CN110512129A - A kind of forging torsion integrated technique preparing superelevation severe deformation magnesium alloy rod - Google Patents

A kind of forging torsion integrated technique preparing superelevation severe deformation magnesium alloy rod Download PDF

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Publication number
CN110512129A
CN110512129A CN201910812838.3A CN201910812838A CN110512129A CN 110512129 A CN110512129 A CN 110512129A CN 201910812838 A CN201910812838 A CN 201910812838A CN 110512129 A CN110512129 A CN 110512129A
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deformation
magnesium alloy
swaging
control
forging
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万迎春
杨正江
刘楚明
高永浩
曾广
蒋树农
陈志永
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Central South University
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Central South University
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J5/00Methods for forging, hammering, or pressing; Special equipment or accessories therefor
    • B21J5/002Hybrid process, e.g. forging following casting
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C23/00Alloys based on magnesium
    • C22C23/06Alloys based on magnesium with a rare earth metal as the next major constituent
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/06Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of magnesium or alloys based thereon

Abstract

The present invention relates to a kind of forgings of magnesium alloy bar with superhigh intensity to turn round integrated technique.The quality of magnesium alloy percent composition are as follows: Mg-8.0 ~ 9.6Gd-1.8 ~ 3.2Y-0.3 ~ 0.7Zr, impurity include Fe, Si, Cu, Ni and other inevitable impurity elements, wherein Fe≤0.02%, Si≤0.02%, Cu≤0.005%, Ni≤0.003%, content of impurities are no more than 0.1%.Process route are as follows: semi-continuous casting, is hot extruded into bar at homogenizing annealing, obtained extruded rod is complete dynamic recrystallized structure, average grain size is 10-15 μm, then deformation of swaging radially is carried out along bar, controlling temperature of swaging is 10 ~ 150 DEG C, controlling pass deformation is 6 ~ 12%, total deformation is 6 ~ 25%, control charging rate is 3 ~ 6mm/min, finally carry out free end torsional deflection, control torsion temperature is 10 ~ 100 DEG C, and control passage torsional shear strain is 5 ~ 30%, and control reverse speed is 5 ~ 100 °/min.Finally obtained tensile strength >=460MPa, yield strength >=370MPa, the magnesium alloy rod of elongation after fracture >=6.5%.

Description

A kind of forging torsion integrated technique preparing superelevation severe deformation magnesium alloy rod
Technical field
The present invention relates to superelevation severe deformation field of magnesium alloy, the in particular to deformation of swaging of Mg-Gd-Y-Zr magnesium-rare earth With torsional deflection field.
Technical background
Magnesium alloy is due to low density, and high rigidity, specific strength and the features such as be easily recycled are known as " 21 generation Discipline green engineering material ", as the lightweight structural material of a new generation, excellent loss of weight is in space flight and aviation, rail traffic etc. The utilization in field has great significance.But one of the technical bottleneck for hindering magnesium alloy to use on a large scale is exactly magnesium alloy power Learn performance it is poor, it is difficult to performance requirement needed for meeting Service Environment, with when there are some potential safety problemss.Compared to casting Magnesium alloy, wrought magnesium alloy is due to receive more and more attention with superior mechanical property, research and utilization.Cause This, exploration prepares the new technology of superhigh strength magnesium alloy to improve magnesium alloy strength, is the important research in wrought magnesium alloy field Target.Have great importance for the popularization of wrought magnesium alloy.
Summary of the invention
The present invention provides a kind of forgings for preparing super high-strength deforming magnesium alloy to turn round integrated technique.It is super its purpose is to prepare High-intensitive wrought magnesium alloy, the quality of magnesium alloy percent composition are as follows: Mg-8.0 ~ 9.6Gd-1.8 ~ 3.2Y-0.3 ~ 0.7Zr produces magnesium alloy ingot blank using semicontinuous electromagnetic casting method first, after magnesium alloy ingot blank is carried out homogenization heat treatment Bar is obtained by hot extrusion, deformation of swaging radially then is carried out to extruded bars, finally the bar after swaging is carried out certainly By end torsional deflection.Using magnesium alloy rod room temperature tensile intensity >=460MPa made from the method, yield strength >=370MPa, Elongation after fracture >=6.5%.It is being proposed in the present invention the specific process is as follows:
1. preparing magnesium alloy ingot using semi-continuous casting method, ingot casting carries out stress relief annealing after casting immediately;
2. ingot casting is carried out Homogenization Treatments, room temperature is then cooled to the furnace;
3. pair ingot casting carries out railway carriage, flaw detection, sawing machine blanking obtains cylindrical ingot blank.
4. cylindrical ingot blank is carried out hot extrusion deformation, obtained extruded rod is complete dynamic recrystallized structure, average crystalline substance Particle size is 10-15 μm.
5. radially carrying out deformation of swaging along extruded bars, controlling temperature of swaging is 10 ~ 150 DEG C, and control pass deformation is 5 ~ 20%, total deformation is 5 ~ 30%, and control charging rate is 3 ~ 6mm/min.
6. the bar after swaging carries out free end torsional deflection, control torsion temperature is 10 ~ 100 DEG C, and control passage is turned round Turning shear strain is 5 ~ 30%, and control reverse speed is 5 ~ 100 °/min.
The deformation of swaging, controlling temperature of swaging is 10 ~ 100 DEG C.
The deformation of swaging controls total deformation 6 ~ 20% of swaging.
The deformation of swaging, control charging rate are 4 ~ 6mm/min.
The free end torsional deflection, control torsion temperature is 10 ~ 50 DEG C.
The free end torsional deflection, control bar torsional shear strain is 10 ~ 30%.
The free end torsional deflection, control reverse speed are 5 ~ 30 °/min.
Advantages of the present invention has:
1. magnesium alloy is first carried out to hot extrusion deformation can reduce defects count and size inside casting alloy, it is tiny to obtain crystal grain Dynamic recrystallized structure, improve alloy deformation plasticity, improve follow-up cold deformation during pass deformation and total deformation, Improve alloy strength.
2. the extruded rod that hot extrusion is formed is carried out deformation of swaging, swaging to deform can be achieved high Steady-State security, reduce The tearing tendency of magnesium alloy improves total deformation;Deformation of swaging can also be achieved high strain rate, and magnesium can be improved in high strain rate The dislocation density that can be accumulated before alloy cracking, high density dislocation, which can induce, forms nanometer scale inside magnesium alloy;Substructure;It swages When the temperature is excessively high, the defects of dynamic recovery or recrystallization are easy to produce when deformation, not only makes the dislocation of intra-die is buried in oblivion, and is cut Weak work-hardening effect, dynamic recrystallization can also make grain coarsening, reduce alloy strength.When swaging for 10-100 DEG C, not only make The hardness of alloy bar material cross section rises overally, and can also obtain high rigidity area in bar center portion.Total deformation of swaging is greater than 30%, bar cracking is not only easily led to, but also the subsequent plastic deformation ability of alloy can be reduced, reduces the change of subsequent torsional deflection Shape amount.If total deformation of swaging is lower than 6%, weaker to the strengthening effect of material.And when being swaged at room temperature, when total Dependent variable is 6%-30%, and the attainable maximum shear strain of the institute of Surface of Rod Bar is respectively 46%-18%.
3. deformation of swaging can make bar centre hardness much higher than edge.And the sample after swaging carries out torsional deflection, Bar edge can be refined, bar edge is induced and generates shear band, improve bar edge hardness and intensity.Add torsion using swaging The integrated technique microstructure and mechanical property of bar radially that can to swage it is more uniform, reach better strengthening effect. It when torsional deflection is lower than 15%, is not enough to excite the generation of shear band, when strain is higher than 30%, is easy inducing materials shearing instability, It cracks, shear strain amount is controlled at 15 ~ 30%, and bar strengthening effect is best.
4. produce magnesium alloy ingot blank using semi-continuous casting method, can reduce be mingled with, stomata, loose, centre burst etc. lack It falls into.Control defects count can reduce its tearing tendency during deformation after unloading, improve magnesium alloy it is subsequent swage deformation and Formability during torsional deflection improves achievable total deformation.
Specific embodiment
Embodiment 1
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
B. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;
C. extruded bars are subjected to deformation of swaging at 20 DEG C, pass deformation 6%, total deformation 6%, controlling charging rate is 4mm/min;
D. the bar that will swage carries out torsional deflection at 20 DEG C, and control Surface of Rod Bar passage torsional strain is 17%, and Surface of Rod Bar is total Torsional shear strain is 17%, and torsion temperature is 20 DEG C, and reverse speed is 10 °/min.
Mechanics Performance Testing is carried out to gained magnesium alloy rod according to GB/T228-2002, the results are shown in Table 1.
Embodiment 2
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
E. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;
B. extruded bars are subjected to deformation of swaging at 20 DEG C, pass deformation 6%, total deformation 6%, controlling charging rate is 4mm/min;
C. the bar that will swage carries out torsional deflection at 20 DEG C, and control Surface of Rod Bar passage torsional strain is 25%, and Surface of Rod Bar is total Torsional shear strain is 25%, and torsion temperature is 20 DEG C, and reverse speed is 10 °/min.
Mechanics Performance Testing is carried out to gained magnesium alloy rod according to GB/T228-2002, the results are shown in Table 1.
Embodiment 3
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
F. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;
B. extruded bars are subjected to deformation of swaging at 20 DEG C, pass deformation 6%, total deformation 6%, controlling charging rate is 4mm/min;
C. the bar that will swage carries out torsional deflection at 20 DEG C, and control Surface of Rod Bar passage torsional strain is 18%, 6%, 4%, bar The strain of total surface torsional shear is 28%, and torsion temperature is 20 DEG C, and reverse speed is 10 °/min.
Mechanics Performance Testing is carried out to gained magnesium alloy rod according to GB/T228-2002, the results are shown in Table 1.
Embodiment 4
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
B. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;
C. extruded bars are subjected to deformation of swaging, pass deformation 12%, total deformation 12%, control charging speed at 20 DEG C Degree is 4mm/min;
D. the bar that will swage carries out torsional deflection at 20 DEG C, and control Surface of Rod Bar passage torsional strain is 15%, and Surface of Rod Bar is total Torsional shear strain is 15%, and torsion temperature is 20 DEG C, and reverse speed is 10 °/min.
Mechanics Performance Testing is carried out to gained nanometer isomery magnesium alloy according to GB/T228-2002, the results are shown in Table 1.
Embodiment 5
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
B. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;
C. extruded bars are subjected to deformation of swaging, pass deformation 12%, total deformation 12%, control charging speed at 20 DEG C Degree is 4mm/min;
D. the bar that will swage carries out torsional deflection at 20 DEG C, and control Surface of Rod Bar passage torsional strain is 23%, and Surface of Rod Bar is total Torsional shear strain is 23%, and torsion temperature is 20 DEG C, and reverse speed is 10 °/min.
Mechanics Performance Testing is carried out to gained magnesium alloy rod according to GB/T228-2002, the results are shown in Table 1.
Embodiment 6
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
B. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;
C. extruded bars are subjected to deformation of swaging at 20 DEG C, control pass deformation is 6%, 6%, total deformation 12%, control into Material speed is 4mm/min;
D. the bar that will swage carries out torsional deflection at 20 DEG C, and control Surface of Rod Bar passage torsional strain is 15%, and Surface of Rod Bar is total Torsional shear strain is 15%, and torsion temperature is 20 DEG C, and reverse speed is 10 °/min.
Mechanics Performance Testing is carried out to gained magnesium alloy rod according to GB/T228-2002, the results are shown in Table 1.
Embodiment 7
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
B. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;;
C. extruded bars are subjected to deformation of swaging at 20 DEG C, control pass deformation is 6%, 6%, total deformation 12%, control into Material speed is 4mm/min;
D. the bar that will swage carries out torsional deflection at 20 DEG C, and control Surface of Rod Bar passage torsional strain is 10%, 10%, 5%, stick The strain of material total surface torsional shear is 25%, and torsion temperature is 20 DEG C, and reverse speed is 10 °/min.
Mechanics Performance Testing is carried out to gained magnesium alloy rod according to GB/T228-2002, the results are shown in Table 1.
Embodiment 8
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
B. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;;
C. extruded bars are subjected to deformation of swaging at 20 DEG C, control pass deformation is 6%, 6%, 5%, total deformation 17%, control Charging rate processed is 4mm/min;
D. the bar that will swage carries out torsional deflection at 20 DEG C, and control Surface of Rod Bar passage torsional strain is 15%, and Surface of Rod Bar is total Torsional shear strain is 15%, and torsion temperature is 20 DEG C, and reverse speed is 10 °/min.
Mechanics Performance Testing is carried out to gained magnesium alloy rod according to GB/T228-2002, the results are shown in Table 1.
Embodiment 9
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
B. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;;
C. extruded bars are subjected to deformation of swaging at 20 DEG C, control pass deformation is 6%, 6%, 5%, total deformation 17%, control Charging rate processed is 4mm/min;
D. the bar that will swage carries out torsional deflection at 20 DEG C, and control Surface of Rod Bar passage torsional strain is 23%, and Surface of Rod Bar is total Torsional shear strain is 23%, torsion temperature is 20 DEG C, and reverse speed is 10 °/min.
Mechanics Performance Testing is carried out to gained magnesium alloy rod according to GB/T228-2002, the results are shown in Table 1.
Embodiment 10
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
B. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;
C. extruded bars are subjected to deformation of swaging at 20 DEG C, control pass deformation is 6%, 6%, 5%, total deformation 17%, control Charging rate processed is 4mm/min;
D. the bar that will swage carries out torsional deflection at 20 DEG C, and control Surface of Rod Bar passage torsional strain is 10%, 10%, 5%, stick The strain of material total surface torsional shear is 25%, and torsion temperature is 20 DEG C, and reverse speed is 10 °/min.
Mechanics Performance Testing is carried out to gained nanometer isomery magnesium alloy according to GB/T228-2002, the results are shown in Table 1.
Comparative example 1
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
B. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;
C. extruded bars are subjected to deformation of swaging at 20 DEG C, control pass deformation is 6%, total deformation 6%, control charging speed Degree is 4mm/min.
Mechanics Performance Testing is carried out to gained magnesium alloy rod according to GB/T228-2002, the results are shown in Table 2.
Comparative example 2
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
B. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;
C. extruded bars are subjected to deformation of swaging at 20 DEG C, control pass deformation is 12%, total deformation 12%, control charging Speed is 4mm/min
Mechanics Performance Testing is carried out to gained magnesium alloy rod according to GB/T228-2002, the results are shown in Table 2.
Comparative example 3
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
B. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;
C. extruded bars are subjected to deformation of swaging at 20 DEG C, control pass deformation is 6%, 6%, total deformation 12%, control into Material speed is 4mm/min;
Mechanics Performance Testing is carried out to gained magnesium alloy rod according to GB/T228-2002, the results are shown in Table 2.
Comparative example 4
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
B. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;
C. extruded bars are subjected to deformation of swaging at 20 DEG C, control pass deformation is 6%, 6%, 5%, total deformation 17%, control Charging rate processed is 4mm/min;
Mechanics Performance Testing is carried out to gained magnesium alloy rod according to GB/T228-2002, the results are shown in Table 2.
Comparative example 5
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
B. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;
C. extruded bars are subjected to torsional deflection at 20 DEG C, control Surface of Rod Bar passage torsional strain is 15%, and Surface of Rod Bar is total Torsional shear strain is 15%, and torsion temperature is 20 DEG C, and reverse speed is 10 °/min.
Mechanics Performance Testing is carried out to gained nanometer isomery magnesium alloy according to GB/T228-2002, the results are shown in Table 2.
Comparative example 6
A. the quality of magnesium alloy percent composition are as follows: Mg-8.0Gd-3.0Y-0.4Zr prepares magnesium using semi-continuous casting method Alloy ingot blank, and carry out homogenization heat treatment;
B. the alloy blank after Homogenization Treatments is subjected to hot extrusion deformation, obtained extruded rod is complete dynamic recrystallization group It knits, average grain size is 12 μm;
C. extruded bars are subjected to torsional deflection at 20 DEG C, control Surface of Rod Bar passage torsional strain is 23%, and Surface of Rod Bar is total Torsional shear strain is 23%, and torsion temperature is 20 DEG C, and reverse speed is 10 °/min.
Mechanics Performance Testing is carried out to gained nanometer isomery magnesium alloy according to GB/T228-2002, the results are shown in Table 2.
Table 1
Table 2

Claims (7)

1. integrated technique is turned round in a kind of forging for preparing superelevation severe deformation magnesium alloy rod, it is characterised in that: the quality of magnesium alloy hundred Divide and compare ingredient are as follows: the mass ratio of Gd:8.0-9.6%, Y:1.8-3.2%, Zr:0.3-0.7%, Gd and Y are as follows: 3≤Gd/Y≤5, remaining For Mg and Fe, Si, Cu, Ni and other inevitable impurity elements, the mass content of impurity element, Fe≤0.02%, Si ≤ 0.02%, Cu≤0.005%, Ni≤0.003%, content of impurities are no more than 0.1%, specifically includes the following steps:
Magnesium alloy ingot blank is prepared using semicontinuous electromagnetic casting method;
Magnesium alloy ingot blank is subjected to homogenization heat treatment, the blank after heat treatment is subjected to hot extrusion deformation, obtained extruded rod For complete dynamic recrystallized structure, average grain size is 10-15 μm;
Deformation of swaging radially is carried out along extruded bars, controlling temperature of swaging is 10 ~ 150 DEG C, and control pass deformation is 6 ~ 12%, Total deformation is 6 ~ 25%, and control charging rate is 3 ~ 6mm/min;
Bar after swaging carries out free end torsional deflection, and control torsion temperature is 10 ~ 100 DEG C, controls passage torsional shear Strain is 5 ~ 30%, and control reverse speed is 5 ~ 60 °/min.
2. integrated technique is turned round in a kind of forging for preparing superelevation severe deformation magnesium alloy rod according to claim 1, it is characterised in that: The deformation of swaging, controlling temperature of swaging is 10 ~ 100 DEG C.
3. integrated technique is turned round in a kind of forging for preparing superelevation severe deformation magnesium alloy rod according to claim 1, it is characterised in that: The deformation of swaging controls total deformation 6 ~ 20% of swaging.
4. integrated technique is turned round in a kind of forging for preparing superelevation severe deformation magnesium alloy rod according to claim 1, it is characterised in that: The deformation of swaging, control charging rate are 4 ~ 6mm/min.
5. integrated technique is turned round in a kind of forging for preparing superelevation severe deformation magnesium alloy rod according to claim 1, it is characterised in that: The free end torsional deflection, control torsion temperature is 10 ~ 50 DEG C.
6. integrated technique is turned round in a kind of forging for preparing superelevation severe deformation magnesium alloy rod according to claim 1, it is characterised in that: The free end torsional deflection, the torsional shear strain for controlling Surface of Rod Bar is 10 ~ 30%.
7. integrated technique is turned round in a kind of forging for preparing superelevation severe deformation magnesium alloy rod according to claim 1, it is characterised in that: The free end torsional deflection, control reverse speed are 5 ~ 30 °/min.
CN201910812838.3A 2019-08-30 2019-08-30 A kind of forging torsion integrated technique preparing superelevation severe deformation magnesium alloy rod Pending CN110512129A (en)

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CN114318187A (en) * 2021-12-08 2022-04-12 中国科学院金属研究所 Biomedical high-purity high-strength corrosion-resistant Mg-Zn-Mn magnesium alloy wire and preparation method thereof
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CN102965557A (en) * 2012-11-30 2013-03-13 东北大学 Mg-8Gd-2Y-Li-Zr magnesium alloy and manufacturing method thereof
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CN108203784A (en) * 2016-12-19 2018-06-26 北京有色金属研究总院 A kind of magnesium alloy net with electro-magnetic screen function and preparation method thereof
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CN108728711A (en) * 2018-07-07 2018-11-02 中南大学 A kind of strong Mg-Gd-Y-Zr nanometer gradients magnesium alloy preparation method of superelevation
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CN112030086A (en) * 2020-08-26 2020-12-04 中南大学 Method for improving fatigue resistance of cast magnesium alloy
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CN114318187B (en) * 2021-12-08 2022-08-05 中国科学院金属研究所 Biomedical high-purity high-strength corrosion-resistant Mg-Zn-Mn magnesium alloy wire and preparation method thereof
CN114522998A (en) * 2022-01-20 2022-05-24 江苏大学 Preparation method of high-strength high-heat coating hardening and corrosion-resistant magnesium alloy
CN114507799A (en) * 2022-02-21 2022-05-17 山西银光华盛镁业股份有限公司 Heat-resistant high-strength rare earth magnesium alloy material and preparation
CN115011824A (en) * 2022-06-30 2022-09-06 中南大学 High-strength and high-creep-resistance magnesium alloy and preparation method and application thereof
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