CN110715901A - Tilt fiber grating comb leaky mode resonance excitation method, polarization filter and sensing system - Google Patents

Tilt fiber grating comb leaky mode resonance excitation method, polarization filter and sensing system Download PDF

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CN110715901A
CN110715901A CN201910952848.7A CN201910952848A CN110715901A CN 110715901 A CN110715901 A CN 110715901A CN 201910952848 A CN201910952848 A CN 201910952848A CN 110715901 A CN110715901 A CN 110715901A
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李志红
李丽
胡贵军
朱加银
阮秀凯
戴瑜兴
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Abstract

本发明公开了一种倾斜光纤光栅梳状泄漏模谐振激发方法、偏振滤波器及传感系统,所述方法包括金属氧化物涂覆倾斜光纤光栅,所述金属氧化物包括纳米量级厚度的氧化铟锡、二氧化锡、三氧化二铟、氧化锌或二氧化钛材料,所述偏振滤波器包括宽带光源、偏振控制器、单模光纤跳线、金属氧化物涂覆光纤光栅、光谱分析仪,所述传感系统包括所述偏振滤波器、样品反应皿和计算机,利用整个光谱包络区域或单个泄漏模谐振峰的变化实现待测样品的传感检测。本发明金属氧化物激发倾斜光纤光栅梳状泄漏模谐振可广泛应用于可调窄带偏振滤波及高灵敏高精度光纤传感领域。

Figure 201910952848

The invention discloses a method for resonant excitation of a comb-like leaky mode of a tilted fiber grating, a polarization filter and a sensing system. The method includes a metal oxide coating the tilted fiber grating, and the metal oxide includes an oxide with a thickness of nanometers. Indium tin, tin dioxide, indium trioxide, zinc oxide or titanium dioxide materials, the polarization filter includes a broadband light source, a polarization controller, a single-mode fiber jumper, a metal oxide coated fiber grating, and a spectrum analyzer, all of which The sensing system includes the polarization filter, the sample reaction vessel and a computer, and utilizes the change of the entire spectral envelope region or the resonance peak of a single leaky mode to realize the sensing and detection of the sample to be tested. The metal oxide excited slanted fiber grating comb leaky mode resonance can be widely used in the fields of adjustable narrow-band polarization filtering and high-sensitivity and high-precision optical fiber sensing.

Figure 201910952848

Description

倾斜光纤光栅梳状泄漏模谐振激发方法、偏振滤波器及传感 系统Tilt fiber grating comb leaky mode resonance excitation method, polarization filter and sensor system

技术领域technical field

本发明属于光纤通信及传感技术领域,具体是指倾斜光纤光栅梳状泄漏模谐振激发方法、偏振滤波器及传感系统。The invention belongs to the technical field of optical fiber communication and sensing, and in particular relates to a method for exciting comb-like leaky mode resonance of a tilted fiber grating, a polarization filter and a sensing system.

背景技术Background technique

光纤因其优异特性如尺寸小、重量轻、高灵敏、不受电磁干扰、远距离传输等而在传感及通信领域受到广泛关注,特别在生化医学、环境监测、污染物检测、光通信等领域具有广阔的应用前景。近年来,光纤传感技术与材料科学、信息处理技术等领域的结合进一步推动了多类型、多功能、多模态、高性能的光纤传感器及可调滤波器的发展。其中,通过在光纤表面集成纳米量级薄膜进而调控光纤电磁场谐振是广泛应用的光纤传感及滤波方法。根据不同纳米材料的特性,目前最广泛报道的电磁场谐振包括表面等离子体共振(surfaceplasmon resonance)和损耗模谐振(lossy mode resonance)。Optical fibers have received extensive attention in the field of sensing and communication due to their excellent characteristics such as small size, light weight, high sensitivity, immunity to electromagnetic interference, long-distance transmission, etc., especially in biochemical medicine, environmental monitoring, pollutant detection, optical communication, etc. The field has broad application prospects. In recent years, the combination of optical fiber sensing technology with materials science, information processing technology and other fields has further promoted the development of multi-type, multi-functional, multi-modal and high-performance optical fiber sensors and tunable filters. Among them, integrating nano-scale thin films on the surface of optical fibers to control the electromagnetic field resonance of optical fibers is a widely used optical fiber sensing and filtering method. According to the properties of different nanomaterials, the most widely reported electromagnetic field resonances include surface plasmon resonance and lossy mode resonance.

表面等离子体以表面等离子体波的形式存在于金属层表面,是由于带电粒子受到外界干扰引起的金属表面正负电荷局部集中现象。在外界电磁场的作用下,电介质和金属层接触区域的等离子体内部自由电子会发生位移,从而破坏了该区域的电中性,进而形成表面电场。在表面电场的作用下,发生位移的自由电子在其平衡位置来回振荡,从而形成振荡波,振荡波沿金属表面向前传输,同时其振幅以指数形式衰减。这种在外界电磁场的作用下,等离子体内部的正负带电粒子发生密度起伏的振荡,称为表面等离子体共振。光纤以其优异特性为设计表面等离子共振传感器提供了非常好的物理媒介:通过在光纤表面涂覆金属薄膜,可以高效地激发表面等离子体共振。目前广泛报道的光纤表面等离子体共振传感器结构主要包括D型光纤、包层腐蚀、光子晶体、光纤光栅等类型。相比于其他结构,倾斜光纤光栅表面等离子体共振传感器具有许多优点,如未破坏光纤结构完整性、稳定的机械特性、优异的偏振特性、极窄的3dB谐振带宽、高品质因子和Q因子等。然而,倾斜光纤光栅表面等离子体共振对应于透射谱中的一个光谱塌陷区域,即弱谐振或低消光比,导致信噪比降低,易受到干扰信号的影响。Surface plasmon exists on the surface of the metal layer in the form of surface plasmon waves, which is a phenomenon of local concentration of positive and negative charges on the metal surface caused by the interference of charged particles with the outside world. Under the action of the external electromagnetic field, the free electrons inside the plasma in the contact area between the dielectric and the metal layer will be displaced, thereby destroying the electrical neutrality of the area, and then forming a surface electric field. Under the action of the surface electric field, the displaced free electrons oscillate back and forth at their equilibrium position, forming an oscillating wave that travels forward along the metal surface while its amplitude decays exponentially. Under the action of the external electromagnetic field, the positive and negative charged particles inside the plasma oscillate with fluctuations in density, which is called surface plasmon resonance. Optical fibers provide a very good physical medium for designing surface plasmon resonance sensors due to their excellent properties: surface plasmon resonance can be efficiently excited by coating metal thin films on the surface of optical fibers. At present, the widely reported fiber surface plasmon resonance sensor structures mainly include D-type fiber, cladding corrosion, photonic crystal, fiber grating and so on. Compared with other structures, tilted fiber grating surface plasmon resonance sensors have many advantages, such as no damage to fiber structural integrity, stable mechanical properties, excellent polarization properties, extremely narrow 3dB resonance bandwidth, high quality factor and Q factor, etc. . However, the tilted FBG surface plasmon resonance corresponds to a spectral collapse region in the transmission spectrum, i.e., weak resonance or low extinction ratio, resulting in reduced signal-to-noise ratio and vulnerability to interfering signals.

损耗模谐振可通过在光纤表面集成高折射率纳米材料激发,且具有较高的传感灵敏度。高折射率薄膜导致部分低阶包层模式逐渐转变为膜层内传输模式,即损耗模,当损耗模的传播常数与纤芯导模匹配时,引起纤芯模能量耦合至损耗模,从而在透射谱中产生强谐振峰或高消光比。目前已报道多种类型的材料可用于激发损耗模谐振,如氧化铟锡(ITO)、二氧化锡(SnO2)、二氧化钛(TiO2)、聚合物材料(PAA/PAH)等;广泛报道的光纤损耗模谐振传感器结构主要包括D型光纤和包层腐蚀结构。然而,相比于倾斜光纤光栅表面等离子体共振,光纤损耗模谐振的3dB带宽较宽(约宽2个数量级),导致其品质因子和Q因子较低,不利于降低检测分辨率。Loss-mode resonance can be excited by integrating high-refractive-index nanomaterials on the surface of the fiber, and has high sensing sensitivity. The high-refractive-index film causes part of the low-order cladding mode to gradually transform into the transmission mode in the film layer, that is, the loss mode. When the propagation constant of the loss mode matches the core guided mode, the energy of the core mode is coupled to the loss mode, so that in the Strong resonance peaks or high extinction ratios are produced in the transmission spectrum. Various types of materials have been reported for excitation of lossy mode resonances, such as indium tin oxide (ITO), tin dioxide (SnO 2 ), titanium dioxide (TiO 2 ), polymer materials (PAA/PAH), etc.; widely reported The structure of fiber loss mode resonant sensor mainly includes D-type fiber and cladding corrosion structure. However, compared with the inclined fiber grating surface plasmon resonance, the 3dB bandwidth of the fiber loss mode resonance is wider (about 2 orders of magnitude wider), resulting in its lower quality factor and Q factor, which is not conducive to reducing the detection resolution.

另一方面,尽管倾斜光纤光栅表面等离子体共振和光纤损耗模谐振在光通信领域展现出广阔的应用前景,但由于倾斜光纤光栅表面等离子体共振的消光比较低、光纤损耗模谐振带宽较宽等因素的限制,目前它们在光通信领域的应用非常有限。On the other hand, although tilted fiber grating surface plasmon resonance and fiber loss mode resonance show broad application prospects in the field of optical communication, due to the low extinction ratio of tilted fiber grating surface plasmon resonance and the wider bandwidth of fiber loss mode resonance, etc. Due to the limitation of factors, their application in the field of optical communication is very limited at present.

发明内容SUMMARY OF THE INVENTION

本发明的第一个目的是为了克服现有技术存在的缺点和不足,而提供一种倾斜光纤光栅梳状泄漏模谐振的激发方法,通过在倾斜光纤光栅表面涂覆金属氧化物可以在宽波段内激发高强度的TE偏振梳状泄漏模谐振。The first object of the present invention is to overcome the shortcomings and deficiencies of the prior art, and to provide a method for exciting the comb-like leaky mode resonance of the inclined fiber grating. Internal excitation of high-intensity TE-polarized comb leaky mode resonances.

本发明的第二个目的是提供一种基于倾斜光纤光栅梳状泄漏模谐振的窄带偏振滤波器,该滤波器可以实现梳状TM偏振光低损耗的通过,而高效率地反射梳状TE偏振光,可以用于通信或信息处理领域的窄带梳状偏振滤波。The second object of the present invention is to provide a narrow-band polarization filter based on tilted fiber grating comb leaky mode resonance, which can realize low-loss passage of comb-shaped TM polarized light and reflect comb-shaped TE polarization with high efficiency light, which can be used for narrow-band comb polarization filtering in the fields of communications or information processing.

本发明的第三个目的是提供一种基于倾斜光纤光栅梳状泄漏模谐振的传感系统,传感环境覆盖低折射率到高折射率区域的气体和液体环境,可以通过整个梳状光谱包络区域变化或单个泄漏模谐振变化进行传感检测。The third object of the present invention is to provide a sensing system based on tilted fiber grating comb leaky mode resonance, the sensing environment covers gas and liquid environments in the low refractive index to high refractive index regions, and can pass through the entire comb spectral package. Sensing detection of network area changes or single leaky mode resonance changes.

为实现本发明的第一个目的,其技术方案是包括倾斜光纤光栅和纳米量级厚度的金属氧化物薄膜,所述倾斜光纤光栅刻写在单模光纤的纤芯区域,所述金属氧化物薄膜涂覆在所述倾斜光纤光栅的包层表面。In order to achieve the first object of the present invention, the technical solution is to include a tilted fiber grating and a nanometer-thick metal oxide film, the tilted fiber grating is written in the core region of the single-mode fiber, and the metal oxide film is Coated on the cladding surface of the tilted fiber grating.

优选的,所述倾斜光纤光栅通过紫外曝光的方法写制在单模光纤的纤芯区域,其中光栅倾斜角度θ大于10度,光栅长度L大于5毫米,轴向光栅周期Λ大于100纳米。Preferably, the tilted fiber grating is written in the core region of the single-mode fiber by ultraviolet exposure, wherein the grating tilt angle θ is greater than 10 degrees, the grating length L is greater than 5 mm, and the axial grating period Λ is greater than 100 nanometers.

优选的,所述金属氧化物薄膜包括氧化铟锡(ITO)、二氧化锡(SnO2)、三氧化二铟(In2O3)、氧化锌(ZnO)和二氧化钛(TiO2)等材料,根据不同材料属性,可通过磁控溅射法、溶胶凝胶法、层层自组装法等方法涂覆在所述倾斜光纤光栅(1)的包层表面,所述金属氧化物薄膜的厚度为纳米量级,厚度大于10纳米。Preferably, the metal oxide film includes indium tin oxide (ITO), tin dioxide (SnO 2 ), indium trioxide (In 2 O 3 ), zinc oxide (ZnO), titanium dioxide (TiO 2 ) and other materials, According to different material properties, the surface of the cladding layer of the tilted fiber grating (1) can be coated by magnetron sputtering method, sol-gel method, layer-by-layer self-assembly method, etc. The thickness of the metal oxide film is Nanoscale, with a thickness greater than 10 nanometers.

优选的,所述倾斜光纤光栅和所述金属氧化物薄膜的参数可根据应用需求(如光谱范围、谐振峰强度等)进行优化调整,包括光栅倾斜角度、光栅轴向周期、光栅长度、光栅调制幅度、金属氧化物材料及厚度,从而在气体和液体环境中都可以激发倾斜光纤光栅梳状泄漏模谐振。Preferably, the parameters of the tilted fiber grating and the metal oxide film can be optimized and adjusted according to application requirements (such as spectral range, resonance peak intensity, etc.), including grating tilt angle, grating axial period, grating length, grating modulation Amplitude, metal oxide material, and thickness to excite slanted fiber grating comb leaky mode resonances in both gas and liquid environments.

本技术方案中,利用金属氧化物激发倾斜光纤光栅梳状泄漏模谐振的工作原理为:由于光纤泄漏模的损耗远高于包层模,因此普通倾斜光纤光栅的谐振光谱由系列强包层模谐振和弱泄漏模谐振构成;在所述倾斜光纤光栅的包层表面涂覆所述高折射率金属氧化物,并通过优化薄膜厚度,能在宽波段内极大降低TE偏振泄漏模的损耗,而对TM偏振泄漏模的影响较小,进而极大增强TE偏振泄漏模和纤芯导模的耦合程度,最后获得增强的TE偏振梳状泄漏模谐振,而TM偏振泄漏模谐振的变化很小。In this technical solution, the working principle of using metal oxide to excite the comb leaky mode resonance of the tilted fiber grating is as follows: since the loss of the fiber leaky mode is much higher than that of the cladding mode, the resonance spectrum of the ordinary tilted fiber grating is determined by a series of strong cladding modes. Resonance and weak leaky mode resonance; coating the high-refractive-index metal oxide on the cladding surface of the tilted fiber grating, and by optimizing the film thickness, the loss of the TE polarization leaky mode can be greatly reduced in a wide band, The effect on the TM polarization leaky mode is small, and the coupling degree between the TE polarization leaky mode and the core guided mode is greatly enhanced, and finally the enhanced TE polarization comb leaky mode resonance is obtained, while the change in the TM polarization leaky mode resonance is small. .

为实现本发明的第二个目的,其技术方案是一种基于倾斜光纤光栅梳状泄漏模谐振的窄带偏振滤波器,包括:宽带光源、偏振控制器、单模光纤跳线、金属氧化物涂覆倾斜光纤光栅及光谱分析仪,其中,所述宽带光源、偏振控制器、金属氧化物涂覆倾斜光纤光栅及光谱分析仪依次通过单模光纤跳线连接。In order to achieve the second object of the present invention, its technical solution is a narrow-band polarization filter based on a tilted fiber grating comb leaky mode resonance, comprising: a broadband light source, a polarization controller, a single-mode fiber jumper, a metal oxide coating A coated tilted fiber grating and a spectrum analyzer, wherein the broadband light source, the polarization controller, the metal oxide coated tilted fiber grating and the spectrum analyzer are sequentially connected through a single-mode fiber jumper.

优选的,所述宽带光源输出非偏振光,光谱范围覆盖所述金属氧化物涂覆倾斜光纤光栅光谱响应范围。Preferably, the broadband light source outputs unpolarized light, and the spectral range covers the spectral response range of the metal oxide-coated tilted fiber grating.

优选的,所述偏振控制器用于将非偏振光调节为单一偏振方向的线偏振光,即将所述宽带光源输出的非偏振光调节为TE偏振光或TM偏振光,其中,TE偏振光的偏振方向与所述倾斜光纤光栅的写入方向垂直,TM偏振光的偏振方向与所述倾斜光纤光栅的写入方向一致。Preferably, the polarization controller is used to adjust the unpolarized light to linearly polarized light with a single polarization direction, that is, to adjust the unpolarized light output from the broadband light source to TE polarized light or TM polarized light, wherein the polarization of the TE polarized light The direction is perpendicular to the writing direction of the tilted fiber grating, and the polarization direction of the TM polarized light is consistent with the writing direction of the tilted fiber grating.

本技术方案中,一种基于倾斜光纤光栅梳状泄漏模谐振的窄带偏振滤波器的方法为:所述宽带光源输出非偏振光,经所述偏振控制器后调节为单一偏振方向的TE偏振光或TM偏振光,然后经所述单模光纤跳线输入至所述金属氧化物涂覆倾斜光纤光栅内,并在其纤芯内激励起纤芯导模,所述纤芯导模在所述倾斜光纤光栅内耦合至反向传播的一系列TE或TM偏振泄漏模(同时包括部分包层模),即激发梳状泄漏模谐振,由于所述金属氧化物会极大降低TE偏振泄漏模损耗,同时对TM偏振泄漏模的影响较小,因此从所述金属氧化物涂覆倾斜光纤光栅输出后产生系列增强的TE偏振梳状泄漏模谐振峰(或损耗峰),所述输出光谱经所述单模光纤跳线输入至所述光谱分析仪并显示透射谱。In this technical solution, a method for a narrow-band polarization filter based on a tilted fiber grating comb leaky mode resonance is as follows: the broadband light source outputs unpolarized light, which is adjusted to TE polarized light with a single polarization direction after being adjusted by the polarization controller or TM polarized light, then input into the metal oxide-coated inclined fiber grating through the single-mode fiber jumper, and excite the core guided mode in its core, and the core guided mode is in the The tilted fiber grating is coupled to a series of counter-propagating TE or TM polarization leaky modes (including partial cladding modes), i.e. excitation of comb-like leaky mode resonances, since the metal oxide will greatly reduce the TE polarization leaky mode loss At the same time, the influence on the TM polarization leaky mode is small, so a series of enhanced TE polarization comb leaky mode resonance peaks (or loss peaks) are generated after the output from the metal oxide-coated tilted fiber grating. The single-mode fiber patch cord is input to the spectrum analyzer and displays the transmission spectrum.

为实现本发明的第三个目的,其技术方案是一种基于倾斜光纤光栅梳状泄漏模谐振的传感系统,包括:宽带光源、偏振控制器、单模光纤跳线、金属氧化物涂覆倾斜光纤光栅、样品反应皿、光谱分析仪及计算机,其中,所述宽带光源、偏振控制器、金属氧化物涂覆倾斜光纤光栅、光谱分析仪依次通过所述单模光纤跳线连接,所述光谱分析仪通过信号线与所述计算机连接。In order to achieve the third object of the present invention, the technical solution is a sensing system based on the comb leaky mode resonance of inclined fiber grating, comprising: a broadband light source, a polarization controller, a single-mode fiber jumper, a metal oxide coating Tilt fiber grating, sample reaction vessel, spectrum analyzer and computer, wherein the broadband light source, polarization controller, metal oxide coated tilt fiber grating, and spectrum analyzer are sequentially connected through the single-mode fiber jumper, and the The spectrum analyzer is connected with the computer through a signal line.

所述偏振控制器用于将非偏振光调节为与所述倾斜光纤光栅写入方向垂直的单一偏振方向的线偏振光,即将所述宽带光源输出的非偏振光调节为TE偏振光。The polarization controller is used to adjust the unpolarized light to linearly polarized light with a single polarization direction perpendicular to the writing direction of the tilted fiber grating, that is, to adjust the unpolarized light output from the broadband light source to TE polarized light.

所述金属氧化物涂覆倾斜光纤光栅置于所述样品反应皿内,待测样品覆盖金属氧化物涂覆倾斜光纤光栅的传感区域,在进行原位检测时,可以去掉所述样品反应皿,并将金属氧化物涂覆倾斜光纤光栅直接置于待测样品内部。The metal oxide-coated tilted fiber grating is placed in the sample reaction vessel, and the sample to be tested covers the sensing area of the metal oxide-coated tilted fiber grating. When performing in-situ detection, the sample reaction vessel can be removed , and place the metal oxide-coated tilted fiber grating directly inside the sample to be tested.

所述光谱分析仪用于显示所述金属氧化物涂覆倾斜光纤光栅的光谱变化,并将采集到的传感信号输入至所述计算机进行数据处理,通过分析传感信号的变化得到待测样品的信息。The spectrum analyzer is used to display the spectral changes of the metal oxide-coated inclined fiber grating, input the collected sensing signals to the computer for data processing, and obtain the sample to be tested by analyzing the changes of the sensing signals Information.

所述计算机内有两种数据处理的方法,包括:There are two data processing methods in the computer, including:

方法一,计算所述光谱分析仪采集到的整个光谱包络区域随待测样品的变化,从而得到待测样品的信息。光谱包络区域

Figure BDA0002226317410000054
变化计算如下:Method 1: Calculate the change of the entire spectral envelope region collected by the spectrum analyzer with the sample to be tested, so as to obtain the information of the sample to be tested. Spectral envelope region
Figure BDA0002226317410000054
The change is calculated as follows:

其中ξu(λ)和ξl(λ)分别表示透射光谱的上下包络曲线,

Figure BDA0002226317410000052
Figure BDA0002226317410000053
分别表示初始外界环境下透射光谱的上下包络曲线,λmin和λmax表示波长区间。where ξ u (λ) and ξ l (λ) represent the upper and lower envelope curves of the transmission spectrum, respectively,
Figure BDA0002226317410000052
and
Figure BDA0002226317410000053
respectively represent the upper and lower envelope curves of the transmission spectrum in the initial external environment, and λ min and λ max represent the wavelength range.

方法二,监测单个泄漏模谐振峰随待测样品的变化,从而得到待测样品的信息。The second method is to monitor the change of the resonance peak of a single leaky mode with the sample to be tested, so as to obtain the information of the sample to be tested.

本技术方案中,一种基于倾斜光纤光栅梳状泄漏模谐振传感系统的检测方法为:所述宽带光源输出的非偏振光经所述偏振控制器后调节为TE偏振光,经所述单模光纤跳线输入至所述金属氧化物涂覆倾斜光纤光栅的纤芯内并激发TE偏振纤芯导模,所述TE偏振纤芯导模在所述倾斜光纤光栅内耦合至反向传播的一系列泄漏模(同时包括部分包层模),即激发TE偏振梳状泄漏模谐振,从而在所述金属氧化物涂覆倾斜光纤光栅的输出光谱中产生系列TE偏振梳状泄漏模谐振峰,外界待测样品的变化会引起所述泄漏模谐振峰的变化,从所述金属氧化物涂覆倾斜光纤光栅输出后经所述单模光纤跳线输入至所述光谱分析仪并显示透射谱,所述光谱分析仪采集到的传感信号输入至所述计算机进行数据处理,即计算整个光谱包络区域或单个泄漏模谐振峰随待测样品的变化,从而得到待测样品的信息。In this technical solution, a detection method based on a tilted fiber grating comb leaky mode resonance sensing system is as follows: the unpolarized light output by the broadband light source is adjusted to TE polarized light after being adjusted by the polarization controller, The mode fiber jumper is input into the core of the metal oxide coated tilted fiber grating and excites the TE polarized core guided mode, which couples to the counter-propagating fiber grating within the tilted fiber grating. A series of leaky modes (including partial cladding modes at the same time), that is, excitation of TE polarization comb leaky mode resonances, resulting in a series of TE polarization comb leaky mode resonance peaks in the output spectrum of the metal oxide-coated tilted fiber grating, The change of the external sample to be tested will cause the change of the leaky mode resonance peak, which is output from the metal oxide-coated inclined fiber grating and is input to the spectrum analyzer through the single-mode fiber jumper and displays the transmission spectrum, The sensing signal collected by the spectrum analyzer is input to the computer for data processing, that is, the change of the entire spectral envelope region or the resonance peak of a single leaky mode with the sample to be tested is calculated, so as to obtain the information of the sample to be tested.

本发明相对于现有技术具有如下的优点及有益效果:Compared with the prior art, the present invention has the following advantages and beneficial effects:

(1)本发明的倾斜光纤光栅梳状泄漏模谐振激发方法,通过在倾斜光纤光栅的包层表面涂覆纳米量级金属氧化物在宽波段内高效率地激发梳状泄漏模谐振,所激发的梳状泄漏模谐振峰强度较强、带宽极窄,在通信领域可用于窄带滤波,在传感领域可用于高灵敏检测,具有广阔的应用前景。(1) The method for exciting the comb-like leaky mode resonance of the tilted fiber grating of the present invention, by coating the surface of the cladding layer of the tilted fiber grating with a nano-scale metal oxide, the comb-like leaky mode resonance is excited efficiently in a wide band, and the excited The comb-like leaky mode resonance peak intensity is strong and the bandwidth is extremely narrow, which can be used for narrow-band filtering in the field of communication, and can be used for high-sensitivity detection in the field of sensing, and has broad application prospects.

(2)本发明的倾斜光纤光栅梳状泄漏模谐振激发方法,很多类型的金属氧化物如氧化铟锡(ITO)、二氧化锡(SnO2)、三氧化二铟(In2O3)、氧化锌(ZnO)和二氧化钛(TiO2)等材料都能用于激发梳状泄漏模谐振,从而极大扩展了倾斜光纤光栅器件的应用领域。(2) In the method for resonant excitation of the inclined fiber grating comb leaky mode of the present invention, many types of metal oxides such as indium tin oxide (ITO), tin dioxide (SnO 2 ), indium trioxide (In 2 O 3 ), Materials such as zinc oxide (ZnO) and titanium dioxide (TiO 2 ) can be used to excite comb leaky mode resonances, thereby greatly expanding the application field of tilted fiber grating devices.

(3)本发明的倾斜光纤光栅梳状泄漏模谐振激发方法,倾斜光纤光栅和金属氧化物的参数可根据应用需求(如光谱范围、谐振峰强度等)进行优化调整,包括光栅倾斜角度、光栅轴向周期、光栅长度、光栅调制幅度、金属氧化物材料及厚度,从而在气体和液体环境中都可以激发倾斜光纤光栅梳状泄漏模谐振。(3) In the method for exciting the comb leaky mode resonance excitation of the tilted fiber grating of the present invention, the parameters of the tilted fiber grating and the metal oxide can be optimized and adjusted according to the application requirements (such as spectral range, resonance peak intensity, etc.), including the grating tilt angle, the grating Axial period, grating length, grating modulation amplitude, metal oxide material and thickness to excite tilted fiber grating comb leaky mode resonances in both gas and liquid environments.

(4)本发明的基于倾斜光纤光栅梳状泄漏模谐振的窄带偏振滤波器,涂覆在倾斜光纤光栅表面的金属氧化物材料会极大降低TE偏振泄漏模损耗,同时对TM偏振泄漏模的影响较小,因此能极大增强TE偏振泄漏模与纤芯导模的耦合强度,从而得到倾斜光纤光栅TE偏振梳状泄漏模谐振峰,而TM偏振泄漏模谐振的变化很小,可实现高消光比窄带偏振滤波。(4) In the narrow-band polarization filter based on the tilted fiber grating comb leaky mode resonance of the present invention, the metal oxide material coated on the surface of the tilted fiber grating can greatly reduce the loss of the TE polarization leaky mode, and at the same time, it can reduce the loss of the TM polarization leaky mode. The influence is small, so the coupling strength of the TE polarization leaky mode and the core guided mode can be greatly enhanced, so that the TE polarization comb leaky mode resonance peak of the tilted fiber grating can be obtained, while the TM polarization leaky mode resonance changes very little, which can achieve high efficiency. Extinction ratio narrow-band polarization filtering.

(5)本发明的基于倾斜光纤光栅梳状泄漏模谐振的传感系统,既可以通过计算整个光谱包络区域变化来确定待测样品的信息,又可以通过监测单个泄漏模谐振确定待测样品的信息,可以多维多角度高灵敏地获取待测样品的信息。(5) The sensing system based on the tilted fiber grating comb leaky mode resonance of the present invention can not only determine the information of the sample to be tested by calculating the change of the entire spectral envelope region, but also determine the sample to be tested by monitoring the resonance of a single leaky mode The information of the sample to be tested can be obtained with high sensitivity in multi-dimensional and multi-angle.

(6)本发明的基于倾斜光纤光栅梳状泄漏模谐振的传感系统,相比于传统的表面等离子体共振和损耗模谐振,极窄线宽的泄漏模谐振能进一步优化倾斜光纤光栅的传感性能,提高传感品质因子、Q因子,进一步降低检测分辨率。(6) Compared with the traditional surface plasmon resonance and lossy mode resonance, the sensing system based on the tilted fiber grating comb leaky mode resonance of the present invention, the leaky mode resonance of the extremely narrow linewidth can further optimize the transmission of the tilted fiber grating. The sensor performance is improved, the quality factor and Q factor of the sensor are improved, and the detection resolution is further reduced.

附图说明Description of drawings

为了更清楚地说明本发明实施例或现有技术中的技术方案,下面将对实施例或现有技术描述中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图仅仅是本发明的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动性的前提下,根据这些附图获得其他的附图仍属于本发明的范畴。In order to explain the embodiments of the present invention or the technical solutions in the prior art more clearly, the following briefly introduces the accompanying drawings that need to be used in the description of the embodiments or the prior art. Obviously, the accompanying drawings in the following description are only These are some embodiments of the present invention, and for those of ordinary skill in the art, obtaining other drawings according to these drawings still belongs to the scope of the present invention without any creative effort.

图1金属氧化物涂覆倾斜光纤光栅原理图;Fig. 1 Schematic diagram of metal oxide coated tilted fiber grating;

图2倾斜光纤光栅梳状泄漏模谐振窄带偏振滤波原理图;Fig. 2 Schematic diagram of slanted fiber grating comb leaky mode resonance narrow-band polarization filtering;

图3倾斜光纤光栅梳状泄漏模谐振传感系统原理图;Figure 3 Schematic diagram of the tilted fiber grating comb leaky mode resonant sensing system;

图4金属氧化物涂覆倾斜光纤光栅透射谱:(a)TM偏振,(b)TE偏振。Figure 4. Transmission spectra of metal oxide-coated tilted fiber gratings: (a) TM polarization, (b) TE polarization.

图5基于倾斜光纤光栅梳状泄漏模谐振窄带偏振滤波器的透射谱;Fig. 5 is based on the transmission spectrum of the slanted fiber grating comb leaky mode resonant narrow-band polarization filter;

图6基于倾斜光纤光栅梳状泄漏模谐振传感系统的光谱包络变化:(a)光谱包络曲线示例,(b)光谱包络区域随待测样品的变化过程;Fig. 6 Changes of spectral envelope based on a tilted fiber grating comb leaky mode resonant sensing system: (a) an example of the spectral envelope curve, (b) the change process of the spectral envelope region with the sample to be measured;

图7基于光谱包络区域变化的传感特性曲线;Fig. 7 is based on the sensing characteristic curve of spectral envelope area change;

图8单个泄漏模谐振峰随待测样品的变化,插图为相应透射谱的变化;Fig. 8 The variation of the resonance peak of a single leaky mode with the sample to be tested, the inset is the variation of the corresponding transmission spectrum;

图9基于单个泄漏模谐振峰变化的传感特性曲线。Figure 9. Sensing characteristic curve based on the variation of the resonance peak of a single leaky mode.

具体实施方式Detailed ways

为使本发明的目的、技术方案和优点更加清楚,下面将结合附图对本发明作进一步地详细描述。In order to make the objectives, technical solutions and advantages of the present invention clearer, the present invention will be further described in detail below with reference to the accompanying drawings.

实施例1Example 1

本实施例公开了倾斜光纤光栅梳状泄漏模谐振的激发方法,如图1所示,包括倾斜光纤光栅1和纳米量级厚度的金属氧化物薄膜2,所述倾斜光纤光栅1刻写在单模光纤的纤芯区域,所述金属氧化物薄膜2涂覆在所述倾斜光纤光栅1的包层表面。This embodiment discloses a method for exciting the comb leaky mode resonance of a tilted fiber grating. As shown in FIG. 1 , it includes a tilted fiber grating 1 and a nanometer-thick metal oxide film 2. The tilted fiber grating 1 is written on a single-mode In the core region of the optical fiber, the metal oxide film 2 is coated on the surface of the cladding of the inclined fiber grating 1 .

本实施例中,所述倾斜光纤光栅1通过紫外曝光的方法写制在单模光纤的纤芯区域,其中单模光纤的纤芯半径为4.1微米,包层半径为62.5微米,光栅倾斜角度θ为13度,光栅长度L为20毫米,轴向光栅周期Λ为600纳米。In this embodiment, the tilted fiber grating 1 is written on the core region of a single-mode fiber by UV exposure, wherein the core radius of the single-mode fiber is 4.1 microns, the cladding radius is 62.5 microns, and the grating tilt angle θ is 13 degrees, the grating length L is 20 mm, and the axial grating period Λ is 600 nm.

本实施例中,所述金属氧化物薄膜2为氧化铟锡(ITO)材料,通过磁控溅射法涂覆在所述倾斜光纤光栅1的包层表面,厚度分别为50纳米、100纳米、150纳米和200纳米。In this embodiment, the metal oxide film 2 is made of indium tin oxide (ITO) material, and is coated on the surface of the cladding layer of the tilted fiber grating 1 by magnetron sputtering, with thicknesses of 50 nanometers, 100 nanometers, and 100 nanometers, respectively. 150nm and 200nm.

本实施例中,倾斜光纤光栅梳状泄漏模谐振激发方法的工作原理为:由于光纤泄漏模的损耗远高于包层模,因此普通倾斜光纤光栅的谐振光谱由系列强包层模谐振和弱泄漏模谐振构成;在所述倾斜光纤光栅1的包层表面涂覆所述高折射率金属氧化物2,并通过优化薄膜厚度,能在宽波段内极大降低TE偏振泄漏模的损耗,而对TM偏振泄漏模的影响较小,进而极大增强TE偏振泄漏模和纤芯导模的耦合程度,最后获得增强的TE偏振梳状泄漏模谐振,而TM偏振泄漏模谐振的变化很小。In this embodiment, the working principle of the method for exciting the comb leaky mode resonance excitation of the tilted fiber grating is as follows: since the loss of the fiber leaky mode is much higher than that of the cladding mode, the resonance spectrum of the ordinary tilted fiber grating consists of a series of strong cladding mode resonance and weak cladding mode resonance. The leaky mode resonance is formed; the high refractive index metal oxide 2 is coated on the cladding surface of the tilted fiber grating 1, and the loss of the TE polarization leaky mode can be greatly reduced in a wide band by optimizing the film thickness, while The influence on the TM polarization leaky mode is small, and the coupling degree of the TE polarization leaky mode and the core guided mode is greatly enhanced, and finally the enhanced TE polarization comb leaky mode resonance is obtained, while the TM polarization leaky mode resonance changes very little.

本实施例中,氧化铟锡厚度分别为0纳米、50纳米、100纳米、150纳米和200纳米时的透射谱如图4所示。在未涂覆氧化铟锡材料时,倾斜光纤光栅透射谱中TE和TM偏振泄漏模谐振均非常微弱。随着氧化铟锡薄膜厚度增加,TE偏振泄漏模谐振逐渐增强,而TM偏振泄漏模谐振的变化很小。当氧化铟锡薄膜厚度大于100纳米后,激发了很强的TE偏振窄带梳状泄漏模谐振。In this embodiment, the transmission spectra when the thicknesses of the indium tin oxide are respectively 0 nanometer, 50 nanometers, 100 nanometers, 150 nanometers and 200 nanometers are shown in FIG. 4 . When the indium tin oxide material is not coated, the TE and TM polarization leaky mode resonances are very weak in the transmission spectrum of the tilted fiber grating. As the thickness of the ITO film increases, the TE-polarized leaky mode resonance increases gradually, while the TM-polarized leaky mode resonance changes little. When the thickness of the indium tin oxide film is greater than 100 nm, a strong TE polarized narrow-band comb leaky mode resonance is excited.

实施例2Example 2

本实施例公开了一种基于倾斜光纤光栅梳状泄漏模谐振的窄带偏振滤波器,如图2所示,包括:宽带光源3、偏振控制器4、单模光纤跳线5、金属氧化物涂覆倾斜光纤光栅6及光谱分析仪7,其中,所述宽带光源3、偏振控制器4、金属氧化物涂覆倾斜光纤光栅6及光谱分析仪7依次通过单模光纤跳线5连接。This embodiment discloses a narrow-band polarization filter based on tilted fiber grating comb leaky mode resonance, as shown in FIG. 2, including: a broadband light source 3, a polarization controller 4, a single-mode fiber jumper 5, a metal oxide coating Coated tilted fiber grating 6 and spectrum analyzer 7 , wherein the broadband light source 3 , polarization controller 4 , metal oxide coated tilted fiber grating 6 and spectrum analyzer 7 are sequentially connected through single-mode fiber jumper 5 .

本实施例中,所述宽带光源输出非偏振光,光谱范围覆盖所述金属氧化物涂覆倾斜光纤光栅6光谱响应范围。In this embodiment, the broadband light source outputs unpolarized light, and the spectral range covers the spectral response range of the metal oxide-coated tilted fiber grating 6 .

本实施例中,所述偏振控制器4用于将非偏振光调节为单一偏振方向的线偏振光,即将所述宽带光源3输出的非偏振光调节为TE偏振光或TM偏振光,其中,TE偏振光的偏振方向与所述倾斜光纤光栅1的写入方向垂直,TM偏振光的偏振方向与所述倾斜光纤光栅1的写入方向一致。In this embodiment, the polarization controller 4 is used to adjust the unpolarized light to linearly polarized light with a single polarization direction, that is, to adjust the unpolarized light output by the broadband light source 3 to TE polarized light or TM polarized light, wherein, The polarization direction of the TE polarized light is perpendicular to the writing direction of the tilted fiber grating 1 , and the polarization direction of the TM polarized light is consistent with the writing direction of the tilted fiber grating 1 .

本实施例中,所述倾斜光纤光栅1与实施例1相同,光栅倾斜角度θ为15度。In this embodiment, the tilted fiber grating 1 is the same as that of the first embodiment, and the tilt angle θ of the grating is 15 degrees.

本实施例中,所述金属氧化物薄膜2与实施例1相同,厚度为260纳米。In this embodiment, the metal oxide film 2 is the same as that in Embodiment 1, and the thickness is 260 nm.

本实施例中,一种基于倾斜光纤光栅梳状泄漏模谐振的窄带偏振滤波器的方法为:所述宽带光源3输出非偏振光,经所述偏振控制器4后调节为单一偏振方向的TE偏振光或TM偏振光,然后经所述单模光纤跳线5输入至所述金属氧化物涂覆倾斜光纤光栅6内,并在其纤芯内激励起纤芯导模,所述纤芯导模在所述倾斜光纤光栅1内耦合至反向传播的一系列TE或TM偏振泄漏模(同时包括部分包层模),即激发梳状泄漏模谐振,由于所述金属氧化物2会极大降低TE偏振泄漏模损耗,同时对TM偏振泄漏模的影响较小,因此从所述金属氧化物涂覆倾斜光纤光栅5输出后产生系列增强的TE偏振梳状泄漏模谐振峰(或损耗峰),所述输出光谱经所述单模光纤跳线5输入至所述光谱分析仪7并显示透射谱。In this embodiment, a method for a narrow-band polarization filter based on tilted fiber grating comb leaky mode resonance is as follows: the broadband light source 3 outputs unpolarized light, which is adjusted to TE with a single polarization direction after being adjusted by the polarization controller 4 The polarized light or TM polarized light is then input into the metal oxide-coated tilted fiber grating 6 through the single-mode fiber jumper 5, and the core guided mode is excited in its core, and the core guide The modes are coupled in the tilted fiber grating 1 to a series of TE or TM polarization leaky modes (including part of the cladding modes) that propagate in the opposite direction, i.e., the comb-like leaky mode resonance is excited, since the metal oxide 2 will greatly The loss of TE polarization leaky mode is reduced, and the influence on TM polarization leaky mode is small, so a series of enhanced TE polarization comb leaky mode resonance peaks (or loss peaks) are generated after output from the metal oxide-coated tilted fiber grating 5 , the output spectrum is input to the spectrum analyzer 7 through the single-mode fiber jumper 5 and displays the transmission spectrum.

本实施例中,图5所示为金属膜涂覆倾斜光纤光栅透射谱。如图所示,在非常宽的波段范围内,TE偏振透射谱中产生了非常强的窄带梳状泄漏模谐振,而TM偏振泄漏模谐振较弱。由于透射谱中的谐振峰对应的是损耗峰,因此谐振波长位置的TE偏振光被耦合至反向传播的TE偏振泄漏模而不能通过倾斜光栅,而谐振波长位置的TM偏振光能以很小的损耗通过倾斜光栅,从而在非常宽的波段范围内实现窄带偏振滤波。In this embodiment, FIG. 5 shows the transmission spectrum of the metal film-coated tilted fiber grating. As shown in the figure, a very strong narrow-band comb leaky mode resonance is generated in the TE polarized transmission spectrum in a very broad band range, while the TM polarized leaky mode resonance is weaker. Since the resonance peak in the transmission spectrum corresponds to the loss peak, the TE polarized light at the resonance wavelength position is coupled to the counter-propagating TE polarized leaky mode and cannot pass through the tilted grating, while the TM polarized light at the resonance wavelength position can be transmitted with a very small The loss is passed through a tilted grating, enabling narrow-band polarization filtering over a very wide wavelength range.

实施例3Example 3

本实施例公开了一种基于倾斜光纤光栅梳状泄漏模谐振的传感系统,如图3所示,包括:宽带光源3、偏振控制器4、单模光纤跳线5、金属氧化物涂覆倾斜光纤光栅6、样品反应皿8、光谱分析仪7及计算机9,其中,所述宽带光源3、偏振控制器4、金属氧化物涂覆倾斜光纤光栅6、光谱分析仪7依次通过所述单模光纤跳线5连接,所述光谱分析仪7通过信号线与所述计算机9连接。This embodiment discloses a sensing system based on tilted fiber grating comb leaky mode resonance, as shown in FIG. 3 , including: a broadband light source 3, a polarization controller 4, a single-mode fiber jumper 5, and a metal oxide coating Tilt fiber grating 6, sample reaction vessel 8, spectrum analyzer 7 and computer 9, wherein the broadband light source 3, polarization controller 4, metal oxide coated tilt fiber grating 6, spectrum analyzer 7 pass through the single The mode fiber jumper 5 is connected, and the spectrum analyzer 7 is connected with the computer 9 through a signal line.

本实施例中,所述偏振控制器4用于将非偏振光调节为与所述倾斜光纤光栅1写入方向垂直的单一偏振方向的线偏振光,即将所述宽带光源3输出的非偏振光调节为TE偏振光。In this embodiment, the polarization controller 4 is used to adjust the unpolarized light to linearly polarized light with a single polarization direction perpendicular to the writing direction of the tilted fiber grating 1 , that is, the unpolarized light output by the broadband light source 3 Adjusted to TE polarized light.

本实施例中,所述倾斜光纤光栅1与实施例1相同。In this embodiment, the tilted fiber grating 1 is the same as that of the first embodiment.

本实施例中,所述金属氧化物薄膜2与实施例1相同,厚度为150纳米。In this embodiment, the metal oxide film 2 is the same as that in Embodiment 1, and the thickness is 150 nanometers.

本实施例中,所述金属氧化物涂覆倾斜光纤光栅6置于所述样品反应皿8内,待测样品覆盖金属氧化物涂覆倾斜光纤光栅6的传感区域,在进行原位检测时,可以去掉所述样品反应皿8,并将金属氧化物涂覆倾斜光纤光栅6直接置于待测样品内部。In this embodiment, the metal oxide-coated tilted fiber grating 6 is placed in the sample reaction vessel 8, and the sample to be tested covers the sensing area of the metal oxide-coated tilted fiber grating 6. When performing in-situ detection , the sample reaction vessel 8 can be removed, and the metal oxide-coated inclined fiber grating 6 can be directly placed inside the sample to be tested.

本实施例中,所述光谱分析仪7用于显示所述金属氧化物涂覆倾斜光纤光栅6的光谱变化,并将采集到的传感信号输入至所述计算机9进行数据处理,通过分析传感信号的变化得到待测样品的信息。In this embodiment, the spectrum analyzer 7 is used to display the spectral changes of the metal oxide-coated tilted fiber grating 6 , and input the collected sensing signals to the computer 9 for data processing. The change of the sensing signal can obtain the information of the sample to be tested.

本实施例中,所述数据处理方法有两种,包括:In this embodiment, there are two data processing methods, including:

方法一,计算所述光谱分析仪7采集到的整个光谱包络区域随待测样品的变化,从而得到待测样品的信息。光谱包络区域A变化计算如下:Method 1: Calculate the change of the entire spectral envelope region collected by the spectrum analyzer 7 with the sample to be tested, so as to obtain the information of the sample to be tested. The spectral envelope region A change is calculated as follows:

Figure BDA0002226317410000101
Figure BDA0002226317410000101

其中ξu(λ)和ξl(λ)分别表示透射光谱的上下包络曲线,

Figure BDA0002226317410000102
Figure BDA0002226317410000103
分别表示参考外界环境下透射光谱的上下包络曲线,参考环境折射率(surrounding refractiveindex,SRI)设为1.0,λmin=1.58μm和λmax=1.72μm表示波长区间。where ξ u (λ) and ξ l (λ) represent the upper and lower envelope curves of the transmission spectrum, respectively,
Figure BDA0002226317410000102
and
Figure BDA0002226317410000103
Respectively represent the upper and lower envelope curves of the transmission spectrum in the reference external environment, the reference ambient refractive index (SRI) is set to 1.0, and λ min =1.58 μm and λ max =1.72 μm represent the wavelength range.

方法二,监测单个泄漏模谐振峰随待测样品的变化,从而得到待测样品的信息。The second method is to monitor the change of the resonance peak of a single leaky mode with the sample to be tested, so as to obtain the information of the sample to be tested.

本实施例中,一种基于倾斜光纤光栅梳状泄漏模谐振传感系统的检测方法为:所述宽带光源3输出的非偏振光经所述偏振控制器4后调节为TE偏振光,经所述单模光纤跳线5输入至所述金属氧化物涂覆倾斜光纤光栅6的纤芯内并激发TE偏振纤芯导模,所述TE偏振纤芯导模在所述倾斜光纤光栅1内耦合至反向传播的一系列泄漏模(同时包括部分包层模),即激发TE偏振梳状泄漏模谐振,从而在所述金属氧化物涂覆倾斜光纤光栅6的输出光谱中产生系列TE偏振梳状泄漏模谐振峰,外界待测样品的变化会引起所述泄漏模谐振峰的变化,从所述金属氧化物涂覆倾斜光纤光栅6输出后经所述单模光纤跳线5输入至所述光谱分析仪7并显示透射谱,所述光谱分析仪7采集到的传感信号输入至所述计算机9进行数据处理,即计算整个光谱包络区域或单个泄漏模谐振峰随待测样品的变化,从而得到待测样品的信息。In this embodiment, a detection method based on a tilted fiber grating comb leaky mode resonance sensing system is as follows: the unpolarized light output by the broadband light source 3 is adjusted to TE polarized light after being adjusted by the polarization controller 4, The single-mode fiber jumper 5 is input into the core of the metal oxide-coated tilted fiber grating 6 and excites the TE polarized core guided mode, which is coupled in the tilted fiber grating 1 A series of leaky modes (including partial cladding modes) to counter-propagating, that is, excitation of TE polarization comb leaky mode resonances, resulting in a series of TE polarization combs in the output spectrum of the metal oxide-coated tilted fiber grating 6 The change of the external sample to be tested will cause the change of the leaky mode resonance peak, which is output from the metal oxide-coated inclined fiber grating 6 and input to the The spectrum analyzer 7 displays the transmission spectrum, and the sensing signal collected by the spectrum analyzer 7 is input to the computer 9 for data processing, that is, the variation of the entire spectral envelope region or a single leaky mode resonance peak with the sample to be measured is calculated , so as to obtain the information of the sample to be tested.

本实施例中,图6所示为整个光谱包络区域的变化,其中,图6(a)给出了光谱包络区域的计算示例,图6(b)所示为整个光谱包络区域随待测样品的变化过程。为了更清晰地表示透射光谱包络区域的变化,图中仅给出了透射光谱下包络曲线ξl(λ)随待测样品折射率的变化,上包络曲线变化很小而未给出。随着待测样品折射率的增大,光谱包络区域逐渐减小,说明光谱包络区域的变化能清晰地反应待测样品的变化。In this embodiment, Fig. 6 shows the change of the entire spectral envelope region, wherein Fig. 6(a) shows a calculation example of the spectral envelope region, and Fig. 6(b) shows the change of the entire spectral envelope region with The change process of the sample to be tested. In order to show the change of the envelope region of the transmission spectrum more clearly, only the change of the lower envelope curve ξ l (λ) of the transmission spectrum with the refractive index of the sample to be measured is given, and the upper envelope curve has little change and is not given. . As the refractive index of the sample to be measured increases, the spectral envelope area gradually decreases, indicating that the change of the spectral envelope area can clearly reflect the change of the sample to be measured.

本实施例中,图7所示为基于光谱包络区域变化的传感特性曲线。分别得到两个线性传感区域,经线性拟合后得到传感灵敏度分别达到6.621/RIU和1.570/RIU(RIU表示refractive index unit,即折射率单位)。In this embodiment, FIG. 7 shows a sensing characteristic curve based on changes in the spectral envelope region. Two linear sensing regions are obtained respectively, and the sensing sensitivity is 6.621/RIU and 1.570/RIU respectively after linear fitting (RIU stands for refractive index unit, that is, refractive index unit).

本实施例中,图8所示为单个泄漏模谐振峰随待测样品的变化。当待测样品折射率增大时,泄漏模谐振峰的强度逐渐单调减小。相应的传感灵敏度如图9所示,在低折射率区域,单个泄漏模谐振峰的传感灵敏度最高达到820dB/RIU,在生化医学等领域普遍关注的低折射率区域具有广阔的应用前景。In this embodiment, Fig. 8 shows the variation of the resonance peak of a single leaky mode with the sample to be tested. When the refractive index of the sample to be measured increases, the intensity of the leaky mode resonance peak gradually decreases monotonically. The corresponding sensing sensitivity is shown in Fig. 9. In the low refractive index region, the sensing sensitivity of a single leaky mode resonance peak can reach up to 820 dB/RIU.

以上所揭露的仅为本发明较佳实施例而已,当然不能以此来限定本发明之权利范围,因此依本发明权利要求所作的等同变化,仍属本发明所涵盖的范围。The above disclosures are only preferred embodiments of the present invention, and of course, the scope of the rights of the present invention cannot be limited by this. Therefore, equivalent changes made according to the claims of the present invention are still within the scope of the present invention.

应当注意,本发明的实施例可以通过硬件、软件或者软件和硬件的结合来实现。硬件部分可以利用专用逻辑来实现;软件部分可以存储在存储器中,由适当的指令执行系统,例如微处理器或者专用设计硬件来执行。本领域的技术人员可以理解上述的设备和方法可以使用计算机可执行指令和/或包含在处理器控制代码中来实现,例如在可编程的存储器或者诸如光学或电子信号载体的数据载体上提供了这样的代码。It should be noted that embodiments of the present invention may be implemented by hardware, software, or a combination of software and hardware. The hardware portion may be implemented using special purpose logic; the software portion may be stored in memory and executed by a suitable instruction execution system, such as a microprocessor or specially designed hardware. Those skilled in the art will appreciate that the apparatus and methods described above may be implemented using computer-executable instructions and/or embodied in processor control code, eg provided on a programmable memory or data carrier such as an optical or electronic signal carrier such code.

此外,尽管在附图中以特定顺序描述了本发明方法的操作,但是,这并非要求或者暗示必须按照该特定顺序来执行这些操作,或是必须执行全部所示的操作才能实现期望的结果。相反,流程图中描绘的步骤可以改变执行顺序。附加地或备选地,可以省略某些步骤,将多个步骤组合为一个步骤执行,和/或将一个步骤分解为多个步骤执行。还应当注意,根据本发明的两个或更多装置的特征和功能可以在一个装置中具体化。反之,上文描述的一个装置的特征和功能可以进一步划分为由多个装置来具体化。Furthermore, although the operations of the methods of the present invention are depicted in the figures in a particular order, this does not require or imply that the operations must be performed in the particular order, or that all illustrated operations must be performed to achieve desirable results. Rather, the steps depicted in the flowcharts may change the order of execution. Additionally or alternatively, certain steps may be omitted, multiple steps may be combined to be performed as one step, and/or one step may be decomposed to be performed as multiple steps. It should also be noted that features and functions of two or more devices according to the present invention may be embodied in one device. Conversely, the features and functions of one apparatus described above may be further divided into being embodied by multiple apparatuses.

虽然已经参考若干具体实施例描述了本发明,但是应当理解,本发明不限于所公开的具体实施例。本发明旨在涵盖所附权利要求的精神和范围内所包括的各种修改和等效布置。While the present invention has been described with reference to several specific embodiments, it is to be understood that the invention is not limited to the specific embodiments disclosed. The invention is intended to cover various modifications and equivalent arrangements included within the spirit and scope of the appended claims.

Claims (8)

1. A comb-shaped leakage mode resonance excitation method for inclined fiber bragg grating is characterized in that: including metal oxide film (2) of slope fiber grating (1) and nanometer magnitude thickness, slope fiber grating (1) is carved with and is write in single mode fiber's fibre core region, metal oxide film (2) coating is in the cladding surface of slope fiber grating (1), realizes arousing the comb-shaped leakage mode resonance of TE polarization of high strength in the broadband.
2. The tilted fiber grating comb-leaky-mode resonance excitation method as claimed in claim 1, wherein: the inclined fiber grating (1) is written in a fiber core area of the single-mode fiber by an ultraviolet exposure method, wherein the inclination angle theta of the grating is larger than 10 degrees, the length L of the grating is larger than 5 millimeters, and the period Lambda of the axial grating is larger than 100 nanometers.
3. The tilted fiber grating comb-leaky-mode resonance excitation method as claimed in claim 1, wherein: the metal oxide film (2) comprises indium tin oxide, tin dioxide, indium oxide, zinc oxide or titanium dioxide, and is coated on the surface of the cladding of the tilted fiber grating (1) by a magnetron sputtering method, a sol-gel method or a layer-by-layer self-assembly method, and the thickness of the metal oxide film (2) is more than 10 nanometers.
4. The tilted fiber grating comb-leaky-mode resonance excitation method as claimed in claim 1, wherein: the parameters of the inclined fiber grating (1) and the metal oxide film (2) are adjusted so that the comb-shaped leakage mode resonance of the inclined fiber grating can be excited in gas and liquid environments, wherein the parameters comprise the inclination angle of the grating, the axial period of the grating, the length of the grating, the modulation amplitude of the grating, and the metal oxide material or the thickness.
5. The utility model provides a narrow band polarization filter based on comb leakage mode resonance of slope fiber grating which characterized in that: the method comprises the following steps: broadband light source (3), polarization controller (4), single mode fiber jumper (5), metal oxide coating slope fiber grating (6) and spectral analysis appearance (7), wherein, broadband light source (3), polarization controller (4), metal oxide coating slope fiber grating (6) and spectral analysis appearance (7) loop through single mode fiber jumper (5) and connect, metal oxide coating slope fiber grating (6) is including slope fiber grating (1) and nanometer magnitude thickness's metal oxide film (2), slope fiber grating (1) is carved and is written in single mode fiber's fibre core region, metal oxide film (2) coating is in the cladding surface of slope fiber grating (1), broadband light source output unpolarized light, polarization controller (4) are used for adjusting unpolarized light for the linear polarization of single polarization direction, namely, the non-polarized light output by the broadband light source (3) is adjusted to be TE polarized light or TM polarized light, wherein the polarization direction of the TE polarized light is vertical to the writing direction of the inclined fiber grating (1), and the polarization direction of the TM polarized light is consistent with the writing direction of the inclined fiber grating (1).
6. The narrow-band polarization filter based on tilted fiber grating comb-like leaky-mode resonance as claimed in claim 5, wherein: the spectral range of the broadband light source covers the spectral response range of the metal oxide coated tilted fiber grating (6).
7. The utility model provides a sensing system based on comb leakage mode resonance of slope fiber grating which characterized in that:
the device comprises a broadband light source (3), a polarization controller (4), a single-mode optical fiber jumper (5), a metal oxide coated inclined fiber grating (6), a sample reaction vessel (8), a spectrum analyzer (7) and a computer (9), wherein the broadband light source (3), the polarization controller (4), the metal oxide coated inclined fiber grating (6) and the spectrum analyzer (7) are sequentially connected through the single-mode optical fiber jumper (5), and the spectrum analyzer (7) is connected with the computer (9) through a signal line;
the metal oxide coated inclined fiber grating (6) comprises an inclined fiber grating (1) and a metal oxide film (2) with nanometer-scale thickness, the inclined fiber grating (1) is inscribed in a fiber core area of a single-mode fiber, and the metal oxide film (2) is coated on the surface of a cladding of the inclined fiber grating (1);
the polarization controller (4) is used for adjusting non-polarized light into linearly polarized light with a single polarization direction perpendicular to the writing direction of the inclined fiber bragg grating (1), namely, the non-polarized light output by the broadband light source (3) is adjusted into TE polarized light;
the metal oxide coated inclined fiber bragg grating (6) is arranged in a sample to be detected, and the sample to be detected covers a sensing area of the metal oxide coated inclined fiber bragg grating (6);
the spectrum analyzer (7) is used for displaying the spectrum change of the metal oxide coated inclined fiber grating (6), inputting the collected sensing signals to the computer (9) for data processing, and obtaining the information of the sample to be detected by analyzing the change of the sensing signals.
8. The slanted fiber grating comb-leaky-mode-resonance-based sensing system of claim 7, wherein: the computer (9) is internally provided with at least one of two data processing methods, which comprise the following steps:
the method comprises the following steps: calculating the change of the whole spectrum envelope region acquired by the spectrum analyzer (7) along with the sample to be detected, thereby obtaining the information of the sample to be detected; region of spectral envelope
Figure FDA0002226317400000034
The change is calculated as follows:
Figure FDA0002226317400000031
in which ξu(lambda) and xil(lambda) represents upper and lower envelope curves of the transmission spectrum,and
Figure FDA0002226317400000033
respectively representing the upper and lower envelope curves, λ, of the transmitted spectrum in the initial ambient environmentminAnd λmaxRepresents a wavelength interval;
and secondly, monitoring the change of the single leakage mode resonance peak along with the sample to be detected, thereby obtaining the information of the sample to be detected.
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CN112146799A (en) * 2020-09-07 2020-12-29 桂林电子科技大学 Optical fiber sensing device for integrated measurement of torsion and humidity
CN112729122A (en) * 2020-12-02 2021-04-30 北京信息科技大学 Femtosecond laser direct writing-based inclined chirped fiber grating sensor testing method
KR20220102004A (en) * 2021-01-12 2022-07-19 한국과학기술연구원 Optical fiber in which grating structure array is patterned in its core, optical fiber device where photoelectric conversion thin film is formed on the optical fiber, and power supply system including the same
WO2023240488A1 (en) * 2022-06-15 2023-12-21 宁德时代新能源科技股份有限公司 Battery state detection method and apparatus, and device and computer-readable storage medium

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CN108680531A (en) * 2018-05-22 2018-10-19 温州大学 Titanium deoxid film coats inclined optical fiber grating index sensor and detecting system
CN108732101A (en) * 2018-07-27 2018-11-02 温州大学 Graphene integrates inclined optical fiber grating index sensor and sensitivity regulates and controls method
CN108872089A (en) * 2018-06-12 2018-11-23 温州大学 Inclined optical fiber grating refractive index sensing device and method are modulated containing inner cladding
CN109187442A (en) * 2018-09-12 2019-01-11 温州大学 Graphene enhances inclined optical fiber grating tunnelling ray resonant transducer and its detection system

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CN108680531A (en) * 2018-05-22 2018-10-19 温州大学 Titanium deoxid film coats inclined optical fiber grating index sensor and detecting system
CN108872089A (en) * 2018-06-12 2018-11-23 温州大学 Inclined optical fiber grating refractive index sensing device and method are modulated containing inner cladding
CN108732101A (en) * 2018-07-27 2018-11-02 温州大学 Graphene integrates inclined optical fiber grating index sensor and sensitivity regulates and controls method
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112146799A (en) * 2020-09-07 2020-12-29 桂林电子科技大学 Optical fiber sensing device for integrated measurement of torsion and humidity
CN112729122A (en) * 2020-12-02 2021-04-30 北京信息科技大学 Femtosecond laser direct writing-based inclined chirped fiber grating sensor testing method
CN112729122B (en) * 2020-12-02 2022-09-27 北京信息科技大学 Femtosecond laser direct writing-based inclined chirped fiber grating sensor testing method
KR20220102004A (en) * 2021-01-12 2022-07-19 한국과학기술연구원 Optical fiber in which grating structure array is patterned in its core, optical fiber device where photoelectric conversion thin film is formed on the optical fiber, and power supply system including the same
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WO2023240488A1 (en) * 2022-06-15 2023-12-21 宁德时代新能源科技股份有限公司 Battery state detection method and apparatus, and device and computer-readable storage medium

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