CN110512464A - A kind of production method of antibacterial shield adornment paper - Google Patents
A kind of production method of antibacterial shield adornment paper Download PDFInfo
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- CN110512464A CN110512464A CN201910717226.6A CN201910717226A CN110512464A CN 110512464 A CN110512464 A CN 110512464A CN 201910717226 A CN201910717226 A CN 201910717226A CN 110512464 A CN110512464 A CN 110512464A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0208—Tissues; Wipes; Patches
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H11/00—Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H11/00—Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
- D21H11/12—Pulp from non-woody plants or crops, e.g. cotton, flax, straw, bagasse
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
- D21H17/675—Oxides, hydroxides or carbonates
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
- D21H17/68—Water-insoluble compounds, e.g. fillers, pigments siliceous, e.g. clays
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/06—Paper forming aids
- D21H21/08—Dispersing agents for fibres
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/06—Paper forming aids
- D21H21/10—Retention agents or drainage improvers
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/16—Sizing or water-repelling agents
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/18—Reinforcing agents
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/18—Reinforcing agents
- D21H21/20—Wet strength agents
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/28—Colorants ; Pigments or opacifying agents
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/002—Tissue paper; Absorbent paper
- D21H27/004—Tissue paper; Absorbent paper characterised by specific parameters
- D21H27/005—Tissue paper; Absorbent paper characterised by specific parameters relating to physical or mechanical properties, e.g. tensile strength, stretch, softness
- D21H27/007—Tissue paper; Absorbent paper characterised by specific parameters relating to physical or mechanical properties, e.g. tensile strength, stretch, softness relating to absorbency, e.g. amount or rate of water absorption, optionally in combination with other parameters relating to physical or mechanical properties
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Abstract
The present invention provides a kind of production method of antibacterial shield adornment paper, which includes: 20~100 parts of ramie pulp fibers, 0~80 part of wood pulp cellulose, 0~80 part of bamboo pulp fiber, 25~35 parts of fillers, 5~13 parts of auxiliary agents according to the raw material composition of parts by weight.Production method includes: to form ingredient according to the raw material of above-mentioned shield adornment paper, and fibrous raw material is first carried out mashing processing, is disposed and filler is added；Obtained mixed slurry is diluted, auxiliary agent is then added, is 60~70% successively forming through wet end with press section dehydration to water content, obtains l Water Paper page；By l Water Paper page successively through half dry-cure, batch to obtain shield adornment paper body paper；Shield adornment paper body paper is subjected to superpressure processing, both.Shield adornment paper of the invention is better than present face-sebum absorbing paper in terms of tensile strength, wet strength, air permeability, positive and negative smoothness and dynamic contact angle, and has good paper pliability, smoothness, oil absorbing effect and shield adornment effect.
Description
Technical field
The invention belongs to paper preparation technical fields used for cosmetic, and in particular to a kind of production method of antibacterial shield adornment paper.
Background technique
With the increasingly raising of people's living standard, people also increasingly pay close attention to self-image, and especially face holds
Face, the most awkward facial oil that is no more than secrete overstock problem.The appearance of face-sebum absorbing paper solves the problems, such as this, at present in Asia
Continent is all the fashion, but discovery in use, and since its oil absorbing effect is too strong, when frequency of usage is more, face can take off adornment, can make
The oil and moisture of skin are reduced, and skin becomes drying, and experience sense is deteriorated.
CN1124312A discloses a kind of face-sebum absorbing paper and its manufacturing method, it is mainly coated with using thermoplasticity and sets
Rouge and body paper carry out hot pressing, and the methods of subsequent release coating film prepares facial tissue, the oil suction face of the facial tissue be single side and oil suction compared with
By force, but the facial tissue does not have bacteria resistance function, and production process is complicated, more falls behind, production efficiency is also relatively low.
For sold face-sebum absorbing paper one is above-mentioned patent is similar to, what is be all made of is that addition oil-absorbing resin technique is raw in the market
It produces, oil suction multiple (oil mass and resinogen mass ratio that are absorbed when resin saturation oil suction) can achieve tens times, oil suction effect
Fruit is very strong, and it is dry that frequent use will cause de- adornment, skin quality.It is another then be to directly adopt acrylic resin to be made into, oil absorption
It is also greatly, to be not easily decomposed in acrylic resin soil, 80 DEG C or less acid-alkali-corrosive-resistings can cause environmental pollution, be applied to
It is airtight on the face, and crowd for sensitive skin quality and be not suitable for.
Summary of the invention
In view of the problems of the existing technology, the present invention provides a kind of production method of antibacterial shield adornment paper.Skill of the invention
Art scheme are as follows:
First aspect, the present invention provide a kind of antibacterial shield adornment paper, include: 20~100 according to the raw material composition of parts by weight
Part ramie pulp fiber, 0~80 part of wood pulp cellulose, 0~80 part of bamboo pulp fiber, 25~35 parts of fillers, 5~13 parts of auxiliary agents.
Further, the ramie pulp fiber is hemp, abaca, sisal hemp, including bleaching and true qualities；The wood pulp is fine
Dimension is softwood pulp, including bleaching and true qualities；The bamboo pulp fiber includes bleaching and true qualities bamboo pulp.
Further, the filler is selected from the kaolin of partial size≤4.0 μm, the magnesium stearate of partial size≤4.2 μm, partial size
One or more of≤3.5 μm of titanium dioxide, the calcium carbonate of partial size≤4.5 μm, talcum powder of partial size≤13 μm.
Further, the auxiliary agent in wet strength agent, reinforcing agent, retention agent, dispersing agent, sizing agent, remover one
Kind is a variety of.
Further, the shield adornment paper further includes 9.1~16 parts of food grade dyes preparation.
Further, the food grade dyes preparation is (0 according to mass ratio by food grade dyes, oxidized starch, salt
~1.0): (8~12): (1.0~3.0) compounding is made.
Further, the food grade dyes are selected from brilliant blue, sunset yellow, lemon yellow, chocolate palm fibre, amaranth, kermes
It is red, Ka Dasuo is red, Ka Dasuo is yellow, one or more of Ka Dasuolan.
Further, the index of the shield adornment paper are as follows: quantitative: 14~25g/ ㎡；Tensile strength: >=1.3kN/m；It is wet strong
Degree >=0.15kN/m；Thickness :≤27 μm；Air permeability: >=2000CU；Smoothness: front >=700S, reverse side >=350S；Ash content:
(10~16) %；Dynamic contact angle (0.06s): front >=55 °, reverse side >=65 °；Print ink penetration: (15~20) l/
mm。
The second aspect, the present invention provide a kind of production method of antibacterial shield adornment paper, comprising the following steps:
(1) ingredient is formed according to the raw material of above-mentioned shield adornment paper, fibrous raw material is first subjected to mashing processing, handled
Finish addition filler；
(2) mixed slurry that step (1) obtains is diluted, auxiliary agent is then added, successively formed and pressing through wet end
Squeezing portion dehydration to water content is 60~70%, obtains l Water Paper page；
(3) by l Water Paper page successively through half dry-cure, batch to obtain shield adornment paper body paper；
(4) shield adornment paper body paper is subjected to superpressure processing, both.
Further, in the step (3) half dry-cure control parameter are as follows: preceding dry temperature is 100~110 DEG C, rear dry
Temperature is 115~125 DEG C, and processing water content into page is 3~10%.
Further, the control parameter that superpressure is handled in the step (4) are as follows: pressure is 1.0~3.0MPa, and temperature is
15~35 DEG C, humidity is 40~60%.
Further, the production method further includes by half-dried treated the page dip-coating dye formulations solution of step (3)
Process.
The beneficial effects of the present invention are:
(1) shield adornment paper of the invention uses hemp, bamboo pulp fiber for raw material, and hemp and bamboo fibre institute are exclusive
Phenolic substances and quinones substance make this product have good antibacterial, fungistatic effect.
(2) shield adornment paper air permeability with higher of the invention and reasonable printing ink penetration performance, can rapidly by
The absorption of face's surface layer grease can reach good oil absorbing effect it is not necessary that any oil-absorbing resin is added, reduce production cost；It is good
Good dry, wet strength can satisfy client and not rupture in wiping；Higher smoothness and extremely low thickness, make paper it is smooth,
It is thin and flexible, it can be preferably bonded skin, good absorption is played to grease, skin is made to feel very comfortable；Have simultaneously
There is reasonable dynamic contact angle that can guarantee that the moisture of skin is not absorbed all by paper, makes face surface layer that there is water appropriate
Divide, oil, imperceptible drying being used for multiple times, shield adornment effect is obvious, is suitable for all skin quality.
(3) shield adornment paper production method of the invention is simple, and the steam consumption is low, and power consumption is low, and speed is high, high production efficiency and cost
It is low.
(4) shield adornment paper index of the invention is in tensile strength, wet strength, air permeability, positive and negative smoothness and dynamic contact angle
Aspect is better than present face-sebum absorbing paper index.Existing face-sebum absorbing paper index are as follows: tensile strength: >=1.1kN/m；Wet strength >=
0.10kN/m；Thickness :≤30 μm；Air permeability: 500~800CU；Smoothness: front >=300S, reverse side >=150S；Ash content: (9
~12) %；Dynamic contact angle (0.06s): front >=45 °, reverse side >=55 °；Print ink penetration: (10~15) l/mm.
Specific embodiment
In the description of the present invention, it should be noted that the person that is not specified actual conditions in embodiment, according to normal conditions
Or the condition that manufacturer suggests carries out.Reagents or instruments used without specified manufacturer is that can be obtained by commercially available purchase
The conventional products obtained.
The present invention is described in further details below with reference to specific embodiment, it is described be explanation of the invention and
It is not to limit.
In the specific embodiment of the invention, the production technology of antibacterial shield adornment paper is special according to the structure of different fibrous raw materials
Point, low various concentration and different mashing parameters handle bleached fiber raw material in, such as by light to hemp
Wire-dividing broom purification carries out medium consistency refining processing to wood pulp cellulose and bamboo pulp fiber, makes hemp and wood pulp cellulose, bamboo pulp fiber
Interweave and combine, keeps high porosity；Retain that the lesser oil suction numerical value of partial size is high to be filled out using preferred retention agent and reinforcing agent
Material；Guarantee the evenness of paper using preferred dispersing agent；Carry out superpressure processing again after padding.
Embodiment 1
The present embodiment provides a kind of antibacterial shield adornment paper and its production technologies, and the antibacterial adornment paper that protects is according to the raw material of parts by weight
Composition includes: 30 parts of big ramie pulp fibers of bleaching, 30 parts of bleached wood pulp fibers, 30 parts of bleaching bamboo pulp fibres, 32 parts of talcum powder, and 9.7
Part auxiliary agent, 13.6 parts of dye formulations.
Auxiliary agent are as follows: wet strength agent polyamide polyamines-epichlorohydrin resins PAE mass concentration is 15%, its adding in paper pulp
Enter 8% that amount is paper pulp total amount；The mass concentration of guar gum reinforcing agent is 0.3%, its additional amount in paper pulp is that paper pulp is total
The 0.5% of amount；The mass concentration of guar gum retention agent is 0.3%, its additional amount in paper pulp is paper pulp total amount
0.06%；The mass concentration of dispersing agent polyethylene glycol oxide PEO is 0.03%, its additional amount in paper pulp is paper pulp total amount
0.85%；The mass concentration of neutral sizing agent alkyl ketene dimer is 10%, its additional amount in paper pulp is paper pulp gross weight
The 0.04% of amount；The mass concentration of remover is 0.2%, its additional amount in paper is the 0.25% of paper pulp total amount.
Dye formulations are red by Ka Dasuo, Ka Dasuo is yellow, Ka Dasuolan, oxidized starch, salt compounding.
Production technology the following steps are included:
(1) beater floor: the big ramie pulp fiber of bleaching, wood pulp cellulose, bamboo pulp fiber are continuously beaten respectively using double plate mill
Slurry, wherein big ramie pulp fiber beating consistency 2.8%, beating degree/weight in wet base (34~36) ° SR/ (7.5-8.5) g；Wood pulp cellulose is beaten
Starch concentration 4.0%, beating degree/weight in wet base (36~40) ° SR/ (12.0~13.0) g；Bamboo pulp fiber beating consistency 4.2%, mashing
Degree/weight in wet base (35~39) ° SR/ (10.0~11.0) g.Big ramie pulp fiber, wood pulp cellulose, bamboo pulp after being beaten by weight
Fiber is mixed to get mixing slurry；Scattered 1250 mesh talcum powder (partial size≤10 μm) is added in mixing slurry mixed to get arriving
Synthetic pulp；Interior addition wet strength agent polyamide polyamines-epichlorohydrin resins PAE is slurried in mixing and obtains mixed slurry, by mixing slurry
Material is manufactured with cylinder mould machine, speed 215m/min.
(2) copy paper workshop section: by above-mentioned mixed slurry, being diluted to concentration is 0.2%, is separately added into melon through the short circulatory system
Ear glue reinforcing agent, guar gum retention agent, dispersing agent PEO guarantee that fiber is evenly dispersed and intensity, add neutral sizing agent alkane
Base ketene dimer carries out sizing water resistant, is successively 66% through wet end molding and press section dehydration to water content, obtains wet
Page；L Water Paper page by half dry-cure, send remover forth and obtain the half-dried page that water content is 45%, wherein half dry-cure
Control parameter are as follows: preceding dry temperature is 105 DEG C, and dry temperature is 120 DEG C afterwards；Half-dried page dip-coating dye formulations solution again passes by
Dry drying and processing afterwards is batched to obtain shield adornment paper body paper.
The wherein formula of dye formulations solution are as follows: Ka Dasuo is red, Ka Dasuo is yellow, in Ka Dasuolan in mass ratio be 1:
3:1 ingredient, the mass ratio according still further to dyestuff, oxidized starch, salt is 0.6:12:1.0 ingredient, is configured to mass concentration respectively
For 0.5% dye solution, 6% oxidized starch solution and 0.5% salt solution, it is uniformly mixed.
(4) the shield adornment paper body paper after ornamenting is subjected to superpressure processing by calender, wherein calender is 12 roll-in light
Machine is handled by 6 press polish, and calender pressure is 2.0MPa, and temperature is 20 DEG C, and humidity 40% obtains shield adornment paper.
The shield adornment paper of the present embodiment: quantitative: 20.2g/ ㎡；Tensile strength: 1.45kN/m；Wet strength: 0.16kN/m；It is thick
Degree: 24 μm；Air permeability: 2320CU；Smoothness: front: 760S, reverse side: 400S；Ash content: 11.5%；Dynamic contact angle
(0.06s): front: 59 °, reverse side: 68 °；Print ink penetration: 16l/mm.
Embodiment 2
The present embodiment provides a kind of antibacterial shield adornment paper and its production technologies, and the antibacterial adornment paper that protects is according to the raw material of parts by weight
Composition includes: 60 parts of big jute pulps of true qualities, 25 parts of true qualities manila pulps, 15 true qualities part sisal hemp pulps, 28 parts of talcum powder, 7 parts of kaolinites
Soil, 9.6 parts of auxiliary agents, 13 parts of dye formulations, auxiliary component are compounded with embodiment 1, dye formulations by oxidized starch, salt.
Production technology the difference from embodiment 1 is that: 1) by 1250 mesh talcum powder (partial size≤10 μm) and kaolin (grain
Diameter≤4.0 μm) it is added in mixing slurry together.2) control parameter of half dry-cure are as follows: preceding dry temperature is 100 DEG C, does temperature afterwards
It is 115 DEG C, processing water content into page is 6%.3) in the formula of dye formulations solution oxidized starch and salt mass ratio
For 12:1.4) control parameter of superpressure processing are as follows: pressure 1.0MPa, temperature are 23 DEG C, humidity 43%.
The shield adornment paper of the present embodiment: quantitative: 20.5g/ ㎡；Tensile strength: 1.47kN/m；Wet strength: 0.17kN/m；It is thick
Degree: 24 μm；Air permeability: 2560CU；Smoothness: front: 860S, reverse side: 450S；Ash content: 12.6%；Dynamic contact angle
(0.06s): front: 60 °, reverse side: 75 °；Print ink penetration: 18l/mm.
Embodiment 3
The present embodiment provides a kind of antibacterial shield adornment paper and its production technologies, and the antibacterial adornment paper that protects is according to the raw material of parts by weight
Composition includes: 70 parts of big jute pulps of bleaching, 30 parts of bleaching manila pulps, 27 parts of talcum powder, 6 parts of kaolin, 2 parts of magnesium stearates,
9.7 parts of auxiliary agents, 13.7 parts of dye formulations, auxiliary component is with embodiment 1, and dye formulations are by sunset yellow, lemon yellow, famille rose, bright
Indigo plant, oxidized starch, salt compounding.
Production technology the difference from embodiment 1 is that: 1) by 1250 mesh talcum powder (partial size≤10 μm), kaolin (partial size
≤ 4.0 μm), magnesium stearate (partial size≤4.2 μm) is added in mixing slurry together.2) control parameter of half dry-cure are as follows: preceding dry
Temperature is 110 DEG C, and dry temperature is 120 DEG C afterwards, and processing water content into page is 5%.3) formula of dye formulations solution is Sino-Japan
Fall Huang, lemon yellow, famille rose, brilliant blue mass ratio be 4:3:2:1, and the mass ratio of dyestuff, oxidized starch, salt is
0.7:11:2.4) control parameter of superpressure processing are as follows: pressure 3.0MPa, temperature are 30 DEG C, humidity 50%.
The shield adornment paper of the present embodiment: quantitative: 20.2g/ ㎡；Tensile strength: 1.48kN/m；Wet strength: 0.16kN/m；It is thick
Degree: 23 μm；Air permeability: 2756CU；Smoothness: front: 789S, reverse side: 426S；Ash content: 10.5%；Dynamic contact angle
(0.06s): front: 59 °, reverse side: 70 °；Print ink penetration: 16l/mm.
Embodiment 4
The present embodiment provides a kind of antibacterial shield adornment paper and its production technologies, and the antibacterial adornment paper that protects is according to the raw material of parts by weight
Composition includes: 100 parts of big jute pulps of bleaching, 33 parts of talcum powder, 9.4 parts of auxiliary agents, 13.8 parts of dye formulations.Auxiliary component is the same as implementation
Example 1, dye formulations are compounded by sunset yellow, lemon yellow, chocolate palm fibre, oxidized starch, salt.
Production technology the difference from embodiment 1 is that: sunset yellow, lemon yellow, chocolate in the formula of dye formulations solution
The mass ratio of palm fibre is 11:8:1.
The shield adornment paper of the present embodiment: quantitative: 20.5g/ ㎡；Tensile strength: 1.51kN/m；Wet strength: 0.17kN/m；It is thick
Degree: 25 μm；Air permeability: 3000CU；Smoothness: front: 831S, reverse side: 512S；Ash content: 11.5%；Dynamic contact angle
(0.06s): front: 62 °, reverse side: 76 °；Print ink penetration: 18l/mm.
Embodiment 5
The present embodiment provides a kind of antibacterial shield adornment paper and its production technologies, and the antibacterial adornment paper that protects is according to the raw material of parts by weight
Composition includes: 30 parts of big ramie pulp fibers of bleaching, 50 parts of bleached wood pulp fibers, 20 parts of bleaching bamboo pulp fibres, 28 parts of talcum powder, and 2 parts
Titanium dioxide, 3 parts of calcium carbonate, 12.1 parts of auxiliary agents, 13.6 parts of dye formulations.
Auxiliary agent are as follows: wet strength agent polyamide polyamines-epichlorohydrin resins PAE mass concentration is 15%, its adding in paper pulp
Enter 10% that amount is paper pulp total amount；The mass concentration of guar gum reinforcing agent is 0.3%, its additional amount in paper pulp is paper pulp
The 0.7% of total amount；The mass concentration of guar gum retention agent is 0.3%, its additional amount in paper pulp is paper pulp total amount
0.09%；The mass concentration of dispersing agent polyethylene glycol oxide PEO is 0.03%, its additional amount in paper pulp is paper pulp total amount
0.98%；The mass concentration of neutral sizing agent alkyl ketene dimer is 10%, its additional amount in paper pulp is paper pulp gross weight
The 0.03% of amount；The mass concentration of remover is 0.2%, its additional amount in paper is the 0.30% of paper pulp total amount.
Dye formulations are red by Ka Dasuo, Ka Dasuo is yellow, Ka Dasuolan, oxidized starch, salt compounding.
Production technology the difference from embodiment 1 is that: 1) ramie pulp fiber beating consistency 3.2%, beating degree/weight in wet base (42~
46)°SR/(7.0-7.5)g；Wood pulp cellulose beating consistency 4.0%, beating degree/weight in wet base (44~50) ° SR/ (10.0~11.0)
g；Bamboo pulp fiber beating consistency 4.2%, beating degree/weight in wet base (40~44) ° SR/ (9.0~10.0) g.2) by talcum powder (partial size
≤ 13 μm), titanium dioxide (partial size≤3.5 μm), calcium carbonate (partial size≤4.5 μm) is added in mixing slurry together.3) half dry-cure
Control parameter are as follows: preceding dry temperature is 110 DEG C, and dry temperature is 125 DEG C afterwards, and processing water content into page is 4.7%.4) it contaminates
Expect that Ka Dasuo is red, Ka Dasuo is yellow in the formula of preparation solution, the mass ratio of Ka Dasuolan is 3:13:4, and dyestuff, oxidation form sediment
Powder, salt mass ratio be 0.6:12:1.0.5) control parameter of superpressure processing are as follows: calender is 12 roll calendar machines, by 5
Road press polish processing, calender pressure be 1.5MPa, 25 DEG C of temperature, humidity 42%.
The shield adornment paper of the present embodiment: quantitative: 14.3g/ ㎡；Tensile strength: 1.49kN/m；Wet strength: 0.13kN/m；It is thick
Degree: 22 μm；Air permeability: 2730CU；Smoothness: front: 823S, reverse side: 425S；Ash content: 10.9%；Dynamic contact angle
(0.06s): 61 °, 72 ° of reverse side of front；Print ink penetration: 18l/mm.
Embodiment 6
The present embodiment provides a kind of antibacterial shield adornment paper and its production technologies, and the antibacterial adornment paper that protects is according to the raw material of parts by weight
Composition includes: 70 parts of big ramie pulp fibers of true qualities, 30 parts of true qualities bamboo pulp fibers, 29 parts of talcum powder, 3 parts of kaolin, 3 parts of stearic acid
Magnesium, 12 parts of auxiliary agents, 12 parts of dye formulations.Auxiliary component is compounded with embodiment 5, dye formulations by oxidized starch, salt.
The difference of production technology and embodiment 5 is: 1) by 1250 mesh talcum powder (partial size≤10 μm), kaolin (partial size
≤ 4.0 μm), magnesium stearate (partial size≤4.2 μm) is added in mixing slurry together.2) it is aoxidized in the formula of dye formulations solution
Starch, salt mass ratio are 11:1.
The shield adornment paper of the present embodiment: quantitative: 14.5g/ ㎡；Tensile strength: 1.48kN/m；Wet strength: 0.14 kN/m；It is thick
Degree: 22 μm；Air permeability: 2836CU；Smoothness: front: 974S, reverse side: 548S；Ash content: 10.8%；Dynamic contact angle
(0.06s): front: 62 °, reverse side: 78 °；Print ink penetration: 19l/mm.
Embodiment 7
The present embodiment provides a kind of antibacterial shield adornment paper and its production technologies, and the antibacterial adornment paper that protects is according to the raw material of parts by weight
Composition includes: 100 parts of big ramie pulp fibers of bleaching, 31 parts of talcum powder, 2 parts of magnesium stearates, 12 parts of auxiliary agents, 13.2 parts of dye formulations.
Auxiliary component is compounded with embodiment 5, dye formulations by sunset yellow, lemon yellow, brilliant blue, oxidized starch, salt.
The difference of production technology and embodiment 5 is: 1) by talcum powder (partial size≤3.5 μm), magnesium stearate (partial size≤
13 μm) it is added in mixing slurry together.2) sunset yellow in the formula of dye formulations solution, lemon yellow, brilliant blue mass ratio be
55:42:3.
The shield adornment paper of the present embodiment: quantitative: 14.5g/ ㎡；Tensile strength: 1.45kN/m；Wet strength: 0.13kN/m；It is thick
Degree: 22 μm；Air permeability: 2719CU；Smoothness: front: 874S, reverse side: 461S；Ash content: 10.2%；Dynamic contact angle
(0.06s): front: 65 °, reverse side: 74 °；Print ink penetration: 20l/mm.
Embodiment 8
The present embodiment provides a kind of antibacterial shield adornment paper and its production technologies, and the antibacterial adornment paper that protects is according to the raw material of parts by weight
Composition includes: 40 parts of big ramie pulp fibers of bleaching, 40 parts of bleached wood pulp fibers, 20 parts of bleaching bamboo pulp fibres, 29 parts of talcum powder, and 2 parts
Titanium dioxide, 3 parts of calcium carbonate, 11.7 parts of auxiliary agents, 13.9 parts of dye formulations.
Auxiliary agent are as follows: wet strength agent polyamide polyamines-epichlorohydrin resins PAE mass concentration is 15%, its adding in paper pulp
Enter 10% that amount is paper pulp total amount；The mass concentration of guar gum reinforcing agent is 0.3%, its additional amount in paper pulp is paper pulp
The 0.5% of total amount；The mass concentration of guar gum retention agent is 0.3%, its additional amount in paper pulp is paper pulp total amount
0.07%；The mass concentration of dispersing agent polyethylene glycol oxide PEO is 0.03%, its additional amount in paper pulp is paper pulp total amount
0.79%；The mass concentration of neutral sizing agent alkyl ketene dimer is 10%, its additional amount in paper pulp is paper pulp gross weight
The 0.05% of amount；The mass concentration of remover is 0.2%, its additional amount in paper is the 0.20% of paper pulp total amount.
Dye formulations are red by Ka Dasuo, Ka Dasuo is yellow, Ka Dasuolan, oxidized starch, salt compounding.
Production technology the difference from embodiment 1 is that: 1) ramie pulp fiber beating consistency 2.8%, beating degree/weight in wet base (30~
34)°SR/(8.5-9.5)g；Wood pulp cellulose beating consistency 3.8%, beating degree/weight in wet base (34~38) ° SR/ (13.0~14.0)
g；Bamboo pulp fiber beating consistency 4.0%, beating degree/weight in wet base (32~36) ° SR/ (12.0~13.0) g.2) by talcum powder (partial size
≤ 13 μm), titanium dioxide (partial size≤3.5 μm), calcium carbonate (partial size≤4.5 μm) is added in mixing slurry together.3) half dry-cure
Control parameter are as follows: preceding dry temperature is 100 DEG C, and dry temperature is 121 DEG C afterwards, and processing water content into page is 4.6%.4) it contaminates
Expect that Ka Dasuo is red, Ka Dasuo is yellow in the formula of preparation solution, the mass ratio of Ka Dasuolan is 4:13:3, and dyestuff, oxidation form sediment
Powder, salt mass ratio be 0.4:11.5:2.5) control parameter of superpressure processing are as follows: calender is 12 roll calendar machines, by 8
Road press polish processing, calender pressure be 2.2MPa, 23 DEG C of temperature, humidity 45%.
The shield adornment paper of the present embodiment: quantitative: 25.2g/ ㎡；Tensile strength: 1.52kN/m；Wet strength: 0.18 kN/m；It is thick
Degree: 25 μm；Air permeability: 2120CU；Smoothness: positive 716S, reverse side: 362S；Ash content: 14.5%；Dynamic contact angle
(0.06s): front: 56 °, reverse side: 66 °；Print ink penetration: 15l/mm.
Embodiment 9
The present embodiment provides a kind of antibacterial shield adornment paper and its production technologies, and the antibacterial adornment paper that protects is according to the raw material of parts by weight
Composition includes: 60 parts of big ramie pulp fibers of bleaching, 40 parts of bleached wood pulp fibers, 32 parts of talcum powder, 3 parts of kaolin, 11.5 parts of auxiliary agents,
14 parts of dye formulations.Auxiliary component is with embodiment 8, and dye formulations are by sunset yellow, lemon yellow, chocolate palm fibre, oxidized starch, food
Salt compounding.
The difference of production technology and embodiment 8 is: 1) by talcum powder (partial size≤10 μm), kaolin (partial size≤4.0 μ
M) it is added in mixing slurry together.2) sunset yellow in the formula of dye formulations solution, lemon yellow, chocolate palm fibre mass ratio be
15:8:2.
The shield adornment paper of the present embodiment: quantitative: 25.3g/ ㎡；Tensile strength: 1.57kN/m；Wet strength: 0.18kN/m；It is thick
Degree: 26 μm；Air permeability: 2204CU；Smoothness: front: 721S, reverse side: 373S；Ash content: 15.1%；Dynamic contact angle
(0.06s): front: 55 °, reverse side: 67 °；Print ink penetration: 15l/mm.
Embodiment 10
Performance detection is carried out to the shield adornment paper that above-mentioned 9 embodiments obtain.
1) technical indicator detects, as shown in table 1.
Table 1
2) microorganism detection, as shown in table 2.
2 microorganism detection result of table
Note: detection method executes GB/T 7918-87 Cosmetics microorganism standard test method.Total number of bacteria limit value
' 500 ', yeast and mold sum limit value ' 100 ', heat-resisting coliform, staphylococcus aureus, pseudomonas aeruginosa, limit
Value is ' must not detect ', and ND is ' being not detected '.
3) harmful substance detects, as shown in table 3.
3 harmful substance testing result of table
Note: detection method executes the GB/T 7917-87 cosmetics health chemical standard method of inspection.Mercury limit value ' 1 ', arsenic limit
Value ' 2 ', lead limit value ' 10 ', cadmium limit value ' 5 ', methanol limit value ' 2000 ', ND are ' being not detected '.
Embodiment 11
Using effect detection
30 female volunteers take part in this experiment, their age was Oily between 20~50 years old.
By totally 1500, shield adornment paper of Examples 1 to 9 preparation, contrast product is that certain cat situation of selling well shield adornment paper 1500 is opened, for 30 women will
Hope person uses one week, and every volunteer distributes each 50, shield adornment paper of the present invention and contrast product, to paper pliability, smooth
Degree, oil absorbing effect and shield adornment effect are given a mark respectively, wherein≤20 points of expressions are excessively poor, 30~40 points of expressions are poor, 50~60 points of tables
Show that generally 70~80 points indicate, >=90 points of expressions are very good, and the results are shown in Table 4.
4 using effect evaluation result of table
Note: when calculating average mark by the way of rounding up.
By table 4 results, it can be seen that shield adornment paper of the invention has good paper pliability, smoothness, suction
Oily effect and shield adornment effect, assessment person's reaction are good.
In short, using the present invention, the shield adornment paper of acquisition has the function of shield adornment, antibacterial, higher air permeability and reasonably
Ink penetration performance is printed, face's surface layer grease can be adsorbed rapidly, can reach good it is not necessary that any oil-absorbing resin is added
Oil absorbing effect, and paper is smooth, thin and flexible, can preferably be bonded skin, plays good absorption to grease, makes
Skin feels very comfortable；There is reasonable dynamic contact angle can guarantee that the moisture of skin is not inhaled all by paper simultaneously
It receives, makes face surface layer that there is moisture appropriate, oil, imperceptible drying being used for multiple times, shield adornment effect is obvious, fits
For all skin quality.
Although the embodiments of the present invention has been shown and described above, it is to be understood that above-described embodiment is example
Property, it is not considered as limiting the invention, those skilled in the art within the scope of the invention can be to above-mentioned
Embodiment is changed, modifies, replacement and variant.
Claims (10)
1. a kind of antibacterial shield adornment paper, which is characterized in that forming according to the raw material of parts by weight includes: 20 ~ 100 parts of ramie pulp fibers, 0 ~
80 parts of wood pulp celluloses, 0 ~ 80 part of bamboo pulp fiber, 25 ~ 35 parts of fillers, 5 ~ 13 parts of auxiliary agents.
2. the antibacterial shield adornment paper of one kind according to claim 1, which is characterized in that the ramie pulp fiber is hemp, Manila
Fiber crops, sisal hemp, including bleaching and true qualities；The wood pulp cellulose is softwood pulp, including bleaching and true qualities；The bamboo pulp fiber includes
Bleaching and true qualities bamboo pulp.
3. the antibacterial shield adornment paper of one kind according to claim 1, which is characterized in that the filler is selected from partial size≤4.0 μm
Kaolin, the magnesium stearate of partial size≤4.2 μm, the titanium dioxide of partial size≤3.5 μm, the calcium carbonate of partial size≤4.5 μm, partial size≤13
μm one or more of talcum powder.
4. the antibacterial shield adornment paper of one kind according to claim 1, which is characterized in that the auxiliary agent be selected from wet strength agent, reinforcing agent,
One of retention agent, dispersing agent, sizing agent, remover are a variety of.
5. the antibacterial shield adornment paper of one kind according to claim 1, which is characterized in that the shield adornment paper further includes 9.1 ~ 16 parts
Food grade dyes preparation.
6. the antibacterial shield adornment paper of one kind according to claim 5, which is characterized in that the food grade dyes preparation is by food-grade
Dyestuff, oxidized starch, salt are (0 ~ 1.0): (8 ~ 12) according to mass ratio: (1.0 ~ 3.0) compounding is made.
7. the antibacterial shield adornment paper of one kind according to claim 6, which is characterized in that the food grade dyes are selected from brilliant blue, day
Fall that Huang, lemon yellow, chocolate palm fibre, amaranth, famille rose, Ka Dasuo is red, Ka Dasuo is yellow, one or more of Ka Dasuolan.
8. the antibacterial shield adornment paper of one kind according to claim 1, which is characterized in that the index of the shield adornment paper are as follows: quantitative: 14
~25g/㎡；Tensile strength: >=1.3kN/m；Wet strength >=0.15 kN/m；Thickness :≤27 μm；Air permeability: >=2000CU；Smoothly
Degree: front >=700S, reverse side >=350S；Ash content: (10 ~ 16) %；Dynamic contact angle (0.06s): front >=55 °, reverse side >=65 °；
Print ink penetration: (15~20) l/mm.
9. the production method of the antibacterial shield adornment paper of one kind described in claim 1 ~ 8 any one claim, which is characterized in that packet
Include following steps:
Ingredient is formed according to the raw material of above-mentioned shield adornment paper, fibrous raw material is first subjected to mashing processing, be disposed addition
Filler；
The mixed slurry that step (1) obtains is diluted, auxiliary agent is then added, is successively being dehydrated through wet end molding and press section
Processing to water content is 60 ~ 70%, obtains l Water Paper page；
By l Water Paper page successively through half dry-cure, batch to obtain shield adornment paper body paper；
Shield adornment paper body paper is subjected to superpressure processing, both.
10. the production method of the antibacterial shield adornment paper of one kind according to claim 9, which is characterized in that the production method is also
Including by the process of half-dried treated the page dip-coating dye formulations solution of step (3).
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| CN112695570A (en) * | 2020-12-25 | 2021-04-23 | 牡丹江恒丰纸业股份有限公司 | Preparation method of antibacterial food wiping paper |
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