CN110742928B - Method and equipment for preparing recovery suppository - Google Patents
Method and equipment for preparing recovery suppository Download PDFInfo
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- CN110742928B CN110742928B CN201911208263.0A CN201911208263A CN110742928B CN 110742928 B CN110742928 B CN 110742928B CN 201911208263 A CN201911208263 A CN 201911208263A CN 110742928 B CN110742928 B CN 110742928B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/70—Polygonaceae (Buckwheat family), e.g. spineflower or dock
- A61K36/708—Rheum (rhubarb)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
- A61J3/00—Devices or methods specially adapted for bringing pharmaceutical products into particular physical or administering forms
- A61J3/08—Devices or methods specially adapted for bringing pharmaceutical products into particular physical or administering forms into the form of suppositories or sticks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/30—Boraginaceae (Borage family), e.g. comfrey, lungwort or forget-me-not
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/0034—Urogenital system, e.g. vagina, uterus, cervix, penis, scrotum, urethra, bladder; Personal lubricants
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/02—Suppositories; Bougies; Bases therefor; Ovules
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P15/00—Drugs for genital or sexual disorders; Contraceptives
- A61P15/02—Drugs for genital or sexual disorders; Contraceptives for disorders of the vagina
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
- A61J2200/00—General characteristics or adaptations
- A61J2200/20—Extrusion means, e.g. for producing pharmaceutical forms
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Abstract
The invention relates to the field of traditional Chinese medicines, in particular to a preparation method and equipment of a rehabilitation suppository. The method and the equipment change the normal temperature static soaking into the normal temperature dynamic soaking, the purple pigment in the lithospermum is soaked and extracted by osmotic pressure, the characteristic of the sesame oil reaches mauve, continuous repeated extrusion is realized, and the precipitation of the effective components of the lithospermum is improved. The device comprises: a pushing rod connected with a pressing plate is arranged on the soaking container, and a mesh plate and an oil outlet are arranged at the bottom of the soaking container; the valve, the oil storage tank, the oil pump and the oil delivery pipeline are sequentially connected outside the oil outlet, and the oil delivery pipeline is connected with the upper part of the soaking container. The stainless steel rope is hung in the container cover, the lower end of the stainless steel rope is connected with the support body, and the stainless steel rope and the support body are connected in series and can be conveniently detached.
Description
Technical Field
The invention relates to the field of traditional Chinese medicines, in particular to a preparation method and equipment of a rehabilitation suppository.
Background
In the prior art, tonghua Baixin pharmaceutical Co., ltd.s.A. for the production of recovery suppository, ministerial standard number WS 3 -B-1644-93. Prescription: 246g of rheum officinale, 10g of catechu, 100g of lithospermum and 7g of borneol. The preparation method comprises the following steps: grinding Borneolum Syntheticum, and pulverizing Catechu into fine powder. Cutting Huang Zhuo, frying with 650ml sesame oil, and removing residues. Soaking radix Arnebiae in the heated oleum Sesami for 72 hr, filtering to remove radix Arnebiae, and adding semisynthetic fatty acid ester if residual oleum Sesami is less than 365ml, stirring to melt, and standingCooling, adding Borneolum Syntheticum and Catechu fine powder, mixing, molding, taking out, and making into 365 granule.
Traits: the product is a mauve suppository.
And (3) identification: (1) Taking 1 granule of the product, adding 5ml of water, slightly heating, melting, dripping the layer number of the oil layer, adding 2ml of sodium hydroxide test solution, shaking, making the solution blue, and adding dilute hydrochloric acid solution to turn into pink. (2) Taking 2 grains of the product, adding 10ml of water, heating and melting, shaking for 10 minutes, separating a water layer, adding 1ml of hydrochloric acid and 2.5ml of formaldehyde solution, heating on a water bath to generate yellow precipitate, cooling, filtering, taking filtrate, adding a plurality of drops of ferric trichloride test solution and 1g of sodium acetate, and developing brownish red color.
The main functions are as follows: clearing away heat and toxic materials, eliminating dampness, killing parasites, astringing and relieving itching. Can be used for treating colpitis due to various causes. The administration method and dosage are vaginal administration, 1 granule each time, once a day, and the suppository is put into the deep vagina before sleeping.
The oil immersed lithospermum process specified by the ministerial quality standard is to add lithospermum into sesame oil of fried rheum officinale, soak for 72 hours, filter out lithospermum, and make the sesame oil into suppository. The process provides that the lithospermum is soaked in sesame oil which is fried with rheum officinale, and is soaked at normal temperature. Under the process conditions, the sesame oil immersed in the lithospermum turns into yellow from pale yellow when the rhubarb is fried, purple in the lithospermum is not immersed, namely naphthoquinone medicinal components represented by the shikonin are not immersed, on one hand, the medicinal effect is reduced, and on the other hand, the yellow does not accord with the 'mauve' character specified by the ministerial quality standard. The product produced by the process is determined to be a defective product when the product is sent to a medicine monitoring department for inspection.
Disclosure of Invention
The invention aims to provide a preparation method and equipment of a recovery suppository aiming at the defects, and an extrusion soaking process and equipment are adopted, so that the extruded sesame oil becomes 'mauve', thereby not only meeting the regulation of 'property' in the ministry of medical science standard, but also extruding medical components and improving the medical effect.
The technical scheme of the invention is as follows: the recovery suppository is prepared from rhubarb, catechu, lithospermum and borneol raw materials and is characterized in that lithospermum is soaked and extruded in sesame oil after being fried with rhubarb; the soaking extrusion is to add lithospermum into a soaking container, the sesame oil added with fried rheum officinale is soaked for two half hours, the ejector rod of an air cylinder or a hydraulic cylinder in the soaking container pushes the pressing plate to downwards extrude the sesame oil contained in the lithospermum, and the sesame oil flows out of the soaking container through the mesh plate below; the method comprises the steps of embedding stainless steel ropes which can be pulled up into lithospermum before extrusion, arranging a plurality of supports at the lower ends of the stainless steel ropes at intervals and capable of being separated section by section, lifting the stainless steel ropes after extrusion to loosen lithospermum pressed into cakes, removing the upper section of the stainless steel ropes and one support, simultaneously connecting the next stainless steel rope and the support, injecting new sesame oil into a soaking container, soaking, extruding, lifting the support, removing the support, repeating for a plurality of times, and fully soaking the purple pigment in the lithospermum, wherein the characteristic of the sesame oil reaches mauve.
The special equipment for implementing the preparation method of the rehabilitation suppository is characterized by comprising the following components:
the soaking container is provided with a container cover, a pushing rod (such as a pneumatic or hydraulic ejector rod) is arranged on the container cover, and the lower end of the pushing rod is inserted into the soaking container and is connected with a pressing plate.
The bottom of the soaking container is provided with a mesh plate and an oil outlet; the valve, the oil storage tank, the oil pump and the oil delivery pipeline are sequentially connected outside the oil outlet, and the oil delivery pipeline is connected with the upper part of the soaking container.
The stainless steel rope is hung in the container cover, the lower end of the stainless steel rope is connected with the support body, and the stainless steel rope and the support body are connected in series and can be conveniently detached.
In the above-described arrangement, the first and second embodiments,
the support body is a disc, a cross rib frame or a supporting plate.
The edge of the support body is provided with a plurality of auxiliary stainless steel ropes connected with the stainless steel ropes.
The center of the mesh plate 7 is provided with a groove for accommodating a plurality of support bodies and stainless steel ropes, and the periphery of the groove is provided with oil-passing meshes.
The invention has the advantages that: 1. the method and the equipment change the normal temperature static soaking into normal temperature dynamic extrusion soaking, the purple pigment in the lithospermum is extracted by osmotic pressure soaking, the extruded sesame oil becomes ' mauve ', the method and the equipment not only meet the specification of ' property ' in the ministry of the Chinese character ' in the standard, but also have obvious precipitation effect of the effective components of the lithospermum, and the medicine effect is improved. 2. The device adopts the stainless steel rope component which can be buried in the lithospermum before extrusion and pulled up, so that the middle of the lithospermum pressed into cakes is convenient to loosen, continuous repeated extrusion is realized, and the precipitation of the effective components of the lithospermum is improved.
Embodiments of the present invention will be described in further detail below with reference to the accompanying drawings.
Drawings
FIG. 1 is a schematic diagram of the apparatus of the present invention.
Detailed Description
Referring to fig. 1, the part names are as follows: the device comprises a support body 1, a push rod 2, an electric hoist 4, a pressing plate 5, a container cover 6, a mesh plate 7, a soaking container 8, a valve 9, an oil storage tank 10, an oil pump 11, a flange 12, a stainless steel rope 13, a groove 14, an oil outlet 15, an oil feeding pipeline 16, an auxiliary stainless steel rope 17, a bolt 18 and a rope hook hanging ring 19.
Referring to FIG. 1, the preparation method of the rehabilitation suppository comprises 246g of rheum officinale, 10g of catechu, 100g of lithospermum and 7g of borneol
And making into 365 granule. Soaking radix Arnebiae in sesame oil of radix et rhizoma Rhei; the soaking extrusion is that lithospermum is added into a soaking container 8, sesame oil fried with rheum officinale is added to submerge the lithospermum, the lithospermum is soaked for two half hours, a pressing plate 5 is pushed to downwards extrude the sesame oil contained in the lithospermum in the soaking container 8, and the sesame oil flows out of the soaking container 8 through a mesh plate 7 and an oil outlet 15 below; the stainless steel rope 13 which can be pulled up is buried in the lithospermum before extrusion, the lower end of the stainless steel rope 13 is provided with a plurality of supports 1 which are spaced and can be separated section by section (the supports 1 are a disc, a cross rib frame or a supporting plate), the stainless steel rope 13 is lifted up after extrusion so as to loosen the middle of the lithospermum pressed into cakes, and after the container cover 6 is opened, the lithospermum in the side wall of the soaking container 8 is manually pried by a stainless steel pry bar until the lithospermum is completely loosened, so that space is reserved and new sesame oil can be sucked. The upper section stainless steel rope 13 and one support body 1 are removed from the pressing plate 5, meanwhile, the next stainless steel rope 13 and the support body 1 (so as to be pulled up for the second time) are connected with the pressing plate 5 (the first stainless steel rope 13 and the support body 1 are pulled out and are not returned, so that the removal is performed), new sesame oil is injected into the soaking container 8, the soaking is performed, the support body 1 is extruded, the support body 1 is removed, and the repeated steps are performed for 1-12 times (the twelve stainless steel ropes 13 and the support body 1 are sequentially connected, namely, the repeated steps are not limited, so that the production needs are standard), the purple pigment in the lithospermum is completely soaked, the characteristic of the sesame oil reaches the mauve color (the effective components are separated out, and the color is heavy, so that the mauve color can be reached). Through detection, the precipitation of the effective components of the lithospermum is extremely high, and meets or is higher than the standard requirement.
Referring to fig. 1, a special device for implementing a method for preparing a rehabilitation suppository, comprising:
a stainless steel soaking vessel 8, the soaking vessel 8 is provided with a stainless steel vessel cover 6, a stainless steel pushing rod 2 is arranged on the vessel cover 6, and the pushing rod 2 is preferably a hydraulic cylinder or an air cylinder. The lower end of the pushing rod 2 is inserted into the soaking container 8 and is connected with a stainless steel pressing plate 5.
The bottom of the soaking container 8 is provided with a stainless steel mesh plate 7 and a stainless steel oil outlet 15; the stainless steel valve 9, the oil storage tank 10, the oil pump 11 and the oil feeding pipeline 16 are sequentially connected to the outside of the oil outlet 15, and the oil feeding pipeline 16 is connected with the upper part of the soaking container 8.
The container cover 6 is internally hung with a stainless steel rope 13, the lower end of the stainless steel rope 13 is connected with a support body 1 (the support body 1 is a disc, a cross rib frame or a supporting plate, and can be used for loosening and compacting lithospermum), the stainless steel rope 13 and the support body 1 are connected in series and can be conveniently detached, and one is connected at a time by pressing (only two are drawn in fig. 1).
The edge of the support body 1 is provided with a plurality of auxiliary stainless steel ropes 17 (such as three auxiliary stainless steel ropes) connected with the stainless steel ropes 13, and the length of each auxiliary stainless steel rope 17 is good close to the thickness of the lithospermum press cake, so that the lithospermum press cake is more beneficial to loosening when lifting, and the lifting resistance is reduced.
The center of the mesh plate 7 is provided with a groove 14 for accommodating a plurality of brackets 1 and stainless steel ropes 13, and the periphery of the groove 14 is provided with oil-passing meshes.
Referring to fig. 1, the sequence of operations: adding radix Arnebiae into soaking container 8, closing valve 9, adding fried radix et rhizoma Rhei oil into oil reservoir 10, and soaking radix Arnebiae. The pipeline oil pump 11 is started, sesame oil is injected into the soaking container 8, and soaking is carried out for two half hours. The electric hoist 4 of the lifting device is started to move downwards to be tightly attached to the upper flange 12 and the lower flange 12, and the bolts 18 are screwed down to fasten the container cover 6. The valve 9 is opened, the pushing rod 2 (hydraulic cylinder, air cylinder or electric) is opened, the pushing rod is operated downwards, the pressing plate 5 is pushed downwards to squeeze sesame oil contained in lithospermum, the sesame oil flows into the oil storage tank 10 through the mesh plate 7, the later the squeezing period is, the purple of the squeezed sesame oil is deeper, and the sesame oil is squeezed until no oil is discharged for half an hour. The bolt 18 is turned on, the pushing rod 2 is opened to move upwards, the electric hoist 4 is opened to move upwards, the stainless steel rope 13 (stainless steel wire rope) is pulled, the first stainless steel support body 1 in the groove 14 is lifted upwards by 1200mm, the stainless steel rope 17 and the first support body 1 are assisted to loosen surrounding lithosperms, the first support body 1 exposes the lithosperms, and the lithosperms pressed into cakes are loosened. The lithospermum in the side wall of the soaking container 8 is manually pried by a stainless steel crow bar until the lithospermum is completely loosened, so that a space is reserved for sucking new sesame oil. The hook of the stainless steel rope 13 of the first support 1 is taken off from the rope hook hanging ring 19, the first support 1 is taken away, the hook of the second support 1 (only two supports 1 are drawn in fig. 1 below) is hung on the rope hook hanging ring 19, then the valve 9 is closed, the pipeline oil pump 11 is started, and the extruded sesame oil is injected into the soaking container 8 again for soaking for two half hours. The device is used for carrying out extrusion, loosening and soaking for 12 times and 72 hours (12 support bodies 1 are hung), the purple pigment in the lithospermum is fully soaked, the characteristic of the sesame oil is mauve, the device changes the normal-temperature static soaking into the normal-temperature dynamic extrusion soaking, the purple pigment in the lithospermum is extracted by osmotic pressure soaking, and the characteristic of the sesame oil is mauve.
The above description is only of specific embodiments of the present invention, and the various illustrations do not limit the essential content of the present invention.
Claims (4)
1. The special equipment for the preparation method of the rehabilitation suppository is characterized by comprising the following components: a soaking container (8), the soaking container (8) is provided with a container cover (6), the container cover (6) is provided with a pushing rod (2), and the lower end of the pushing rod (2) is inserted into the soaking container (8) and is connected with a pressing plate (5); the bottom of the soaking container (8) is provided with a mesh plate (7) and an oil outlet (15); the valve (9), the oil storage tank (10), the oil pump (11) and the oil feeding pipeline (16) are sequentially connected outside the oil outlet (15), and the oil feeding pipeline (16) is connected with the upper part of the soaking container (8); a stainless steel rope (13) is hung in the container cover (6), the lower end of the stainless steel rope (13) is connected with the support body (1), and the stainless steel rope (13) and the support body (1) are connected in series and can be conveniently detached.
2. The special equipment for the preparation method of the rehabilitation suppository according to claim 1, which is characterized in that the support body (1) is a disc, a cross rib frame or a supporting plate.
3. The special equipment for the rehabilitation suppository preparation method according to claim 2, which is characterized in that a plurality of auxiliary stainless steel ropes (17) connected with the stainless steel ropes (13) are arranged at the edge of the support body (1).
4. A special device for a rehabilitation suppository preparation method according to claim 1, 2 or 3, which is characterized in that a groove (14) for accommodating a plurality of brackets (1) and stainless steel ropes (13) is arranged at the center of the mesh plate (7), and oil-passing meshes are arranged around the groove (14).
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2019108495823 | 2019-09-09 | ||
| CN201910849582 | 2019-09-09 |
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| CN110742928A CN110742928A (en) | 2020-02-04 |
| CN110742928B true CN110742928B (en) | 2023-05-26 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201179360Y (en) * | 2007-10-29 | 2009-01-14 | 东莞广州中医药大学中医药数理工程研究院 | Double-dynamic state high-efficiency energy conservation extracting apparatus |
| CN101455729A (en) * | 2009-01-14 | 2009-06-17 | 通化百信药业有限公司 | Kangfulingshuan medicine production technique |
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| CN208641307U (en) * | 2018-03-26 | 2019-03-26 | 天津华延园机械有限公司 | A kind of boiling machine with electric extruder |
| CN109998919A (en) * | 2019-04-23 | 2019-07-12 | 上海华禾生物科技有限公司 | A kind of food materials and Chinese medicine decoction decocting extraction element and extraction process |
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2019
- 2019-11-30 CN CN201911208263.0A patent/CN110742928B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201179360Y (en) * | 2007-10-29 | 2009-01-14 | 东莞广州中医药大学中医药数理工程研究院 | Double-dynamic state high-efficiency energy conservation extracting apparatus |
| CN101455729A (en) * | 2009-01-14 | 2009-06-17 | 通化百信药业有限公司 | Kangfulingshuan medicine production technique |
| CN201441838U (en) * | 2009-03-30 | 2010-04-28 | 滁州润海甜叶菊高科有限公司 | Traditional Chinese medicine dynamic immersion-extraction pot |
| CN208641307U (en) * | 2018-03-26 | 2019-03-26 | 天津华延园机械有限公司 | A kind of boiling machine with electric extruder |
| CN109998919A (en) * | 2019-04-23 | 2019-07-12 | 上海华禾生物科技有限公司 | A kind of food materials and Chinese medicine decoction decocting extraction element and extraction process |
Non-Patent Citations (1)
| Title |
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| 王爱萍 等.紫草素的提取工艺及制剂研究概况.中国医药指南.2013,第11卷(第04期),90-93. * |
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