CN110541306A - biomass antistatic agent and preparation method thereof - Google Patents
biomass antistatic agent and preparation method thereof Download PDFInfo
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- CN110541306A CN110541306A CN201910828266.8A CN201910828266A CN110541306A CN 110541306 A CN110541306 A CN 110541306A CN 201910828266 A CN201910828266 A CN 201910828266A CN 110541306 A CN110541306 A CN 110541306A
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- polyoxyethylene ether
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/203—Unsaturated carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/2035—Aromatic acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/2243—Mono-, di-, or triglycerides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
the invention discloses a biomass antistatic agent and a preparation method thereof, wherein the biomass antistatic agent is prepared from the following raw materials in parts by weight: 15-20 parts of fatty alcohol-polyoxyethylene ether, 10-20 parts of acetic acid, 5-10 parts of alcohol, 3-8 parts of cinnamic acid, 10-20 parts of natural oleyl ester, 5-10 parts of sodium stearate and 30-50 parts of water. The biomass antistatic agent has the advantages of simple and easily-operated manufacturing process, low price and easily-obtained raw materials, no toxicity, no harm, no stimulation to human bodies and no damage to base materials.
Description
Technical Field
the invention belongs to the technical field of auxiliaries, and particularly relates to a biomass antistatic agent and a preparation method thereof.
background
static electricity brings inconvenience to daily life of people, and along with the continuous improvement of the living standard of people, the demand of antistatic clothes can be continuously improved. The antistatic agent which is popular in the market at present adopts chemical agents to perform chemical treatment on the antistatic agent, so that the antistatic effect can be achieved to a certain degree, but most of fiber surface tissues after the chemical treatment are damaged, and the appearance and the wearing comfort are affected. Meanwhile, the chemical treatment of the fiber causes environmental pollution to a certain extent. Therefore, an antistatic agent which has no pollution to the environment and little or no damage to the fiber is pursued by more and more people.
Disclosure of Invention
The invention aims to provide a biomass antistatic agent and a preparation method thereof, which aim to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
a biomass antistatic agent is characterized in that: the biomass antistatic agent comprises the following raw materials in parts by weight: 15-20 parts of fatty alcohol-polyoxyethylene ether, 10-20 parts of acetic acid, 5-10 parts of alcohol, 3-8 parts of cinnamic acid, 10-20 parts of natural oleyl ester, 5-10 parts of sodium stearate and 30-50 parts of water.
Preferably, the biomass antistatic agent comprises the following components in parts by weight: 15 parts of fatty alcohol-polyoxyethylene ether, 10 parts of acetic acid, 5 parts of alcohol, 3 parts of cinnamic acid, 10 parts of natural oil ester, 5 parts of sodium stearate and 30 parts of water.
preferably, the biomass antistatic agent comprises the following components in parts by weight: 16 parts of fatty alcohol-polyoxyethylene ether, 12 parts of acetic acid, 6 parts of alcohol, 4 parts of cinnamic acid, 12 parts of natural oil ester, 6 parts of sodium stearate and 35 parts of water.
Preferably, the biomass antistatic agent comprises the following components in parts by weight: 17 parts of fatty alcohol-polyoxyethylene ether, 14 parts of acetic acid, 7 parts of alcohol, 5 parts of cinnamic acid, 14 parts of natural oil ester, 7 parts of sodium stearate and 40 parts of water.
Preferably, the biomass antistatic agent comprises the following components in parts by weight: 18 parts of fatty alcohol-polyoxyethylene ether, 16 parts of acetic acid, 8 parts of alcohol, 6 parts of cinnamic acid, 16 parts of natural oil ester, 8 parts of sodium stearate and 45 parts of water.
preferably, the biomass antistatic agent comprises the following components in parts by weight: 19 parts of fatty alcohol-polyoxyethylene ether, 18 parts of acetic acid, 9 parts of alcohol, 7 parts of cinnamic acid, 18 parts of natural oil ester, 9 parts of sodium stearate and 50 parts of water.
Preferably, the biomass antistatic agent comprises the following components in parts by weight: 20 parts of fatty alcohol-polyoxyethylene ether, 20 parts of acetic acid, 10 parts of alcohol, 8 parts of cinnamic acid, 20 parts of natural oil ester, 10 parts of sodium stearate and 50 parts of water.
preferably, the preparation method of the biomass antistatic agent comprises the following specific steps:
step 1, adding 10-20 parts of natural oil ester into a reaction kettle, raising the temperature to 60-80 ℃, adding 30-50 parts of water after the natural oil ester is molten, stirring for 20-30 minutes at the speed of 1000 revolutions per minute;
step 2, adding 3-8 parts of cinnamic acid when the temperature is reduced to 25-30 ℃, stirring for 10 minutes at 500-;
Step 3, adding 5-10 parts of sodium stearate when the temperature is reduced to room temperature, stirring for 10 minutes at 500-1000 rpm;
And 4, adding 10-20 parts of acetic acid, 5-10 parts of alcohol, 15-20 parts of fatty alcohol-polyoxyethylene ether at the speed of 500 revolutions per minute, and stirring for 10-20 minutes. Discharging and packaging to obtain the finished product.
compared with the prior art, the invention has the beneficial effects that:
1. The biomass antistatic agent provided by the invention is prepared from raw materials which are basically from nature, are purely natural, nontoxic and noncorrosive, and are widely applicable to various fabrics such as knitted fabrics, woven fabrics, non-woven fabrics and the like.
2. The biomass softener adopts natural grease, can reduce the friction force between fibers and the friction force between the fibers and a human body, and can ensure that fabrics obtain soft hand feeling and reduce the generation of static electricity.
3. the fatty alcohol-polyoxyethylene ether adopted by the biomass antistatic agent is used as an emulsifier, a penetrating agent and an activator, so that the antistatic capability of the fabric surface is improved radically.
4. the biomass antistatic agent adopts the cinnamic acid, and the cinnamic acid has certain fragrance and can provide pleasant mood for users.
5. The biomass antistatic agent adopts alcohol, has certain antibacterial and antistatic capabilities, and is a good solvent.
6. The raw materials used by the biomass antistatic agent are compatible and synergistic, and the raw materials jointly form a product with excellent performance.
7. The biomass antistatic agent can be used by spraying, dipping and other methods, and has good effect.
8. The process is simplified, the operation is safe and simple, and the industrial production is easy to realize.
9. The invention can be used with good economic benefit.
Detailed description of the preferred embodiment
the invention discloses a biomass antistatic agent which comprises the following components in parts by weight: 15-20 parts of fatty alcohol-polyoxyethylene ether, 10-20 parts of acetic acid, 5-10 parts of alcohol, 3-8 parts of cinnamic acid, 10-20 parts of natural oleyl ester, 5-10 parts of sodium stearate and 30-50 parts of water.
The invention also provides a preparation method of the antistatic agent, which comprises the following specific steps:
Step 1, adding 10-20 parts of natural oil ester into a reaction kettle, raising the temperature to 60-80 ℃, adding 30-50 parts of water after the natural oil ester is molten, stirring for 20-30 minutes at the speed of 1000 revolutions per minute;
step 2, adding 3-8 parts of cinnamic acid when the temperature is reduced to 25-30 ℃, stirring for 10 minutes at 500-;
step 3, adding 5-10 parts of sodium stearate when the temperature is reduced to room temperature, stirring for 10 minutes at 500-1000 rpm;
And 4, adding 10-20 parts of acetic acid, 5-10 parts of alcohol, 15-20 parts of fatty alcohol-polyoxyethylene ether at the speed of 500 revolutions per minute, and stirring for 10-20 minutes. Discharging and packaging to obtain the finished product.
Example 1
The invention discloses a biomass antistatic agent which comprises the following components in parts by weight: 15 parts of fatty alcohol-polyoxyethylene ether, 10 parts of acetic acid, 5 parts of alcohol, 3 parts of cinnamic acid, 10 parts of natural oil ester, 5 parts of sodium stearate and 30 parts of water.
The invention also provides a preparation method of the antistatic agent, which comprises the following specific steps:
Step 1, adding 10 parts of natural oil ester into a reaction kettle, raising the temperature to 60-80 ℃, adding 30 parts of water after the natural oil ester is molten, stirring for 20-30 minutes at 500 revolutions per minute;
Step 2, adding 3 parts of cinnamic acid when the temperature is reduced to 25-30 ℃, stirring for 10 minutes at 500-1000 r/min;
Step 3, adding 5 parts of sodium stearate when the temperature is reduced to room temperature, stirring for 10 minutes at 500-;
And step 4, adding 10 parts of acetic acid, 5 parts of alcohol and 15 parts of fatty alcohol-polyoxyethylene ether at 500 revolutions per minute, and stirring for 10-20 minutes. Discharging and packaging to obtain the finished product.
example 2
the invention discloses a biomass antistatic agent which comprises the following components in parts by weight: 16 parts of fatty alcohol-polyoxyethylene ether, 12 parts of acetic acid, 6 parts of alcohol, 4 parts of cinnamic acid, 12 parts of natural oil ester, 6 parts of sodium stearate and 35 parts of water.
The invention also provides a preparation method of the antistatic agent, which comprises the following specific steps:
Step 1, adding 12 parts of natural oil ester into a reaction kettle, raising the temperature to 60-80 ℃, adding 35 parts of water after the natural oil ester is molten, stirring for 20-30 minutes at the speed of 500 revolutions per minute;
Step 2, adding 4 parts of cinnamic acid when the temperature is reduced to 25-30 ℃, stirring for 10 minutes at 500-1000 r/min;
step 3, adding 6 parts of sodium stearate when the temperature is reduced to room temperature, stirring for 10 minutes at 500-;
and step 4, adding 12 parts of acetic acid, 6 parts of alcohol and 16 parts of fatty alcohol-polyoxyethylene ether at the speed of 500-. Discharging and packaging to obtain the finished product.
example 3
The invention discloses a biomass antistatic agent which comprises the following components in parts by weight: 17 parts of fatty alcohol-polyoxyethylene ether, 14 parts of acetic acid, 7 parts of alcohol, 5 parts of cinnamic acid, 14 parts of natural oil ester, 7 parts of sodium stearate and 40 parts of water.
The invention also provides a preparation method of the antistatic agent, which comprises the following specific steps:
Step 1, adding 14 parts of natural oil ester into a reaction kettle, raising the temperature to 60-80 ℃, adding 40 parts of water after the natural oil ester is molten, stirring for 20-30 minutes at 500 revolutions per minute;
Step 2, adding 5 parts of cinnamic acid when the temperature is reduced to 25-30 ℃, stirring for 10 minutes at 500-1000 r/min;
Step 3, adding 7 parts of sodium stearate when the temperature is reduced to room temperature, stirring for 10 minutes at 500-;
and 4, adding 14 parts of acetic acid, 7 parts of alcohol and 18 parts of fatty alcohol-polyoxyethylene ether at 500 revolutions per minute, and stirring for 10-20 minutes. Discharging and packaging to obtain the finished product.
Comparative example 1
The invention discloses a biomass antistatic agent which comprises the following components in parts by weight: 10 parts of acetic acid, 5 parts of alcohol, 3 parts of cinnamic acid, 10 parts of natural oil ester, 5 parts of sodium stearate and 30 parts of water.
The invention also provides a preparation method of the antistatic agent, which comprises the following specific steps:
Step 1, adding 10 parts of natural oil ester into a reaction kettle, raising the temperature to 60-80 ℃, adding 30 parts of water after the natural oil ester is molten, stirring for 20-30 minutes at 500 revolutions per minute;
Step 2, adding 3 parts of cinnamic acid when the temperature is reduced to 25-30 ℃, stirring for 10 minutes at 500-1000 r/min;
Step 3, adding 5 parts of sodium stearate when the temperature is reduced to room temperature, stirring for 10 minutes at 500-;
step 4, adding 10 parts of acetic acid and 5 parts of alcohol at 500 revolutions per minute, and stirring for 10-20 minutes. Discharging and packaging to obtain the finished product.
Comparative example 2
The invention discloses a biomass antistatic agent which comprises the following components in parts by weight: 16 parts of fatty alcohol-polyoxyethylene ether, 12 parts of acetic acid, 6 parts of alcohol, 4 parts of cinnamic acid, 6 parts of sodium stearate and 35 parts of water.
the invention also provides a preparation method of the antistatic agent, which comprises the following specific steps:
Step 1, adding 35 parts of water, 4 parts of cinnamic acid and 500-1000 revolutions per minute into a reaction kettle, and stirring for 10 minutes;
Step 2, adding 6 parts of sodium stearate when the temperature is reduced to room temperature, stirring for 10 minutes at 500-;
And step 3, adding 12 parts of acetic acid, 6 parts of alcohol and 16 parts of fatty alcohol-polyoxyethylene ether at the speed of 500-. Discharging and packaging to obtain the finished product.
and (3) testing results:
5 pieces of the same cotton fabric were padded in the solutions of the biomass antistatic agents of examples 1, 2, and 3 and comparative examples 1 and 2, and were subjected to two-padding and two-rolling, and then washed with water and dried, to obtain 5 pieces of fabric having antistatic properties. The test results were as follows:
in comparative example 1, no fatty alcohol polyoxyethylene ether was added, and the antistatic effect was greatly reduced.
comparative example 2 had no addition of natural oil ester, and its antistatic effect was reduced.
The various embodiments listed above can be combined with each other without contradiction, and a person skilled in the art can combine the above explanations of the embodiments as a basis for combining technical features in different embodiments.
although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (8)
1. a biomass antistatic agent is characterized in that: the biomass antistatic agent comprises the following raw materials in parts by weight: 15-20 parts of fatty alcohol-polyoxyethylene ether, 10-20 parts of acetic acid, 5-10 parts of alcohol, 3-8 parts of cinnamic acid, 10-20 parts of natural oleyl ester, 5-10 parts of sodium stearate and 30-50 parts of water.
2. the biomass antistatic agent of claim 1, characterized in that: the paint comprises the following components in parts by weight: 15 parts of fatty alcohol-polyoxyethylene ether, 10 parts of acetic acid, 5 parts of alcohol, 3 parts of cinnamic acid, 10 parts of natural oil ester, 5 parts of sodium stearate and 30 parts of water.
3. The biomass antistatic agent of claim 1, characterized in that: the paint comprises the following components in parts by weight: 16 parts of fatty alcohol-polyoxyethylene ether, 12 parts of acetic acid, 6 parts of alcohol, 4 parts of cinnamic acid, 12 parts of natural oil ester, 6 parts of sodium stearate and 35 parts of water.
4. The biomass antistatic agent of claim 1, characterized in that: the paint comprises the following components in parts by weight: 17 parts of fatty alcohol-polyoxyethylene ether, 14 parts of acetic acid, 7 parts of alcohol, 5 parts of cinnamic acid, 14 parts of natural oil ester, 7 parts of sodium stearate and 40 parts of water.
5. The biomass antistatic agent of claim 1, characterized in that: the paint comprises the following components in parts by weight: 18 parts of fatty alcohol-polyoxyethylene ether, 16 parts of acetic acid, 8 parts of alcohol, 6 parts of cinnamic acid, 16 parts of natural oil ester, 8 parts of sodium stearate and 45 parts of water.
6. The biomass antistatic agent of claim 1, characterized in that: the paint comprises the following components in parts by weight: 19 parts of fatty alcohol-polyoxyethylene ether, 18 parts of acetic acid, 9 parts of alcohol, 7 parts of cinnamic acid, 18 parts of natural oil ester, 9 parts of sodium stearate and 50 parts of water.
7. The biomass antistatic agent of claim 1, characterized in that: the paint comprises the following components in parts by weight: 20 parts of fatty alcohol-polyoxyethylene ether, 20 parts of acetic acid, 10 parts of alcohol, 8 parts of cinnamic acid, 20 parts of natural oil ester, 10 parts of sodium stearate and 50 parts of water.
8. a method for preparing the biomass antistatic agent according to any one of the claims 1 to 7, which is characterized in that: the method comprises the following specific steps:
Step 1, adding 10-20 parts of natural oil ester into a reaction kettle, raising the temperature to 60-80 ℃, adding 30-50 parts of water after the natural oil ester is molten, stirring for 20-30 minutes at the speed of 1000 revolutions per minute;
Step 2, adding 3-8 parts of cinnamic acid when the temperature is reduced to 25-30 ℃, stirring for 10 minutes at 500-;
step 3, adding 5-10 parts of sodium stearate when the temperature is reduced to room temperature, stirring for 10 minutes at 500-1000 rpm;
and 4, adding 10-20 parts of acetic acid, 5-10 parts of alcohol, 15-20 parts of fatty alcohol-polyoxyethylene ether at the speed of 500 revolutions per minute, and stirring for 10-20 minutes. Discharging and packaging to obtain the finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910828266.8A CN110541306A (en) | 2019-09-03 | 2019-09-03 | biomass antistatic agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910828266.8A CN110541306A (en) | 2019-09-03 | 2019-09-03 | biomass antistatic agent and preparation method thereof |
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| CN110541306A true CN110541306A (en) | 2019-12-06 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201910828266.8A Pending CN110541306A (en) | 2019-09-03 | 2019-09-03 | biomass antistatic agent and preparation method thereof |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103757896A (en) * | 2013-12-31 | 2014-04-30 | 吴江市七都镇庙港雅迪针织制衣厂 | Antistatic agent for silk fabrics |
| CN104559125A (en) * | 2015-01-22 | 2015-04-29 | 南通恒隆化工有限公司 | Antistatic agent |
-
2019
- 2019-09-03 CN CN201910828266.8A patent/CN110541306A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103757896A (en) * | 2013-12-31 | 2014-04-30 | 吴江市七都镇庙港雅迪针织制衣厂 | Antistatic agent for silk fabrics |
| CN104559125A (en) * | 2015-01-22 | 2015-04-29 | 南通恒隆化工有限公司 | Antistatic agent |
Non-Patent Citations (1)
| Title |
|---|
| 王兴国等: "《油料科学原理》", 31 August 2017, 中国轻工业出版社 * |
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Application publication date: 20191206 |