CN110724600A - Perfume essence and preparation method thereof - Google Patents
Perfume essence and preparation method thereof Download PDFInfo
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- CN110724600A CN110724600A CN201911019958.4A CN201911019958A CN110724600A CN 110724600 A CN110724600 A CN 110724600A CN 201911019958 A CN201911019958 A CN 201911019958A CN 110724600 A CN110724600 A CN 110724600A
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- molecular distillation
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- sandalwood
- perfume essence
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- 239000002304 perfume Substances 0.000 title claims abstract description 51
- 238000002360 preparation method Methods 0.000 title claims description 18
- KVWWIYGFBYDJQC-UHFFFAOYSA-N methyl dihydrojasmonate Chemical compound CCCCCC1C(CC(=O)OC)CCC1=O KVWWIYGFBYDJQC-UHFFFAOYSA-N 0.000 claims abstract description 46
- 241000221035 Santalaceae Species 0.000 claims abstract description 38
- 235000008632 Santalum album Nutrition 0.000 claims abstract description 38
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 claims abstract description 36
- 241000282375 Herpestidae Species 0.000 claims abstract description 36
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 claims abstract description 34
- QMVPMAAFGQKVCJ-UHFFFAOYSA-N citronellol Chemical compound OCCC(C)CCC=C(C)C QMVPMAAFGQKVCJ-UHFFFAOYSA-N 0.000 claims abstract description 34
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims abstract description 34
- YPZUZOLGGMJZJO-UHFFFAOYSA-N ambrofix Natural products C1CC2C(C)(C)CCCC2(C)C2C1(C)OCC2 YPZUZOLGGMJZJO-UHFFFAOYSA-N 0.000 claims abstract description 28
- YPZUZOLGGMJZJO-LQKXBSAESA-N ambroxan Chemical compound CC([C@@H]1CC2)(C)CCC[C@]1(C)[C@@H]1[C@]2(C)OCC1 YPZUZOLGGMJZJO-LQKXBSAESA-N 0.000 claims abstract description 28
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 claims abstract description 28
- -1 methyl hexyl Chemical group 0.000 claims abstract description 27
- 239000002994 raw material Substances 0.000 claims abstract description 27
- GUUHFMWKWLOQMM-UHFFFAOYSA-N alpha-n-hexylcinnamic aldehyde Natural products CCCCCCC(C=O)=CC1=CC=CC=C1 GUUHFMWKWLOQMM-UHFFFAOYSA-N 0.000 claims abstract description 20
- XRHCAGNSDHCHFJ-UHFFFAOYSA-N Ethylene brassylate Chemical compound O=C1CCCCCCCCCCCC(=O)OCCO1 XRHCAGNSDHCHFJ-UHFFFAOYSA-N 0.000 claims abstract description 19
- 235000019501 Lemon oil Nutrition 0.000 claims abstract description 18
- 239000010501 lemon oil Substances 0.000 claims abstract description 18
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims abstract description 17
- QMVPMAAFGQKVCJ-SNVBAGLBSA-N (R)-(+)-citronellol Natural products OCC[C@H](C)CCC=C(C)C QMVPMAAFGQKVCJ-SNVBAGLBSA-N 0.000 claims abstract description 17
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims abstract description 17
- GLZPCOQZEFWAFX-JXMROGBWSA-N Nerol Natural products CC(C)=CCC\C(C)=C\CO GLZPCOQZEFWAFX-JXMROGBWSA-N 0.000 claims abstract description 17
- CDJJKTLOZJAGIZ-UHFFFAOYSA-N Tolylacetate Chemical compound CC(=O)OC1=CC=C(C)C=C1 CDJJKTLOZJAGIZ-UHFFFAOYSA-N 0.000 claims abstract description 17
- JGQFVRIQXUFPAH-UHFFFAOYSA-N beta-citronellol Natural products OCCC(C)CCCC(C)=C JGQFVRIQXUFPAH-UHFFFAOYSA-N 0.000 claims abstract description 17
- 235000000484 citronellol Nutrition 0.000 claims abstract description 17
- 229930007744 linalool Natural products 0.000 claims abstract description 17
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 claims abstract description 16
- CHLICZRVGGXEOD-UHFFFAOYSA-N 1-Methoxy-4-methylbenzene Chemical compound COC1=CC=C(C)C=C1 CHLICZRVGGXEOD-UHFFFAOYSA-N 0.000 claims abstract description 15
- UZFLPKAIBPNNCA-BQYQJAHWSA-N alpha-ionone Chemical compound CC(=O)\C=C\C1C(C)=CCCC1(C)C UZFLPKAIBPNNCA-BQYQJAHWSA-N 0.000 claims abstract description 15
- UZFLPKAIBPNNCA-UHFFFAOYSA-N alpha-ionone Natural products CC(=O)C=CC1C(C)=CCCC1(C)C UZFLPKAIBPNNCA-UHFFFAOYSA-N 0.000 claims abstract description 15
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims abstract description 14
- 239000003205 fragrance Substances 0.000 claims abstract description 12
- YGSDEFSMJLZEOE-UHFFFAOYSA-M salicylate Chemical compound OC1=CC=CC=C1C([O-])=O YGSDEFSMJLZEOE-UHFFFAOYSA-M 0.000 claims abstract description 12
- 229960001860 salicylate Drugs 0.000 claims abstract description 12
- 238000000199 molecular distillation Methods 0.000 claims description 72
- 238000002156 mixing Methods 0.000 claims description 30
- 238000003756 stirring Methods 0.000 claims description 20
- OVBPIULPVIDEAO-LBPRGKRZSA-N Folic acid Natural products C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)N[C@@H](CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-LBPRGKRZSA-N 0.000 claims description 17
- OVBPIULPVIDEAO-UHFFFAOYSA-N N-Pteroyl-L-glutaminsaeure Natural products C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)NC(CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-UHFFFAOYSA-N 0.000 claims description 10
- 238000001914 filtration Methods 0.000 claims description 10
- 229960000304 folic acid Drugs 0.000 claims description 10
- 235000019152 folic acid Nutrition 0.000 claims description 10
- 239000011724 folic acid Substances 0.000 claims description 10
- 244000153234 Hibiscus abelmoschus Species 0.000 claims description 8
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 6
- 241000903946 Clematidis Species 0.000 claims description 5
- 229940117916 cinnamic aldehyde Drugs 0.000 claims description 2
- KJPRLNWUNMBNBZ-UHFFFAOYSA-N cinnamic aldehyde Natural products O=CC=CC1=CC=CC=C1 KJPRLNWUNMBNBZ-UHFFFAOYSA-N 0.000 claims description 2
- 238000000034 method Methods 0.000 claims description 2
- GVQUJSXHKIUDCK-UHFFFAOYSA-N pentadecan-4-ol Chemical compound CCCCCCCCCCCC(O)CCC GVQUJSXHKIUDCK-UHFFFAOYSA-N 0.000 claims description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 2
- 239000007864 aqueous solution Substances 0.000 claims 1
- 239000000243 solution Substances 0.000 claims 1
- AILDTIZEPVHXBF-UHFFFAOYSA-N Argentine Natural products C1C(C2)C3=CC=CC(=O)N3CC1CN2C(=O)N1CC(C=2N(C(=O)C=CC=2)C2)CC2C1 AILDTIZEPVHXBF-UHFFFAOYSA-N 0.000 abstract description 2
- 244000308495 Potentilla anserina Species 0.000 abstract description 2
- 235000016594 Potentilla anserina Nutrition 0.000 abstract description 2
- UFLHIIWVXFIJGU-ARJAWSKDSA-N (Z)-hex-3-en-1-ol Chemical compound CC\C=C/CCO UFLHIIWVXFIJGU-ARJAWSKDSA-N 0.000 abstract 1
- 239000000686 essence Substances 0.000 description 39
- 230000000052 comparative effect Effects 0.000 description 12
- 238000011156 evaluation Methods 0.000 description 5
- 230000001953 sensory effect Effects 0.000 description 5
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 3
- DTFKRVXLBCAIOZ-UHFFFAOYSA-N 2-methylanisole Chemical compound COC1=CC=CC=C1C DTFKRVXLBCAIOZ-UHFFFAOYSA-N 0.000 description 2
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 description 2
- 239000005792 Geraniol Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229940113087 geraniol Drugs 0.000 description 2
- 230000005923 long-lasting effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000402754 Erythranthe moschata Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000019445 benzyl alcohol Nutrition 0.000 description 1
- VEZXCJBBBCKRPI-UHFFFAOYSA-N beta-propiolactone Chemical compound O=C1CCO1 VEZXCJBBBCKRPI-UHFFFAOYSA-N 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 229960000380 propiolactone Drugs 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/003—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing less than six carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/0038—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing more than six carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0042—Essential oils; Perfumes compounds containing condensed hydrocarbon rings
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses perfume essence which comprises the following raw materials: ambrox, musk T, sandalwood 803, methyl hexyl cinnamaldehyde, methyl dihydrojasmonate, sandalwood 208, citronellol, phenethyl alcohol, linalool, benzyl alcohol, p-methyl anisole, p-cresol acetate, folic alcohol salicylate, alpha-ionone, propyl dodecalactone, civet extract, nerol, argentine lemon oil and dipropylene glycol. The perfume essence disclosed by the invention not only has the attraction of perfume, but also has good fragrance quality, excellent long-acting property and storage stability, and very good popularization and application values.
Description
Technical Field
The invention relates to the technical field of perfume, in particular to perfume essence and a preparation method thereof.
Background
The perfume is one of important cosmetics, has volatility, can be sensed by smell or taste of people, can emit pleasant fragrance when being sprayed on parts such as lappets, handkerchiefs, hairlines and the like, and achieves the purposes of being loved and spiritual pleasure. For a long time, how to prepare the perfume essence with good fragrance and long-acting property has important significance.
Disclosure of Invention
The invention aims to make up for the defects of the prior art and provides the perfume essence which has the advantages of good fragrance and long-lasting effect.
The invention is realized by the following technical scheme:
the perfume essence comprises the following raw materials in parts by weight:
0.10-0.30 part of ambrox, 5.00-10.00 parts of musk T, 8030.10-0.25 part of sandalwood, 2.00-5.00 parts of methyl-hexyl cinnamaldehyde, 1.00-2.00 parts of methyl dihydrojasmonate, 2081.00-2.00 parts of sandalwood, 0.20-0.60 part of citronellol, 2.40-4.80 parts of phenethyl alcohol, 1.40-3.60 parts of linalool, 0.10-0.20 part of benzyl alcohol, 0.30-0.50 part of p-methyl anisole, 0.01-0.05 part of p-cresol acetate, 0.15-0.35 part of folic acid leaf alcohol ester, 0.20-1.20 part of alpha-irisone, 0.01-0.05 part of propyl dodecanol, 5.00-10.00 parts of civet extract, 0.01-0.05 part of nerol, 1.00-2.20 parts of Argentina lemon oil and 30.00-49.00 parts of dipropylene glycol.
Preferably, the perfume essence comprises the following raw materials in parts by weight: 0.10 parts of ambrox, 5.00 parts of musk T, 8030.10 parts of sandalwood, 2.00 parts of methyl hexyl cinnamaldehyde, 1.00 parts of methyl dihydrojasmonate, 2081.00 parts of sandalwood, 0.20 part of citronellol, 2.40 parts of phenethyl alcohol, 1.40 parts of linalool, 0.10 part of benzyl alcohol, 0.30 part of p-methyl anisole, 0.01 part of p-cresol acetate, 0.15 part of folic acid salicylate, 0.20 part of alpha-ionone, 0.01 part of propyl dodecalactone, 5.00 parts of civet extract, 0.01 part of nerol, 1.00 part of Argentina lemon oil and 30.00 parts of dipropylene glycol.
Preferably, the perfume essence comprises the following raw materials in parts by weight: 0.20 of ambrox, 8.00 of musk T, 8030.15 of sandalwood, 3.00 of methyl hexyl cinnamaldehyde, 1.50 of methyl dihydrojasmonate, 2081.50 of sandalwood, 0.40 of citronellol, 3.50 of phenethyl alcohol, 1.80 of linalool, 0.15 of benzyl alcohol, 0.40 of p-methyl anisole, 0.02 of p-cresol acetate, 0.25 of folic salicylate, 0.60 of alpha-ionone, 0.04 of propyl dodecalactone, 8.00 of civet extract, 0.04 of nerol, 1.6 of Argentina lemon oil and 40.00 of dipropylene glycol.
Preferably, the perfume essence comprises the following raw materials in parts by weight: 0.30 parts of ambrox, 10.00 parts of musk T, 8030.25 parts of sandalwood, 5.00 parts of methyl hexyl cinnamaldehyde, 2.00 parts of methyl dihydrojasmonate, 2082.00 parts of sandalwood, 0.60 part of citronellol, 4.80 parts of phenethyl alcohol, 3.60 parts of linalool, 0.20 part of benzyl alcohol, 0.50 part of p-methyl anisole, 0.05 part of p-cresol acetate, 0.35 part of folic acid salicylate, 1.20 parts of alpha-ionone, 0.05 part of propyl dodecalactone, 10.00 parts of civet extract, 0.05 part of nerol, 2.20 parts of Argentina lemon oil and 49.00 parts of dipropylene glycol.
Preferably, the preparation method of the civet extract comprises the following steps:
(1) mixing civet and ethanol water solution according to the weight ratio of 1: (4-5) uniformly mixing, then performing primary molecular distillation, secondary molecular distillation and tertiary molecular distillation at 50 ℃, 60 ℃ and 80 ℃ respectively, and collecting to obtain a primary molecular distillation distillate, a secondary molecular distillation distillate and a tertiary molecular distillation distillate;
(2) mixing the first-stage molecular distillation distillate, the second-stage molecular distillation distillate and the third-stage molecular distillation distillate according to the weight ratio of 1: (2-4): (5-7) mixing uniformly to obtain the civet extract.
Preferably, in the step (1), the first-stage molecular distillation, the second-stage molecular distillation and the third-stage molecular distillation are carried out in a wiped film type molecular distillation device, wherein the feeding speed is 4-5ml/min, the operating pressure is 5-10Pa, and the wiped film speed is 80-120 r/min.
Preferably, the volume concentration of the ethanol water solution is 80-90%.
A preparation method of perfume essence comprises the following steps:
(1) mixing ambrox, Moschus T, lignum Santali albi 803, radix Clematidis Finetianae extract and dipropylene glycol, dissolving, and stirring;
(2) adding the rest raw materials, stirring, homogenizing under high pressure, standing, and filtering to obtain perfume essence.
The invention has the beneficial effects that:
the ambrox, the musk T, the sandalwood 803, the methyl dihydrojasmonate and the dipropylene glycol are compounded to play a role in fixing fragrance, reduce the loss of effective fragrance components, prolong the long-acting property of the fragrance and improve the storage stability of the essence; the ambrox, the musk T, the sandalwood 803, the sandalwood 208 and the argentine lemon oil are compounded, so that the fragrance of the civet extract can be gained, and the excellent fragrance quality of the perfume essence can be improved. In the preparation process of the civet extract, the molecular distillation method is adopted, the civet extract is obtained by respectively carrying out primary molecular distillation, secondary molecular distillation and tertiary molecular distillation at 50 ℃, 60 ℃ and 80 ℃, and compounding the collected primary molecular distillation distillate, the secondary molecular distillation distillate and the tertiary molecular distillation distillate according to a certain proportion, so that the proportion of high-boiling-point and low-boiling-point aroma substances in the civet extract and the proportion of the aroma substances which have synergistic and gain effects with other components in the essence can be adjusted, the optimal proportion is obtained, the civet extract can be matched with components with a fixed aroma effect in the essence, the long-lasting property of the essence is further improved, and the excellent aroma quality of the perfume essence is better improved. The perfume essence disclosed by the invention not only has the attraction of perfume, but also has good fragrance quality, excellent long-acting property and storage stability, and very good popularization and application values.
Detailed Description
Example 1
The perfume essence comprises the following raw materials in parts by weight: 0.10 parts of ambrox, 5.00 parts of musk T, 8030.10 parts of sandalwood, 2.00 parts of methyl hexyl cinnamaldehyde, 1.00 parts of methyl dihydrojasmonate, 2081.00 parts of sandalwood, 0.20 part of citronellol, 2.40 parts of phenethyl alcohol, 1.40 parts of linalool, 0.10 part of benzyl alcohol, 0.30 part of p-methyl anisole, 0.01 part of p-cresol acetate, 0.15 part of folic acid salicylate, 0.20 part of alpha-ionone, 0.01 part of propyl dodecalactone, 5.00 parts of civet extract, 0.01 part of nerol, 1.00 part of Argentina lemon oil and 30.00 parts of dipropylene glycol.
The preparation method of the civet extract comprises the following steps:
(1) mixing civet and 80% ethanol water solution according to the weight ratio of 1: 4, uniformly mixing, and then respectively carrying out primary molecular distillation, secondary molecular distillation and tertiary molecular distillation at 50 ℃, 60 ℃ and 80 ℃, wherein the primary molecular distillation, the secondary molecular distillation and the tertiary molecular distillation are carried out in a wiped film type molecular distillation device, the feeding speed is 4ml/min, the operating pressure is 5Pa, the wiped film speed is 80r/min, and the primary molecular distillation distillate, the secondary molecular distillation distillate and the tertiary molecular distillation distillate are obtained by collection;
(2) mixing the first-stage molecular distillation distillate, the second-stage molecular distillation distillate and the third-stage molecular distillation distillate according to the weight ratio of 1: 2: 5, mixing uniformly to obtain the civet extract.
A preparation method of perfume essence comprises the following steps:
(1) mixing ambrox, Moschus T, lignum Santali albi 803, radix Clematidis Finetianae extract and dipropylene glycol, dissolving, and stirring;
(2) adding the rest raw materials, stirring, homogenizing under high pressure, standing, and filtering to obtain perfume essence.
Example 2
The perfume essence comprises the following raw materials in parts by weight: 0.20 of ambrox, 8.00 of musk T, 8030.15 of sandalwood, 3.00 of methyl hexyl cinnamaldehyde, 1.50 of methyl dihydrojasmonate, 2081.50 of sandalwood, 0.40 of citronellol, 3.50 of phenethyl alcohol, 1.80 of linalool, 0.15 of benzyl alcohol, 0.40 of p-methyl anisole, 0.02 of p-cresol acetate, 0.25 of folic salicylate, 0.60 of alpha-ionone, 0.04 of propyl dodecalactone, 8.00 of civet extract, 0.04 of nerol, 1.6 of Argentina lemon oil and 40.00 of dipropylene glycol.
The preparation method of the civet extract comprises the following steps:
(1) mixing civet and 85% ethanol water solution according to the weight ratio of 1: 4.5, uniformly mixing, and then respectively carrying out primary molecular distillation, secondary molecular distillation and tertiary molecular distillation at 50 ℃, 60 ℃ and 80 ℃, wherein the primary molecular distillation, the secondary molecular distillation and the tertiary molecular distillation are carried out in a wiped film type molecular distillation device, the feeding speed is 4.5ml/min, the operating pressure is 8Pa, the film-wiping speed is 100r/min, and collecting to obtain primary molecular distillation distillate, secondary molecular distillation distillate and tertiary molecular distillation distillate;
(2) mixing the first-stage molecular distillation distillate, the second-stage molecular distillation distillate and the third-stage molecular distillation distillate according to the weight ratio of 1: 3: 6 mixing uniformly to obtain the civet extract.
A preparation method of perfume essence comprises the following steps:
(1) mixing ambrox, Moschus T, lignum Santali albi 803, radix Clematidis Finetianae extract and dipropylene glycol, dissolving, and stirring;
(2) adding the rest raw materials, stirring, homogenizing under high pressure, standing, and filtering to obtain perfume essence.
Example 3
The perfume essence comprises the following raw materials in parts by weight: 0.30 parts of ambrox, 10.00 parts of musk T, 8030.25 parts of sandalwood, 5.00 parts of methyl hexyl cinnamaldehyde, 2.00 parts of methyl dihydrojasmonate, 2082.00 parts of sandalwood, 0.60 part of citronellol, 4.80 parts of phenethyl alcohol, 3.60 parts of linalool, 0.20 part of benzyl alcohol, 0.50 part of p-methyl anisole, 0.05 part of p-cresol acetate, 0.35 part of folic acid salicylate, 1.20 parts of alpha-ionone, 0.05 part of propyl dodecalactone, 10.00 parts of civet extract, 0.05 part of nerol, 2.20 parts of Argentina lemon oil and 49.00 parts of dipropylene glycol.
The preparation method of the civet extract comprises the following steps:
(1) mixing civet and 90% ethanol water solution according to the weight ratio of 1: 5, uniformly mixing, and then respectively carrying out primary molecular distillation, secondary molecular distillation and tertiary molecular distillation at 50 ℃, 60 ℃ and 80 ℃, wherein the primary molecular distillation, the secondary molecular distillation and the tertiary molecular distillation are carried out in a wiped film type molecular distillation device, the feeding speed is 5ml/min, the operating pressure is 10Pa, the film-wiping speed is 120r/min, and collecting to obtain primary molecular distillation distillate, secondary molecular distillation distillate and tertiary molecular distillation distillate;
(2) mixing the first-stage molecular distillation distillate, the second-stage molecular distillation distillate and the third-stage molecular distillation distillate according to the weight ratio of 1: 4: 7, mixing uniformly to obtain the civet extract.
A preparation method of perfume essence comprises the following steps:
(1) mixing ambrox, Moschus T, lignum Santali albi 803, radix Clematidis Finetianae extract and dipropylene glycol, dissolving, and stirring;
(2) adding the rest raw materials, stirring, homogenizing under high pressure, standing, and filtering to obtain perfume essence.
Comparative example 1
Comparative example 1 differs from example 2 only in that: contains no ambrox and civet extract, and comprises the following specific steps:
the perfume essence comprises the following raw materials in parts by weight: musk T8.00, sandalwood 8030.15, methyl hexyl cinnamaldehyde 3.00, methyl dihydrojasmonate 1.50, sandalwood 2081.50, citronellol 0.40, phenethyl alcohol 3.50, linalool 1.80, benzyl alcohol 0.15, p-methyl anisole 0.40, p-cresol acetate 0.02, folic acid ester 0.25, alpha-ionone 0.60, propyl dodecalactone 0.04, nerol 0.04, Argentina lemon oil 1.6 and dipropylene glycol 40.00.
A preparation method of perfume essence comprises the following steps:
(1) mixing Moschus T, lignum Santali albi 803, methyl hexyl cinnamic aldehyde, methyl dihydrojasmonate, and dipropylene glycol, dissolving, and stirring;
(2) adding the rest raw materials, stirring, homogenizing under high pressure, standing, and filtering.
Comparative example 2
Comparative example 2 differs from example 2 only in that: contains no musk T and civet extract, and comprises the following specific parts:
the perfume essence comprises the following raw materials in parts by weight: 0.20 of ambrox, 8030.15 of sandalwood, 3.00 of methyl hexyl cinnamaldehyde, 1.50 of methyl dihydrojasmonate, 2081.50 of sandalwood, 0.40 of citronellol, 3.50 of phenethyl alcohol, 1.80 of linalool, 0.15 of benzyl alcohol, 0.40 of methyl anisole, 0.02 of p-cresol acetate, 0.25 of folic salicylate, 0.60 of alpha-ionone, 0.04 of propyl dodecalactone, 0.04 of nerol, 1.6 of Argentina lemon oil and 40.00 of dipropylene glycol.
A preparation method of perfume essence comprises the following steps:
(1) mixing ambrox, sandalwood 803, methyl hexyl cinnamic aldehyde, methyl dihydrojasmonate and dipropylene glycol, dissolving and stirring uniformly;
(2) adding the rest raw materials, stirring, homogenizing under high pressure, standing, and filtering.
Comparative example 3
Comparative example 3 differs from example 2 only in that: the extract does not contain sandalwood 803 and civet, and is as follows:
the perfume essence comprises the following raw materials in parts by weight: 0.20 of ambrox, 8.00 of musk T, 3.00 of methyl hexyl cinnamaldehyde, 1.50 of methyl dihydrojasmonate, 2081.50 of sandalwood, 0.40 of citronellol, 3.50 of phenethyl alcohol, 1.80 of linalool, 0.15 of benzyl alcohol, 0.40 of methyl anisole, 0.02 of p-cresol acetate, 0.25 of geraniol ester, 0.60 of alpha-ionone, 0.04 of propyl dodecalactone, 0.04 of nerol, 1.6 of Argentina lemon oil and 40.00 of dipropylene glycol.
A preparation method of perfume essence comprises the following steps:
(1) mixing ambrox, musk T, methyl hexyl cinnamic aldehyde, methyl dihydrojasmonate and dipropylene glycol, dissolving, and stirring;
(2) adding the rest raw materials, stirring, homogenizing under high pressure, standing, and filtering.
Comparative example 4
Comparative example 4 differs from example 2 only in that: does not contain sandalwood 208 and civet extract, and comprises the following specific steps:
the perfume essence comprises the following raw materials in parts by weight: 0.20 of ambrox, 8.00 of musk T, 8030.15 of sandalwood, 3.00 of methyl hexyl cinnamaldehyde, 1.50 of methyl dihydrojasmonate, 0.40 of citronellol, 3.50 of phenethyl alcohol, 1.80 of linalool, 0.15 of benzyl alcohol, 0.40 of p-methyl anisole, 0.02 of p-cresol acetate, 0.25 of geraniol ester, 0.60 of alpha-ionone, 0.04 of propiolactone, 0.04 of nerol, 1.6 of Argentina lemon oil and 40.00 of dipropylene glycol.
A preparation method of perfume essence comprises the following steps:
(1) mixing ambrox, Moschus T, lignum Santali albi 803, methyl hexyl cinnamic aldehyde, methyl dihydrojasmonate and dipropylene glycol, dissolving, and stirring;
(2) adding the rest raw materials, stirring, homogenizing under high pressure, standing, and filtering.
Comparative example 5
Comparative example 5 differs from example 2 only in that: contains no Argentina lemon oil and Zibethum extract, and comprises the following specific parts:
the perfume essence comprises the following raw materials in parts by weight: 0.20 of ambrox, 8.00 of musk T, 8030.15 of sandalwood, 3.00 of methyl hexyl cinnamaldehyde, 1.50 of methyl dihydrojasmonate, 2081.50 of sandalwood, 0.40 of citronellol, 3.50 of phenethyl alcohol, 1.80 of linalool, 0.15 of benzyl alcohol, 0.40 of p-methyl anisole, 0.02 of p-cresol acetate, 0.25 of folic acid salicylate, 0.60 of alpha-ionone, 0.04 of propyl dodecalactone, 0.04 of nerol and 40.00 of dipropylene glycol.
A preparation method of perfume essence comprises the following steps:
(1) mixing ambrox, Moschus T, lignum Santali albi 803, methyl hexyl cinnamic aldehyde, methyl dihydrojasmonate and dipropylene glycol, dissolving, and stirring;
(2) adding the rest raw materials, stirring, homogenizing under high pressure, standing, and filtering.
50 testers were arranged to perform sensory evaluation on the perfume essences prepared in examples 1 to 3 and comparative examples 1 to 5, respectively, wherein the full score was 10 points, and the result was recorded as sensory evaluation (before storage); after the perfume essences prepared in examples 1 to 3 and comparative examples 1 to 5 were stored at room temperature in the dark for 100 days, sensory evaluation was performed again, and the results were recorded as sensory evaluation (after storage), and the results of the sensory evaluation for two times are shown in the following table:
as can be seen from the table, the perfume essence of the present invention has high quality fragrance and excellent storage stability.
Claims (8)
1. The perfume essence is characterized by comprising the following raw materials in parts by weight:
0.10-0.30 part of ambrox, 5.00-10.00 parts of musk T, 8030.10-0.25 part of sandalwood, 2.00-5.00 parts of methyl-hexyl cinnamaldehyde, 1.00-2.00 parts of methyl dihydrojasmonate, 2081.00-2.00 parts of sandalwood, 0.20-0.60 part of citronellol, 2.40-4.80 parts of phenethyl alcohol, 1.40-3.60 parts of linalool, 0.10-0.20 part of benzyl alcohol, 0.30-0.50 part of p-methyl anisole, 0.01-0.05 part of p-cresol acetate, 0.15-0.35 part of folic acid leaf alcohol ester, 0.20-1.20 part of alpha-irisone, 0.01-0.05 part of propyl dodecanol, 5.00-10.00 parts of civet extract, 0.01-0.05 part of nerol, 1.00-2.20 parts of Argentina lemon oil and 30.00-49.00 parts of dipropylene glycol.
2. The perfume essence according to claim 1, wherein the raw materials comprise the following components in parts by weight: 0.10 parts of ambrox, 5.00 parts of musk T, 8030.10 parts of sandalwood, 2.00 parts of methyl hexyl cinnamaldehyde, 1.00 parts of methyl dihydrojasmonate, 2081.00 parts of sandalwood, 0.20 part of citronellol, 2.40 parts of phenethyl alcohol, 1.40 parts of linalool, 0.10 part of benzyl alcohol, 0.30 part of p-methyl anisole, 0.01 part of p-cresol acetate, 0.15 part of folic acid salicylate, 0.20 part of alpha-ionone, 0.01 part of propyl dodecalactone, 5.00 parts of civet extract, 0.01 part of nerol, 1.00 part of Argentina lemon oil and 30.00 parts of dipropylene glycol.
3. The perfume essence according to claim 1, wherein the raw materials comprise the following components in parts by weight: 0.20 of ambrox, 8.00 of musk T, 8030.15 of sandalwood, 3.00 of methyl hexyl cinnamaldehyde, 1.50 of methyl dihydrojasmonate, 2081.50 of sandalwood, 0.40 of citronellol, 3.50 of phenethyl alcohol, 1.80 of linalool, 0.15 of benzyl alcohol, 0.40 of p-methyl anisole, 0.02 of p-cresol acetate, 0.25 of folic salicylate, 0.60 of alpha-ionone, 0.04 of propyl dodecalactone, 8.00 of civet extract, 0.04 of nerol, 1.6 of Argentina lemon oil and 40.00 of dipropylene glycol.
4. The perfume essence according to claim 1, wherein the raw materials comprise the following components in parts by weight: 0.30 parts of ambrox, 10.00 parts of musk T, 8030.25 parts of sandalwood, 5.00 parts of methyl hexyl cinnamaldehyde, 2.00 parts of methyl dihydrojasmonate, 2082.00 parts of sandalwood, 0.60 part of citronellol, 4.80 parts of phenethyl alcohol, 3.60 parts of linalool, 0.20 part of benzyl alcohol, 0.50 part of p-methyl anisole, 0.05 part of p-cresol acetate, 0.35 part of folic acid salicylate, 1.20 parts of alpha-ionone, 0.05 part of propyl dodecalactone, 10.00 parts of civet extract, 0.05 part of nerol, 2.20 parts of Argentina lemon oil and 49.00 parts of dipropylene glycol.
5. The perfume essence of claim 1, wherein the civet extract is prepared by the following steps:
(1) mixing civet and ethanol water solution according to the weight ratio of 1: (4-5) uniformly mixing, then performing primary molecular distillation, secondary molecular distillation and tertiary molecular distillation at 50 ℃, 60 ℃ and 80 ℃ respectively, and collecting to obtain a primary molecular distillation distillate, a secondary molecular distillation distillate and a tertiary molecular distillation distillate;
(2) mixing the first-stage molecular distillation distillate, the second-stage molecular distillation distillate and the third-stage molecular distillation distillate according to the weight ratio of 1: (2-4): (5-7) mixing uniformly to obtain the civet extract.
6. The perfume essence according to claim 5, wherein in the step (1), the first molecular distillation, the second molecular distillation and the third molecular distillation are carried out in a wiped film type molecular distillation device, wherein the feeding speed is 4-5ml/min, the operating pressure is 5-10Pa, and the wiped film speed is 80-120 r/min.
7. The perfume essence according to claim 5, wherein the volume concentration of the ethanol aqueous solution is 80-90%.
8. A process for the preparation of a perfume fragrance according to any of claims 1 to 7, comprising the steps of:
(1) mixing ambrox, Moschus T, lignum Santali albi 803, radix Clematidis Finetianae extract and dipropylene glycol, dissolving, and stirring;
(2) adding the rest raw materials, stirring, homogenizing under high pressure, standing, and filtering to obtain perfume essence.
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| CN112210438A (en) * | 2020-10-19 | 2021-01-12 | 广东芬豪生物科技有限公司 | Daily chemical essence with flower fragrance and preparation method thereof |
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