CN110455852A - A kind of video camera automatic distillation analyzer - Google Patents

A kind of video camera automatic distillation analyzer Download PDF

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Publication number
CN110455852A
CN110455852A CN201910755073.4A CN201910755073A CN110455852A CN 110455852 A CN110455852 A CN 110455852A CN 201910755073 A CN201910755073 A CN 201910755073A CN 110455852 A CN110455852 A CN 110455852A
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CN
China
Prior art keywords
distillation
video camera
tracking
temperature
planker
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910755073.4A
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Chinese (zh)
Inventor
谭剑英
苟振清
刘成林
许帅杰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JINSHI PETROCHEMICAL INSTRUMENT CO Ltd
SHENZHEN JINSHI PETROCHEMICAL INSTRUMENT CO Ltd
Original Assignee
JINSHI PETROCHEMICAL INSTRUMENT CO Ltd
SHENZHEN JINSHI PETROCHEMICAL INSTRUMENT CO Ltd
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Application filed by JINSHI PETROCHEMICAL INSTRUMENT CO Ltd, SHENZHEN JINSHI PETROCHEMICAL INSTRUMENT CO Ltd filed Critical JINSHI PETROCHEMICAL INSTRUMENT CO Ltd
Priority to CN201910755073.4A priority Critical patent/CN110455852A/en
Publication of CN110455852A publication Critical patent/CN110455852A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means
    • G01N25/14Investigating or analyzing materials by the use of thermal means by using distillation, extraction, sublimation, condensation, freezing, or crystallisation

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Or Analyzing Materials Using Thermal Means (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The invention discloses a kind of video camera automatic distillation analyzers, including bottom plate, shell, electric furnace heating component, the cold and hot bath component of distillation, graduated cylinder volume tracking component and temperature measurement component;The temperature measurement component includes the second tracking planker, the thermometer for measuring vapo(u)rizing temperature and the video camera for reading temperature count value, and on the shell, the video camera is mounted on the second tracking planker for the second tracking planker installation.The video camera automatic distillation analyzer uses utensil of the thermometer substitution temperature sensor as automatic temperature measurement, image recognition technology is used simultaneously, temperature count value is carried out with high-definition camera to acquire in real time, thermometer mercury position can be automatically tracked and read mercurial thermometer reading automatically, it is easy to operate intuitive, when eliminating dynamic temperature measurement between temperature sensor and mercurial thermometer because physical characteristic it is inconsistent caused by non-thread sex differernce and heat sensitivity difference.

Description

A kind of video camera automatic distillation analyzer
Technical field
The present invention relates to a kind of determination of distillation device, specifically a kind of video camera automatic distillation analyzer.
Background technique
As long as having manual test and automatic test for the determination of distillation of oil product at present, manual test is in test bar Under part, observes the temperature of the corresponding glass-stem thermometer of each physical examination point and record.It needs to adjust at any time in distillation process Furnace power guarantees defined distilling rate.Also often there is error in reading during the test in user, causes result overproof, Therefore, large labor intensity more demanding to operator.Automatic test is under test conditions, to be detected and distilled using temperature sensor Temperature, the volume point of every setting, automatically records vapo(u)rizing temperature.
Since the physical characteristic of temperature sensor and mercurial thermometer is inconsistent, there are non-thread sex differernce and heat sensitivities There is error during continuous warming in difference, leads to automatic test result just the having differences property between manual test result.
Summary of the invention
The purpose of the present invention is to provide a kind of video camera automatic distillation analyzers, to solve to propose in above-mentioned background technique The problem of.
To achieve the above object, the invention provides the following technical scheme:
A kind of video camera automatic distillation analyzer, including bottom plate, shell, electric furnace heating component, the cold and hot bath component of distillation, amount Cylinder product tracking component and temperature measurement component;The temperature measurement component includes the second tracking planker, the temperature for measuring vapo(u)rizing temperature Meter and the video camera for reading temperature count value, on the shell, the video camera is mounted on for the second tracking planker installation On second tracking planker.
As a further solution of the present invention: the electric furnace heating component includes furnace transformer, distilling flask, distillation cascade Upper end and low-pressure distillation electric aircraft, the furnace transformer are mounted on bottom plate, and the low-pressure distillation electric aircraft is mounted on electric furnace Transformer upper right side, the distilling flask are mounted on low-pressure distillation electric aircraft, and the branch pipe of the distilling flask is inserted into distillation cascade Upper end.
As a further solution of the present invention: fire extinguishing system fire defector biography is additionally provided with above the low-pressure distillation electric aircraft Sensor.
As a further solution of the present invention: the cold and hot bath component of distillation includes compressor, refrigerant system condenser, steaming Evaporate pipe, electrical assembly case and power switch;The compressor is mounted on bottom plate, the refrigerant system condenser and compressor phase Even, the electrical assembly case is mounted on the interlayer above compressor, and the cold and hot bath of distillation is equipped on the left of the electrical assembly case, The distillation cascade is mounted in the cold and hot bath of distillation;The power switch is mounted on shell front side.
As a further solution of the present invention: the graduated cylinder volume tracking component includes graduated cylinder, initial boiling point detection plate, liquid level Detection plate and the first liquid-level tracking planker, the graduated cylinder are placed on bottom plate vertically, and the first liquid-level tracking planker is mounted on On the left of graduated cylinder, the level sensing plate is installed on the first liquid-level tracking planker.
As a further solution of the present invention: the thermostat for controlling graduated cylinder temperature is additionally provided on the right side of the graduated cylinder.
As a further solution of the present invention: the cold and hot bath of distillation is bathed using the Metal constant temperature without circulation fluid.
As a further solution of the present invention: the LED illumination lamp with uniform light board is equipped in front of the camera lens of the video camera.
Compared with prior art, the beneficial effects of the present invention are:
The video camera automatic distillation analyzer uses utensil of the thermometer substitution temperature sensor as automatic temperature measurement, simultaneously Using image recognition technology, temperature count value is carried out with high-definition camera and is acquired in real time, it is strong to ambient light by software algorithm The influence of weak variation carries out intelligent background intensity amplification, guarantees that ambient light variation does not have an impact identification, can automatically track Thermometer mercury position, automatic identification graduation of thermometer read mercurial thermometer reading in real time, easy to operate intuitive, eliminate When dynamic temperature measurement between temperature sensor and mercurial thermometer because physical characteristic it is inconsistent caused by non-thread sex differernce and sense Warm sensitivity difference.
Detailed description of the invention
Fig. 1 is the front view of video camera automatic distillation analyzer;
Fig. 2 is the side view of video camera automatic distillation analyzer;
Fig. 3 is the rearview of video camera automatic distillation analyzer.
In figure: 1- graduated cylinder, 2- level sensing plate, 3- initial boiling point detection plate, 4- distillation cascade, the first liquid-level tracking of 5- planker, The cold and hot bath of 6- distillation, 7- electrically assemble case, 8- thermostat, 9- compressor, the second liquid-level tracking of 10- planker, 11- thermometer, 12- Video camera, 13- power switch, 14- distilling flask, 15- distillation cascade upper end, 16- low-pressure distillation electric aircraft, 17- furnace transformer, 18- refrigerant system condenser, 19- fire extinguishing system flame detection sensor, 20- bottom plate, 21 shells.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
Embodiment 1
Please refer to Fig. 1-3, a kind of video camera automatic distillation analyzer, including bottom plate 20, shell 21, electric furnace heating component, Distill cold and hot bath component, graduated cylinder volume tracking component and temperature measurement component;The temperature tracks the concrete form of component with no restrictions, In the present embodiment, it is preferred that the temperature measurement component includes the second tracking planker 10,11 and of thermometer for measuring vapo(u)rizing temperature For reading the video camera 12 of 11 numerical value of thermometer, the second tracking planker 10 is mounted on shell 21, the video camera 12 It is mounted on the second tracking planker 10, the video camera 12 can simulate the operation of human eye, directly read the temperature on thermometer 11 Degree value thoroughly avoids error in reading caused by due to the difference of other physical characteristics, guarantees the vapo(u)rizing temperature detected Accuracy;
The electric furnace heating component makes it be become oil vapour by thermal evaporation for heat oil sample;
The cold and hot bath component of distillation makes its liquefaction for cooling down oil vapour;
The graduated cylinder volume tracking component is used to measure the volume of liquefied petroleum;
The concrete form of the electric furnace heating component with no restrictions, in the present embodiment, it is preferred that the electric furnace heating component Including furnace transformer 17, distilling flask 14 and low-pressure distillation electric aircraft 16, the furnace transformer 17 is installed on the base plate 20, The low-pressure distillation electric aircraft 16 is mounted on 17 upper right side of furnace transformer, and the distilling flask 14 is mounted on low-pressure distillation electric furnace On frame 16, the branch pipe of the distilling flask 14 is inserted into distillation cascade upper end 15;
It is additionally provided with fire extinguishing system flame detection sensor 19 above the low-pressure distillation electric aircraft 16, for detecting flame, Promote security performance;
It is described to distill the cold and hot concrete form for bathing component with no restrictions, in the present embodiment, it is preferred that the cold and hot bath of distillation Component includes compressor 9, refrigerant system condenser 18, distillation cascade 4, electrical assembly case 7 and power switch 13;The compressor 9 On the base plate 20, the refrigerant system condenser 18 is connected with compressor 9, and the electrical assembly case 7 is mounted on compressor 9 for installation On the interlayer of top, the cold and hot bath 6 of distillation is installed on the left of the electrical assembly case 7, the distillation cascade 4 is mounted on the cold and hot bath of distillation In 6;The power switch 13 is mounted on 21 front side of shell;
The graduated cylinder volume tracks the concrete form of component with no restrictions, in the present embodiment, it is preferred that the graduated cylinder volume Tracking component includes graduated cylinder 1, initial boiling point detection plate 3, level sensing plate 2 and the first liquid-level tracking planker 5, and the graduated cylinder 1 is vertical It places on the base plate 20, the first liquid-level tracking planker 5 is mounted on the left side of graduated cylinder 1, and the level sensing plate 2 is installed in the On one liquid-level tracking planker 5;
It is additionally provided with thermostat 8 on the right side of the graduated cylinder 1, for controlling the temperature of graduated cylinder 1;
Furnace silk in the low-pressure distillation electric aircraft 16 is import furnace silk, and thermal inertia is small, and heating adjusts sensitive;
The graduated cylinder 1 and distilling flask 14 are all made of special glass graduated cylinder and special glass flask, ensure that the survey of graduated cylinder Accuracy of measurement, troublesome in poeration caused by reducing because of the difference between different flasks and measurement error;
The cold and hot bath 6 of distillation is bathed using the Metal constant temperature without circulation fluid, and warming and cooling rate is fast, and temperature is uniform, failure Few, the service life is long.
In front of the camera lens of the video camera 12, positioned at the left side of mercurial thermometer 11, it is additionally provided with the LED illumination with uniform light board It is more acurrate to read registration to keep the shooting light of video camera 12 more sufficient for lamp.
The network operation feature that it networking unified operation that the video camera automatic distillation analyzer, which also has computer, is uniformly controlled, The lims network system that may be incorporated into laboratory, facilitates transimiison analysis data.
The working principle of the present embodiment is:
Distillation sample to be tested distilling flask 14 is packed into according to standard first to carry out under the rated condition for being suitble to its property Distillation, computer set the electric furnace heating on specified power control low-pressure distillation electric aircraft 16 according to sample, pass through video camera 12 The mercury for tracking thermometer 11 directly reads the steam temperature value of the instruction of thermometer 11.After detecting that initial boiling point comes out, liquid The laser sensor of detection liquid level in the detection plate 2 of position starts to track liquid level, according to the return information of laser sensor, computer Distillation speed is calculated, fine tuning heating power is allowed to meet specified heating speed.Screen shows the distillation every fixed volume Temperature and distillation time show in addition it can be converted into volume curve figure or time plot.When vapo(u)rizing temperature reaches end When the requirement of mode, electric furnace stops heating, continues to test liquid level and no longer changes until by standard liquid level, when warm in distilling flask 14 Pop-up window requires input residual volume when degree is lower than user's set temperature, can remove distilling flask 14 at this time and measure raffinate body Product obtains test result after inputting residual quantity and prints.
Embodiment 2
A kind of video camera automatic distillation analyzer as described in Example 1 is provided in the present embodiment does quadrat method, specifically Steps are as follows:
The video camera automatic distillation analyzer is powered on, turns on the power switch 13, then open computer by the first step, will Automatic distillation program is opened;
Second step, double click " enter setting ", and it is to be used that drop down button selection institute is clicked at " thermometer selection " Thermometer number, clicks drop down button at " oil sample selection " and selects the oil sample title to be done, then clicks " confirmation " and exits; Host controls the temperature for carrying out condenser pipe temperature and graduated cylinder room by selected oil sample parameter setting at this time;
Third step installs sample by standard, flag bit temperature value is arranged, 14 branch pipe of distilling flask is put in condenser pipe, temperature The camera lens of 11 reading face video camera 12 of degree meter, then " start-up operation " button is clicked, username and password is inputted, is joined into work Number setting screen;
4th step chooses sample type, thermometer and graduated cylinder number, input sample number and current atmospheric pressure, by " really There is working environment parameter setting dialog box in key calmly ", clicks " confirmation " key after checking each parameter, starts to do sample test.Electric furnace is opened Begin to heat, work timing column starts timing, and red line starts to track mercury, and automatically records temperature;
5th step, computer screen show every 10% volume and initial boiling point, 5%, 95% and the end point of distillation vapo(u)rizing temperature and Distillation time shows in addition it can be converted into volume curve figure or time plot.Screen shows the steaming every the set time Temperature and distillation time are evaporated, is shown in addition it can be converted into volume curve figure or time plot.When vapo(u)rizing temperature reaches knot When the requirement of beam mode, electric furnace stops heating, continues to test liquid level and no longer changes until by standard liquid level, when in distilling flask 14 Pop-up window requires input residual volume when temperature is lower than user's set temperature, can remove distilling flask 14 at this time and measure raffinate Volume obtains test result after inputting residual quantity and prints.
The video camera automatic distillation analyzer uses utensil of the thermometer substitution temperature sensor as automatic temperature measurement, simultaneously Using image recognition technology, temperature count value is carried out with high-definition camera and is acquired in real time, it is strong to ambient light by software algorithm The influence of weak variation carries out intelligent background intensity amplification, guarantees that ambient light variation does not have an impact identification, can automatically track Thermometer mercury position, automatic identification graduation of thermometer read mercurial thermometer reading in real time, easy to operate intuitive;It eliminates When dynamic temperature measurement between temperature sensor and mercurial thermometer because physical characteristic it is inconsistent caused by non-thread sex differernce and sense Warm sensitivity difference.It is controlled simultaneously using computer, real-time display distills overall process parameter;With perfect network operation feature, Can be networked unified operation by computer, be uniformly controlled, and be may be incorporated into the lims network system in laboratory, facilitated transimiison analysis data.
The preferred embodiment of the patent is described in detail above, but this patent is not limited to above-mentioned embodiment party Formula within the knowledge of one of ordinary skill in the art can also be under the premise of not departing from this patent objective It makes a variety of changes.

Claims (8)

1. a kind of video camera automatic distillation analyzer, including bottom plate (20), shell (21), electric furnace heating component, the cold and hot bath of distillation Component, graduated cylinder volume tracking component and temperature measurement component;It is characterized in that, the temperature measurement component include second tracking planker (10), Video camera (12) for measuring the thermometer (11) of vapo(u)rizing temperature and for reading thermometer (11) numerical value, second tracking Planker (10) is mounted on shell (21), and the video camera (12) is mounted on the second tracking planker (10).
2. video camera automatic distillation analyzer according to claim 1, which is characterized in that the electric furnace heating component includes Furnace transformer (17), distilling flask (14), distillation cascade upper end (15) and low-pressure distillation electric aircraft (16), the furnace transformer (17) it is mounted on bottom plate (20), the low-pressure distillation electric aircraft (16) is mounted on furnace transformer (17) upper right side, the steaming It evaporates flask (14) to be mounted on low-pressure distillation electric aircraft (16), be arranged on distillation cascade outside distilling flask (14) the side branch It holds (15).
3. video camera automatic distillation analyzer according to claim 2, which is characterized in that the low-pressure distillation electric aircraft (16) top is additionally provided with fire extinguishing system flame detection sensor (19).
4. video camera automatic distillation analyzer according to claim 1 or 2, which is characterized in that the cold and hot bath group of distillation Part includes compressor (9), refrigerant system condenser (18), distillation cascade (4), electrically assembles case (7) and power switch (13);It is described Compressor (9) is mounted on bottom plate (20), and the refrigerant system condenser (18) is connected with compressor (9), the electrical assembly Case (7) is mounted on the interlayer above compressor (9), and the cold and hot bath (6) of distillation, institute are equipped on the left of the electrical assembly case (7) Distillation cascade (4) is stated to be mounted in the cold and hot bath (6) of distillation;The power switch (13) is mounted on front side of shell (21).
5. video camera automatic distillation analyzer according to claim 1 or 2, which is characterized in that the graduated cylinder volume tracking Component includes graduated cylinder (1), initial boiling point detection plate (3), level sensing plate (2) and the first liquid-level tracking planker (5), the graduated cylinder (1) it is placed in vertically on bottom plate (20), the first liquid-level tracking planker (5) is mounted on the left of graduated cylinder (1), the level sensing Plate (2) is installed on the first liquid-level tracking planker (5).
6. video camera automatic distillation analyzer according to claim 5, which is characterized in that also set on the right side of the graduated cylinder (1) There is the thermostat (8) for control amount cylinder (1) temperature.
7. video camera automatic distillation analyzer according to claim 4, which is characterized in that the cold and hot bath (6) of distillation is adopted It is bathed with the Metal constant temperature without circulation fluid.
8. video camera automatic distillation analyzer according to claim 1, which is characterized in that the camera lens of the video camera (12) Front is equipped with the LED illumination lamp with uniform light board.
CN201910755073.4A 2019-08-15 2019-08-15 A kind of video camera automatic distillation analyzer Pending CN110455852A (en)

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Application Number Priority Date Filing Date Title
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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1129319A (en) * 1994-10-05 1996-08-21 顺德珠江传感器厂 Method for reading and processing data measured for petroleum product distillation
US20180036648A1 (en) * 2016-08-03 2018-02-08 Instrumentation Scientifique de Laboratoire - I.S. L. System and Method for Auto Distilling Liquids at Strictly Defined Conditions Regardless of Composition
CN107843613A (en) * 2017-11-22 2018-03-27 郑泽宇 Vision-based detection automatic distillation range analyzer
CN210442286U (en) * 2019-08-15 2020-05-01 深圳市湘津石仪器有限公司 Automatic distillation tester for camera

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1129319A (en) * 1994-10-05 1996-08-21 顺德珠江传感器厂 Method for reading and processing data measured for petroleum product distillation
US20180036648A1 (en) * 2016-08-03 2018-02-08 Instrumentation Scientifique de Laboratoire - I.S. L. System and Method for Auto Distilling Liquids at Strictly Defined Conditions Regardless of Composition
CN107843613A (en) * 2017-11-22 2018-03-27 郑泽宇 Vision-based detection automatic distillation range analyzer
CN210442286U (en) * 2019-08-15 2020-05-01 深圳市湘津石仪器有限公司 Automatic distillation tester for camera

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