CN110387740A - A kind of electric-welding protective garment fabric preparation method based on graphene heat dissipation and electric-welding protective garment fabric obtained - Google Patents
A kind of electric-welding protective garment fabric preparation method based on graphene heat dissipation and electric-welding protective garment fabric obtained Download PDFInfo
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- CN110387740A CN110387740A CN201910645651.9A CN201910645651A CN110387740A CN 110387740 A CN110387740 A CN 110387740A CN 201910645651 A CN201910645651 A CN 201910645651A CN 110387740 A CN110387740 A CN 110387740A
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- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D13/00—Professional, industrial or sporting protective garments, e.g. surgeons' gowns or garments protecting against blows or punches
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D31/00—Materials specially adapted for outerwear
- A41D31/04—Materials specially adapted for outerwear characterised by special function or use
- A41D31/08—Heat resistant; Fire retardant
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
- D06M11/74—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon or graphite; with carbides; with graphitic acids or their salts
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D2600/00—Uses of garments specially adapted for specific purposes
- A41D2600/20—Uses of garments specially adapted for specific purposes for working activities
- A41D2600/202—Welding
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/18—Synthetic fibres consisting of macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/24—Polymers or copolymers of alkenylalcohols or esters thereof; Polymers or copolymers of alkenylethers, acetals or ketones
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/34—Polyamides
- D06M2101/36—Aromatic polyamides
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Physical Education & Sports Medicine (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Professional, Industrial, Or Sporting Protective Garments (AREA)
Abstract
The present invention provides a kind of electric-welding protective garment fabric preparation method based on graphene heat dissipation and electric-welding protective garment fabric obtained, it is characterized by: first carrying out positive application to flame retardant base cloth using graphene oxide solution, it is dried at 60 DEG C or less, the modified fabric of graphene oxide is made；Reduction treatment is carried out to the modified fabric of graphene oxide again, the electric-welding protective garment fabric to radiate based on graphene is made in drying.Electric-welding protective garment fabric obtained has good surface radiating performance, reduces the heating of envers, and the heating after 15 drop molten metal drippages is no more than 37 DEG C；Wash front and back char length≤50mm, after flame time≤2s, smoldering time≤2s, fabric through latitudinal strength be greater than 800N × 600N.Present invention process is simple, easily operated, and fabric obtained has the function of excellent fusion proof metal drippage heating.
Description
Technical field
The invention belongs to textile product manufacturing technology fields, and in particular to the textile fabric processing technology of safeguard function.More
In particular it relates to a kind of electric-welding protective garment fabric preparation method based on graphene heat dissipation and electric-welding protective garment obtained
Fabric.
Background technique
In China, there is nearly 2,000,000 people to be engaged in electric welding field.Electric welding field employee especially carries out facing upward appearance in narrow space
The employee of weld job is faced with infringement of the molten metal to body.
Existing electric-welding protective garment fabric also has the advanced electric welding using leather or kevlar fabric based on fire-retardant pure cotton fabric
Protective garment, but price is expensive.The unrestrained scald caused on the fabric to human body of molten metal in order to obstruct electrical welding operation generation,
It generallys use and is greater than 300g/m2Thick and heavy fabric.GB8965.2-2009 (protective clothes, flame protection, part 2: welding clothes)
Regulation: weld protective fabric through latitudinal strength should be greater than 450N, 15 drop molten metals drippage after heating be no more than 40 DEG C, thoroughly
Moisture is greater than 6000g/m2·24h；The after flame time and smoldering time of A grades of protective garments are respectively less than 2s, char length is less than 50mm；
The after flame time and smoldering time of B grades of protective garments are respectively less than 4s, char length is less than 100mm.
Therefore the research of electric-welding protective garment needs to have both anti-flammability, circumferential thermal conductivity, penetrability and light-weighted fabric.
Graphene is the mono-layer graphite piece being stripped out from graphite, has bi-dimensional cellular shape structure, carbon atom is with sp2It is miscellaneous
The form for changing track combines, and has unique two-dimentional atomic structure of carbon, possesses good conductive, thermally conductive, ultraviolet resistance,
Fire retardant be can also be used as to improve the flame retardant property of polymer.Graphene oxide (GO) is the important derivative of graphene, it
Surface have the oxygen containing functional group such as a large amount of carboxyl, hydroxyl, epoxy group, these functional groups impart many spies of graphene oxide
Property for example good dispersibility, hydrophily and with the compatibility of some polymer etc., it is anti-that this can assign the more chemistry of material
Performance is answered, adjacent layer can also be made to form the interaction force that network structure improves monolithic interlayer by being crosslinked, so as to improve material
Physical property.Graphene research both at home and abroad at present is conceived to its electric conductivity, optical property, there is researcher on the textile
Attempt to replace conductive carbon black to produce the lower antistatic fibre of resistivity with graphene；And using graphene or black stock as
Infrared-emitting materials use, however have not yet to see the heat-transfer character of all graphenes in terms of textile, particularly protective garment
Using.
Being disclosed in the information of background parts of the present invention, it is only intended to increase understanding of the overall background of the invention, without answering
When being considered as recognizing or imply that the information constitutes the prior art already known to those of ordinary skill in the art in any form.
Summary of the invention
The present invention in order to solve the problems existing in the prior art, provides a kind of electric-welding protective garment fabric based on graphene heat dissipation
Preparation method, the preparation method simple process is easily operated, and the electric-welding protective garment fabric produced has excellent circumferential direction thermally conductive
Effect can make the hot-fluid for welding the input of flower (molten drop or scorching hot solid) contact fabric front quick around along fabric surface
Diffusion and cooling, play the effect realized to zephyr and inhibit back side heating；Because light and thin type substrate fabric, electric welding can be used
Flexibility, penetrability and the comfort of protective garment are all improved.
The purpose of the present invention is what is be achieved through the following technical solutions: a kind of electric-welding protective garment face based on graphene heat dissipation
Preparation method for material, which is characterized in that the method includes following process:
1) modified process: single side application is carried out to flame retardant base cloth front using graphene oxide solution, is dried at 60 DEG C or less
It is dry, the modified fabric of graphene oxide is made；
2) it restores process: the modified fabric of above-mentioned graphene oxide being subjected to reduction treatment, drying is made and is dissipated based on graphene
The electric-welding protective garment fabric of heat.
Preferably, in modified process, the flame retardant base cloth is that cellulose fiber content is greater than 75% or in cellulose
The arrangement type inflaming retarding fabric of a small amount of reinforcing fiber such as mixed polyvinyl, terylene in fiber, the cellulose fibre are selected from cotton fiber, big
Flaxen fiber, flax fiber, ramee, viscose rayon, Modal fibre, tencel fiber and its mixture.
Preferably, in modified process, the flame retardant base cloth is using inherent fire-retardant fiber or partially modified fire resistance fibre
Or inflaming retarding fabric made of a small amount of non-flame resistant fiber blend, the inherent fire-retardant fiber are selected from aramid fiber, polyimides, poly- virtue and dislike two
Azoles fiber, PSA fiber, alginate fibre and its mixture；The modified flame-retardant fiber includes Flame Vinylon, anti-flaming viscose, fire-retardant washs
Synthetic fibre, fire-retardant polyamide fibre, flame-retardant acrylic fibre etc.；The non-flame resistant fiber includes that polyvinyl, terylene, polyamide fibre, acrylic fibers etc. are used to improve intensity
Additive.
Preferably, in modified process, the single side applying mode includes that full bottom printing, transfer, blade coating, spray etc. apply
Method.
Preferably, in modified process, the graphene oxide solution concentration is 0.5mg/ml~3mg/ml, graphite oxide
The applied amount of alkene solution is 80~160g/m2, drying temperature is 30~45 DEG C, and drying time is 0.5~1h.
Preferably, described to be reduced to electronation in reduction process；Reducing agent is selected from hydrazine and its derivative, hydroboration
The metal hydrides such as sodium, sulfonic derivative, vitamin, glucose；Reducing agent dosage is 1mg/ml~10mg/ml, when reduction
Between be 0.5~3h, reduction temperature be 80~100 DEG C.
Another aspect of the present invention relates to the electric-welding protective garment fabrics based on graphene heat dissipation made from the preparation method.
Preferably, heat of the electric-welding protective garment fabric after Contact welding is spent can on front plan quickly diffusion, from
And envers heating caused by weldering flower contact fabric is reduced, by test method as defined in GB/T17599,15 drip melts melt gold
Heating after belonging to drippage is no more than 37 DEG C；Electric-welding protective garment fabric washing front and back char length≤50mm, after flame time≤
2s, smoldering time≤2s, protective fabric are greater than 800N × 600N through latitudinal strength.
The present invention has many advantages compared with prior art and good effect: the production technology letter of preparation method of the present invention
It is single, it is easily operated；The electric-welding protective garment fabric of preparation has the function of excellent fusion proof metal drippage heating.
Specific embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, the following example is merely to illustrate this
Invention, and should not be taken as limiting the scope of the invention.
A kind of electric-welding protective garment fabric preparation method based on graphene heat dissipation, which is characterized in that the method includes such as
Lower process；
1) modified process: single side application is carried out to flame retardant base cloth front using graphene oxide solution, is dried at 60 DEG C or less
It is dry, the modified fabric of graphene oxide is made；
2) it restores process: the modified fabric of above-mentioned graphene oxide being subjected to reduction treatment, drying is made and is dissipated based on graphene
The electric-welding protective garment fabric of heat.
Specific embodiments of the present invention are as follows:
Graphene oxide solution is produced by Beijing world Zhong Lun new material Science and Technology Ltd., and partial size is less than 10 μm, pH value
About 5；Reducing agent hydrazine hydrate is produced by Jinan Kai Jun Chemical Co., Ltd., and sodium dithionite is by the limited public affairs of Yantai Jin He industry
Department's production；Flame-proof cotton fabric, retardant cotton/polyvinyl fabric, aramid fiber/poly- fragrant oxadiazoles fiber/high-strength fire-retarding polyvinyl/anti-flaming viscose are mixed
Textile fabric is provided by Shandong Woyuan New Fabrics Co., Ltd..
Embodiment 1: a kind of electric-welding protective garment fabric preparation method based on graphene heat dissipation comprises the following steps:
1) modified process: carrying out full bottom printing to flame-proof cotton fabric front using the graphene oxide solution of 0.5mg/ml,
The applied amount of graphene oxide solution is 160g/m2, 2h is dried at a temperature of 35 DEG C, graphene oxide modified flame-retardant cotton is made and knits
Object；
2) it restores process: above-mentioned cotton fabric being placed in 10mg/ml hydrazine hydrate reduction liquid bath, handles 3h at a temperature of 80 DEG C,
It is dried at a temperature of 85 DEG C, graphene modified flame-retardant cotton fabric is made.
The thus obtained electric-welding protective garment fabric weight per square meter 280g based on graphene heat dissipation, through latitudinal strength 940N ×
690N, 15 drip 36.7 DEG C of heating after molten metals drippage；It is through broadwise after flame time 1.4s × 1.5s, through broadwise smoldering time
0.8s × 1.0s, through broadwise char length be 41 × 45mm.And the base fabric of not oxidised graphene reduction fixation, in mechanical property
Under the premise of similar with flame retardant property, the heating after 15 drop molten metal drippages is 42.1 DEG C.
Embodiment 2: a kind of electric-welding protective garment fabric preparation method based on graphene heat dissipation comprises the following steps:
1) modified process: using the graphene oxide solution of 2mg/ml to 80/ high strength vinylon of cotton, 20 FLAME RETARDANT FINISH FABRIC just
Face carries out transfer printing, and the applied amount for the graphene oxide solution that concentration is 0.5mg/ml is 120g/m2, dried at a temperature of 45 DEG C
Modified cotton/polyvinyl the flame-retardant textile of graphene oxide is made in dry 1h；
2) it restores process: above-mentioned flame-retardant textile being placed in the sodium dithionite reduction liquid bath of 5mg/ml, 90 DEG C of temperature
Lower processing 1.5h is dried at a temperature of 85 DEG C, and the modified cotton/polyvinyl flame-retardant textile of graphene is made.
The thus obtained electric-welding protective garment fabric weight per square meter 290g based on graphene heat dissipation, through latitudinal strength 1035N
× 890N, 15 drip 35.8 DEG C of heating after molten metals drippage；Through broadwise after flame time 1.3s × 1.6s, through broadwise smoldering time
It is 39 × 42mm for 0.5s × 0.8s, through broadwise char length.And the base fabric of not oxidised graphene reduction fixation, in mechanical property
Under the premise of energy is similar with flame retardant property, the heating after 15 drop molten metals drippages is 43.4 DEG C.
Embodiment 3: a kind of electric-welding protective garment fabric preparation method based on graphene heat dissipation comprises the following steps:
1) modified process: using the high-strength resistance of the graphene oxide solution of 3mg/ml fragrant oxadiazoles fiber 15/ poly- to aramid fiber 40/
Combustion 30/ anti-flaming viscose of polyvinyl, 15 fabric face is sprayed, and the applied amount of graphene oxide solution is 80g/m2, in 55 DEG C of temperature
Graphene oxide modifying aramid fiber fabric is made in lower drying 0.5h；
2) it restores process: above-mentioned kevlar fabric being placed in the hydrazine hydrate reduction liquid bath of 10mg/ml, at a temperature of 100 DEG C
0.5h is managed, is dried at a temperature of 85 DEG C, graphene modifying aramid fiber fabric is made.
The thus obtained electric-welding protective garment fabric weight per square meter 305g based on graphene heat dissipation, through latitudinal strength 1206N
× 810N, 15 drip 36.2 DEG C of heating after molten metals drippage；It is through broadwise after flame time 0s × 0s, through broadwise smoldering time
0.8s × 1.0s, through broadwise char length be 30 × 31mm.And the base fabric of not oxidised graphene reduction fixation, in mechanical property
Under the premise of similar with flame retardant property, the heating after 15 drop molten metal drippages is 42.4 DEG C.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than is limited；Although referring to aforementioned reality
Applying example, invention is explained in detail, for those of ordinary skill in the art, still can be to aforementioned implementation
Technical solution documented by example is modified or equivalent replacement of some of the technical features；And these are modified or replace
It changes, the spirit and scope for claimed technical solution of the invention that it does not separate the essence of the corresponding technical solution.
Claims (10)
1. a kind of preparation method of the electric-welding protective garment fabric based on graphene heat dissipation, which is characterized in that the method includes such as
Lower process:
1) modified process: single side application is carried out to flame retardant base cloth front using graphene oxide solution, is dried at 60 DEG C or less, system
Obtain the modified fabric of graphene oxide；
2) it restores process: the modified fabric of above-mentioned graphene oxide is subjected to reduction treatment, drying is made and is radiated based on graphene
Electric-welding protective garment fabric.
2. the preparation method of the electric-welding protective garment fabric according to claim 1 based on graphene heat dissipation, which is characterized in that
In modified process, the flame retardant base cloth is that cellulose fiber content is greater than 75% or a small amount of choosing of mixture in cellulose fibre
From the arrangement type inflaming retarding fabric of the reinforcing fiber of polyvinyl or terylene.
3. the preparation method of the electric-welding protective garment fabric according to claim 2 based on graphene heat dissipation, which is characterized in that
The cellulose fibre is selected from cotton fiber, hemp, flax fiber, ramee, viscose rayon, Modal fibre, tencel
Fiber and its mixture.
4. the preparation method of the electric-welding protective garment fabric according to claim 1 based on graphene heat dissipation, which is characterized in that
In modified process, the flame retardant base cloth is using inherent fire-retardant fiber or partially modified fire resistance fibre or a small amount of non-flame resistant fiber
Inflaming retarding fabric made of blended.
5. the preparation method of the electric-welding protective garment fabric according to claim 4 based on graphene heat dissipation, which is characterized in that
The inherent fire-retardant fiber is selected from aramid fiber, polyimides, poly- fragrant oxadiazoles fiber, PSA fiber, alginate fibre and its mixture；Institute
Stating modified flame-retardant fiber includes Flame Vinylon, anti-flaming viscose, flame-resistant terylene, fire-retardant polyamide fibre and flame-retardant acrylic fibre；The non-flame resistant fibre
Dimension includes polyvinyl, terylene, polyamide fibre and acrylic fibers.
6. the preparation method of the electric-welding protective garment fabric according to claim 1 based on graphene heat dissipation, which is characterized in that
In modified process, it includes the printing of full bottom, transfer, blade coating and spray that the single side, which applies,.
7. the preparation method of the electric-welding protective garment fabric according to claim 1 based on graphene heat dissipation, which is characterized in that
In modified process, the graphene oxide solution concentration is 0.5mg/ml~3mg/ml, the applied amount of graphene oxide solution
For 80-160g/m2, drying temperature is 30~45 DEG C, and drying time is 0.5~2h.
8. the preparation method of the electric-welding protective garment fabric according to claim 1 based on graphene heat dissipation, which is characterized in that
It is described to be reduced to electronation in reduction process；It is derivative that reducing agent is selected from hydrazine and its derivative, metal hydride, sulphonic acids
Object, vitamin, glucose；Reducing agent dosage be 1mg/ml~10mg/ml, the recovery time be 0.5~3h, reduction temperature be 80~
100℃。
9. a kind of electric-welding protective garment fabric based on graphene heat dissipation, preparation according to any one of claim 1 to 8
Method is made.
10. the electric-welding protective garment fabric according to claim 9 based on graphene heat dissipation, which is characterized in that the electric welding
Protective garment fabric test method according to as defined in GB/T17599 measures the heating after 15 drop molten metals drip and is no more than 37 DEG C；
Electric-welding protective garment fabric washing front and back char length≤50mm, after flame time≤2s, smoldering time≤2s, protective fabric
It is greater than 800N × 600N through latitudinal strength.
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