step S3, a sheet-like hot melt adhesive with a thickness of 0.2mm is obtained after uniform solidification.
The invention has the beneficial effects that: difluoromethane, methyl alcohol, chloroform and potassium permanganate's among the hot melt adhesive synergism for under the high temperature effect, the molten hot melt adhesive produces the corrosion action a little to the rubber surface fabric, makes the opening part of rubber sealed and fuse as an organic whole completely with the hot melt adhesive, and under the condition of high temperature, the corruption composition that wherein a little volatilizes, leaves components such as PU glue and fuses with the surface fabric, and bonding effect is good and harmless to the human body, and the security is high.
Detailed Description
Example 1
A method of making and using a hot melt strip comprising the steps of:
s1, preparing primary backing: soaking a nylon fabric or a polyester fabric in liquid ammonium polyphosphate for 1h, and placing the soaked fabric at 100 ℃ for high-temperature drying for 30min to obtain a primary fabric;
s2: preparing a hot melt adhesive: the raw materials comprise the following components in parts by weight: 45 parts of PU adhesive, 20 parts of ceramic powder, 2 parts of difluoromethane, 5 parts of methanol, 5 parts of chloroform, 5 parts of potassium permanganate and 2 parts of flame retardant, preliminarily mixing the PU adhesive and the ceramic powder, putting the mixture into a heating container, raising the temperature to 200 ℃, continuously stirring for 30min by a stirring device in the container, putting the difluoromethane, the methanol, the chloroform, the potassium permanganate and the flame retardant into the heating container, raising the temperature to 250 ℃, and continuously stirring for 30min by the stirring device in the container to obtain a mixture, namely the hot melt adhesive;
s3: preparing a hot melt adhesive layer: collecting hot melt adhesive into a glue trough, drying the hot melt adhesive by using a dryer, and uniformly solidifying to obtain sheet hot melt adhesive with the thickness of 0.1 mm;
s3: and (3) combining the hot melt adhesive layer with the primary backing: laying a layer of flaky hot melt adhesive on the upper surface of the base fabric, performing hot-press molding, cooling, laying a layer of flaky hot melt adhesive above the flaky hot melt adhesive again, and performing hot-press molding for multiple times according to the method to obtain a hot-melt strip;
s4: cutting the hot-melt strip into a width of 1-2cm and a length of 100-200m by using a cutting machine;
s5: laying a hot-melting strip on an opening on the surface of the rubber fabric, and fusing the hot-melting strip and the rubber fabric under the action of 300 ℃ in cooperation with a hot-melting compound machine;
s6: the fusion site was again heat-fused using a high-frequency machine.
Example 2
A method of making and using a hot melt strip comprising the steps of:
s1, preparing primary backing: soaking a nylon fabric or a polyester fabric in liquid ammonium polyphosphate for 2 hours, and placing the soaked fabric at 150 ℃ for high-temperature drying for 30min to obtain a primary fabric;
s2: preparing a hot melt adhesive: the raw materials comprise the following components in parts by weight: the preparation method comprises the following steps of firstly mixing 55 parts of PU adhesive, 23 parts of ceramic powder, 3 parts of difluoromethane, 8 parts of methanol, 6 parts of chloroform, 6 parts of potassium permanganate and 4 parts of flame retardant, putting the PU adhesive and the ceramic powder into a heating container after preliminary mixing, raising the temperature to 230 ℃, continuously stirring for 40min by using a stirring device in the container, putting the difluoromethane, the methanol, the chloroform, the potassium permanganate and the flame retardant into the heating container, raising the temperature to 280 ℃, and continuously stirring for 35min by using the stirring device in the container to obtain a mixture, namely the hot melt adhesive;
s3: preparing a hot melt adhesive layer: collecting hot melt adhesive into a glue trough, drying the hot melt adhesive by using a dryer, and uniformly solidifying to obtain sheet hot melt adhesive with the thickness of 0.2 mm;
s3: and (3) combining the hot melt adhesive layer with the primary backing: laying a layer of flaky hot melt adhesive on the upper surface of the base fabric, performing hot-press molding, cooling, laying a layer of flaky hot melt adhesive above the flaky hot melt adhesive again, and performing hot-press molding for multiple times according to the method to obtain a hot-melt strip;
s4: cutting the hot-melt strip into a width of 1-2cm and a length of 100-200m by using a cutting machine;
s5: laying a hot-melting strip on an opening on the surface of the rubber fabric, and fusing the hot-melting strip and the rubber fabric under the action of 300 ℃ in cooperation with a hot-melting compound machine;
s6: the fusion site was again heat-fused using a high-frequency machine.
Example 3
A method of making and using a hot melt strip comprising the steps of:
s1, preparing primary backing: soaking a nylon fabric or a polyester fabric in liquid ammonium polyphosphate for 3 hours, and placing the soaked fabric at 200 ℃ for high-temperature drying for 30min to obtain a primary fabric;
s2: preparing a hot melt adhesive: the raw materials comprise the following components in parts by weight: 65 parts of PU adhesive, 25 parts of ceramic powder, 4 parts of difluoromethane, 10 parts of methanol, 7 parts of chloroform, 7 parts of potassium permanganate and 6 parts of flame retardant, preliminarily mixing the PU adhesive and the ceramic powder, putting the mixture into a heating container, raising the temperature to 250 ℃, continuously stirring by a stirring device in the container for 60min, putting the difluoromethane, the methanol, the chloroform, the potassium permanganate and the flame retardant into the heating container, raising the temperature to 300 ℃, and continuously stirring by the stirring device in the container for 40min to obtain a mixture, namely the hot melt adhesive;
s3: preparing a hot melt adhesive layer: collecting hot melt adhesive into a glue tank, drying the hot melt adhesive by using a dryer, and uniformly solidifying to obtain sheet hot melt adhesive with the thickness of 0.3 mm;
s3: and (3) combining the hot melt adhesive layer with the primary backing: laying a layer of flaky hot melt adhesive on the upper surface of the base fabric, performing hot-press molding, cooling, laying a layer of flaky hot melt adhesive above the flaky hot melt adhesive again, and performing hot-press molding for multiple times according to the method to obtain a hot-melt strip;
s4: cutting the hot-melt strip into a width of 1-2cm and a length of 100-200m by using a cutting machine;
s5: laying a hot-melting strip on an opening on the surface of the rubber fabric, and fusing the hot-melting strip and the rubber fabric under the action of 300 ℃ in cooperation with a hot-melting compound machine;
s6: the fusion site was again heat-fused using a high-frequency machine.
The properties of the hot melt tapes of examples 1-3 were verified and the results are shown in Table 1:
TABLE 1
The effect comparison of the above embodiments shows that the hot melt adhesive tape has good performance and is suitable for popularization and application by improving and researching the formula and the process steps of the hot melt adhesive layer.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (6)
1. A method of producing and using a hot melt strip, comprising the steps of:
s1, preparing primary backing: soaking a nylon fabric or a polyester fabric in liquid ammonium polyphosphate for 1-3h, and placing the soaked fabric at the temperature of 100-200 ℃ for high-temperature drying for 30min to obtain a primary fabric;
s2: preparing a hot melt adhesive: the raw materials comprise the following components in parts by weight: 45-65 parts of PU adhesive, 20-25 parts of ceramic powder, 2-4 parts of difluoromethane, 5-10 parts of methanol, 5-7 parts of chloroform, 5-7 parts of potassium permanganate and 2-6 parts of flame retardant, the PU adhesive and the ceramic powder are initially mixed and then put into a heating container, the temperature is increased to 200-250 ℃, the stirring of a stirring device in the container is continued for 30-60min, the difluoromethane, the methanol, the chloroform, the potassium permanganate and the flame retardant are put into the heating container, the temperature is increased to 250-300 ℃, the stirring of the stirring device in the container is continued for 30-40min, and the prepared mixture is the hot melt adhesive;
s3: preparing a hot melt adhesive layer: collecting hot melt adhesive into a glue tank, drying the hot melt adhesive by using a dryer, and uniformly solidifying to obtain sheet hot melt adhesive with the thickness of 0.1-0.3 mm;
s3: and (3) combining the hot melt adhesive layer with the primary backing: laying a layer of flaky hot melt adhesive on the upper surface of the base fabric, performing hot-press molding, cooling, laying a layer of flaky hot melt adhesive above the flaky hot melt adhesive again, and performing hot-press molding for multiple times according to the method to obtain a hot-melt strip;
s4: cutting the hot-melt strip into a width of 1-2cm and a length of 100-200m by using a cutting machine;
s5: laying a hot-melting strip on an opening on the surface of the rubber fabric, and fusing the hot-melting strip and the rubber fabric under the action of 300 ℃ in cooperation with a hot-melting compound machine;
s6: the fusion site was again heat-fused using a high-frequency machine.
2. The production and use method of the hot melt tape according to claim 1, wherein in step S1, the nylon fabric or the polyester fabric is soaked in the liquid ammonium polyphosphate for 2 hours, and the soaked fabric is dried at 150 ℃ for 30 min.
3. The method for producing and using the hot melt tape as claimed in claim 2, wherein in the step S2, the raw materials comprise the following components in parts by weight: 55 parts of PU glue, 23 parts of ceramic powder, 3 parts of difluoromethane, 8 parts of methanol, 6 parts of chloroform, 6 parts of potassium permanganate and 4 parts of flame retardant.
4. The method of claim 3, wherein the flame retardant in step S2 is one of tributyl phosphate, triphenyl phosphate, or dibromomethane.
5. The method for producing and using the hot-melt tape as claimed in claim 4, wherein in step S2, the PU glue and the ceramic powder are initially mixed and then put into a heating container, the temperature is raised to 230 ℃, the stirring of a stirring device in the container is continued for 45min, the difluoromethane, the methanol, the chloroform, the potassium permanganate and the fire retardant are put into the heating container, the temperature is raised to 280 ℃, and the stirring of the stirring device in the container is continued for 35 min.
6. The method for producing and using a hot melt adhesive tape as claimed in claim 5, wherein in step S3, the uniform solidification results in a sheet-like hot melt adhesive with a thickness of 0.2 mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911047012.9A CN110746893A (en) | 2019-10-30 | 2019-10-30 | Production and use method of hot melt belt |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911047012.9A CN110746893A (en) | 2019-10-30 | 2019-10-30 | Production and use method of hot melt belt |
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| CN110746893A true CN110746893A (en) | 2020-02-04 |
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| CN201911047012.9A Pending CN110746893A (en) | 2019-10-30 | 2019-10-30 | Production and use method of hot melt belt |
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|---|---|---|---|---|
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2019
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Application publication date: 20200204 |