CN110467964A - Application of the extraction process and gained Rosa Damascana of Rosa Damascana in facial mask - Google Patents
Application of the extraction process and gained Rosa Damascana of Rosa Damascana in facial mask Download PDFInfo
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- CN110467964A CN110467964A CN201910808670.9A CN201910808670A CN110467964A CN 110467964 A CN110467964 A CN 110467964A CN 201910808670 A CN201910808670 A CN 201910808670A CN 110467964 A CN110467964 A CN 110467964A
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- rosa damascana
- roseleaf
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/10—Anti-acne agents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
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- Pharmacology & Pharmacy (AREA)
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Abstract
The invention discloses the application of a kind of extraction process of Rosa Damascana and gained Rosa Damascana in facial mask comprising following steps: taking fresh roseleaf, is rinsed with clear water and removes silt, and drips moisture to the greatest extent;The roseleaf for dripping moisture to the greatest extent is subjected to microwave disinfection;Roseleaf after sterilizing is impregnated with saline solution, distills the mixed liquor of roseleaf and saline solution, it is to be distilled to finish, organic solvent extraction is added into fraction, separates organic phase;Organic phase is concentrated, ethyl alcohol is added into concentrate, is mixed evenly, filters, removes filter residue, filtrate is concentrated, and carry out ultraviolet-sterilization and obtain Rosa Damascana.The invention has the benefit that during the extraction process, being impregnated using saline solution, distillation extraction, being conducive to the precipitation of effective component in roseleaf, improve the yield of gained Rosa Damascana;Rosa Damascana material source of the present invention is relatively simple, and Rosa Damascana obtained is purer, is free of any additive, belongs to all-natural product.
Description
Technical field
The present invention relates to extraction of essential oil technical fields, and in particular to a kind of extraction process and gained rhodamine toner of Rosa Damascana
Application of the oil in facial mask.
Background technique
Rosa Damascana, which is referred to as, to be adjustable female incretion, nourishes uterus, alleviate dysmenorrhea, improve frigidity " after essential oil "
With climacteric discomfort.Especially there is good beautifying skin-protection function, melanin can be promoted to decompose with internal oxidition Kohakuhi,
Skin elasticity is replied, allows women to possess healthy skin pale, full of elasticity, is the volatile oil for being suitable for female health.
Currently, the traditional extraction technique of Rosa Damascana mainly has steam distillation and organic solvent extractionprocess.It is domestic big
Most manufacturers are using extraction by steam distillation Rosa Damascana, which has equipment simple, at low cost, easy to operate
The features such as, but since operation temperature is close to 100 DEG C, lead to low-boiling Rosa Damascana and water-soluble fragrance ingredient such as 2- benzene
Ethyl alcohol etc. is possible to incur loss or be destroyed, and causes Rosa Damascana yield lower, and due to the ill-effect of high-temperature steam, mentions
The Rosa Damascana color of taking-up is deep, and has and be charred taste.Organic solvent extractionprocess can simultaneously mention low boiling point and high boiling component
Take out, reduce the loss of fragrant oil component, the fragrance of gained Rosa Damascana closer to natural rose petal fragrance, and it is oily
Rate is higher than steam distillation, but extraction time is long, and the head perfume (or spice) of gained essential oil shows slightly insufficient, and is easy to produce dissolvent residual.
In recent years, on the basis of traditional extraction technique, some new separation and purification technique such as supercritical fluid extractions
Technology and molecular distillation technique have been successfully applied to the extraction of Rosa Damascana.As CN106281713A discloses a kind of Rosa Damascana
Extracting method, continuous cycling extraction is carried out using supercritical carbon dioxide fluid, extraction pressure is up to 15-25MPa, separation pressure
Power is also reached for 8-10MPa, it is seen that supercritical carbon dioxide extraction method equipment operation pressure is high, can not large-scale standardized life
It produces.
Summary of the invention
The object of the present invention is to provide a kind of purity is highs of gained Rosa Damascana, and extracting method is simple, extraction cost is low
Rosa Damascana the application in facial mask of extraction process and gained Rosa Damascana.
A kind of extraction process of Rosa Damascana, comprising the following steps:
(1) fresh roseleaf is taken, is rinsed with clear water and removes silt, and drips moisture to the greatest extent;
(2) roseleaf for dripping moisture to the greatest extent is subjected to microwave disinfection;Microwave disinfection is microorganism, while by microwave thermal effect
Its vivo protein and physiological activator should be made to morph with the collective effect of non-thermal effect, and cause microbial body raw
Long development delays and dead, achievees the purpose that sterilizing and fresh-keeping;
(3) roseleaf after sterilizing is impregnated with saline solution, distills the mixed liquor of roseleaf and saline solution,
It is to be distilled to finish, organic solvent extraction is added into fraction, separates organic phase;
It is distilled using saline solution, the effective component facilitated in roseleaf is precipitated, and can increase distillation gained essence
The content of effective component in liquid.
(4) organic phase is concentrated, ethyl alcohol is added into concentrate, is mixed evenly, filters, removes filter residue, filtrate is concentrated,
And it carries out ultraviolet-sterilization and obtains Rosa Damascana.
For the using effect for preventing remaining organic solvent influence Rosa Damascana, ethyl alcohol is added into concentrate, through overrich
Contracting makes ethyl alcohol take away remaining organic solvent during volatilization, and ethyl alcohol itself has effects that pore is stimulated to shrink, can
It solves the problems, such as that effective component absorptivity is low, also can change the form of skin oil and fat, active constituent is made to be easier to penetrate skin
It is absorbed, and there is certain inhibiting effect to small pox and acne.Remaining a small amount of ethyl alcohol, can be improved rose i.e. in Rosa Damascana
The skin effect of rare essential oil.
Further, in step (2), the temperature of the microwave disinfection is 70-80 DEG C, and sterilizing time is 6- at this temperature
8min。
Further, in step (3), the concentration of the saline solution is 1%-3%, the saline solution and need to impregnate rose
The weight ratio of valve is 8-10:1, soaking time 4-6h.
Further, in step (3), the temperature of the distillation is 80-100 DEG C.Temperature setting when distillation is in 80-100
DEG C, distillation when, divide four-stage to carry out, successively set temperature be 80-85 DEG C, 85-90 DEG C, 90-95 DEG C, 95-100 DEG C, to
When not having fraction outflow, then temperature is increased into next stage.
Further, in step (3), the organic solvent is petroleum ether or ethyl acetate.
Further, in step (4), the concentration of the ethyl alcohol is 25%-30%, the amount of added ethyl alcohol and the weight of concentrate
Amount is than being 5-8:1.
Application of the Rosa Damascana in facial mask.
Further, face paper is immersed in Rosa Damascana, is finished wait impregnate, taken out face paper and obtain rhodamine toner pasta
Film.
Further, the face paper is 384 silk mask paper.384 silk mask paper are frivolous free of a burden, and weight is only
1g, thickness are only 0.1mm, the Essence of 25 times of support of energy, and silk is porous fiber, and water imbibition is strong, and penetration is good, has
Help rose essence liquid to be absorbed by the skin.
Further, the time that the face paper impregnates in Rosa Damascana is 40-50h.
Beneficial effects of the present invention: the extraction process of Rosa Damascana of the present invention, before extraction to roseleaf into
The processing of row microwave disinfection guarantees to dispel its contained bacterium and impurity in the complete situation of roseleaf, ensure that gained rhodamine toner
The purity and freshness of oil.
During the extraction process, it is impregnated using saline solution, distillation extraction, is conducive to the precipitation of effective component in roseleaf,
The effective rate of utilization for improving roseleaf improves the yield of gained Rosa Damascana;Rosa Damascana material of the present invention comes
Source is relatively simple, and Rosa Damascana obtained is purer, relative to the Rosa Damascana sold in the market, present invention gained Rosa Damascana
Without any additive, belong to all-natural product, using effect is obviously superior to the using effect of commercially available Rosa Damascana.
It can reach quick anti-acne, nti-freckle using facial mask made from Rosa Damascana of the present invention, pore refining highlights skin
Color makes the flexible effect of skin, because Rosa Damascana of the present invention is pure plant product, without any additive, In
It is not in allergic phenomena in use process.
Specific embodiment
Embodiment 1
A kind of extraction process of Rosa Damascana, comprising the following steps:
(1) fresh roseleaf is taken, is rinsed with clear water and removes silt, and drips moisture to the greatest extent;
(2) roseleaf for dripping moisture to the greatest extent is subjected to microwave disinfection;
(3) roseleaf after sterilizing is impregnated with saline solution, distills the mixed liquor of roseleaf and saline solution,
It is to be distilled to finish, organic solvent extraction is added into fraction, separates organic phase;
(4) organic phase is concentrated, ethyl alcohol is added into concentrate, is mixed evenly, filters, removes filter residue, filtrate is concentrated,
And it carries out ultraviolet-sterilization and obtains Rosa Damascana.
Embodiment 2
A kind of extraction process of Rosa Damascana, comprising the following steps:
(1) fresh roseleaf is taken, is rinsed with clear water and removes silt, and drips moisture to the greatest extent;
(2) roseleaf for dripping moisture to the greatest extent is subjected to microwave disinfection, and the temperature of microwave disinfection is controlled at 70 DEG C, it is warm herein
Sterilizing time under degree is 8h;
(3) roseleaf after sterilizing is impregnated into 6h in the saline solution that concentration is 1%, and the amount of saline solution used with
Need to impregnate roseleaf weight ratio be 8:1, finished wait impregnate, temperature be 80-100 DEG C under conditions of distillation roseleaf and
The mixed liquor of saline solution, it is to be distilled to finish, organic solvent petroleum ether extraction is added into fraction, separates organic phase;
(4) organic phase is concentrated, is added the ethyl alcohol that concentration is 25% into concentrate, and the amount of added ethyl alcohol and concentrate
Weight ratio is 5:1, is mixed evenly, and filtering removes filter residue, filtrate is concentrated, and carry out ultraviolet-sterilization and obtain Rosa Damascana.
Application of the gained Rosa Damascana in facial mask, impregnates 40h for face paper in Rosa Damascana, finishes wait impregnate, take
Face paper obtains Rosa Damascana facial mask out, it is preferable that face paper used is 384 silk mask paper.
When using facial mask made from Rosa Damascana of the present invention, which can apply 1 hour or so (according to personal face in face
It, can when Rosa Damascana effective component is completely absorbed on face paper depending on portion absorbs the speed of Rosa Damascana effective component
Remove facial mask), skin is not in malaise symptoms, and skin can be made to reach the state of a hypersorption from inside to outside.
Embodiment 3
A kind of extraction process of Rosa Damascana, comprising the following steps:
(1) fresh roseleaf is taken, is rinsed with clear water and removes silt, and drips moisture to the greatest extent;
(2) roseleaf for dripping moisture to the greatest extent is subjected to microwave disinfection, and the temperature of microwave disinfection is controlled at 75 DEG C, it is warm herein
Sterilizing time under degree is 7h;
(3) roseleaf after sterilizing is impregnated into 5h in the saline solution that concentration is 2%, and the amount of saline solution used with
Need to impregnate roseleaf weight ratio be 9:1, finished wait impregnate, temperature be 80-100 DEG C under conditions of distillation roseleaf and
The mixed liquor of saline solution, it is to be distilled to finish, the extraction of organic solvent ethyl acetate is added into fraction, separates organic phase;
(4) organic phase is concentrated, is added the ethyl alcohol that concentration is 26% into concentrate, and the amount of added ethyl alcohol and concentrate
Weight ratio is 6:1, is mixed evenly, and filtering removes filter residue, filtrate is concentrated, and carry out ultraviolet-sterilization and obtain Rosa Damascana.
Application of the gained Rosa Damascana in facial mask, impregnates 43h for face paper in Rosa Damascana, finishes wait impregnate, take
Face paper obtains Rosa Damascana facial mask out, it is preferable that face paper used is 384 silk mask paper.
Embodiment 4
A kind of extraction process of Rosa Damascana, comprising the following steps:
(1) fresh roseleaf is taken, is rinsed with clear water and removes silt, and drips moisture to the greatest extent;
(2) roseleaf for dripping moisture to the greatest extent is subjected to microwave disinfection, and the temperature of microwave disinfection is controlled at 78 DEG C, it is warm herein
Sterilizing time under degree is 7h;
(3) roseleaf after sterilizing is impregnated into 5h in the saline solution that concentration is 2%, and the amount of saline solution used with
Need to impregnate roseleaf weight ratio be 9:1, finished wait impregnate, temperature be 80-100 DEG C under conditions of distillation roseleaf and
The mixed liquor of saline solution, it is to be distilled to finish, organic solvent petroleum ether extraction is added into fraction, separates organic phase;
(4) organic phase is concentrated, is added the ethyl alcohol that concentration is 28% into concentrate, and the amount of added ethyl alcohol and concentrate
Weight ratio is 7:1, is mixed evenly, and filtering removes filter residue, filtrate is concentrated, and carry out ultraviolet-sterilization and obtain Rosa Damascana.
Application of the gained Rosa Damascana in facial mask, impregnates 48h for face paper in Rosa Damascana, finishes wait impregnate, take
Face paper obtains Rosa Damascana facial mask out, it is preferable that face paper used is 384 silk mask paper.
Embodiment 5
A kind of extraction process of Rosa Damascana, comprising the following steps:
(1) fresh roseleaf is taken, is rinsed with clear water and removes silt, and drips moisture to the greatest extent;
(2) roseleaf for dripping moisture to the greatest extent is subjected to microwave disinfection, and the temperature of microwave disinfection is controlled at 80 DEG C, it is warm herein
Sterilizing time under degree is 6h;
(3) roseleaf after sterilizing is impregnated into 4h in the saline solution that concentration is 3%, and the amount of saline solution used with
The weight ratio that roseleaf need to be impregnated is 10:1, is finished wait impregnate, and distills roseleaf under conditions of temperature is 80-100 DEG C
It is to be distilled to finish with the mixed liquor of saline solution, organic solvent petroleum ether extraction is added into fraction, separates organic phase;
(4) organic phase is concentrated, is added the ethyl alcohol that concentration is 30% into concentrate, and the amount of added ethyl alcohol and concentrate
Weight ratio is 8:1, is mixed evenly, and filtering removes filter residue, filtrate is concentrated, and carry out ultraviolet-sterilization and obtain Rosa Damascana.
Application of the gained Rosa Damascana in facial mask, impregnates 50h for face paper in Rosa Damascana, finishes wait impregnate, take
Face paper obtains Rosa Damascana facial mask out, it is preferable that face paper used is 384 silk mask paper.
When using facial mask made from Rosa Damascana of the present invention, which can apply 1 hour or so (according to personal face in face
It, can when Rosa Damascana effective component is completely absorbed on face paper depending on portion absorbs the speed of Rosa Damascana effective component
Remove facial mask), skin is not in malaise symptoms, and skin can be made to reach the state of a hypersorption from inside to outside.
Facial mask made from reason Rosa Damascana of the present invention can apply 1 hour or so in face, and contained effective component can
Slowly skin permeation (skin of people can be divided into five layers: cuticula, hyaline layer, stratum granulosum, spinous layer and basal layer), enables basal layer
The effective component being enough absorbed into facial mask does thorough improvement to skin, so continuously applying 1 hour or so, skin is not in
Discomfort, and comprehensive absorption will be done to effective component from inside to outside, and general commercially available facial mask, the uptake of skin are two to three
Layer, it will be difficult to by sub-percolation again, will appear very much discomfort long so applying, the phenomenon that facial water loss.
Comparative example 1
The extraction process of 1 Rosa Damascana of comparative example are as follows: impregnated without using saline solution, make to be soaked in water, be finished wait impregnate, steamed
The mixed liquor of roseleaf and water is evaporated, phase the step of extraction process of remaining operating procedure with Rosa Damascana described in embodiment 3
Together.
The comparative study of embodiment 1-5 and Rosa Damascana recovery rate obtained by technique described in comparative example 1:
600 kilograms of fresh rose flowers are weighed, are divided into 6 groups, take rhodamine toner described in embodiment 1-5 and comparative example 1 respectively
The extraction process of oil extracts Rosa Damascana, calculates the recovery rate of every group of Rosa Damascana, the results are shown in Table 1:
Table 1
As can be drawn from Table 1, the yield of Rosa Damascana is extracted using the extraction process of Rosa Damascana of the present invention, hence it is evident that
Higher than the yield for the Rosa Damascana that 1 extraction process of comparative example obtains.
The present invention is not limited to above-mentioned preferred forms, anyone can show that other are various under the inspiration of the present invention
The product of form, however, make any variation in its details, it is all that there is technical solution identical or similar to the present application,
It is within the scope of the present invention.
Claims (10)
1. a kind of extraction process of Rosa Damascana, which comprises the following steps:
(1) fresh roseleaf is taken, is rinsed with clear water and removes silt, and drips moisture to the greatest extent;
(2) roseleaf for dripping moisture to the greatest extent is subjected to microwave disinfection;
(3) roseleaf after sterilizing is impregnated with saline solution, the mixed liquor of roseleaf and saline solution is distilled, wait steam
It evaporates and finishes, organic solvent extraction is added into fraction, separates organic phase;
(4) organic phase is concentrated, ethyl alcohol is added into concentrate, is mixed evenly, filters, removes filter residue, filtrate is concentrated, goes forward side by side
Row ultraviolet-sterilization obtains Rosa Damascana.
2. the extraction process of Rosa Damascana according to claim 1, which is characterized in that in step (2), the microwave disinfection
Temperature is 70-80 DEG C, and sterilizing time is 6-8min at this temperature.
3. the extraction process of Rosa Damascana according to claim 1, which is characterized in that in step (3), the saline solution it is dense
Degree is 1%-3%, and the saline solution is 8-10:1, soaking time 4-6h with the weight ratio that need to impregnate roseleaf.
4. the extraction process of Rosa Damascana according to claim 1, which is characterized in that in step (3), the temperature of the distillation
It is 80-100 DEG C.
5. the extraction process of Rosa Damascana according to claim 1, which is characterized in that in step (3), the organic solvent is
Petroleum ether or ethyl acetate.
6. the extraction process of Rosa Damascana according to claim 1, which is characterized in that in step (4), the concentration of the ethyl alcohol
For 25%-30%, the amount of added ethyl alcohol and the weight ratio of concentrate are 5-8:1.
7. application of the Rosa Damascana described in claim 1-6 in facial mask.
8. application of the Rosa Damascana in facial mask according to claim 7, which is characterized in that face paper is immersed in rhodamine toner
It in oil, is finished wait impregnate, takes out face paper and obtain Rosa Damascana facial mask.
9. application of the Rosa Damascana in facial mask according to claim 7, which is characterized in that the face paper is 384 silks
Face paper.
10. application of the Rosa Damascana in facial mask according to claim 7, which is characterized in that the face paper is in rhodamine toner
The time impregnated in oil is 40-50h.
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Cited By (2)
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CN112106863A (en) * | 2020-09-30 | 2020-12-22 | 湖北友花茶业科技有限公司 | Preparation method of cymbidium sinense extract |
CN113930290A (en) * | 2021-11-29 | 2022-01-14 | 山东省食品发酵工业研究设计院 | High-quality rose essential oil efficient extraction method |
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CN104906007A (en) * | 2015-06-24 | 2015-09-16 | 陈琳仁 | Method for extracting rose essential oil, pigment and flavone from roses simultaneously and application of extracts |
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CN108949354A (en) * | 2018-07-14 | 2018-12-07 | 安徽扬子生物科技有限公司 | A kind of Rosa Damascana condensation extraction process |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112106863A (en) * | 2020-09-30 | 2020-12-22 | 湖北友花茶业科技有限公司 | Preparation method of cymbidium sinense extract |
CN113930290A (en) * | 2021-11-29 | 2022-01-14 | 山东省食品发酵工业研究设计院 | High-quality rose essential oil efficient extraction method |
CN113930290B (en) * | 2021-11-29 | 2024-04-16 | 山东省食品发酵工业研究设计院 | Efficient extraction method of high-quality rose essential oil |
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Application publication date: 20191119 |