CN110669390A - Water-based multifunctional self-drying coloring base material and preparation method thereof - Google Patents
Water-based multifunctional self-drying coloring base material and preparation method thereof Download PDFInfo
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- CN110669390A CN110669390A CN201910852589.0A CN201910852589A CN110669390A CN 110669390 A CN110669390 A CN 110669390A CN 201910852589 A CN201910852589 A CN 201910852589A CN 110669390 A CN110669390 A CN 110669390A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/43—Thickening agents
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/45—Anti-settling agents
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/10—Transparent films; Clear coatings; Transparent materials
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
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Abstract
The invention discloses a water-based multifunctional self-drying coloring base material which consists of a film forming material, an auxiliary agent and water and is prepared from the following components in parts by weight. The invention also discloses a preparation method of the water-based multifunctional self-drying coloring base material. The invention has the beneficial effects that: (1) the emulsion is used as a film forming material, and has self-drying property, good transparency, excellent adhesive force and no delamination phenomenon; (2) the paint has a uniform paint film, is uniform in coloring and has no flowering phenomenon; (3) the moisture retention and slow drying performance is achieved, the opening time is long, the construction tolerance is good, and the construction technical requirement on constructors is low; (4) the paint has multiple functions, and can meet different construction requirements, such as wiping, brushing, spraying and beating; (5) the paint is suitable for coloring and wiping of most woodenware coatings on the market, and has a high use value.
Description
Technical Field
The invention relates to the field of coatings, in particular to a water-based multifunctional self-drying coloring base material with multifunctional application, good transparency, uniform coloring, excellent adhesive force and good construction tolerance and a preparation method thereof.
Technical Field
The water-based multifunctional self-drying coloring base material is used as paint film coloring paint, also called as 'glaze', is matched with color paste to prepare different colors and is mainly used for American antique painting and floor painting; the application adopts the mode of brushing, spraying, wiping or beating points. The water-based multifunctional self-drying coloring base material flexibly reserves the residual amount of the coloring liquid according to the requirements of the color depth, and after the coloring liquid is constructed, steel velvet or loofah is used for carrying out light and shade contrast treatment along wood grains, so that the effects of soft and natural color are achieved, and the classical charm is revealed.
Most of the existing coloring base materials are made of oily transparent or semitransparent pigments, and have common transparency and no dryness, so that the problems of paint film delamination and the like are caused. With the demand of the market on environment-friendly products, some aqueous coloring base materials appear in different regions throughout the country, but the single use affects the wider popularization and application of the products, and the existing aqueous coloring base materials have the defects of poor transparency, coloring and blooming, easiness in delamination, poor construction tolerance and the like. Therefore, there is an urgent need to provide multi-purpose colored base materials to meet the urgent market demand. Namely, the development of a multifunctional water-based coloring base material with good transparency, uniform coloring, excellent adhesion and good construction tolerance is very necessary.
Disclosure of Invention
One of the purposes of the invention is to provide a multifunctional water-based self-drying coloring base material with multiple functions, transparent paint film, uniform coloring, excellent adhesive force and good construction compatibility aiming at the defects of single use, poor transparency, coloring and floating, easy delamination, poor construction compatibility and the like of the existing coloring base material.
The second object of the present invention is to provide a method for preparing the above aqueous multifunctional self-drying coloring base material.
In order to achieve the purpose, the invention adopts the following technical scheme: the water-based multifunctional self-drying coloring base material consists of a film forming material, an auxiliary agent and water, and specifically comprises the following components in parts by weight:
preferably, the water-based multifunctional self-drying coloring base material consists of the following components in parts by weight:
the emulsion can be selected from one or more of emulsions manufactured by basf (China) Limited liability company under the number JONCRYL 95 or Joncryl 8383, and emulsions manufactured by Wanhua chemical (cigarette Tai) sales Limited company under the number 5530.
The multifunctional adjuvant may be 2-amino-2-methyl-1-propanol, preferably 2-amino-2-methyl-1-propanol from Dow chemical, China, Inc., under the trade name AMP-95.
The film forming aid can be one or two of dipropylene glycol butyl ether (DPnB) or dipropylene glycol methyl ether (DPM), preferably dipropylene glycol butyl ether and dipropylene glycol methyl ether of Dow chemical, China Limited.
The alcoholic solvent may be 1, 2-propanediol, preferably 1, 2-propanediol from the dow chemical china limited company.
The defoaming agent is a molecular defoaming agent and can be selected from the defoaming agents with the reference number of ST2410AC, which are produced by the company of GmbH (China). The molecular defoaming agent is beneficial to reducing system micro bubbles and mechanical bubbles, keeps stable production and has no obvious bubbles in the using process.
The thickener is polyether polyurethane thickener, and can be one or two of polyether polyurethane thickeners of Homing Siemens 299 or DeuRheo WT108f in chemical industry.
The anti-settling agent may be selected from bentonite thickeners, selected from bentonite ATT-50 manufactured by Limited liability company of Bass Fuv (China). The bentonite thickener has obvious thixotropic effect, can effectively improve the viscosity and the anti-settling property of the system, and ensures the stable viscosity of the system after storage.
The bactericide is a preservative in the tank, and can be selected from one or two of the bactericides with the reference numbers ROCIMA631 and Bioban 586 manufactured by the Dow chemical China Co.
The mildew preventive can be one or two of the mildew preventives which are produced by Tokaiyi Chemicals Co.Ltd in Shanghai and are marked as PW40 and PP 678.
The humectant can be selected from humectant XH-CN-80 of Dongguan new Ye new material science and technology company, can mix and compatibilize water molecules and alcohols solvent in a molecular structure, does not cause layering, effectively buffers the volatilization speed of the water molecules and the solvent, and simultaneously slows down the film forming speed of the emulsion and prolongs the opening time.
The preparation method of the water-based multifunctional self-drying coloring base material comprises the following steps:
(1) feeding in the first stage: adding the emulsion and all water into a dispersion cylinder, then respectively adding the multifunctional additive, the film-forming additive, the alcohol solvent, the defoaming agent, the thickening agent and the anti-settling agent, fully stirring and mixing to form a mixture, controlling the rotation speed of mixing and stirring to be 1000-1500rpm, simultaneously keeping dispersion for 10-15min, then grinding to the fineness of 30-50 mu m, and entering the next stage;
(2) feeding in the second stage: adding a bactericide, a mildew preventive and a moisturizing agent into a dispersion cylinder, controlling the rotation speed to be 1000-1500rpm, simultaneously treating by using ultrasonic waves with the frequency of 150-350 khz and the power density of 40-80 w/L, keeping for 10-15min, and then grinding to the fineness of 20-30 mu m to obtain the water-based multifunctional self-drying coloring base material;
(3) packaging: the filter cloth was 80 mesh filter cloth and filled in a 20L paint can as required.
Preferably, the frequency of ultrasonic treatment is 200-300 khz, the power density is 50-70 w/L, and the ultrasonic treatment can effectively improve the synergistic effect among the components, improve the uniformity and integrally improve the corresponding performance of the invention.
When in use, the coloring base material and the glaze color paste are uniformly mixed according to the ratio of 100:5-20, the water adding proportion is determined according to the coloring depth, the construction is carried out according to the construction mode required by customers, the water-based clear finish paint is sprayed according to the conventional construction procedure, and after the water-based clear finish paint is dried, the interlayer has very good adhesion. The difference of the adhesion force of the invention and the competitive products is small when the lattice hair is used for testing, but the invention has obvious advantages when the paint film is cut by an art designer knife and peeled by hands.
Compared with the existing preparation method, the invention has the beneficial effects that: (1) the emulsion is used as a film forming object, has self-drying property, good transparency, excellent adhesive force and no delamination phenomenon; (2) the coating has a uniform paint film, is uniform in coloring and has no flowering phenomenon; (3) the moisture retention and slow drying performance is achieved, the opening time is long, the construction tolerance is good, and the construction technical requirement on constructors is low; (4) the paint has multiple functions, and can meet different construction requirements, such as wiping, brushing, spraying and beating; (5) is suitable for coloring and wiping of most woodenware coatings on the market, and has great use value.
Drawings
FIG. 1 is a photograph 1 of a rubbing color of an aqueous multifunctional self-drying coloring base according to the present invention;
FIG. 2 is a photograph 2 of a rubbing color of the water-based multifunctional self-drying coloring base material of the present invention;
FIG. 3 is a photograph 3 of a rubbing color of the water-based multifunctional self-drying coloring base material of the present invention;
FIG. 4 is a dot-colored photograph of the aqueous multifunctional self-drying coloring base of the present invention;
FIG. 5 is a dot-colored photograph 2 of the aqueous multifunctional self-drying coloring base material of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings and specific embodiments, and it is to be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without any inventive step based on the embodiments of the present invention, are within the scope of the present invention.
Example 1
A multifunctional self-drying coloring base material comprises the following components in parts by weight:
the preparation method of the water-based multifunctional self-drying coloring base material comprises the following preparation steps:
(1) feeding in the first stage: adding the emulsion and all water into a dispersion cylinder, respectively adding the multifunctional auxiliary agent, the film-forming auxiliary agent, the alcohol solvent, the defoaming agent, the thickening agent and the anti-settling agent, fully stirring and mixing to form a mixture, controlling the rotation speed of mixing and stirring to be 1100rpm, simultaneously keeping dispersion for 11min, then grinding to the fineness of 35 mu m, and entering the next stage;
(2) feeding in the second stage: adding bactericide, mildew preventive and humectant into a dispersion tank, controlling the rotation speed at 1100rpm, treating with ultrasonic wave with frequency of 160khz and power density of 50w/L for 11min, and grinding to fineness of 25 μm to obtain water-based multifunctional self-drying coloring base material;
(3) packaging: the base material was filtered through an 80 mesh filter cloth as required and filled in a 20L paint can.
Example 2
A multifunctional self-drying coloring base material comprises the following components in parts by weight:
the preparation method of the water-based multifunctional self-drying coloring base material comprises the following preparation steps:
(1) feeding in the first stage: adding the emulsion and all water into a dispersion cylinder, respectively adding the multifunctional auxiliary agent, the film-forming auxiliary agent, the alcohol solvent, the defoaming agent, the thickening agent and the anti-settling agent, fully stirring and mixing to form a mixture, controlling the rotation speed of mixing and stirring to 1400rpm, simultaneously keeping dispersion for 14min, then grinding to the fineness of 45 mu m, and entering the next stage;
(2) feeding in the second stage: adding bactericide, mildew preventive and humectant into a dispersion tank, controlling the rotation speed at 1400rpm, treating with ultrasonic wave with frequency of 340khz and power density of 70w/L for 14min, and grinding to fineness of 30 μm to obtain water-based multifunctional self-drying coloring base material;
(3) packaging: the base material was filtered through an 80 mesh filter cloth as required and filled in a 20L paint can.
Example 3
A multifunctional self-drying coloring base material comprises the following components in parts by weight:
the preparation method of the water-based multifunctional self-drying coloring base material comprises the following preparation steps:
(1) feeding in the first stage: adding the emulsion and all water into a dispersion cylinder, respectively adding the multifunctional auxiliary agent, the film-forming auxiliary agent, the alcohol solvent, the defoaming agent, the thickening agent and the anti-settling agent, fully stirring and mixing to form a mixture, controlling the rotation speed of mixing and stirring at 1300rpm, simultaneously keeping dispersion for 13min, then grinding to the fineness of 40 mu m, and entering the next stage.
(2) Feeding in the second stage: adding bactericide, mildew preventive and humectant into a dispersion tank, controlling the rotation speed at 1300rpm, treating with ultrasonic waves with the frequency of 250khz and the power density of 60w/L for 13min, and grinding to the fineness of 25 μm to obtain the water-based multifunctional self-drying coloring base material.
(3) Packaging: the base material was filtered through an 80 mesh filter cloth as required and filled in a 20L paint can.
When in use, the coloring base material and the glaze color paste are uniformly mixed, and the painting construction is carried out, after the painting construction, the water-based clear finish paint is sprayed according to the conventional construction procedure, and after the painting construction is dried, the interlayer has very good adhesive force. The difference between the adhesion force of the invention and that of a competitive product is small when the lattice-cutting hair is used for testing, but the invention has obvious advantages when an art designer cuts a paint film and peels off by hands.
Effect test
The comparison of the product of the present invention obtained in the above examples with the existing on-sale reference product according to the corresponding standard is shown in the following table, and the corresponding effects are shown in fig. 1-4, which have excellent effects.
The following can be obtained by the performance test data: the aqueous multifunctional coloring base material prepared by the embodiment of the invention has the following performance characteristics: (1) after the coloring base material is constructed and dried, the adhesive force of the sprayed water-based finish reaches level 1, the adhesive force of the finish is not influenced, and the commercial product takes grease as the base material, and the severe delamination occurs at the thicker part of construction, so that the overall performance of a paint film is influenced; (2) after the coloring base material is constructed, the emulsion particles are uniformly distributed on the surface of a paint film, the film is formed uniformly, the sprayed finish paint has no flowering phenomenon, and the coloring is uniform; (3) after the base material is colored, the base material is dried completely, and water-based clear finish paint is sprayed, so that the color plate has good coloring transparency and clear wood grains; (4) the construction is wide and compatible, and can meet different construction requirements, such as brushing coloring, spraying coloring, beating point coloring and the like.
The emulsion is added in the formula of the invention, so that the adhesive force is good, and the paint can be suitable for coloring different paint films, so that the interlayer adhesive force of the coloring base material is excellent. In the aspect of construction wide compatibility, firstly, different film-forming aids and alcohol solvents are added, so that the opening time is prolonged, and meanwhile, the stepped drying rate of the solvents in the system enables the surface drying time and the actual drying time of a paint film to be close; the humectant is added, so that the solvent of water molecules and alcohols is mixed and compatible in a molecular structure, the volatilization speed of the water molecules and the solvent is effectively buffered, the film forming speed of the emulsion is reduced, and the opening time is further prolonged. In general, after the emulsion is combined with the film-forming assistant, the alcohol solvent and the humectant, the emulsion takes effect synergistically, so that a paint film has the advantages of good transparency, uniform coloring, excellent adhesive force and high construction latitude, and is suitable for wiping coloring, brushing coloring, spraying coloring and dot coloring.
The above description is only a preferred embodiment of the present invention, and the scope of the present invention should not be limited thereby, and all the simple equivalent changes and modifications made in the claims and the description of the present invention are within the scope of the present invention.
Claims (8)
1. The water-based multifunctional self-drying coloring base material is characterized by comprising the following components in parts by weight:
2. the aqueous multifunctional self-drying coloring base according to claim 1, wherein said emulsion is selected from one or a combination of two or more of the emulsions manufactured by basf (china) llc under the reference JONCRYL 95 or JONCRYL 8383 and the emulsions manufactured by wawa chemical (cigarette bench) sales ltd under the reference 5530.
3. The aqueous multifunctional self-drying coloring base material according to claim 1, wherein the multifunctional auxiliary agent is 2-amino-2-methyl-1-propanol; the film-forming assistant is one or the combination of two of dipropylene glycol butyl ether or dipropylene glycol methyl ether; the alcohol solvent is 1, 2-propylene glycol.
4. The aqueous multifunctional self-drying coloring base according to claim 1, wherein said antifoaming agent is selected from the group consisting of antifoaming agents of ST2410AC, manufactured by basf (china) llc; the thickener is selected from one or two of polyether polyurethane thickeners of Hamming Smoded chemical industry, with the reference number RHELATE 299 or DeuRheo WT108 f.
5. The aqueous multifunctional self-drying color base according to claim 1, wherein the anti-settling agent is selected from bentonite ATT-50 manufactured by Pasteur (China) Limited; the bactericide is selected from one or two of the bactericides with the reference numbers ROCIMA631 and Bioban 586 manufactured by the Dow chemical China Co., Ltd; the mildew preventive is one or two of the mildew preventives which are produced by Shanghai Trojan chemical company Limited and are marked as PW40 and PP 678.
6. The aqueous multifunctional self-drying coloring base according to claim 1, wherein said humectant is selected from the group consisting of the humectants XH-CN-80 from eastern skimmia new materials technology limited.
7. The preparation method of the water-based multifunctional self-drying coloring base material as claimed in claim 1, characterized by comprising the following steps:
(1) feeding in the first stage: adding the emulsion and all water into a dispersion cylinder, then respectively adding the multifunctional additive, the film-forming additive, the alcohol solvent, the defoaming agent, the thickening agent and the anti-settling agent, fully stirring and mixing to form a mixture, controlling the rotation speed of mixing and stirring to be 1000-1500rpm, simultaneously keeping dispersion for 10-15min, and then grinding to the fineness of 30-50 mu m;
(2) feeding in the second stage: adding a bactericide, a mildew preventive and a humectant into a dispersion cylinder, controlling the rotation speed to be 1000-1500rpm, simultaneously treating by ultrasonic waves with the frequency of 150-350 khz and the power density of 40-80 w/L, keeping for 10-15min, and then grinding to the fineness of 20-30 mu m.
8. The method for preparing the water-based multifunctional self-drying coloring base material as claimed in claim 7, wherein the frequency of ultrasonic treatment is 200-300 khz, and the power density is 50-70 w/L.
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0614955B1 (en) * | 1993-03-08 | 1998-05-06 | Minnesota Mining And Manufacturing Company | Stain-resistant latex paint |
| CN102675986A (en) * | 2012-05-23 | 2012-09-19 | 江苏海田技术有限公司 | Water-based coloring base material and preparation method thereof |
| CN104046240A (en) * | 2014-07-02 | 2014-09-17 | 江苏海田技术有限公司 | Aqueous color-wrapping glaze base material and preparation method thereof |
| CN105440924A (en) * | 2015-12-09 | 2016-03-30 | 三棵树涂料股份有限公司 | Waterborne woodenware bleeding-resistant seal primer |
| CN106046977A (en) * | 2016-06-03 | 2016-10-26 | 上海展辰涂料有限公司 | Water-based woodware coloring paint with low VOC (volatile organic compounds) |
| CN108285710A (en) * | 2018-02-09 | 2018-07-17 | 上海马利画材销售有限公司 | A kind of color compositions and preparation method thereof and purposes |
| CN110105854A (en) * | 2019-04-21 | 2019-08-09 | 嘉宝莉化工集团股份有限公司 | A kind of woodenware antique coating coating and preparation method thereof |
-
2019
- 2019-09-10 CN CN201910852589.0A patent/CN110669390A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0614955B1 (en) * | 1993-03-08 | 1998-05-06 | Minnesota Mining And Manufacturing Company | Stain-resistant latex paint |
| CN102675986A (en) * | 2012-05-23 | 2012-09-19 | 江苏海田技术有限公司 | Water-based coloring base material and preparation method thereof |
| CN104046240A (en) * | 2014-07-02 | 2014-09-17 | 江苏海田技术有限公司 | Aqueous color-wrapping glaze base material and preparation method thereof |
| CN105440924A (en) * | 2015-12-09 | 2016-03-30 | 三棵树涂料股份有限公司 | Waterborne woodenware bleeding-resistant seal primer |
| CN106046977A (en) * | 2016-06-03 | 2016-10-26 | 上海展辰涂料有限公司 | Water-based woodware coloring paint with low VOC (volatile organic compounds) |
| CN108285710A (en) * | 2018-02-09 | 2018-07-17 | 上海马利画材销售有限公司 | A kind of color compositions and preparation method thereof and purposes |
| CN110105854A (en) * | 2019-04-21 | 2019-08-09 | 嘉宝莉化工集团股份有限公司 | A kind of woodenware antique coating coating and preparation method thereof |
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Application publication date: 20200110 |