CN110507603A - A kind of solidification seawater gel and preparation method thereof - Google Patents
A kind of solidification seawater gel and preparation method thereof Download PDFInfo
- Publication number
- CN110507603A CN110507603A CN201910864003.2A CN201910864003A CN110507603A CN 110507603 A CN110507603 A CN 110507603A CN 201910864003 A CN201910864003 A CN 201910864003A CN 110507603 A CN110507603 A CN 110507603A
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- seawater
- gel
- sodium hyaluronate
- solidification
- preparation
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/30—Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
- A61K47/36—Polysaccharides; Derivatives thereof, e.g. gums, starch, alginate, dextrin, hyaluronic acid, chitosan, inulin, agar or pectin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/06—Ointments; Bases therefor; Other semi-solid forms, e.g. creams, sticks, gels
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/02—Drugs for dermatological disorders for treating wounds, ulcers, burns, scars, keloids, or the like
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Abstract
The invention discloses a kind of solidification seawater gels and preparation method thereof, belong to drug, medical instrument and cosmetics manufacturing technology field, and the present invention can cooperate delivery device to use.The present invention provides a kind of solidification seawater gel and preparation method thereof with good adhesion.Solidify seawater gel, component is made of seawater and Sodium Hyaluronate, and every 1000L solidifies in seawater gel to be made of the raw material of following parts by weight: 260~990kg of seawater, 0.1~50kg of Sodium Hyaluronate, surplus are purified water.The relative molecular weight of the Sodium Hyaluronate are as follows: 1 × 104~6 × 106.The preparation method for solidifying seawater gel, includes the following steps: step 1: seawater and purified water are mixed and heated to 60~80 DEG C；Step 2: Sodium Hyaluronate, stirring to abundant dissolution are slowly added into the mixed liquor after heating；Step 3: the solution described in the step 2 be fully cooled after to get the solidification seawater gel.
Description
Technical field
The invention belongs to drug, medical instrument and cosmetics manufacturing technology fields, solidifying more particularly to a kind of solidification seawater
Glue and preparation method thereof, the present invention can cooperate delivery device to use.
Background technique
Physiological seawater nasal sprayer (main component is seawater) is two class medical instruments, and the scope of application is for improving
Acute, chronic, drying property, atrophic, allergic rhinitis and the postoperative caused symptom of nasal cavity, restore nasal cavity function.But seawater
Mobility is big, and most of seawater is flowed out by nostril after spraying into nasal cavity, without good adhesion, cannot be attached to nose for a long time
It is intracavitary, substantially reduce therapeutic effect.
Summary of the invention
In view of the problems of the existing technology, the present invention provide a kind of solidification seawater gel with good adhesion and
Preparation method.
To achieve the goals above, the present invention adopts the following technical scheme: a kind of solidification seawater gel, component by seawater and
Sodium Hyaluronate composition, every 1000L solidifies in seawater gel to be made of the raw material of following parts by weight: 260~990kg of seawater, thoroughly
Bright matter acid 0.1~50kg of sodium, surplus is purified water.
Preferably, the relative molecular weight of the Sodium Hyaluronate are as follows: 1 × 104~6 × 106。
The preparation method for solidifying seawater gel, includes the following steps:
Step 1: seawater and purified water are mixed and heated to 60~80 DEG C；
Step 2: Sodium Hyaluronate, stirring to abundant dissolution are slowly added into the mixed liquor after heating；
Step 3: the solution described in the step 2 be fully cooled after to get the solidification seawater gel.
Seawater: minerals and restraining and sterilizing bacteria effect rich in has the effect of improving inflammatory surface.
Sodium Hyaluronate: having very high clinical value, is applied to Lens implantation, corneal transplantation, in operation for glaucoma,
Can the diseases such as treatment of arthritis, have and moisten protection skin, restore the effect of skin physiology function, accelerating wound healing.
The present invention combines both seawater and Sodium Hyaluronate, and effect complements each other, and it is big to solve seawater mobility
Problem reduces its mobility, increases the function and effect of product, can be widely applied to medical instrument, drug, in cosmetics,
This blank of multiple fields is filled up.
Major function: solidification seawater gel of the invention have good adhesion, can skin surface include people and
Certain time is stopped in animal cavity and on mucous membrane, there is nourishing and restraining and sterilizing bacteria for inflammatory surface, improve inflammatory surface's
Effect.In addition, solidification seawater gel of the invention can moisten protection skin, restore skin physiology function, accelerating wound healing,
It is mainly used for the positions such as skin, mucous membrane, oral cavity, nasal cavity, throat.
The formula of the invention is reasonable, and preparation method is simple, and medicine source is wide, at low cost, easy to use；Through more people's application verifications, treat
Effect is reliable, without any side effects.Clinical application effective percentage of the present invention is up to 90% or more, and cure rate is up to 85%.
Specific embodiment
The present invention is described in further detail below by specific embodiment, but embodiment is not to skill of the present invention
The restriction of art scheme, it is all based on present invention teach that made transformation, all should belong to protection scope of the present invention.
Embodiment 1
A kind of solidification seawater gel, component are made of seawater and Sodium Hyaluronate, in every 1000L solidification seawater gel by with
The raw material of lower parts by weight forms: seawater 900kg, Sodium Hyaluronate 15kg, surplus are purified water.
The relative molecular weight of the Sodium Hyaluronate are as follows: 8 × 105。
The preparation method for solidifying seawater gel, includes the following steps:
Step 1: seawater and purified water are mixed and heated to 60 DEG C；
Step 2: being slowly added to Hyal powder into the mixed liquor after heating, uniforms stirring on one side add while,
Cohere Hyal powder agglomerating, stirring to abundant dissolution, the addition speed of Hyal powder determines dissolution
Speed；
Step 3: the solution described in the step 2 be fully cooled after to get the solidification seawater gel.
Case:
Mr. Li, 47 years old, rhinitis chronic patient；
Symptom: nasal obstruction, mucus nasal mucus are with mild headache；
Using the solidification seawater gel of the present embodiment, it was used continuously by 10 days, solves the symptoms such as nasal obstruction, rhinorrhea.
Embodiment 2
A kind of solidification seawater gel, component are made of seawater and Sodium Hyaluronate, in every 1000L solidification seawater gel by with
The raw material of lower parts by weight forms: seawater 900kg, Sodium Hyaluronate 10kg, surplus are purified water.
The relative molecular weight of the Sodium Hyaluronate are as follows: 7 × 105。
The preparation method for solidifying seawater gel, includes the following steps:
Step 1: seawater and purified water are mixed and heated to 80 DEG C；
Step 2: being slowly added to Hyal powder into the mixed liquor after heating, uniforms stirring on one side add while,
Cohere Hyal powder agglomerating, stirring to abundant dissolution, the addition speed of Hyal powder determines dissolution
Speed；
Step 3: the solution described in the step 2 be fully cooled after to get the solidification seawater gel.
Case:
Mr. Liu, 32 years old, patients with chronic pharyngitis；
Symptom: pharyngeal discomfort sense has foreign body sensation, pharyngeal gargalesthesia；
Using the solidification seawater gel of the present embodiment, it was used continuously by 7 days, alleviates the symptom of throat discomfort.
Embodiment 3
A kind of solidification seawater gel, component are made of seawater and Sodium Hyaluronate, in every 1000L solidification seawater gel by with
The raw material of lower parts by weight forms: seawater 900kg, Sodium Hyaluronate 20kg, surplus are purified water.
The relative molecular weight of the Sodium Hyaluronate are as follows: 8 × 105。
The preparation method for solidifying seawater gel, includes the following steps:
Step 1: seawater and purified water are mixed and heated to 70 DEG C；
Step 2: being slowly added to Hyal powder into the mixed liquor after heating, uniforms stirring on one side add while,
Cohere Hyal powder agglomerating, stirring to abundant dissolution, the addition speed of Hyal powder determines dissolution
Speed；
Step 3: the solution described in the step 2 be fully cooled after to get the solidification seawater gel.
Case:
Mr. Ma, 38 years old, patients with acne；
Symptom: there is red pimple, tumour occur under skin；
Using the solidification seawater gel of the present embodiment, it was used continuously by 15 days, improves skin of face inflammatory patch etc.
Symptom.
Embodiment 4
A kind of solidification seawater gel, component are made of seawater and Sodium Hyaluronate, in every 1000L solidification seawater gel by with
The raw material of lower parts by weight forms: seawater 600kg, Sodium Hyaluronate 15kg, surplus are purified water.
The relative molecular weight of the Sodium Hyaluronate are as follows: 7 × 105。
The preparation method for solidifying seawater gel, includes the following steps:
Step 1: seawater and purified water are mixed and heated to 62 DEG C；
Step 2: being slowly added to Hyal powder into the mixed liquor after heating, uniforms stirring on one side add while,
Cohere Hyal powder agglomerating, stirring to abundant dissolution, the addition speed of Hyal powder determines dissolution
Speed；
Step 3: the solution described in the step 2 be fully cooled after to get the solidification seawater gel.
Case:
Mr. Zhao, 41 years old, patients with acne；
Symptom: there are red pimple and dark sore；
Using the solidification seawater gel of the present embodiment, it was used continuously by 20 days, improves skin of face pimple and dark sore
Etc. symptoms.
Embodiment 5
A kind of solidification seawater gel, component are made of seawater and Sodium Hyaluronate, in every 1000L solidification seawater gel by with
The raw material of lower parts by weight forms: seawater 600kg, Sodium Hyaluronate 10kg, surplus are purified water.
The relative molecular weight of the Sodium Hyaluronate are as follows: 3 × 105。
The preparation method for solidifying seawater gel, includes the following steps:
Step 1: seawater and purified water are mixed and heated to 65 DEG C；
Step 2: being slowly added to Hyal powder into the mixed liquor after heating, uniforms stirring on one side add while,
Cohere Hyal powder agglomerating, stirring to abundant dissolution, the addition speed of Hyal powder determines dissolution
Speed；
Step 3: the solution described in the step 2 be fully cooled after to get the solidification seawater gel.
Case:
Mr. Zheng, 36 years old, patients with chronic pharyngitis；
Symptom: pharyngeal discomfort sense has foreign body sensation；
Using the solidification seawater gel of the present embodiment, it was used continuously by 12 days, alleviates throat discomfort and foreign body sensation etc.
Symptom.
Embodiment 6
A kind of solidification seawater gel, component are made of seawater and Sodium Hyaluronate, in every 1000L solidification seawater gel by with
The raw material of lower parts by weight forms: seawater 600kg, Sodium Hyaluronate 20kg, surplus are purified water.
The relative molecular weight of the Sodium Hyaluronate are as follows: 3 × 105。
The preparation method for solidifying seawater gel, includes the following steps:
Step 1: seawater and purified water are mixed and heated to 70 DEG C；
Step 2: being slowly added to Hyal powder into the mixed liquor after heating, uniforms stirring on one side add while,
Cohere Hyal powder agglomerating, stirring to abundant dissolution, the addition speed of Hyal powder determines dissolution
Speed；
Step 3: the solution described in the step 2 be fully cooled after to get the solidification seawater gel.
Case:
Mr. Chen, 52 years old, patients with chronic pharyngitis；
Symptom: pharyngeal gargalesthesia is retched often；
Using the solidification seawater gel of the present embodiment, it was used continuously by 20 days, alleviates pharyngeal gargalesthesia, retch often etc.
Symptom.
Embodiment 7
A kind of solidification seawater gel, component are made of seawater and Sodium Hyaluronate, in every 1000L solidification seawater gel by with
The raw material of lower parts by weight forms: seawater 300kg, Sodium Hyaluronate 15kg, surplus are purified water.
The relative molecular weight of the Sodium Hyaluronate are as follows: 3 × 105。
The preparation method for solidifying seawater gel, includes the following steps:
Step 1: seawater and purified water are mixed and heated to 72 DEG C；
Step 2: being slowly added to Hyal powder into the mixed liquor after heating, uniforms stirring on one side add while,
Cohere Hyal powder agglomerating, stirring to abundant dissolution, the addition speed of Hyal powder determines dissolution
Speed；
Step 3: the solution described in the step 2 be fully cooled after to get the solidification seawater gel.
Case:
Mr. Shen, 39 years old, rhinitis chronic patient；
Symptom: nasal obstruction, mucus nasal mucus；
Using the solidification seawater gel of the present embodiment, it was used continuously by 14 days, solves the symptoms such as nasal obstruction, rhinorrhea.
Embodiment 8
A kind of solidification seawater gel, component are made of seawater and Sodium Hyaluronate, in every 1000L solidification seawater gel by with
The raw material of lower parts by weight forms: seawater 300kg, Sodium Hyaluronate 10kg, surplus are purified water.
The relative molecular weight of the Sodium Hyaluronate are as follows: 1 × 106。
The preparation method for solidifying seawater gel, includes the following steps:
Step 1: seawater and purified water are mixed and heated to 75 DEG C；
Step 2: being slowly added to Hyal powder into the mixed liquor after heating, uniforms stirring on one side add while,
Cohere Hyal powder agglomerating, stirring to abundant dissolution, the addition speed of Hyal powder determines dissolution
Speed；
Step 3: the solution described in the step 2 be fully cooled after to get the solidification seawater gel.
Case:
Mr. Li, 46 years old, patients with acne；
Symptom: there are red pimple, red swelling of the skin；
Using the solidification seawater gel of the present embodiment, it was used continuously by 20 days, improves the symptoms such as skin of face inflammatory.
Embodiment 9
A kind of solidification seawater gel, component are made of seawater and Sodium Hyaluronate, in every 1000L solidification seawater gel by with
The raw material of lower parts by weight forms: seawater 300kg, Sodium Hyaluronate 20kg, surplus are purified water.
The relative molecular weight of the Sodium Hyaluronate are as follows: 1 × 106。
The preparation method for solidifying seawater gel, includes the following steps:
Step 1: seawater and purified water are mixed and heated to 78 DEG C；
Step 2: being slowly added to Hyal powder into the mixed liquor after heating, uniforms stirring on one side add while,
Cohere Hyal powder agglomerating, stirring to abundant dissolution, the addition speed of Hyal powder determines dissolution
Speed；
Step 3: the solution described in the step 2 be fully cooled after to get the solidification seawater gel.
Case:
Mr. Lan, 54 years old, rhinitis chronic patient；
Symptom: mucus nasal mucus is with mild headache；
Using the solidification seawater gel of the present embodiment, it was used continuously by 24 days, solves the symptoms such as mucus nasal mucus.
Application method of the invention:
The present invention is early, middle and late to be used stage by stage, can increase access times according to the actual situation.
The above is only presently preferred embodiments of the present invention, is not intended to limit the present invention in any form, answers
When pointing out, for those of ordinary skill in the art, to the above embodiments according to the technical essence of the invention
What simple modification, equivalent change and modification, all of which are still within the scope of the technical scheme of the invention.
Claims (10)
1. a kind of solidification seawater gel, which is characterized in that component is made of seawater and Sodium Hyaluronate, and every 1000L solidifies seawater
Be made of in gel the raw material of following parts by weight: 260~990kg of seawater, 0.1~50kg of Sodium Hyaluronate, surplus are purified water.
2. solidification seawater gel according to claim 1, it is characterised in that the relative molecular weight of the Sodium Hyaluronate are as follows:
1×104~6 × 106。
3. solidification seawater gel according to claim 1, which is characterized in that component is made of seawater and Sodium Hyaluronate,
Every 1000L solidifies in seawater gel to be made of the raw material of following parts by weight: seawater 900kg, Sodium Hyaluronate 15kg, and surplus is pure
Change water.
4. solidification seawater gel according to claim 1, which is characterized in that component is made of seawater and Sodium Hyaluronate,
Every 1000L solidifies in seawater gel to be made of the raw material of following parts by weight: seawater 900kg, Sodium Hyaluronate 10kg, and surplus is pure
Change water.
5. solidification seawater gel according to claim 1, which is characterized in that component is made of seawater and Sodium Hyaluronate,
Every 1000L solidifies in seawater gel to be made of the raw material of following parts by weight: seawater 900kg, Sodium Hyaluronate 20kg, and surplus is pure
Change water.
6. solidification seawater gel according to claim 1, which is characterized in that component is made of seawater and Sodium Hyaluronate,
Every 1000L solidifies in seawater gel to be made of the raw material of following parts by weight: seawater 600kg, Sodium Hyaluronate 15kg, and surplus is pure
Change water.
7. solidification seawater gel according to claim 1, which is characterized in that component is made of seawater and Sodium Hyaluronate,
Every 1000L solidifies in seawater gel to be made of the raw material of following parts by weight: seawater 600kg, Sodium Hyaluronate 10kg, and surplus is pure
Change water.
8. solidification seawater gel according to claim 1, which is characterized in that component is made of seawater and Sodium Hyaluronate,
Every 1000L solidifies in seawater gel to be made of the raw material of following parts by weight: seawater 600kg, Sodium Hyaluronate 20kg, and surplus is pure
Change water.
9. the preparation method described in claim 1 for solidifying seawater gel, which comprises the steps of:
Step 1: seawater and purified water are mixed and heated to 60~80 DEG C；
Step 2: Sodium Hyaluronate, stirring to abundant dissolution are slowly added into the mixed liquor after heating；
Step 3: the solution described in the step 2 be fully cooled after to get the solidification seawater gel.
10. the preparation method according to claim 9 for solidifying seawater gel, it is characterised in that heating described in step 1
Temperature is 70 DEG C.
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| CN201910864003.2A CN110507603A (en) | 2019-09-12 | 2019-09-12 | A kind of solidification seawater gel and preparation method thereof |
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| CN201910864003.2A CN110507603A (en) | 2019-09-12 | 2019-09-12 | A kind of solidification seawater gel and preparation method thereof |
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Application publication date: 20191129 |