CN110684469A - Animal horn treating agent and animal horn treating method - Google Patents
Animal horn treating agent and animal horn treating method Download PDFInfo
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- CN110684469A CN110684469A CN201910865231.1A CN201910865231A CN110684469A CN 110684469 A CN110684469 A CN 110684469A CN 201910865231 A CN201910865231 A CN 201910865231A CN 110684469 A CN110684469 A CN 110684469A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/06—Other polishing compositions
- C09G1/08—Other polishing compositions based on wax
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B30B—PRESSES IN GENERAL
- B30B9/00—Presses specially adapted for particular purposes
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Abstract
The invention discloses an animal horn treatment agent and an animal horn treatment method, wherein the treatment agent comprises the following components in percentage by mass: 93-96% of alkane oil; 0.1-1% of D-panthenol; 3.55 to 8.5 percent of auxiliary agent. The invention has the following advantages: the alkane oil can be used as a solvent to dissolve the D-panthenol and the auxiliary agent, so that all the components can be uniformly mixed into a whole to ensure the treatment effect on the animal horn product. And the compatibility of the alkane oil and the animal horn is higher, and the surface of the animal horn can be fully wetted by the alkane oil, so that the D-panthenol and the auxiliary agent can fully contact the animal horn to improve the treatment effect. The D-panthenol has good permeability for the animal horn product, can improve the glossiness of the processed product, can enable the animal horn product to be rich in elasticity after being modified at high temperature, and can improve the toughness of the animal horn product. The angle of the animal is not easy to crack in the process of compression molding, and related products have good elasticity and toughness and are not easy to break, so that the processing performance is effectively improved, and the service life of the product is effectively prolonged.
Description
Technical Field
The invention relates to the technical field of animal horn product processing, in particular to an animal horn processing agent and an animal horn processing method.
Background
The animal horn product has the characteristics of nature, harmlessness, beauty, fashion and the like, has good collection value, and is used more frequently in daily life.
The ox horn spectacle frame is taken as an example, firstly, the ox horn has the medicinal effects of clearing away heat and toxic materials, nourishing yin and cooling blood, reducing blood pressure, removing rheumatism and the like, particularly contains natural cutin components, does not generate allergy and static phenomenon when contacting with human skin, and integrates the health care function and the artistic collection.
Chinese patent publication No. CN108669762A discloses a method for preparing a cow horn comb blank, which comprises the following steps: (1) manufacturing a primary blank: selecting the oxhorn with the shape and thickness suitable for manufacturing the comb, cleaning the selected oxhorn, naturally drying, simultaneously placing for 4-6 months, cutting off leftover materials, then cutting the oxhorn from the middle part along the direction from the oxhorn tip to the ox head to manufacture an oxhorn comb blank for later use; (2) softening treatment: putting the primary ox horn comb blank manufactured in the step 1 into heat conducting oil at the temperature of 125-plus-one 145 ℃, performing primary heating softening for 3-5min, then putting the softened primary ox horn comb blank into a constant-temperature hot pressing device, flattening and straightening by using the pressure of 8-10t, wherein the temperature of constant-temperature hot pressing is controlled to be between 135-plus-one 145 ℃, the time of flattening and straightening is controlled to be 2-3min, performing secondary heating treatment on the primary ox horn comb blank while flattening and straightening, and flattening and straightening for later use; (3) cooling and setting treatment: and transferring the softened horn comb primary blank into a cold pressing and shaping device, carrying out cold pressing and shaping treatment, and cooling to obtain the horn comb blank.
However, the softening treatment of the horn is only temporary softening for cooling and setting treatment, and the horn is still hardened after setting, so that the softening treatment has the defect of poor flexibility and needs to be improved.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide an animal horn treating agent which can improve the flexibility of animal horn products.
In order to achieve the purpose, the invention provides the following technical scheme:
an animal horn treating agent comprises the following components in percentage by mass:
93-96% of alkane oil;
0.1-1% of D-panthenol;
3.55 to 8.5 percent of auxiliary agent.
By adopting the technical scheme, the alkane oil can be used as a solvent to dissolve the D-panthenol and the auxiliary agent, so that all the components can be uniformly mixed into a whole to ensure the treatment effect on the animal horn product. And the compatibility of the alkane oil and the animal horn is higher, and the surface of the animal horn can be fully wetted by the alkane oil, so that the D-panthenol and the auxiliary agent can fully contact the animal horn to improve the treatment effect.
The D-panthenol has good permeability for the animal horn product, can improve the glossiness of the processed product, can enable the animal horn product to be rich in elasticity after being modified at high temperature, and can improve the toughness of the animal horn product. The angle of the animal is not easy to crack in the process of compression molding, and related products have good elasticity and toughness and are not easy to break, so that the processing performance is effectively improved, and the service life of the product is effectively prolonged.
Further, the alkane oil is No. 5 white oil.
By adopting the technical scheme, the white oil is a mixture of refined liquid hydrocarbons obtained from petroleum, generally consists of alkane and cycloalkane with the molecular weight of 300-400, and has the advantages of no color, no odor, no chemical inertness, excellent light and heat stability. The No. 5 white oil can form an oil film on the surface of an animal horn, and can improve the glossiness of an animal horn product besides endowing the animal horn product with a smooth feeling. In addition, the No. 5 white oil can play a lubricating role in the pressing process of the animal horn products, so that the ox horn products can be conveniently demoulded while cracking is avoided.
Further, the auxiliary agent comprises 3.0-5.0% of carnauba wax by mass percentage.
By adopting the technical scheme, the glossiness is improved to be a great function of the carnauba wax, so that the animal horn product can have good brightness. And the carnauba wax has good emulsibility, adhesiveness and lubricity, can improve the dispersibility of the components in the alkane oil, and simultaneously forms a layer of film on the surface of the animal horn product, so that the animal horn product can obtain better polishing and polishing effects in the later period.
Further, the auxiliary agent comprises 0.05-0.5% of 2, 6-di-tert-butyl-4-methylphenol by mass percent.
By adopting the technical scheme, the 2, 6-di-tert-butyl-4-methylphenol is also called as antioxidant BHT, and the antioxidant BHT is added into the alkane oil, so that the protein component in the animal horn can not be coked in the high-temperature treatment process, the brightness of the animal horn product is ensured, and the animal horn product is prevented from being embrittled to keep good elasticity and toughness.
Further, the auxiliary agent comprises 0.5-3.0% of white wax by mass percentage.
Through adopting above-mentioned technical scheme, white wax can show the fracture rate that reduces the animal angle at the in-process of suppressing the plate when improving animal angle goods polishing and polishing effect to show the production rate that reduces the waste material, and then reduction in production cost.
Another object of the present invention is to provide a method for treating animal corners, comprising the steps of,
s1, preheating corner materials: cutting the angle material into the required processing size, pressing into the required plate material, putting the plate material into an oven, adjusting the temperature to 80-100 ℃, and baking for 2-2.5 h;
s2, preparing a treating agent: heating the alkane oil to the temperature of 200-220 ℃, adding D-panthenol, carnauba wax, 2, 6-di-tert-butyl-4-methylphenol and white wax, uniformly stirring and preserving heat for 30-60 min;
s3, modified corner material: taking out the preheated angle material, soaking in the prepared treating agent, and keeping the temperature for 10-30 min;
s4, bending and shaping: putting the modified angle material into a press for bending and shaping, taking out after shaping for 3-5min, and cooling for 20-30 min;
and S5, finishing.
Through adopting above-mentioned technical scheme, preheat through the diagonal material for the angle material can be fully heated and take place to soften, with improve the processing property, can avoid the too big and fracture that leads to of the difference in temperature between angle material and the treating agent simultaneously. After the angle material is modified by the treating agent, the angle material is softened by heating and endowed with good elasticity and toughness, the fracture rate of the angle material is obviously reduced in the bending and shaping process, and a finished product can obtain certain elastic deformation performance.
Further, S1 and S2 can be performed simultaneously or in an interchangeable order.
Further, S5, finishing: laser cutting, engraving, polishing and polishing are carried out.
In conclusion, the invention has the following beneficial effects:
1. the alkane oil can be used as a solvent to dissolve the D-panthenol and the auxiliary agent, so that all the components can be uniformly mixed into a whole to ensure the treatment effect on the animal horn product. And the compatibility of the alkane oil and the animal horn is higher, and the surface of the animal horn can be fully wetted by the alkane oil, so that the D-panthenol and the auxiliary agent can fully contact the animal horn to improve the treatment effect. The D-panthenol has good permeability for the animal horn product, can improve the glossiness of the processed product, can enable the animal horn product to be rich in elasticity after being modified at high temperature, and can improve the toughness of the animal horn product. The angle of the animal is not easy to crack in the process of compression molding, and related products have good elasticity and toughness and are not easy to break, so that the processing performance is effectively improved, and the service life of the product is effectively prolonged.
2. The improvement of the glossiness is a great function of the carnauba wax, so that the animal horn product can have good brightness. And the carnauba wax has good emulsibility, adhesiveness and lubricity, can improve the dispersibility of the components in the alkane oil, and simultaneously forms a layer of film on the surface of the animal horn product, so that the animal horn product can obtain better polishing and polishing effects in the later period.
The 3, 6-di-tert-butyl-4-methylphenol is also called antioxidant BHT, and the antioxidant BHT is added into the alkane oil, so that protein components in animal corners can not be coked in the high-temperature treatment process, the brightness of the animal corner products is ensured, and the animal corner products are prevented from being embrittled to keep good elasticity and toughness.
4. The white wax can remarkably reduce the cracking rate of the animal horn in the plate pressing process while improving the polishing and polishing effects of the animal horn product, thereby remarkably reducing the generation rate of waste materials and further reducing the production cost.
Drawings
FIG. 1 is a flow chart of a method provided by the present invention.
Detailed Description
The present invention will be described in further detail with reference to the following drawings and examples.
Examples
Example 1
An animal horn conditioning agent comprises the raw materials in percentage by mass as shown in table 1.
An animal horn processing method applying the animal horn processing agent takes the preparation of a horn glasses leg as an example, as shown in figure 1, and comprises the following steps:
s1, preheating corner materials: cutting the ox horn into the size and the shape required to be processed, pressing the ox horn into a required plate material, putting the plate material into an oven, adjusting the temperature to 80 ℃, and baking the plate material for 2.5 hours to ensure that the ox horn plate material is heated and softened;
s2, preparing a treating agent: heating the alkane oil to 200 ℃, adding the D-panthenol, the carnauba wax, the antioxidant and the white wax, uniformly stirring and preserving heat for 30 min;
s3, modified corner material: taking out the preheated ox horn plate, putting the preheated ox horn plate into a prepared treating agent for soaking, and preserving heat for 10min to obtain a modified ox horn plate;
s4, bending and shaping: putting the modified ox horn plate into a press for bending and shaping to ensure that the glasses legs obtain the bending radian adapting to the head of a human body, taking out after shaping for 3min, and cooling for 20 min;
s5, finishing: and carrying out laser cutting, carving, polishing and polishing to obtain a finished product.
Wherein, S1 and S2 can be performed simultaneously or in an interchangeable order.
The alkane oil adopts No. 5 white oil, and the antioxidant adopts 2, 6-di-tert-butyl-4-methylphenol (namely antioxidant BHT).
Example 2
An animal horn conditioning agent comprises the raw materials in percentage by mass as shown in table 1.
An animal horn processing method applying the animal horn processing agent takes the preparation of a horn glasses leg as an example, and comprises the following steps:
s1, preheating corner materials: cutting the ox horn into the size and the shape required to be processed, pressing the ox horn into a required plate material, putting the plate material into an oven, adjusting the temperature to 90 ℃, and baking the plate material for 2.5 hours to ensure that the ox horn plate material is heated and softened;
s2, preparing a treating agent: heating the alkane oil to 210 ℃, adding the D-panthenol, the carnauba wax, the antioxidant and the white wax, uniformly stirring and keeping the temperature for 45 min;
s3, modified corner material: taking out the preheated ox horn plate, putting the preheated ox horn plate into a prepared treating agent for soaking, and preserving heat for 20min to obtain a modified ox horn plate;
s4, bending and shaping: putting the modified ox horn plate into a press for bending and shaping to ensure that the glasses legs obtain the bending radian adapting to the head of a human body, taking out after shaping for 4min, and cooling for 25 min;
s5, finishing: and carrying out laser cutting, carving, polishing and polishing to obtain a finished product.
Wherein, S1 and S2 can be performed simultaneously or in an interchangeable order.
The alkane oil adopts No. 5 white oil, and the antioxidant adopts 2, 6-di-tert-butyl-4-methylphenol (namely antioxidant BHT).
Example 3
An animal horn conditioning agent comprises the raw materials in percentage by mass as shown in table 1.
An animal horn processing method applying the animal horn processing agent takes the preparation of a horn glasses leg as an example, and comprises the following steps:
s1, preheating corner materials: cutting the ox horn into the size and the shape required to be processed, pressing the ox horn into a required plate material, putting the plate material into an oven, adjusting the temperature to 100 ℃, and baking for 2 hours to ensure that the ox horn plate material is heated and softened;
s2, preparing a treating agent: heating the alkane oil to 220 ℃, adding the D-panthenol, the carnauba wax, the antioxidant and the white wax, uniformly stirring and preserving heat for 60 min;
s3, modified corner material: taking out the preheated ox horn plate, putting the preheated ox horn plate into a prepared treating agent for soaking, and preserving heat for 30min to obtain a modified ox horn plate;
s4, bending and shaping: putting the modified ox horn plate into a press for bending and shaping to ensure that the glasses legs obtain the bending radian adapting to the head of a human body, taking out after shaping for 5min, and cooling for 30 min;
s5, finishing: and carrying out laser cutting, carving, polishing and polishing to obtain a finished product.
Wherein, S1 and S2 can be performed simultaneously or in an interchangeable order.
The alkane oil adopts No. 5 white oil, and the antioxidant adopts 2, 6-di-tert-butyl-4-methylphenol (namely antioxidant BHT).
Example 4
An animal horn conditioning agent comprises the raw materials in percentage by mass as shown in table 1.
An animal horn processing method applying the animal horn processing agent takes the preparation of a horn glasses leg as an example, and comprises the following steps:
s1, preheating corner materials: cutting the ox horn into the size and the shape required to be processed, pressing the ox horn into a required plate material, putting the plate material into an oven, adjusting the temperature to 100 ℃, and baking the plate material for 2.5 hours to ensure that the ox horn plate material is heated and softened;
s2, preparing a treating agent: heating the alkane oil to 210 ℃, adding the D-panthenol, the carnauba wax, the antioxidant and the white wax, uniformly stirring and keeping the temperature for 50 min;
s3, modified corner material: taking out the preheated ox horn plate, putting the preheated ox horn plate into a prepared treating agent for soaking, and preserving heat for 20min to obtain a modified ox horn plate;
s4, bending and shaping: putting the modified ox horn plate into a press for bending and shaping to ensure that the glasses legs obtain the bending radian adapting to the head of a human body, taking out after shaping for 4min, and cooling for 25 min;
s5, finishing: and carrying out laser cutting, carving, polishing and polishing to obtain a finished product.
Wherein, S1 and S2 can be performed simultaneously or in an interchangeable order.
The alkane oil adopts No. 5 white oil, and the antioxidant adopts 2, 6-di-tert-butyl-4-methylphenol (namely antioxidant BHT).
Example 5
The difference from example 2 is that the animal horn treating agent raw materials are shown in table 1 in mass percentage.
Wherein, the alkane oil adopts No. 120 solvent oil.
Example 6
The difference from example 2 is that the animal horn treating agent raw materials are shown in table 1 in mass percentage.
Wherein, the carnauba wax is replaced with the same amount of white wax.
Example 7
The difference from example 2 is that the animal horn treating agent raw materials are shown in table 1 in mass percentage.
Wherein the white wax is replaced by the same amount of carnauba wax.
Example 8
The difference from example 2 is that the animal horn treating agent raw materials are shown in table 1 in mass percentage.
Wherein the antioxidant is antioxidant 1010.
Comparative example
Comparative example 1
The difference from example 2 is that the animal horn treating agent raw materials are shown in table 1 in mass percentage.
Wherein D-panthenol is replaced with an equal amount of No. 5 white oil.
Comparative example 2
The difference from example 2 is that the horn was not modified with a treatment agent, i.e. S2 and S3 were omitted.
Performance test
Modifying each group of angle materials by adopting a corresponding treating agent, and processing by adopting a corresponding processing method (the step of bending and shaping is cancelled), wherein the specification of a cut and pressed plate material sample is as follows: the length is 150mm, the width is 10mm, the thickness is 4mm, and appearance detection and bending performance detection are carried out on each group of ox horn plate samples.
And (3) appearance detection: the appearance of each group of ox horn plate samples and the fracture after the fracture are recorded through observation and compared, and the observation results are shown in table 2.
And (3) detecting the bending property: the method comprises the steps that 10mm clamping areas are drawn at two ends of a horn plate sample, an inverted protractor is fixed at the bottom of the plate sample, the plate sample coincides with 0-degree scale lines of the protractor, the clamping area at the left end of the plate sample is fixed through a clamping piece, a detector holds the clamping area at the other side with the right hand and applies bending force to the plate sample until the plate sample is broken, a recorder observes the bending angle of the plate and records the bending angle during the breaking, 5 sample tests are conducted on each group, the average bending angle is calculated, and the test results are shown in table 2.
Table 1 (animal horn treating agent formulation table,%)
Table 2 (appearance and performance detecting meter)
The present embodiment is only for explaining the present invention, and it is not limited to the present invention, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present invention.
Claims (8)
1. An animal horn conditioning agent, comprising: the composite material comprises the following components in percentage by mass:
93-96% of alkane oil;
0.1-1% of D-panthenol;
3.55 to 8.5 percent of auxiliary agent.
2. The animal horn treatment of claim 1, wherein: the alkane oil adopts No. 5 white oil.
3. The animal horn treatment of claim 1, wherein: the auxiliary agent comprises 3.0-5.0% of carnauba wax by mass percentage.
4. The animal horn treatment of claim 1, wherein: the auxiliary agent comprises 0.05-0.5% of 2, 6-di-tert-butyl-4-methylphenol by mass percent.
5. The animal horn treatment of claim 1, wherein: the auxiliary agent comprises 0.5-3.0% of white wax by mass percent.
6. The animal corner treatment method of any one of claims 1-5, wherein: comprises the following steps of (a) carrying out,
s1, preheating corner materials: cutting the angle material into the required processing size, pressing into the required plate material, putting the plate material into an oven, adjusting the temperature to 80-100 ℃, and baking for 2-2.5 h;
s2, preparing a treating agent: heating the alkane oil to the temperature of 200-220 ℃, adding D-panthenol, carnauba wax, 2, 6-di-tert-butyl-4-methylphenol and white wax, uniformly stirring and preserving heat for 30-60 min;
s3, modified corner material: taking out the preheated angle material, soaking in the prepared treating agent, and keeping the temperature for 10-30 min;
s4, bending and shaping: putting the modified angle material into a press for bending and shaping, taking out after shaping for 3-5min, and cooling for 20-30 min;
and S5, finishing.
7. The animal corner processing method according to claim 6, characterized in that: s1 and S2 can be performed simultaneously or in an interchangeable order.
8. The animal corner processing method according to claim 6, characterized in that: s5, finishing: laser cutting, engraving, polishing and polishing are carried out.
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| CN1621247A (en) * | 2005-01-07 | 2005-06-01 | 许玉奇 | Making process of embossment board picture with animal horns and bones |
| CN1816287A (en) * | 2003-01-31 | 2006-08-09 | 宝洁公司 | Means for improving the appearance of mammalian keratinous tissue |
| CN102078069A (en) * | 2010-12-20 | 2011-06-01 | 娄作富 | Method for processing yak horn comb blank |
| CN102300551A (en) * | 2009-01-29 | 2011-12-28 | 宝洁公司 | Regulation of mammalian keratinous tissue using skin and/or hair care actives |
| JP2012019753A (en) * | 2010-07-16 | 2012-02-02 | Yamatoya:Kk | Processing method for shaving finished dried bonito to optimum state |
| CN103789465A (en) * | 2012-11-05 | 2014-05-14 | 中国石油化工股份有限公司 | Leather greasing treatment agent and preparation method thereof |
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2019
- 2019-09-12 CN CN201910865231.1A patent/CN110684469A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1816287A (en) * | 2003-01-31 | 2006-08-09 | 宝洁公司 | Means for improving the appearance of mammalian keratinous tissue |
| CN1621247A (en) * | 2005-01-07 | 2005-06-01 | 许玉奇 | Making process of embossment board picture with animal horns and bones |
| CN102300551A (en) * | 2009-01-29 | 2011-12-28 | 宝洁公司 | Regulation of mammalian keratinous tissue using skin and/or hair care actives |
| JP2012019753A (en) * | 2010-07-16 | 2012-02-02 | Yamatoya:Kk | Processing method for shaving finished dried bonito to optimum state |
| CN102078069A (en) * | 2010-12-20 | 2011-06-01 | 娄作富 | Method for processing yak horn comb blank |
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Application publication date: 20200114 |