CN110477378B - Mouth-soluble instant drinking powder containing fat-soluble components and preparation method thereof - Google Patents

Mouth-soluble instant drinking powder containing fat-soluble components and preparation method thereof Download PDF

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CN110477378B
CN110477378B CN201910709728.4A CN201910709728A CN110477378B CN 110477378 B CN110477378 B CN 110477378B CN 201910709728 A CN201910709728 A CN 201910709728A CN 110477378 B CN110477378 B CN 110477378B
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soluble
mouth
fat
powder
instant
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CN110477378A (en
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李倩
陈剑彬
马宇骥
石超
吴文忠
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Innobio Corp ltd
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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/385—Concentrates of non-alcoholic beverages
    • A23L2/39—Dry compositions
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/015—Inorganic compounds
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/03—Organic compounds
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P10/00—Shaping or working of foodstuffs characterised by the products
    • A23P10/20—Agglomerating; Granulating; Tabletting
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs

Abstract

The instant powder of mouth-soluble type containing fat soluble ingredient and its preparation method, said instant powder of mouth-soluble type is to contain fat soluble ingredient, instant raw materials and disperse raw material mixture of material to get final product through microencapsulation, wherein said instant raw materials are selected from xylitol, erythritol or their mixture; the dispersing material is selected from calcium silicate, silicon dioxide or a mixture thereof. The product of the invention is immediately melted after being drunk for 3s, and has fine and refreshing mouthfeel. Through the screening and combination of sugar alcohol direct drinking materials and dispersing materials, the problems that fat soluble active ingredients are difficult to absorb and swallowing is difficult are effectively solved. On one hand, the mouth-soluble instant drinking powder containing fat-soluble components can be directly provided for terminal customers, and can also be mixed with other nutrients for application in health care products and functional foods.

Description

Mouth-soluble instant drinking powder containing fat-soluble components and preparation method thereof
Technical Field
The invention relates to a functional dietary supplement, in particular to a direct drinking preparation of fat-soluble active ingredients and a preparation method thereof.
Background
The fat-soluble carotenoid has stronger functions of oxidation resistance and the like, and the market demand is continuously increased. Wherein the lutein, zeaxanthin and lutein ester derived from flos Tagetis Erectae have unique eye protection function and can prevent ultraviolet injury. And simultaneously can be used as a strong oxidant to inhibit the activity of active oxygen free radicals, and has the effects of protecting skin and heart and enhancing immunity. No. 12 of the national ministry of health bulletin 2008, establishes approval of lutein ester as a functional new resource food. Meanwhile, zeaxanthin is also obtained in 2017 as a new resource food.
Astaxanthin which is found from natural sources at present has the strongest antioxidant capacity and has various physiological effects, such as unique effects of resisting oxidation, delaying senility, enhancing resistance, resisting tumors, preventing and treating senile dementia and cancers. Astaxanthin crosses the blood-brain barrier and thus protects the brain, the central nervous system and the eyes. Astaxanthin also has other effects: improving body endurance and reducing the risk of muscle damage; relieving asthenopia symptom, and improving visual sensitivity; reduction of wrinkles by internal supplementation; relieving the symptoms of hyperpigmentation (known as age spots); regulating cytokines, inhibiting gene expression of inflammatory cytokines and chemokines; improving stomach health, and relieving infection or inflammation caused by helicobacter pylori.
The functional oil is edible oil containing nutritional components capable of regulating human health. Camellia oil, walnut oil, linseed oil, perilla seed oil, DHA, and the like are considered the first choice of healthy oils because they can provide more unsaturated fatty acids. Medium Chain Triglyceride (MCT) and conjugated linoleic acid glyceride (CLA-TG) have remarkable effects on reducing body weight, abdominal fat area and waist circumference of human body, and thus are receiving more and more attention.
However, the poor solubility of various fat-soluble active ingredients in water limits the absorption of nutrient components. Some fat-soluble active substances have certain odors which are difficult to mask, such as fishy smell and the like, so that the active substances are difficult to eat. Therefore, the preparation of fat-soluble active ingredients is the key point for improving the mouthfeel and expanding the application of the fat-soluble active ingredients.
The fat-soluble active ingredient preparation is mainly in the form of soft capsule, solid beverage and tablet. Among which solid beverages are also most common. But people are more and more aware of the inconvenience of solid water taking, such as drinking water when taking water, which affects the milk amount of infants; the edible method is characterized in that after the edible product is infused with boiled water, the nutritional ingredients of the product are destroyed; meanwhile, the large amount of water is not beneficial to the taking and absorption of the old and the infant who have dysphagia. More and more people are noticing the disadvantages of the solid beverage formulation. Therefore, the solid product which can be instantly dissolved in the mouth, can be instantly melted in the mouth and does not need to be taken with water, and has fine and smooth mouthfeel is a new product form of the nutritional supplement pursued by people.
In recent years, people also pay attention to the point, and some products in the aspect of oral direct drinking are made. For example, CN 104687178A discloses a solid beverage for direct oral administration and a preparation method thereof, wherein 20-95 parts of sugar alcohol, DHA powder, shell powder and vitamin D powder are mixed and granulated to obtain the solid beverage, but the formulation with high sugar alcohol content has poor mouthfeel and may bring high health risk. CN 106259943A, CN 105105128A provide a kind of infant nutritional supplement formula suitable for weaning-away breast feeding and its preparation method. But the effect of improving the direct drinking property cannot be achieved by adding lecithin, in addition, the preparation process is complex, the prepared ultrafine powder is at risk of inhalation asphyxiation when being taken, especially for the old and infants with small salivary secretion, and the crystal sugar is used, so that the crystal sugar is not suitable for being taken too much by diabetics and infants.
In view of the above problems, the search for materials, formulations and preparation methods which can really achieve the direct drinking effect is a key factor for obtaining excellent direct drinking products.
Disclosure of Invention
The invention aims to provide a direct drinking product which can really achieve an excellent direct drinking effect.
Firstly, the invention provides a mouth-soluble instant drinking powder containing fat-soluble ingredients, which is prepared by microencapsulating a raw material mixture containing the fat-soluble ingredients, an instant drinking material and a dispersing material, wherein the instant drinking material is selected from xylitol, erythritol or a mixture thereof; the dispersing material is selected from calcium silicate, silicon dioxide or a mixture thereof.
Another object of the present invention is to provide a method for preparing the above-mentioned instant powder containing fat-soluble components, comprising the following steps:
(1) Uniformly mixing and sieving the raw material mixture to ensure that the mass ratio of the 60-120 meshes of material is not less than 90%;
(2) Granulating;
(3) Drying at 30-50 ℃;
(4) And (6) screening.
In the above description of the preparation method, the granulation can be performed by using granulation methods well known in the industry, such as wet granulation, dry granulation, swing granulation, extrusion granulation, fluidized bed granulation, spray granulation; the drying mode can be fluidized drying, oven drying and the like.
In the screening step, the particle size of the product is uniformly dispersed in 30-100 meshes according to requirements, and the proportion of particles passing through 80 meshes is less than 10%. The qualified product can be obtained after the product is sieved by a 30-mesh sieve through sieving, the particle size distribution of the qualified product is optimized by the process and the formula, the particle size distribution is uniform, no fine or coarse particles exist, the particle size distribution is approximately 1.
The mouth-soluble instant drinking powder containing fat-soluble components is prepared by processing a raw material mixture containing the fat-soluble active components, an instant drinking material and a dispersing material through an embedding process such as emulsification dispersion, spray drying and the like and a granulation process. The product has a mouth feel of 3s, and is fine and refreshing. Through the screening and combination of sugar alcohol direct drinking materials and dispersing materials, the problems that fat soluble active ingredients are difficult to absorb and swallowing is difficult are effectively solved. On the one hand, the invention provides the mouth-soluble instant drinking powder containing fat-soluble components, which can directly provide products for end customers and can also be mixed with other nutrients for application in health care products and functional foods.
Detailed Description
The invention provides a mouth-soluble instant drinking powder containing fat-soluble components, which is prepared by microencapsulating a raw material mixture containing the fat-soluble components, an instant drinking material and a dispersing material, wherein the instant drinking material is selected from xylitol, erythritol or a mixture thereof; the dispersing material is selected from calcium silicate, silicon dioxide or a mixture thereof.
In the technical scheme of the invention, the selection of the direct drinking material and/or the dispersing material is the key characteristic for determining the effect of the fat-soluble component-containing oral instant drinking powder. In the long-term search for suitable direct-drinking materials and formulation methods, we have found that the properties of the active ingredients have a very important influence on the choice of direct-drinking materials. By taking this factor into account in the development of products, it is possible to obtain really instant drinking particles with excellent effects. The research results to date found that: when the fat-soluble or non-fat-soluble active ingredients are prepared into the mouth-soluble instant drinking powder according to the technical framework of the invention, different combination requirements are provided for the compatible instant drinking material and/or dispersing material. On one hand, when the fat-soluble active ingredient is combined with a direct drinking material of xylitol/erythrose and a dispersed material of silicon dioxide/calcium silicate, the mouth-soluble direct drinking powder with excellent property characteristics can be obtained, but when the same direct drinking material and/or dispersed material is compatible with the representative non-fat-soluble active ingredient, the property and the quality of the obtained direct drinking powder product are unsatisfactory. The tests and results of examples 8, 9 and 10 as listed in the present specification. Thus, in a particular embodiment of the invention, the drink-through material is a mixture of xylitol and erythritol; preferably xylitol and erythritol in a mass ratio of 1; more preferably the mass ratio of xylitol to erythritol is 1. When the dispersion material is silicon dioxide, the dispersion material can obtain more excellent effect by matching with the active component and other materials.
On the other hand, the preparation process of the non-fat-soluble active ingredient is also explored, and the discovery shows that when some typical non-fat-soluble active ingredients are matched with erythrose (direct drinking material) and maltodextrin (dispersing material), direct drinking particle products with excellent quality can be obtained. Also, in comparative experiments, when erythrose and/or maltodextrin were used in combination with typical fat-soluble ingredients in an attempt, satisfactory products could not be obtained, and the results are shown in examples 5, 11, and 12.
In another embodiment of the present invention, the fat soluble ingredient is selected from lutein, lutein esters, zeaxanthin, astaxanthin, beta carotene, lycopene or mixtures thereof. Preferably lutein, lutein esters, zeaxanthin, beta-carotene, lycopene or mixtures thereof.
In another embodiment of the present invention, the raw material mixture comprises, by weight: 1 part of fat-soluble component, 0.5-3 parts of direct drinking material and 0.01-0.5 part of dispersing material. Preferably contains 1 part of fat-soluble component, 1-2 parts of direct drinking material and 0.01-0.2 part of dispersing material.
On the basis, the raw material mixture for preparing the oral instant drinking powder can also contain 0.01 to 0.1 weight part of flavoring agent. The correctant mainly comprises various essences and fruit powder substances, including citric acid, sodium citrate, malic acid, various essences and fruit powder. The addition was done according to the methods and amounts described in the prior art.
In still another aspect, the fat-soluble ingredients used to prepare the instant powder further comprise an antioxidant selected from tocopherol, ascorbic acid esters of fatty acids, butylated Hydroxytoluene (BHT), butylated Hydroxyanisole (BHA), propyl gallic acid, t-butylhydroxyquinoline, or mixtures thereof; the antioxidant accounts for 0.1-5% of the fat-soluble component by mass. Preferably 1 to 5%.
The present invention is further illustrated by the following non-limiting examples, which should not be construed as limiting the invention in any way, unless otherwise specified, and the fat-soluble active agents used in the present invention are commercially available. The active substances used in the examples of the present invention were purchased from Dalian Yi Nuo Bio Inc. Mainly comprises lutein ester, lutein, astaxanthin, lycopene, beta-carotene, zeaxanthin, linseed oil, perilla seed oil, DHA, CLA-TG and MCT.
The following methods were used in the present application to measure and evaluate the products, unless otherwise specified:
in the invention, the disintegration time limit is adopted to represent the dissolution efficiency of the direct drinking powder in the mouth, and the longer the disintegration time limit is, the poorer the direct drinking effect is. The method for measuring the disintegration time limit comprises the following steps: 500mL of the prepared phosphate buffer solution is placed in a beaker of a disintegration time-limit instrument, the instrument is installed, the water temperature is adjusted to 37 +/-0.5 ℃, and a 100-mesh screen is used as the bottom. The 1g sample was placed in a disintegration time-limit apparatus (Tianjin New Tianguang BJ-1 type), and the apparatus was started while counting time. And (5) finishing timing after the sample powder on the screen completely sinks and dissolves, and recording the disintegration time of the product. ( Preparation of phosphate buffer solution: 6.8g of potassium dihydrogen phosphate is weighed, dissolved in 500mL of water, adjusted to pH 6.8 with 0.1mol/mL sodium hydroxide solution and diluted to 1000mL with water. )
The product accelerated stability evaluation method provided by the invention is a method provided by Chinese pharmacopoeia: the measured changes in appearance, content, etc. of the product were made at 40 ℃ and 75% RH.
The sensory evaluation method comprises the following steps: randomly compiling sample numbers, requiring more than 10 evaluators to evaluate the appearance, smell, drinking property, gritty feeling, sweetness, acidity, taste (former taste) and taste (latter taste) of the samples in the same place by an evaluation group, dividing the total score by 9, scoring and summarizing to calculate an average value, namely a sensory evaluation value of each index of the product, and taking the sample with the highest score as an optimal sample.
The granulometry method described in the present invention is to use a American standard sieve to sieve and record the percentage of products passing 30 mesh, 80 mesh and 100 mesh.
Example 1
494g of xylitol, 494g of lutein ester, 2g of citric acid and 10g of strawberry fruit powder are weighed (the granularity of each raw material needs to be between 60 and 120 meshes). The raw materials are uniformly mixed, the lutein ester direct drinking powder is obtained by a wet granulation process, and the lutein ester direct drinking powder is fluidized and dried at 30 ℃. And (6) sieving. The yield thereof was found to be 45%. The 30, 60 and 80 mesh screen rates are 45%,10% and 2%, respectively. The disintegration time was 80s. The sensory evaluation score was 3 points, and the mouth was not quickly dissolved, had a strong gritty sensation, and was difficult to swallow.
Example 2
Weighing 300g of erythritol, 488g of lutein, DHA200g, 2g of malic acid and 10g of lemon fruit powder (the particle size of each raw material needs to be 60-120 meshes). The raw materials are uniformly mixed, and the lutein-DHA direct drinking powder is obtained through a dry granulation process. The yield thereof was found to be 55%. The screen mesh rates of 30 meshes, 60 meshes and 80 meshes are respectively 90%,50% and 40%. The disintegration time was 98s. The sensory evaluation of the powder is divided into 1 point, the powder is pasted with dry mouth, the mouth is flushed out after the mouth is opened, and the throat is stuck after the mouth is sucked.
Example 3
Weighing 375g of erythritol, 125g of xylitol, 500g of lycopene, 2g of sodium citrate and 10g of apple powder (the granularity of each raw material needs to be between 60 and 120 meshes). The raw materials are uniformly mixed, the lycopene direct drinking powder is obtained by a fluidized bed granulation process, and the lycopene direct drinking powder is dried by a 40-DEG oven. The yield thereof was found to be 75%. The 30, 60 and 80 mesh screen rates are respectively 90%,35% and 5%. The disintegration time was 25s. The sensory evaluation score of the sweet potato is 8 points, the taste is fine and smooth, the sweet potato is instantly melted in the mouth, and the sweet and sour degree is moderate. The product was agglomerated at 40 ℃ and 75% RH for 10 days.
Compared with the examples 1 and 2, the yield of the product obtained by mixing and using the xylitol and the erythritol in the implementation is greatly improved, the particle size distribution of the product is relatively uniform, the mouthfeel is fine and smooth, and the product is molten in the mouth.
Example 4
Weighing 241g of erythritol, 241g of xylitol, 482g of astaxanthin, 1g of malic acid, 30g of apple powder and 5g of silicon dioxide (the granularity of each raw material needs to be 60-120 meshes). The raw materials are uniformly mixed, and the astaxanthin direct drinking powder is obtained through a fluidized bed granulation process. The yield thereof was found to be 95%. The 30, 60 and 80 mesh screen rates are 95%,40% and 7% respectively. The disintegration time was 19s. The sensory evaluation score of the product is 8.2, the product has fine and smooth mouthfeel, is instantly melted in the mouth and has moderate sour and sweet degree. The product had no clumping at 40 ℃ and 75% RH for 6 months.
Compared with the embodiment 3, the xylitol and the erythritol are mixed and used in the embodiment to be matched with the silicon dioxide, so that the obtained product is improved in yield, more uniform in particle size distribution, fine and smooth in taste and instantly melted in the mouth. And simultaneously, the problem of caking of the product in the process of accelerating storage is solved.
Example 5
Weighing 333g of erythritol, 67g of xylitol, 200g of linseed oil, 319g of lutein ester, 1g of malic acid, 30g of apple powder and 50g of maltodextrin (the granularity of each raw material needs to be between 60 and 120 meshes). The raw materials are uniformly mixed, the lutein ester-linseed oil direct drinking powder is obtained through a fluidized bed granulation process, and the 50-DEG fluidized drying is carried out. The yield thereof was found to be 80%. The screen rates of 30 meshes, 60 meshes and 80 meshes are respectively 85%,40% and 9%. The disintegration time was 30s. The sensory evaluation score of the product is 7.2, the taste is fine and smooth, and the product can be dissolved in 5s after being eaten. The product agglomerated at 40 ℃ and 75% RH for 1 month.
Example 6
500g of sorbitol, 188g of beta-carotene, 100g of perilla seed oil, 2g of citric acid, 10g of blueberry powder and 200g of silicon dioxide (the granularity of each raw material needs to be between 60 and 120 meshes) are weighed. The raw materials are uniformly mixed, the beta carotene-perilla seed oil direct drinking powder is obtained by a swing granulation process, and the beta carotene-perilla seed oil direct drinking powder is fluidized and dried at 50 ℃. The yield thereof was found to be 58%. The screen mesh rates of 30 meshes, 60 meshes and 80 meshes are respectively 70%,50% and 10%. The disintegration time was 135s. The sensory evaluation score was 1 point, and the granules were insoluble in the mouth, remained a lot, and had a strong gritty feeling.
Example 7
Weighing 455g erythritol, 364g EGCG (epigallocatechin gallate), 1g malic acid, 30g apple powder and 150g maltodextrin, wherein the granularity of each raw material is 60-120 meshes. The raw materials are evenly mixed, and the EGCG direct drinking powder is obtained through a fluidized bed granulation process. The yield thereof was found to be 95%. The 30, 60 and 80 mesh screen rates are 95%,40% and 7% respectively. The disintegration time was 10s. The sensory evaluation score of the product is 8.5, the product has fine and smooth mouthfeel, instant melting in the mouth, no afterbitterness and moderate sour-sweet degree. The product had no clumping at 40 ℃ and 75% RH for 6 months.
Example 8
Weighing 150g of erythritol, 150g of xylitol, 469g of BCAA (branched chain amino acid), 1g of malic acid, 30g of apple powder and 200g of maltodextrin, wherein the granularity of each raw material is between 60 and 120 meshes. The raw materials are uniformly mixed, and the BCAA direct drinking powder is obtained through a fluidized bed granulation process. The yield thereof was found to be 55%. The screen mesh rates of 30 meshes, 60 meshes and 80 meshes are respectively 70%,40% and 7%. The disintegration time was 65s. The sensory evaluation score is 5 points, the dissolution time is longer in the mouth, and the sweet and sour degree is moderate.
Example 9
Weighing 300g of erythritol, 150g of xylitol, 2g of EGCG488g of sodium citrate, 10g of apple powder and 50g of silicon dioxide, wherein the granularity of each raw material is between 60 and 120 meshes. The raw materials are uniformly mixed, the EGCG direct drinking powder is obtained through a fluidized bed granulation process, and the EGCG direct drinking powder is dried in a 40-DEG oven. The yield thereof was found to be 75%. The screen mesh rates of 30 meshes, 60 meshes and 80 meshes are respectively 100%,80% and 60%. The disintegration time was 70s. The sensory evaluation score is 5.3, the powder is dry and difficult to swallow, the mouth cavity is flushed after the mouth is opened, the throat is stuck after the mouth is opened, the aftertaste is slightly bitter and astringent, the time for dissolving the powder in the mouth is 10s, and the sour and sweet degree is moderate. The product did not cake at 40 ℃ and 75% RH for 6 months.
Example 10
450g of erythritol, 488g of tricalcium phosphate, 2g of sodium citrate, 10g of apple powder and 5g of silicon dioxide are weighed, and the granularity of each raw material is between 60 and 120 meshes. The raw materials are uniformly mixed, tricalcium phosphate direct drinking powder is obtained through a fluidized bed granulation process, and the tricalcium phosphate direct drinking powder is dried in a 40-DEG oven. The yield thereof was found to be 85%. The 30, 60 and 80 mesh screen rates are respectively 90%,51% and 39%. The disintegration time was 16s. The sensory evaluation score is 4.3 points, the mouth feel is burnt and insoluble, the mouth is opened and then the mouth is flushed out of the cavity, the throat is stuck after the mouth is opened, the taste is slightly bitter, and the sour and sweet degree is moderate. The product agglomerated at 40 ℃ and 75% RH for 3 months.
Example 11
Weighing 300g of erythritol, 488g of lutein, DHA200g, 2g of malic acid, 10g of lemon fruit powder and 50g of calcium silicate (the granularity of each raw material needs to be between 60 and 120 meshes). The raw materials are uniformly mixed, and the lutein-DHA direct drinking powder is obtained through a dry granulation process. The yield thereof was found to be 55%. The screen mesh rates of 30 meshes, 60 meshes and 80 meshes are respectively 90%,50% and 40%. The disintegration time was 98s. The sensory evaluation of the powder is divided into 1 point, the powder is pasted with dry mouth, the mouth is flushed out after the mouth is opened, and the throat is stuck after the mouth is sucked. The product was agglomerated at 40 ℃ and 75% RH for 2 months.
Example 12
Weighing 300g of erythritol, 338g of lutein ester, DHA200g, 2g of malic acid, 10g of lemon fruit powder and 150g of maltodextrin, wherein the granularity of each raw material is between 60 and 120 meshes. The raw materials are uniformly mixed, and the lutein ester-DHA direct drinking powder is obtained through a dry granulation process. The yield thereof was found to be 53%. The screen mesh rates of 30 meshes, 60 meshes and 80 meshes are 65%,40% and 8% respectively. The disintegration time was 98s. The sensory evaluation score was 2 points, and the powder had a strong gritty feeling and was difficult to dissolve. The product was agglomerated at 40 ℃ and 75% RH for 15 days.

Claims (2)

1. The mouth-soluble instant drinking powder containing fat-soluble components is characterized in that:
the preparation raw materials comprise the following components in parts by weight: 1 part of fat-soluble component, 1-2 parts of direct drinking material and 0.01-0.2 part of dispersing material;
the fat-soluble component is selected from lutein, lutein ester, astaxanthin, lycopene or a mixture thereof;
the direct drinking material is a mixture of xylitol and erythritol according to the mass ratio of 1;
the dispersion material is silicon dioxide;
the preparation method of the mouth-soluble instant powder containing fat-soluble components comprises the following steps: (1) Uniformly mixing and sieving the raw material mixture to ensure that the mass ratio of the materials of 60 to 120 meshes is not less than 90%; (2) granulating; (3) drying at 30-50 ℃; and (4) screening.
2. A potpourri according to claim 1, wherein said fat soluble ingredients comprise antioxidants selected from the group consisting of tocopherol, butylated hydroxytoluene, butylated hydroxyanisole and mixtures thereof; the mass of the antioxidant is 0.1 to 5 percent of the fat-soluble component.
CN201910709728.4A 2019-08-02 2019-08-02 Mouth-soluble instant drinking powder containing fat-soluble components and preparation method thereof Active CN110477378B (en)

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