CN110606766A - Preparation method of multi-melting composite non-combustible insulation board - Google Patents
Preparation method of multi-melting composite non-combustible insulation board Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/04—Portland cements
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/40—Porous or lightweight materials
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/20—Mortars, concrete or artificial stone characterised by specific physical values for the density
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/30—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values
- C04B2201/32—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values for the thermal conductivity, e.g. K-factors
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
Abstract
The invention discloses a preparation method of a multi-melting composite non-combustible insulation board, which adopts the following raw materials in parts by weight: 8-15 parts of polyphenyl particles, 100-150 parts of portland cement, 1-5 parts of a curing agent, 5-10 parts of acrylic emulsion, 1-3 parts of a silicone waterproofing agent, 50-80 parts of inorganic micro silicon powder, 1-3 parts of an ammonium polyphosphate flame retardant, 1-2 parts of PP (polypropylene) reinforced fiber and 48-100 parts of water, is suitable for various newly-built buildings and old house reconstruction outer wall heat insulation systems, and has the advantages of good heat insulation effect, high bonding strength, long service life, fire resistance, heat insulation resistance, no pollution, strong tensile resistance, light weight, simple production and capability of reducing the operation cost of enterprises.
Description
Technical Field
The invention relates to the field of building structures, in particular to a preparation method of a multi-melting composite non-combustible insulation board.
Background
The heat insulation materials used in the market at present comprise inorganic heat insulation materials and organic heat insulation materials, the organic heat insulation materials have good heat insulation performance, light capacity and easy processing, but have poor stability and poor ageing resistance and are easy to deform, and perlite, silica, cotton, bromine foam glass, slag cotton, foamed Australian mud plates and other fire prevention functions are covered in the inorganic heat insulation materials.
At present, two types of organic heat-insulating boards are available in the market, one type of organic heat-insulating board is formed by combining inorganic materials such as inorganic component materials including glass wool, rock wool boards, foamed cement, foamed glass and the like, the organic heat-insulating board has the defects of high cost and price, the construction is complex, for example, mortar which is about a few centimeters more than the outer wall is needed in the construction, the work and the waste materials are wasted, the time is wasted, and some components of the organic heat-insulating board belong to
In the case of hazardous substances, similar skin allergy symptoms can occur in the case of improper construction. The organic heat-insulation board is a molded polystyrene or extruded polystyrene heat-insulation board, a foamed polyurethane heat-insulation board and the like, the construction is more convenient, the cost is saved by about half compared with the cost of the conventional inorganic heat-insulation board, and the organic heat-insulation board is also highly popular in the market at present and has certain market share. But present organic insulation board is though with low costs, and it is effectual to keep warm, and construction convenience, but the burning grade is not up to standard, is about to be faced the market and eliminates, though can add fire-retardant thing at organic insulation board, but the effect is not very obvious, and most can produce the poison gas when taking place the conflagration, can lead to puzzling, endangers life safety.
Disclosure of Invention
The present invention aims to overcome the above-mentioned shortcomings and provide a technical solution to solve the above-mentioned problems.
A preparation method of a multi-melting composite non-combustible insulation board adopts the following raw materials in parts by weight: 8-15 parts of polyphenyl granules, 100-150 parts of Portland cement, 1-5 parts of curing agent, 5-10 parts of acrylic emulsion, 1-3 parts of silicone waterproofing agent, 50-80 parts of inorganic micro silicon powder, 1-3 parts of ammonium polyphosphate flame retardant, 1-2 parts of PP reinforced fiber and 48-100 parts of water, and the production method comprises the following production steps:
the method comprises the following steps: adding portland cement and inorganic silica fume into stirring equipment for mixing and stirring, then adding PP (polypropylene) reinforced fibers and a silicone waterproofing agent into the stirring equipment for mixing and stirring again, then adding water into the stirring equipment for mixing and stirring for the third time, then adding acrylic emulsion into the stirring equipment for mixing again to obtain mixed raw pulp;
step two: adding an ammonium polyphosphate flame retardant into water, stirring and melting to obtain ammonium polyphosphate flame retardant slurry;
step three: adding the polyphenyl particles and the ammonium polyphosphate flame retardant slurry obtained in the second step into a mixing device for mixing, and coating the ammonium polyphosphate flame retardant slurry on the polyphenyl particles by mixing to obtain granular slurry;
step four: and (3) mixing the mixed raw slurry obtained in the step one with the granular slurry obtained in the step three again, pouring the mixture into a mold for pressure maintaining molding after mixing, demolding after molding, and then performing natural curing, saw cutting, polishing, packaging and warehousing treatment.
As a further scheme of the invention: the polyphenyl granules are one of common white polyphenyl granules or graphite type polyphenyl granules.
As a further scheme of the invention: the particle diameter of the polyphenyl particles is 3-4 mm.
As a further scheme of the invention: the portland cement is 1250-mesh superfine powder.
As a further scheme of the invention: the inorganic micro silicon powder is 1250-mesh superfine powder.
As a further scheme of the invention: in the first step, the mixing time of mixing and stirring for three times is 1 min.
As a further scheme of the invention: and the mixing time of the mixed raw pulp obtained in the step one in the step four and the granular slurry obtained in the step three is 30S.
As a further scheme of the invention: the pressure maintaining and forming time in the fourth step is 10H; the natural curing time after demoulding is 24H-96H.
Compared with the prior art, the invention has the beneficial effects that: the heat-insulating system is suitable for various newly-built buildings and old houses to transform the external wall, and has the advantages of good heat-insulating effect, high bonding strength, long service life, fire resistance, heat insulation resistance, no pollution, strong tensile strength, light weight, simple production and capability of reducing the operation cost of enterprises.
Additional aspects and advantages of the invention will be set forth in part in the description which follows and, in part, will be obvious from the description, or may be learned by practice of the invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In the embodiment of the invention, a preparation method of a multi-melting composite non-combustible heat-insulation board adopts the following raw materials in parts by weight: 8-15 parts of polyphenyl granules, 100-150 parts of Portland cement, 1-5 parts of curing agent, 5-10 parts of acrylic emulsion, 1-3 parts of silicone waterproofing agent, 50-80 parts of inorganic micro silicon powder, 1-3 parts of ammonium polyphosphate flame retardant, 1-2 parts of PP reinforced fiber and 48-100 parts of water, and the production method comprises the following production steps:
the method comprises the following steps: adding portland cement and inorganic silica fume into stirring equipment for mixing and stirring, then adding PP (polypropylene) reinforced fibers and a silicone waterproofing agent into the stirring equipment for mixing and stirring again, then adding water into the stirring equipment for mixing and stirring for the third time, then adding acrylic emulsion into the stirring equipment for mixing again to obtain mixed raw pulp;
step two: adding an ammonium polyphosphate flame retardant into water, stirring and melting to obtain ammonium polyphosphate flame retardant slurry;
step three: adding the polyphenyl particles and the ammonium polyphosphate flame retardant slurry obtained in the second step into a mixing device for mixing, and coating the ammonium polyphosphate flame retardant slurry on the polyphenyl particles by mixing to obtain granular slurry;
step four: and (3) mixing the mixed raw slurry obtained in the step one with the granular slurry obtained in the step three again, pouring the mixture into a mold for pressure maintaining molding after mixing, demolding after molding, and then performing natural curing, saw cutting, polishing, packaging and warehousing treatment.
As a further scheme of the invention: the polyphenyl granules are one of common white polyphenyl granules or graphite type polyphenyl granules.
As a further scheme of the invention: the particle diameter of the polyphenyl particles is 3-4 mm.
As a further scheme of the invention: the portland cement is 1250-mesh superfine powder.
As a further scheme of the invention: the inorganic micro silicon powder is 1250-mesh superfine powder.
As a further scheme of the invention: in the first step, the mixing time of mixing and stirring for three times is 1 min.
As a further scheme of the invention: and the mixing time of the mixed raw pulp obtained in the step one in the step four and the granular slurry obtained in the step three is 30S.
As a further scheme of the invention: the pressure maintaining and forming time in the fourth step is 10H; the natural curing time after demoulding is 24H-96H.
The first embodiment is as follows:
a preparation method of a multi-melting composite non-combustible insulation board adopts the following raw materials in parts by weight: the production method comprises the following steps of preparing polystyrene particles 12 parts, portland cement 99 parts, a curing agent 2 parts, an acrylic emulsion 8 parts, a silicone waterproofing agent 1 part, inorganic silica fume 23 parts, an ammonium polyphosphate fire retardant 1 part, PP (polypropylene) reinforced fibers 1 part and water 52 part, and adopting the following production steps:
the method comprises the following steps: adding portland cement and inorganic silica fume into stirring equipment for mixing and stirring, then adding PP (polypropylene) reinforced fibers and a silicone waterproofing agent into the stirring equipment for mixing and stirring again, then adding water into the stirring equipment for mixing and stirring for the third time, then adding acrylic emulsion into the stirring equipment for mixing again to obtain mixed raw pulp;
step two: adding an ammonium polyphosphate flame retardant into water, stirring and melting to obtain ammonium polyphosphate flame retardant slurry;
step three: adding the polyphenyl particles and the ammonium polyphosphate flame retardant slurry obtained in the second step into a mixing device for mixing, and coating the ammonium polyphosphate flame retardant slurry on the polyphenyl particles by mixing to obtain granular slurry;
step four: and (3) mixing the mixed raw slurry obtained in the step one with the granular slurry obtained in the step three again, pouring the mixture into a mold for pressure maintaining molding after mixing, demolding after molding, and then performing natural curing, saw cutting, polishing, packaging and warehousing treatment.
Example two:
a preparation method of a multi-melting composite non-combustible insulation board adopts the following raw materials in parts by weight: 8 parts of polyphenyl granules, 90 parts of Portland cement, 2 parts of a curing agent, 6 parts of acrylic emulsion, 2 parts of a silicone waterproofing agent, 21 parts of inorganic silica fume, 2 parts of an ammonium polyphosphate fire retardant, 1 part of PP (polypropylene) reinforced fiber and 48 parts of water, and the production method comprises the following production steps:
the method comprises the following steps: adding portland cement and inorganic silica fume into stirring equipment for mixing and stirring, then adding PP (polypropylene) reinforced fibers and a silicone waterproofing agent into the stirring equipment for mixing and stirring again, then adding water into the stirring equipment for mixing and stirring for the third time, then adding acrylic emulsion into the stirring equipment for mixing again to obtain mixed raw pulp;
step two: adding an ammonium polyphosphate flame retardant into water, stirring and melting to obtain ammonium polyphosphate flame retardant slurry;
step three: adding the polyphenyl particles and the ammonium polyphosphate flame retardant slurry obtained in the second step into a mixing device for mixing, and coating the ammonium polyphosphate flame retardant slurry on the polyphenyl particles by mixing to obtain granular slurry;
step four: and (3) mixing the mixed raw slurry obtained in the step one with the granular slurry obtained in the step three again, pouring the mixture into a mold for pressure maintaining molding after mixing, demolding after molding, and then performing natural curing, saw cutting, polishing, packaging and warehousing treatment.
Example three:
a preparation method of a multi-melting composite non-combustible insulation board adopts the following raw materials in parts by weight: 8 parts of polyphenyl granules, 92 parts of Portland cement, 2 parts of a curing agent, 6 parts of acrylic emulsion, 2 parts of a silicone waterproofing agent, 22 parts of inorganic silica fume, 3 parts of an ammonium polyphosphate flame retardant, 2 parts of PP (polypropylene) reinforced fiber and 49.5 parts of water, and the production method comprises the following production steps:
the method comprises the following steps: adding portland cement and inorganic silica fume into stirring equipment for mixing and stirring, then adding PP (polypropylene) reinforced fibers and a silicone waterproofing agent into the stirring equipment for mixing and stirring again, then adding water into the stirring equipment for mixing and stirring for the third time, then adding acrylic emulsion into the stirring equipment for mixing again to obtain mixed raw pulp;
step two: adding an ammonium polyphosphate flame retardant into water, stirring and melting to obtain ammonium polyphosphate flame retardant slurry;
step three: adding the polyphenyl particles and the ammonium polyphosphate flame retardant slurry obtained in the second step into a mixing device for mixing, and coating the ammonium polyphosphate flame retardant slurry on the polyphenyl particles by mixing to obtain granular slurry;
step four: and (3) mixing the mixed raw slurry obtained in the step one with the granular slurry obtained in the step three again, pouring the mixture into a mold for pressure maintaining molding after mixing, demolding after molding, and then performing natural curing, saw cutting, polishing, packaging and warehousing treatment.
Example four:
a preparation method of a multi-melting composite non-combustible insulation board adopts the following raw materials in parts by weight: 11 parts of polyphenyl particles, 97 parts of Portland cement, 2 parts of a curing agent, 7 parts of acrylic emulsion, 3 parts of a silicone waterproofing agent, 22 parts of inorganic silica fume, 3 parts of an ammonium polyphosphate fire retardant, 3 parts of PP (polypropylene) reinforced fiber and 51 parts of water, and the production method comprises the following production steps:
the method comprises the following steps: adding portland cement and inorganic silica fume into stirring equipment for mixing and stirring, then adding PP (polypropylene) reinforced fibers and a silicone waterproofing agent into the stirring equipment for mixing and stirring again, then adding water into the stirring equipment for mixing and stirring for the third time, then adding acrylic emulsion into the stirring equipment for mixing again to obtain mixed raw pulp;
step two: adding an ammonium polyphosphate flame retardant into water, stirring and melting to obtain ammonium polyphosphate flame retardant slurry;
step three: adding the polyphenyl particles and the ammonium polyphosphate flame retardant slurry obtained in the second step into a mixing device for mixing, and coating the ammonium polyphosphate flame retardant slurry on the polyphenyl particles by mixing to obtain granular slurry;
step four: and (3) mixing the mixed raw slurry obtained in the step one with the granular slurry obtained in the step three again, pouring the mixture into a mold for pressure maintaining molding after mixing, demolding after molding, and then performing natural curing, saw cutting, polishing, packaging and warehousing treatment.
Example five:
a preparation method of a multi-melting composite non-combustible insulation board adopts the following raw materials in parts by weight: 10 parts of polyphenyl particles, 95 parts of Portland cement, 2 parts of curing agent, 6 parts of acrylic emulsion, 2 parts of silicone waterproofing agent, 23 parts of inorganic silica fume, 3 parts of ammonium polyphosphate flame retardant, 2.8 parts of PP (polypropylene) reinforced fiber and 50 parts of water, and the production method comprises the following production steps:
the method comprises the following steps: adding portland cement and inorganic silica fume into stirring equipment for mixing and stirring, then adding PP (polypropylene) reinforced fibers and a silicone waterproofing agent into the stirring equipment for mixing and stirring again, then adding water into the stirring equipment for mixing and stirring for the third time, then adding acrylic emulsion into the stirring equipment for mixing again to obtain mixed raw pulp;
step two: adding an ammonium polyphosphate flame retardant into water, stirring and melting to obtain ammonium polyphosphate flame retardant slurry;
step three: adding the polyphenyl particles and the ammonium polyphosphate flame retardant slurry obtained in the second step into a mixing device for mixing, and coating the ammonium polyphosphate flame retardant slurry on the polyphenyl particles by mixing to obtain granular slurry;
step four: and (3) mixing the mixed raw slurry obtained in the step one with the granular slurry obtained in the step three again, pouring the mixture into a mold for pressure maintaining molding after mixing, demolding after molding, and then performing natural curing, saw cutting, polishing, packaging and warehousing treatment.
And (3) carrying out performance inspection test on the product obtained by the forming mode 1-5, wherein the specific result is shown in the table I:
the dry apparent density detection method is according to JG/T563-2017 and DBHJ/T015-2014;
the compressive strength detection method is according to JG/T563-2017 and DBHJ/T015-2014;
the flexural strength detection method is according to JG/T563-2017 and DBHJ/T015-2014;
the volume water absorption detection method is according to JG/T563-2017 and DBHJ/T015-2014;
the heat accumulation coefficient detection method is according to JG/T563-2017 and DBHJ/T015-2014.
Watch forming modes 1-5
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Claims (8)
1. The preparation method of the multi-melting composite non-combustible insulation board is characterized by adopting the following raw materials in parts by weight: 8-15 parts of polyphenyl granules, 100-150 parts of Portland cement, 1-5 parts of curing agent, 5-10 parts of acrylic emulsion, 1-3 parts of silicone waterproofing agent, 50-80 parts of inorganic micro silicon powder, 1-3 parts of ammonium polyphosphate flame retardant, 1-2 parts of PP reinforced fiber and 48-100 parts of water, and the production method comprises the following production steps:
the method comprises the following steps: adding portland cement and inorganic silica fume into stirring equipment for mixing and stirring, then adding PP (polypropylene) reinforced fibers and a silicone waterproofing agent into the stirring equipment for mixing and stirring again, then adding water into the stirring equipment for mixing and stirring for the third time, then adding acrylic emulsion into the stirring equipment for mixing again to obtain mixed raw pulp;
step two: adding an ammonium polyphosphate flame retardant into water, stirring and melting to obtain ammonium polyphosphate flame retardant slurry;
step three: adding the polyphenyl particles and the ammonium polyphosphate flame retardant slurry obtained in the second step into a mixing device for mixing, and coating the ammonium polyphosphate flame retardant slurry on the polyphenyl particles by mixing to obtain granular slurry;
step four: and (3) mixing the mixed raw slurry obtained in the step one with the granular slurry obtained in the step three again, pouring the mixture into a mold for pressure maintaining molding after mixing, demolding after molding, and then performing natural curing, saw cutting, polishing, packaging and warehousing treatment.
2. The preparation method of the multi-melt composite non-combustible insulation board according to claim 1, wherein the polyphenyl particles are one of common white polyphenyl particles or graphite type polyphenyl particles.
3. The preparation method of the multi-melt composite non-combustible heat preservation plate according to claim 1, wherein the particle diameter of the polyphenyl particles is 3-4 mm.
4. The preparation method of the multi-melt composite non-combustible insulation board according to claim 1, wherein the portland cement is 1250-mesh ultrafine powder.
5. The preparation method of the multi-melt composite non-combustible insulation board according to claim 1, wherein the inorganic micro silicon powder is 1250-mesh ultrafine powder.
6. The preparation method of the multi-melt composite non-combustible heat preservation plate according to claim 1, wherein in the first step, the mixing time of three times of mixing and stirring is 1 min.
7. The preparation method of the multi-melt composite non-combustible insulation board according to claim 1, wherein the mixing time of the mixed raw pulp obtained in the first step in the fourth step and the granular slurry obtained in the third step is 30S.
8. The preparation method of the multi-melt composite non-combustible insulation board according to claim 1, wherein the pressure maintaining forming time in the fourth step is 10H; the natural curing time after demoulding is 24H-96H.
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| CN111960782A (en) * | 2020-08-24 | 2020-11-20 | 杭州五友建材有限公司 | Environment-friendly lightweight concrete prepared from waste sintered bricks and tiles and preparation method thereof |
| CN112479738A (en) * | 2020-12-15 | 2021-03-12 | 安徽艾米伦特建材科技有限公司 | Hierarchical-pore inorganic composite polyphenyl non-combustible heat-insulating material and preparation method thereof |
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Application publication date: 20191224 |