CN110436548A - A kind of complete processing equipment of high-salt wastewater vaporation-type zero-emission - Google Patents

A kind of complete processing equipment of high-salt wastewater vaporation-type zero-emission Download PDF

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Publication number
CN110436548A
CN110436548A CN201910839340.6A CN201910839340A CN110436548A CN 110436548 A CN110436548 A CN 110436548A CN 201910839340 A CN201910839340 A CN 201910839340A CN 110436548 A CN110436548 A CN 110436548A
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CN
China
Prior art keywords
separator
primary
outlet
steam
entrance
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Pending
Application number
CN201910839340.6A
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Chinese (zh)
Inventor
舒俭
何汉锋
罗璞
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Guangzhou City Xinde Industrial Co ltd
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Guangzhou City Xinde Industrial Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Priority to CN201910839340.6A priority Critical patent/CN110436548A/en
Publication of CN110436548A publication Critical patent/CN110436548A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/02Treatment of water, waste water, or sewage by heating
    • C02F1/04Treatment of water, waste water, or sewage by heating by distillation or evaporation

Abstract

The invention discloses a kind of complete processing equipments of high-salt wastewater vaporation-type zero-emission, including fixed gas cooler, primary separator, second-stage separator, level-one vapour compression machine and second steam compressor, the side of the fixed gas cooler is provided with preheater, the outlet of the fixed gas cooler and the entrance of preheater connect, the other side of the preheater is provided with primary heater, the outlet of the preheater and the entrance of primary heater connect, the other side of the primary heater is provided with primary separator, the outlet of the primary heater and the entrance of primary separator connect, the other side of the primary separator is provided with secondary heater.The present invention passes through setting primary separator, second-stage separator, level-one vapour compression machine and second steam compressor, solves existing higher boiling, the problem that fresh steam consumption is big, energy consumption is high in the more demanding material concentration and evaporation concentration process of thermal sensitivity, cocnentration factor, product is rotten.

Description

A kind of complete processing equipment of high-salt wastewater vaporation-type zero-emission
Technical field
The present invention relates to evaporation concentration technique field, specially a kind of complete processing dress of high-salt wastewater vaporation-type zero-emission It is standby.
Background technique
In recent years because of the urgent need of energy-saving and emission-reduction, simple tradition multiple-effect evaporation has been not suitable with this demand, at the same time MVR Evaporation concentration technique is widely used in the world.Existing single-action MVR evaporation concentration technique is limited to steam The temperature rise of the technological limit of vapour compressor, single compressor can only be within 25 DEG C, still, for higher boiling, thermal sensitivity, concentration Than more demanding material situation, currently, existing single-action MVR working method and simple multiple-effect evaporation, which are no longer satisfied, to be needed It wants, often faces the problems such as compressor temperature rise is insufficient, evaporating temperature high product is rotten, energy consumption is high, it is therefore necessary to existing skill Art improves, to solve the above problems.
Summary of the invention
(1) the technical issues of solving
In view of the deficiencies of the prior art, the present invention provides a kind of complete processing equipment of high-salt wastewater vaporation-type zero-emission, Solve existing higher boiling, in the more demanding material concentration and evaporation concentration process of thermal sensitivity, cocnentration factor fresh steam consumption it is big, The problem that energy consumption is high, product is rotten.
(2) technical solution
To achieve the above object, the invention provides the following technical scheme: a kind of complete place of high-salt wastewater vaporation-type zero-emission Reason equipment, including fixed gas cooler, primary separator, second-stage separator, level-one vapour compression machine and second steam compressor, The side of the fixed gas cooler is provided with preheater, and the outlet of the fixed gas cooler and the entrance of preheater connect, The other side of the preheater is provided with primary heater, and the outlet of the preheater and the entrance of primary heater connect, institute The other side for stating primary heater is provided with primary separator, and the outlet of the primary heater and the entrance of primary separator connect It connects, the other side of the primary separator is provided with secondary heater, the outlet of the primary separator and secondary heater Entrance connection, the other side of the secondary heater are provided with second-stage separator, the outlet of the secondary heater and two fractions Entrance connection from device, the other side of the second-stage separator are provided with solid-liquid separating machine, the outlet of the second-stage separator with The entrance of solid-liquid separating machine connects, the primary heater, primary separator, secondary heater and second-stage separator top set Be equipped with braced frame, the braced frame upper end be fixed with level-one vapour compression machine, second steam compressor and and vacuum equipment, The outlet of the entrance and second-stage separator of the second steam compressor connects, the outlet and level-one of the second steam compressor The entrance of vapour compression machine connects, and the outlet of the level-one vapour compression machine is heated with the entrance of primary heater and second level respectively The entrance of device connects, and the outlet of the primary heater and secondary heater is connect with the entrance of preheater, two fraction Outlet from device is connect with the entrance of fixed gas cooler, and the outlet of the fixed gas cooler and the entrance of vacuum equipment connect It connects.
Preferably, the evaporating pressure of the second-stage separator is lower than the evaporating pressure of primary separator, the second-order separation The secondary steam temperature that device generates is lower than the secondary steam temperature that primary separator generates.
Preferably, vapor (steam) temperature and pressure that the steam after the second steam compressor compresses and primary separator generate Unanimously, the inlet temperature of the level-one vapour compression machine goes out with the vapor (steam) temperature and primary separator of second steam compressor outlet The secondary steam temperature of mouth is consistent.
Preferably, the steam inlet end of the primary heater and the steam inlet end of secondary heater are respectively arranged with One throttle valve and second throttle.
Preferably, the inside of the primary separator and second-stage separator is provided with wire mesh demister.
Preferably, the vacuum equipment is Hydraulic Circulation vacuum pump.
(3) beneficial effect
The present invention provides a kind of complete processing equipment of high-salt wastewater vaporation-type zero-emission, have it is following the utility model has the advantages that
(1) present invention compresses the steam of second-stage separator by second steam compressor, can be second-stage separator Pressure reduced, reduce the evaporating temperature of second-stage separator, guarantee that material is evaporated at low temperature, effectively prevent object Expect that thermal sensitivity is destroyed;
(2) vapor (steam) temperature raising is reached 30-50 DEG C by two second compressions by the present invention, effectively increases steam and material Heat transfer temperature difference allows high boiling material in secondary heater to carry out the concentration of high magnification numbe;
(3) present invention is combined using compressor vapor recompression with double-effect evaporation, solves object in Multi-effect Evaporation Processes Material temperature spends high problem;By compressor vapor recompression, recovery section steam gasification latent heat reduces the use of fresh steam Amount;
(4) present invention flexibly can effectively adjust the steam flow of primary heater and secondary heater, thus control two The evaporation capacity of effect;
(5) second steam compressor of the present invention is small flow, and low temperature compression, level-one vapour compression machine is big flow, high temperature Compression, than common MVR partial pressure method, (level-one vapour compression machine is big flow, low temperature to the compressor cost of investment of this processing method Compression, another grade of vapour compression machine is small flow, high temperature compressed) processing method compression cost of investment it is lower.
Detailed description of the invention
Fig. 1 is overall diagram of the invention;
Fig. 2 is flow diagram of the invention;
Fig. 3 is the structure chart of primary separator of the present invention.
Appended drawing reference in figure are as follows: 1, fixed gas cooler;2, preheater;3, primary heater;4, primary separator;5, two Grade heater;6, second-stage separator;7, solid-liquid separating machine;8, level-one vapour compression machine;9, second steam compressor;10, it supports Frame;11, vacuum equipment;12, first throttle valve;13, second throttle;14, wire mesh demister.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
As shown in Figure 1-3, the present invention provides a kind of technical solution: a kind of complete processing dress of high-salt wastewater vaporation-type zero-emission It is standby, including fixed gas cooler 1, primary separator 4, second-stage separator 6, level-one vapour compression machine 8 and second steam compressor 9, the side of fixed gas cooler 1 is provided with preheater 2, and the outlet of fixed gas cooler 1 is connect with the entrance of preheater 2, in advance The other side of hot device 2 is provided with primary heater 3, and the outlet of preheater 2 is connect with the entrance of primary heater 3, level-one heating The other side of device 3 is provided with primary separator 4, and the outlet of primary heater 3 is connect with the entrance of primary separator 4, a fraction The other side from device 4 is provided with secondary heater 5, and the outlet of primary separator 4 is connect with the entrance of secondary heater 5, second level The other side of heater 5 is provided with second-stage separator 6, and the outlet of secondary heater 5 is connect with the entrance of second-stage separator 6, and two The other side of grade separator 6 is provided with solid-liquid separating machine 7, and the outlet of second-stage separator 6 is connect with the entrance of solid-liquid separating machine 7, Primary heater 3, primary separator 4, secondary heater 5 and second-stage separator 6 top be provided with braced frame 10, support frame 10 upper end of frame is fixed with level-one vapour compression machine 8, second steam compressor 9 and vacuum equipment 11, and second steam compressor 9 enters Mouth is connect with the outlet of second-stage separator 6, and the outlet of second steam compressor 9 is connect with the entrance of level-one vapour compression machine 8, and one The outlet of grade vapour compression machine 8 is connect with the entrance of the entrance of primary heater 3 and secondary heater 5 respectively, primary heater 3 It is connect with the entrance of preheater 2 with the outlet of secondary heater 5, the outlet of second-stage separator 6 and entering for fixed gas cooler 1 Mouth connection, the outlet of fixed gas cooler 1 is connect with the entrance of vacuum equipment 11.
Further, the evaporating pressure of second-stage separator 6 is lower than the evaporating pressure of primary separator 4, and second-stage separator 6 generates Secondary steam temperature be lower than primary separator 4 generate secondary steam temperature, guarantee material be evaporated at low temperature, effectively Avoid the destruction of material thermal sensitivity.
Further, vapor (steam) temperature and pressure one that the compressed steam of second steam compressor 9 and primary separator 4 generate It causes, the vapor (steam) temperature and primary separator 4 that the inlet temperature and second steam compressor 9 of level-one vapour compression machine 8 export export Secondary steam temperature it is consistent.
Further, the steam inlet end of primary heater 3 and the steam inlet end of secondary heater 5 are respectively arranged with first Throttle valve 12 and second throttle 13 flexibly can effectively adjust the steam flow of primary heater 3 and secondary heater 5, from And control the evaporation capacity of two effects.
Further, the inside of primary separator 4 and second-stage separator 6 is provided with wire mesh demister 14, wire mesh demister 14 can carry out foam removal to the gas in uphill process containing mist after steam separation, make mist is biggish to condense under water droplet It falls, realizes further steam separation.
Further, vacuum equipment 11 is Hydraulic Circulation vacuum pump, and vacuum equipment 11 is for adjusting 1 vacuum of fixed gas cooler Degree.
Working principle;It is carried out in use, material first passes through the fixed gas that fixed gas cooler 1 and second-stage separator 6 are discharged Heat exchange, recovery section heat;Then after cooling cold by preheater 2 and primary heater 3,5 compressed steam of secondary heater Condensate exchanges heat, and further recycles heat;The material temperature of temperature of charge after exchanging heat twice close to primary heater 3 Degree, then into primary heater 3, material enters primary separator 4 after the heating of primary heater 3 and carries out vapour-liquid point From, after material cocnentration factor reaches setting value, is heated into secondary heater 5 and separated using second-stage separator 6, material When concentration reaches the discharge concentration of setting, it is discharged by 6 products export of second-stage separator;It enters solid-liquid separating machine 7 and carries out solid-liquid Separation, obtains product, and isolated liquid, which returns to secondary heater 5, to be continued to heat, while the separation generation of second-stage separator 6 is secondary Steam enters back into level-one vapour compression machine 8 and divides with primary separator 4 after the wire mesh demister 14 of second-stage separator 6 is handled Both vapor compression is carried out by level-one vapour compression machine 8 after secondary steam mixing from generation, improves temperature, some vapor after compression 3 steam inlet of primary heater is entered, as 3 heat source of primary heater, some vapor enters secondary heater 5, as 5 heat source of secondary heater, specifically, after the secondary steam that second-stage separator 6 generates is compressed by second steam compressor 9, temperature Degree, pressure rise, and the volume of steam becomes smaller, generated by the compressed secondary steam of second steam compressor 9 with primary separator 4 Secondary steam enter back into level-one vapour compression machine 8, after making second-compressed, steam enters primary heater 3, secondary heater 5 It exchanges heat, vapor (steam) temperature raising is reached 30-50 DEG C by two second compressions, improves the heat transfer temperature difference of steam and material, so that High boiler material after primary concentration into secondary concentration can carry out the concentration of high magnification numbe, meanwhile, into primary heater 3 Flow control is carried out by steam measurement device and steam flow throttle valve with the steam of secondary heater 5.
It can to sum up obtain, the present invention passes through setting primary separator 4, second-stage separator 6, level-one vapour compression machine 8 and second level Vapour compression machine 9 realizes that compressor vapor recompression is combined with double-effect evaporation, solves existing technology Multi-effect Evaporation Processes Middle temperature of charge is excessively high, problem apt to deteriorate, and by compressor vapor recompression, recovery section steam gasification latent heat is reduced The usage amount of fresh steam, solves the problems, such as that the usage amount of the fresh steam of existing technology is big.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment Intrinsic element.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (6)

1. a kind of complete processing equipment of high-salt wastewater vaporation-type zero-emission, including fixed gas cooler (1), primary separator (4), Second-stage separator (6), level-one vapour compression machine (8) and second steam compressor (9), it is characterised in that: the fixed gas is cooling The side of device (1) is provided with preheater (2), and the outlet of the fixed gas cooler (1) is connect with the entrance of preheater (2), institute The other side for stating preheater (2) is provided with primary heater (3), the outlet of the preheater (2) and entering for primary heater (3) Mouthful connection, the other side of the primary heater (3) is provided with primary separator (4), the outlet of the primary heater (3) with The entrance of primary separator (4) connects, and the other side of the primary separator (4) is provided with secondary heater (5), the level-one The outlet of separator (4) is connect with the entrance of secondary heater (5), and the other side of the secondary heater (5) is provided with second level The outlet of separator (6), the secondary heater (5) is connect with the entrance of second-stage separator (6), the second-stage separator (6) The other side be provided with solid-liquid separating machine (7), the outlet of the second-stage separator (6) is connect with the entrance of solid-liquid separating machine (7), The primary heater (3), primary separator (4), secondary heater (5) and second-stage separator (6) top be provided with support Frame (10), braced frame (10) upper end are fixed with level-one vapour compression machine (8), second steam compressor (9) and vacuum The entrance of equipment (11), the second steam compressor (9) is connect with the outlet of second-stage separator (6), the second steam pressure The outlet of contracting machine (9) is connect with the entrance of level-one vapour compression machine (8), the outlet of the level-one vapour compression machine (8) respectively with The entrance of primary heater (3) is connected with the entrance of secondary heater (5), the primary heater (3) and secondary heater (5) Outlet connect with the entrance of preheater (2), the entrance of the outlet of the second-stage separator (6) and fixed gas cooler (1) Connection, the outlet of the fixed gas cooler (1) is connect with the entrance of vacuum equipment (11).
2. a kind of complete processing equipment of high-salt wastewater vaporation-type zero-emission according to claim 1, it is characterised in that: described The evaporating pressure of second-stage separator (6) is lower than the evaporating pressure of primary separator (4), the second-stage separator (6) generate two Secondary vapor (steam) temperature is lower than the secondary steam temperature that primary separator (4) generate.
3. a kind of complete processing equipment of high-salt wastewater vaporation-type zero-emission according to claim 1, it is characterised in that: described Second steam compressor (9) compressed steam is consistent with vapor (steam) temperature and pressure that primary separator (4) generates, the level-one The vapor (steam) temperature and primary separator (4) outlet of the inlet temperature of vapour compression machine (8) and second steam compressor (9) outlet Secondary steam temperature is consistent.
4. a kind of complete processing equipment of high-salt wastewater vaporation-type zero-emission according to claim 1, it is characterised in that: described The steam inlet end of primary heater (3) and the steam inlet end of secondary heater (5) are respectively arranged with first throttle valve (12) With second throttle (13).
5. a kind of complete processing equipment of high-salt wastewater vaporation-type zero-emission according to claim 1, it is characterised in that: described The inside of primary separator (4) and second-stage separator (6) is provided with wire mesh demister (14).
6. a kind of complete processing equipment of high-salt wastewater vaporation-type zero-emission according to claim 1, it is characterised in that: described Vacuum equipment (11) is Hydraulic Circulation vacuum pump.
CN201910839340.6A 2019-09-05 2019-09-05 A kind of complete processing equipment of high-salt wastewater vaporation-type zero-emission Pending CN110436548A (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
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JPH1057702A (en) * 1996-08-26 1998-03-03 Sasakura Eng Co Ltd Auto-vapor compression type concentration method of water solution and device therefor
CN101497466A (en) * 2008-02-02 2009-08-05 上海达源环境科技工程有限公司 Vapor compression sewage treatment system
CN101683569A (en) * 2008-09-25 2010-03-31 笹仓机械工程有限公司 Evaporation-concentration apparatus and evaporation-concentration method for aqueous solution
CN106540471A (en) * 2016-10-28 2017-03-29 广西大学 A kind of employing triple effect evaporation technique concentrates the method and device of biogas slurry
CN107162297A (en) * 2016-03-08 2017-09-15 广州市心德实业有限公司 One kind one imitates four body MVR mixed salts waste water separators and separation method
CN107628660A (en) * 2017-11-03 2018-01-26 深圳市纯水号水处理科技有限公司 A kind of high salinity waste water mechanical vapor recompresses MVR systems technologies
CN108910992A (en) * 2018-07-19 2018-11-30 江苏京源环保股份有限公司 A kind of rectifying applied to high saliferous high-COD waste water, MVR vaporising device
CN109279673A (en) * 2018-10-18 2019-01-29 国家能源投资集团有限责任公司 The processing method and processing system of methanol-to-olefins sewage

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU486046A1 (en) * 1974-03-13 1975-09-30 Всесоюзный Проектноконструкторский И Научно-Исследовательский Институт Автоматизации Пищевой Промышленности "Пищепромавтоматика" Method for automatic control of multi-unit evaporating unit without intermediate vapor collection
JPH1057702A (en) * 1996-08-26 1998-03-03 Sasakura Eng Co Ltd Auto-vapor compression type concentration method of water solution and device therefor
CN101497466A (en) * 2008-02-02 2009-08-05 上海达源环境科技工程有限公司 Vapor compression sewage treatment system
CN101683569A (en) * 2008-09-25 2010-03-31 笹仓机械工程有限公司 Evaporation-concentration apparatus and evaporation-concentration method for aqueous solution
CN107162297A (en) * 2016-03-08 2017-09-15 广州市心德实业有限公司 One kind one imitates four body MVR mixed salts waste water separators and separation method
CN106540471A (en) * 2016-10-28 2017-03-29 广西大学 A kind of employing triple effect evaporation technique concentrates the method and device of biogas slurry
CN107628660A (en) * 2017-11-03 2018-01-26 深圳市纯水号水处理科技有限公司 A kind of high salinity waste water mechanical vapor recompresses MVR systems technologies
CN108910992A (en) * 2018-07-19 2018-11-30 江苏京源环保股份有限公司 A kind of rectifying applied to high saliferous high-COD waste water, MVR vaporising device
CN109279673A (en) * 2018-10-18 2019-01-29 国家能源投资集团有限责任公司 The processing method and processing system of methanol-to-olefins sewage

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