CN110373301A - A kind of brewing method of alcoholic strength low applejack - Google Patents
A kind of brewing method of alcoholic strength low applejack Download PDFInfo
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- 238000000034 method Methods 0.000 title claims abstract description 27
- 230000001476 alcoholic effect Effects 0.000 title claims description 6
- 235000020052 applejack Nutrition 0.000 title 1
- 235000019987 cider Nutrition 0.000 claims abstract description 77
- 241000220225 Malus Species 0.000 claims abstract description 45
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 28
- 238000005352 clarification Methods 0.000 claims abstract description 14
- 235000021016 apples Nutrition 0.000 claims abstract description 13
- 239000002253 acid Substances 0.000 claims abstract description 9
- 150000001875 compounds Chemical class 0.000 claims abstract description 8
- 235000019990 fruit wine Nutrition 0.000 claims abstract description 8
- 238000001914 filtration Methods 0.000 claims abstract description 7
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 235000010724 Wisteria floribunda Nutrition 0.000 claims abstract description 6
- 238000011514 vinification Methods 0.000 claims abstract description 5
- 238000000855 fermentation Methods 0.000 claims description 38
- 230000004151 fermentation Effects 0.000 claims description 38
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims description 32
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 24
- 235000015197 apple juice Nutrition 0.000 claims description 22
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 20
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 18
- 235000021448 clear apple juice Nutrition 0.000 claims description 16
- 229910000278 bentonite Inorganic materials 0.000 claims description 14
- 239000000440 bentonite Substances 0.000 claims description 14
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 14
- 239000002131 composite material Substances 0.000 claims description 13
- 235000014101 wine Nutrition 0.000 claims description 11
- 229920001661 Chitosan Polymers 0.000 claims description 10
- 229930006000 Sucrose Natural products 0.000 claims description 10
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 10
- 235000010323 ascorbic acid Nutrition 0.000 claims description 10
- 229960005070 ascorbic acid Drugs 0.000 claims description 10
- 239000011668 ascorbic acid Substances 0.000 claims description 10
- 235000018417 cysteine Nutrition 0.000 claims description 10
- XUJNEKJLAYXESH-UHFFFAOYSA-N cysteine Natural products SCC(N)C(O)=O XUJNEKJLAYXESH-UHFFFAOYSA-N 0.000 claims description 10
- 239000005720 sucrose Substances 0.000 claims description 10
- 239000012153 distilled water Substances 0.000 claims description 8
- RWPGFSMJFRPDDP-UHFFFAOYSA-L potassium metabisulfite Chemical compound [K+].[K+].[O-]S(=O)S([O-])(=O)=O RWPGFSMJFRPDDP-UHFFFAOYSA-L 0.000 claims description 8
- 235000010263 potassium metabisulphite Nutrition 0.000 claims description 8
- 108010059892 Cellulase Proteins 0.000 claims description 6
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- 108010059820 Polygalacturonase Proteins 0.000 claims description 6
- 229940106157 cellulase Drugs 0.000 claims description 6
- 108010093305 exopolygalacturonase Proteins 0.000 claims description 6
- 229940043349 potassium metabisulfite Drugs 0.000 claims description 6
- 238000009928 pasteurization Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 230000008859 change Effects 0.000 claims description 4
- 229960002433 cysteine Drugs 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 239000003755 preservative agent Substances 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 238000011282 treatment Methods 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- 235000013399 edible fruits Nutrition 0.000 abstract description 5
- 235000008935 nutritious Nutrition 0.000 abstract description 3
- 238000012545 processing Methods 0.000 abstract description 3
- 235000009508 confectionery Nutrition 0.000 abstract description 2
- 238000009924 canning Methods 0.000 abstract 1
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- 239000000243 solution Substances 0.000 description 15
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 14
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- 238000004519 manufacturing process Methods 0.000 description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 5
- 239000011259 mixed solution Substances 0.000 description 5
- 229910052760 oxygen Inorganic materials 0.000 description 5
- 239000001301 oxygen Substances 0.000 description 5
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 4
- 239000000796 flavoring agent Substances 0.000 description 4
- 235000019634 flavors Nutrition 0.000 description 4
- 239000011975 tartaric acid Substances 0.000 description 4
- 235000002906 tartaric acid Nutrition 0.000 description 4
- 238000013124 brewing process Methods 0.000 description 3
- 229940088598 enzyme Drugs 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000035622 drinking Effects 0.000 description 2
- 235000012041 food component Nutrition 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 235000007686 potassium Nutrition 0.000 description 2
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- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000002526 effect on cardiovascular system Effects 0.000 description 1
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- 238000006047 enzymatic hydrolysis reaction Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
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- 235000015097 nutrients Nutrition 0.000 description 1
- 235000015040 sparkling wine Nutrition 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/02—Preparation of other alcoholic beverages by fermentation
- C12G3/024—Preparation of other alcoholic beverages by fermentation of fruits other than botanical genus Vitis
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/02—Preparation of other alcoholic beverages by fermentation
- C12G3/025—Low-alcohol beverages
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
- C12H1/02—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
- C12H1/04—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material
- C12H1/0408—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material with the aid of inorganic added material
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
- C12H1/02—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
- C12H1/04—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material
- C12H1/0416—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material with the aid of organic added material
- C12H1/0424—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material with the aid of organic added material with the aid of a polymer
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- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- Genetics & Genomics (AREA)
- Wood Science & Technology (AREA)
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Abstract
本发明提供了一种低酒精度苹果酒的酿造方法,其特征在于,包括:选用富士苹果作为酿酒原料,用水清洗,晾干,去除果核,切成苹果块,将苹果块浸泡于复合护色液中5~15min,捞出,破碎机榨汁,获得100%质量浓度的苹果果浆;解,巴氏杀菌,调整总糖含量和总酸含量,发酵,得到苹果酒;进行下胶澄清处理,冷藏2‑5天后,过滤,罐装,即得低酒精度苹果酒成品。本发明酿造的苹果酒色泽浅金黄色,澄清透亮,酒体优雅柔和,果香浓郁且细腻,口感酸甜适中,清爽怡人,是一款男女老少皆宜,营养健康的果酒饮料。
The invention provides a brewing method of low-alcohol cider, which is characterized in that it comprises: selecting Fuji apples as wine-making raw materials, washing them with water, drying them in the air, removing the fruit core, cutting them into apple pieces, soaking the apple pieces in a compound protective Put it in the color liquid for 5-15 minutes, remove it, squeeze the juice with a crusher, and obtain apple pulp with a mass concentration of 100%; decompose, pasteurize, adjust the total sugar content and total acid content, and ferment to obtain cider; carry out gumming and clarification After processing, refrigerating for 2-5 days, filtering, and canning, the finished product of low-alcohol cider is obtained. The cider brewed by the invention is light golden in color, clear and translucent, elegant and soft in body, rich and delicate in fruit aroma, moderately sweet and sour in taste, refreshing and pleasant, and is a nutritious and healthy fruit wine drink suitable for all ages.
Description
技术领域technical field
本发明涉及到一种低酒精度苹果酒的酿造方法,特别是涉及到对苹果汁的护色处理、双酶联合酶解以及一种商业酵母的添加使用,属于食品酿造技术领域。The invention relates to a brewing method of low-alcohol cider, in particular to the color protection treatment of apple juice, combined enzymatic hydrolysis with double enzymes and the addition and use of a commercial yeast, belonging to the technical field of food brewing.
背景技术Background technique
我国是世界上苹果产量最多的国家,年产量约占世界苹果总产量的46%。要想综合利用苹果资源提高苹果产业经济效益,提高苹果的深加工技术就是解决问题的必由之路,其中深加工系列产品中值得大力开发的就是苹果酒。在全球范围内,苹果酒是一种产量仅次于葡萄酒的果酒,苹果酒在英、法、美、德等国家,属于大众流通产品,苹果酒口感醇厚,果香优雅,风格独特,更多的保留了苹果中的营养成分,比粮食发酵的酒更富有营养。苹果酒含有高水平的抗氧化物,具有保健功能,还可以调节人体新陈代谢、促进血液循环、助消化、软化血管、预防心血管硬化等疾病的产生。my country is the country with the largest apple production in the world, and its annual production accounts for about 46% of the world's total apple production. In order to comprehensively utilize apple resources and improve the economic benefits of the apple industry, improving the deep processing technology of apples is the only way to solve the problem. Among the deep processing products, cider is worth developing. On a global scale, cider is a kind of fruit wine whose output is second only to wine. Apple cider is a mass circulation product in countries such as Britain, France, the United States, and Germany. Apple cider has a mellow taste, elegant fruit aroma, and unique style. More The nutrient content of apples is preserved, which is more nutritious than grain fermented wine. Apple cider contains high levels of antioxidants and has health care functions. It can also regulate human metabolism, promote blood circulation, help digestion, soften blood vessels, and prevent cardiovascular sclerosis and other diseases.
常见苹果酒多为静止酒或人为起泡酒,酒精含量一般是8~12%vol,以新鲜苹果活浓缩苹果汁为原料酿造。由于苹果酒的生产流程还有很多因素影响其品质,其发酵条件直接关系到苹果酒的品质、稳定性、风味、以及贮存时间,因此为了保证苹果酒工业化的产品质量,对苹果酒酿造工艺的进一步探讨十分重要。现有苹果酒酿造技术中苹果酒酿造的周期长,苹果本身的营养成分和风味损失严重,口味不佳,香气不足的技术问题。Common cider is mostly still wine or artificial sparkling wine, the alcohol content is generally 8-12% vol, brewed with fresh apples or concentrated apple juice as raw materials. Since there are many factors in the production process of cider that affect its quality, the fermentation conditions are directly related to the quality, stability, flavor, and storage time of cider. Therefore, in order to ensure the product quality of cider industrialization, the cider brewing process It is important to explore further. In the existing cider brewing technology, the cycle of cider brewing is long, the nutritional components and flavor of the apple itself are seriously lost, the taste is not good, and the technical problems of insufficient aroma.
发明内容Contents of the invention
本发明目的是提供一种酒精度较低,适宜饮用,香气浓郁、口感良好的低酒精度苹果酒的酿造方法。The purpose of the present invention is to provide a low-alcohol cider brewing method with low alcohol content, suitable for drinking, strong aroma and good taste.
为了达到上述目的,本发明提供了一种低酒精度苹果酒的酿造方法,其特征在于,包括:In order to achieve the above object, the invention provides a brewing method of low-alcohol cider, which is characterized in that, comprising:
步骤1:选用富士苹果作为酿酒原料,用水清洗,晾干,去除果核,切成苹果块;Step 1: Select Fuji apples as raw materials for wine making, wash with water, dry, remove the core, and cut into apple pieces;
步骤2:配制复合护色液,所述的复合护色液含有抗坏血酸、半胱氨酸和焦亚硫酸钾,复合护色液中游离SO2的含量为60~80mg/L,将苹果块浸泡于复合护色液中5~15min,捞出,破碎机榨汁,不添加水,获得100%质量浓度的苹果果浆;Step 2 : Prepare a composite color protection solution, the composite color protection solution contains ascorbic acid, cysteine and potassium metabisulfite, the content of free SO2 in the composite color protection solution is 60-80mg/L, soak the apple pieces Put it in the compound color protection solution for 5-15 minutes, remove it, squeeze the juice with a crusher, without adding water, and obtain apple pulp with 100% mass concentration;
步骤3:将纤维素酶和果胶酶以1:0.9-1.1的重量比例,分别以50mg/L~60mg/L的添加量加入到步骤2所得的苹果果浆中,在50~60℃下恒温酶解0.5-1.5h,静置澄清,用纱布过滤后,用低温冷冻离心机离心5~8min,分离得到苹果清汁;Step 3: Add cellulase and pectinase to the apple pulp obtained in step 2 at a weight ratio of 1:0.9-1.1, respectively, in an amount of 50mg/L-60mg/L, and heat at 50-60°C Enzymolysis at constant temperature for 0.5-1.5h, standing for clarification, filtering with gauze, centrifuging with a low-temperature refrigerated centrifuge for 5-8min, and separating to obtain clear apple juice;
步骤4:将步骤3所得的苹果清汁进行巴氏杀菌,冷却到2-5℃;Step 4: pasteurize the clear apple juice obtained in step 3, and cool it to 2-5°C;
步骤5:在步骤4所得苹果清汁中加入蔗糖调整总糖含量,用手持折光仪测得可溶性固形物含量为18~20°Brix,加入柠檬酸,在柠檬酸的添加过程中检测苹果汁pH的变化,最终测得苹果汁pH值在3.30-3.50;Step 5: Add sucrose to the clear apple juice obtained in step 4 to adjust the total sugar content, measure the soluble solids content as 18-20°Brix with a hand-held refractometer, add citric acid, and detect the pH value of the apple juice during the addition of citric acid Change, and finally measured the pH value of apple juice at 3.30-3.50;
步骤6:将酵母用32~35℃、1.5-2.5wt%蔗糖水进行15~30min的活化,得到活化后的酵母液,将活化后的酵母液加入步骤5得到的苹果汁中,酵母的添加量为0.06~0.09g/L,将苹果汁放入生化培养箱进行发酵,当酒精度在2-8vol%,降温,冷藏,终止发酵,得到苹果酒;Step 6: Activate the yeast with 32-35°C and 1.5-2.5wt% sucrose water for 15-30 minutes to obtain the activated yeast liquid, add the activated yeast liquid to the apple juice obtained in step 5, and add the yeast The amount is 0.06-0.09g/L, put the apple juice into a biochemical incubator for fermentation, when the alcohol content is 2-8vol%, cool down, refrigerate, and stop the fermentation to obtain cider;
步骤7:将皂土和壳聚糖按照1:0.8-1.2的重量比例加入到蒸馏水中,搅拌均匀后封口,静置24~36h,将所得的混合液按照1:8-12的体积比(混合液:苹果酒)添加到步骤6所得到的苹果酒中进行下胶澄清处理,皂土和壳聚糖在苹果酒中的总添加量为0.06~1g/L,静置澄清3~5天后,过滤分离;Step 7: Add bentonite and chitosan to distilled water according to the weight ratio of 1:0.8-1.2, stir evenly, seal the seal, let stand for 24-36 hours, and mix the obtained mixture according to the volume ratio of 1:8-12 ( Mixed solution: cider) is added to the cider obtained in step 6 to carry out the clarification process under the glue, and the total amount of bentonite and chitosan in the cider is 0.06~1g/L, and after standing for clarification for 3~5 days , separated by filtration;
步骤8:将步骤7过滤分离后的苹果酒冷藏2-5天后,过滤,罐装,即得低酒精度苹果酒成品。Step 8: Refrigerate the cider filtered and separated in step 7 for 2-5 days, filter, and pack in cans to obtain a low-alcohol cider product.
优选地,所述的低酒精度苹果酒的酿造过程中无人为添加水,不添加任何的防腐剂。Preferably, no water is artificially added during the brewing process of the low-alcohol cider, and no preservatives are added.
优选地,所述的步骤6中的酵母为商业酵母:帝伯仕葡萄酒·果酒专用酵母。Preferably, the yeast in the step 6 is a commercial yeast: Diboshi wine and fruit wine special yeast.
优选地,所述的步骤7中的皂土为帝伯仕皂土。Preferably, the bentonite in the step 7 is Dibers bentonite.
优选地,所述的低酒精度苹果酒成品的酒精度为3%vol,总糖含量为16°Brix,总酸含量(以酒石酸计算)为8.0g/L。Preferably, the low-alcohol cider finished product has an alcohol content of 3% vol, a total sugar content of 16°Brix, and a total acid content (calculated as tartaric acid) of 8.0 g/L.
优选地,所述的步骤1中的苹果块的大小为3-5cm。Preferably, the size of the apple pieces in the step 1 is 3-5cm.
优选地,所述的巴氏杀菌包括将苹果清汁加热到68~70℃,保持温度25-35min。Preferably, the pasteurization includes heating the clear apple juice to 68-70° C. and keeping the temperature for 25-35 minutes.
优选地,所述的步骤6中苹果酒的酒精度在3-5vol%.Preferably, the alcohol content of the cider in the step 6 is 3-5vol%.
优选地,所述的步骤6中酵母和蔗糖水的体积比为1:8-12。Preferably, the volume ratio of yeast and sucrose water in step 6 is 1:8-12.
优选地,所述的步骤6中的发酵时间为5-10天,第二天要加入发酵助剂,发酵前期要定时倒罐,搅拌5~15min,发酵中期密闭发酵罐,酵母在缺氧、无氧的条件下进行酒精发酵。Preferably, the fermentation time in step 6 is 5-10 days, the fermentation aid should be added the next day, the tank should be poured regularly in the early stage of fermentation, and stirred for 5-15 minutes, and the fermentation tank should be closed in the middle stage of fermentation, and the yeast should be in anoxic, Alcoholic fermentation takes place in the absence of oxygen.
优选地,所述的低酒精度苹果酒的酒精度为3-5%vol,总糖含量为16-18°Brix,总酸含量(以酒石酸计算)为8.0g-10.0/L。Preferably, the low-alcohol cider has an alcohol content of 3-5% vol, a total sugar content of 16-18°Brix, and a total acid content (calculated as tartaric acid) of 8.0g-10.0/L.
优选地,所述复合护色液含有0.2-0.3wt%抗坏血酸、0.07-0.1wt%半胱氨酸和0.125-0.2wt%焦亚硫酸钾,通过将抗坏血酸、半胱氨酸和焦亚硫酸钾溶解于蒸馏水中配制得到,复合护色液中游离SO2的含量为60mg/L-80mg/L。Preferably, the composite color protecting solution contains 0.2-0.3wt% ascorbic acid, 0.07-0.1wt% cysteine and 0.125-0.2wt% potassium metabisulfite, by ascorbic acid, cysteine and potassium metabisulfite It is prepared by dissolving in distilled water, and the content of free SO2 in the composite color protection solution is 60mg/L - 80mg/L.
与现有技术相比,本发明的有益效果是:Compared with prior art, the beneficial effect of the present invention is:
1、本发明的酿造方法包括对苹果汁的护色处理,纤维素酶和果胶酶双酶联合酶解,巴氏灭菌,酒精发酵,以及使用的皂土和壳聚糖共同添加进行苹果酒的下胶澄清,最后对成品进行低温冷藏。所述的苹果酒选用100%纯新鲜富士苹果清汁,酿造过程中无人为添加水,不添加任何的防腐剂,采用本方法酿造的苹果酒酒精度仅为3%vol,总糖含量为16°Brix,总酸含量(以酒石酸计算)为8.0g/L,总二氧化硫为100mg/L(低于国家标准200mg/L),属于一款低酒度型果酒。克服了现有技术中营养成分损失、香气不足、酒体不足等缺点,而得到一种酒精度较低,适宜饮用,香气浓郁、口感良好的低酒精度苹果酒。1. The brewing method of the present invention includes color-protecting treatment of apple juice, joint enzymolysis of cellulase and pectinase, pasteurization, alcoholic fermentation, and the joint addition of bentonite and chitosan to carry out apple juice production. The gumming of the wine is clarified, and finally the finished product is refrigerated at low temperature. The cider is made of 100% pure fresh Fuji apple clear juice, no water is artificially added during the brewing process, and no preservatives are added. The cider brewed by this method has an alcohol content of only 3% vol and a total sugar content of 16° Brix, with a total acid content (calculated as tartaric acid) of 8.0g/L and a total sulfur dioxide of 100mg/L (lower than the national standard of 200mg/L), is a low-alcohol fruit wine. The disadvantages of the prior art, such as the loss of nutritional components, insufficient aroma, and insufficient wine body, are overcome, and a low-alcohol cider with low alcohol content, suitable for drinking, strong aroma and good taste is obtained.
2、本发明所用的发酵菌种为商业酵母:帝伯仕葡萄酒·果酒专用酵母。该菌种能使发酵迅速启发,并且发酵完全,对酒精的耐度高,发酵过程中需要的氮含量少,产生的挥发酸和H2S的量少,可以更好的保留水果本身含有的香气。此苹果酒不添加任何防腐剂,通过自然发酵而成。2. The fermentation strain used in the present invention is a commercial yeast: special yeast for Diboshi wine and fruit wine. This strain can make the fermentation quick and complete, with high tolerance to alcohol, less nitrogen content needed in the fermentation process, less volatile acid and H 2 S produced, and better retention of the fruit itself. aroma. This cider is naturally fermented without any preservatives.
3、本发明经过一些预实验,确定了护色液的配方。改进了传统上在榨汁后单一使用SO2护色的方法,减少了可能造成的健康危害,同时还保证了护色的效果,有效的防止了苹果汁的褐变,保证了苹果酒的颜色和品质。3. The present invention has determined the formula of the color protection solution through some preliminary experiments. Improved the traditional method of single use of SO2 color protection after juicing , reducing possible health hazards, while also ensuring the effect of color protection, effectively preventing browning of apple juice and ensuring the color of cider and quality.
4、本发明澄清上分别采用了双酶酶解以及壳聚糖、皂土两者结合的方法,酒体经发酵达到技术指标之后,低温终止发酵,得到的苹果酒香气丰富,具有苹果的独特风味,色泽金黄,澄清透亮,入口清爽,留香丰富,感官指标良好。4. The clarification of the present invention adopts the method of double-enzyme enzymolysis and the combination of chitosan and bentonite respectively. After the wine body reaches the technical index through fermentation, the fermentation is terminated at low temperature, and the obtained cider has rich aroma and has the unique flavor of apple. Flavor, golden color, clear and translucent, refreshing in the mouth, rich in fragrance, good sensory indicators.
5、本发明得到的苹果酒的酒精度较低,仅有3%vol,在甜度和酸度上都有很好的控制,酸度使酒体更加的清爽,更加活泼,糖度也成品更受消费者喜欢,扩大了消费的群众,男女老少皆宜。5. The alcohol content of the cider obtained by the present invention is low, only 3% vol, and has good control on sweetness and acidity. The acidity makes the wine body more refreshing and lively, and the sugar content is also more popular for consumption. Lovers like it, expanding the masses of consumption, suitable for both men, women and children.
6、本发明限定了发酵初始的糖度和酸度,依照本酿造方法,以酒精度为最终的发酵终止的参照标准,即使是不同批次的苹果得到的酒精度都在一定的范围内,相对而言,一致性可以得到保证。6. The present invention limits the initial sugar content and acidity of fermentation. According to the brewing method, the alcohol content is used as the reference standard for the final fermentation termination. Even if the alcohol content obtained from different batches of apples is within a certain range, it is relatively In other words, consistency can be guaranteed.
7、本发明的酿造方法科学合理,简单易重复,成品品质优良。7. The brewing method of the present invention is scientific and reasonable, simple and easy to repeat, and the quality of the finished product is excellent.
8、本发明酿造的苹果酒色泽浅金黄色,澄清透亮,酒体优雅柔和,果香浓郁且细腻,口感酸甜适中,清爽怡人,是一款男女老少皆宜,营养健康的果酒饮料。8. The cider brewed by the present invention is light golden in color, clear and translucent, elegant and soft in body, rich and delicate in fruit aroma, moderately sweet and sour in taste, refreshing and pleasant, and is a nutritious and healthy fruit wine drink suitable for all ages.
附图说明Description of drawings
图1苹果酒生产工艺流程图。Fig. 1 Flow chart of cider production process.
具体实施方式Detailed ways
下面结合具体实施例,进一步阐述本发明。应理解,这些实施例仅用于说明本发明而不用于限制本发明的范围。此外应理解,在阅读了本发明讲授的内容之后,本领域技术人员可以对本发明作各种改动或修改,这些等价形式同样落于本申请所附权利要求书所限定的范围。Below in conjunction with specific embodiment, further illustrate the present invention. It should be understood that these examples are only used to illustrate the present invention and are not intended to limit the scope of the present invention. In addition, it should be understood that after reading the teachings of the present invention, those skilled in the art can make various changes or modifications to the present invention, and these equivalent forms also fall within the scope defined by the appended claims of the present application.
以下实施例中所用到的各原料均为市售产品。其中,帝伯仕酵母为帝伯仕葡萄酒·果酒专用酵母。纤维素酶(烟台帝伯仕自酿机有限公司,EC3.2.1.15,>22500AJDU/g)。果胶酶(烟台帝伯仕自酿机有限公司,CE3.2.1.89,>90000mSU/g)。All raw materials used in the following examples are commercially available products. Among them, Diboshi yeast is a special yeast for Diboshi wine and fruit wine. Cellulase (Yantai Diboshi Brewing Machine Co., Ltd., EC3.2.1.15, >22500AJDU/g). Pectinase (Yantai Diboshi Brewing Machine Co., Ltd., CE3.2.1.89, >90000mSU/g).
实施例1:Example 1:
一种低酒精度苹果酒的酿造方法,所述的苹果酒成品酒精度为3%vol,总糖含量为16°Brix,总酸含量(以酒石酸计算)为8.0g/L,总二氧化硫为100mg/L(低于国家标准200mg/L)。A method for brewing low-alcohol cider, the finished cider has an alcohol content of 3%vol, a total sugar content of 16°Brix, a total acid content (calculated as tartaric acid) of 8.0g/L, and a total sulfur dioxide of 100mg /L (lower than the national standard 200mg/L).
上述低酒精度苹果酒的酿造方法,如图1所示,包括如下步骤:The brewing method of above-mentioned low-alcohol cider, as shown in Figure 1, comprises the steps:
步骤一:选用新鲜、无污染、无损伤、成熟优质的富士苹果作为酿酒原料,将选好的苹果用清水清洗干净,晾干,去除果核,带皮,将苹果切成3cm大的苹果块。Step 1: Select fresh, non-polluted, non-damaged, mature and high-quality Fuji apples as raw materials for wine making, wash the selected apples with clean water, dry them, remove the core, remove the skin, and cut the apples into 3cm-large apple pieces .
步骤二:配制复合护色液,所述的复合护色液含有0.2wt%抗坏血酸、0.07wt%半胱氨酸和0.125wt%焦亚硫酸钾,通过将抗坏血酸、半胱氨酸和焦亚硫酸钾溶解于蒸馏水中配制得到,复合护色液中游离SO2的含量为60mg/L,将苹果块浸泡于复合护色液中15min,捞出,破碎机榨汁,不添加水,获得100%质量浓度的苹果果浆。Step 2: prepare compound color-protecting solution, described compound color-protecting solution contains 0.2wt% ascorbic acid, 0.07wt% cysteine and 0.125wt% potassium pyrosulfite, by ascorbic acid, cysteine and pyrosulfite Prepared by dissolving potassium in distilled water. The content of free SO2 in the composite color protection solution is 60mg/L. Soak the apple pieces in the composite color protection solution for 15 minutes, remove them, squeeze the juice with a crusher, and obtain 100% without adding water. Mass concentration of apple pulp.
步骤三:经过试验,选择双酶酶解来提高出汁率,通过澄清度的比较,将纤维素酶和果胶酶以1:1的重量比例,分别以50mg/L的添加量加入到步骤二所得的苹果果浆中,置于恒温水浴锅中在55℃下恒温酶解1h,静置澄清,用四层纱布过滤后,用低温冷冻离心机4℃离心8min,分离得到的苹果清汁,颜色浅黄,澄清无杂质。Step 3: After testing, choose dual-enzyme hydrolysis to increase the juice yield. Through the comparison of clarity, add cellulase and pectinase in the weight ratio of 1:1, and add 50mg/L to step 2 respectively. Put the obtained apple pulp in a constant temperature water bath at 55°C for 1 hour, let it stand for clarification, filter it with four layers of gauze, and centrifuge it with a low-temperature refrigerated centrifuge at 4°C for 8 minutes to separate the clear apple juice. Light yellow, clear without impurities.
步骤四:将步骤三得到的苹果清汁进行巴氏杀菌,所述的巴氏杀菌为:将苹果清汁加热到70℃,保持温度30min;急速冷却到2℃。最大限度的使苹果清汁的色、香、味及营养成分免受高温长时间处理的破坏。Step 4: Pasteurize the clear apple juice obtained in Step 3. The pasteurization is as follows: heating the clear apple juice to 70° C. and keeping the temperature for 30 minutes; rapidly cooling to 2° C. Maximize the color, aroma, taste and nutrients of apple juice from being damaged by high temperature and long-term treatment.
步骤五:在步骤四所得苹果清汁中加入蔗糖调整总糖含量,用手持折光仪测得可溶性固形物含量为20°Brix。糖度确定好以后在此基础上加入柠檬酸调整总酸含量,在柠檬酸的添加过程中检测苹果汁pH的变化,最终测得苹果汁pH值在3.40,进而保证苹果酒的发酵基质环境。Step 5: Add sucrose to the clear apple juice obtained in Step 4 to adjust the total sugar content, and measure the soluble solids content to be 20°Brix with a hand-held refractometer. After the sugar content is determined, citric acid is added on this basis to adjust the total acid content, and the pH change of the apple juice is detected during the addition of citric acid. Finally, the pH value of the apple juice is measured at 3.40, thereby ensuring the fermentation substrate environment of the cider.
步骤六:将帝伯仕酵母用10倍体积的35℃、2wt%蔗糖水进行20min的活化,再将活化后的酵母液按比例加入步骤五得到的苹果汁,帝伯仕酵母(干酵母)的添加量为0.08g/L。苹果汁放入22℃的生化培养箱开始为期7天的发酵,第二天要加入10wt%帝伯仕发酵助剂。发酵前期(第1天到第3天)要每隔4h倒罐一次,搅拌10min,提供酵母生长繁殖所需充足的氧气,发酵中期(第4天到第5天)密闭发酵罐,酵母在缺氧、无氧的条件下进行酒精发酵。发酵后期(第6天到第7天),当酒精度在3%vol,降温至0℃,4℃低温冷藏,终止发酵,得到苹果酒。Step 6: Use 10 times the volume of 35°C, 2wt% sucrose water to activate Diboshi yeast for 20 minutes, and then add the activated yeast liquid to the apple juice obtained in Step 5 in proportion, Diboshi yeast (dry yeast) The amount added is 0.08g/L. The apple juice is put into a biochemical incubator at 22° C. to start fermentation for 7 days, and 10 wt % Diboshi fermentation aid will be added the next day. In the early stage of fermentation (from day 1 to day 3), the tank should be poured every 4 hours and stirred for 10 minutes to provide sufficient oxygen for the growth and reproduction of the yeast. Alcoholic fermentation is carried out under oxygen and anaerobic conditions. In the later stage of fermentation (6th day to 7th day), when the alcohol content is 3% vol, the temperature is lowered to 0° C., and the fermentation is terminated at 4° C. to obtain cider.
步骤七:将帝伯仕皂土和壳聚糖按照1:1的重量比例加入到蒸馏水中,搅拌均匀后封口,静置24h。将所得混合液按照1:10的体积比(混合液:苹果酒)添加到步骤六所得到的苹果酒中进行下胶澄清处理,皂土和壳聚糖在苹果酒中的总添加量为1.0g/L,静置澄清5天后,过滤分离。Step 7: Add Diboshi bentonite and chitosan into distilled water in a weight ratio of 1:1, stir evenly, seal, and let stand for 24 hours. The resulting mixed solution is added to the cider obtained in step 6 according to a volume ratio of 1:10 (mixed solution: cider) to carry out gumming and clarification treatment, and the total amount of bentonite and chitosan in the cider is 1.0 g/L, after standing for clarification for 5 days, filter and separate.
步骤八:将步骤七过滤分离后的苹果酒2-4℃冷藏5天后,过滤,罐装,即得低酒精度苹果酒成品。Step 8: Refrigerate the cider obtained by filtering and separating in step 7 at 2-4°C for 5 days, filter, and pack in cans to obtain a low-alcohol cider product.
本实施例产品的感官评定平均得分为96分(满分100分)。参照表1中详细的苹果酒的感官评分标准,邀请了30名男女各半,经过感官评价专业知识培训的群众来进行打分,其中处在小孩,青年,中年三个年龄阶段的群众各10人。本实施例的感官评价具有一定的依据性。The average sensory evaluation score of the product of this embodiment is 96 points (out of 100 points). Referring to the detailed sensory evaluation criteria for cider in Table 1, 30 people, half male and half male, who have been trained in sensory evaluation expertise were invited to score the scores. people. The sensory evaluation of this embodiment has certain basis.
实施例2Example 2
一种低酒精度苹果酒的酿造方法,具体步骤为:A kind of brewing method of low-alcohol cider, concrete steps are:
步骤一:选用新鲜、无污染、无损伤、成熟优质的富士苹果作为酿酒原料,将选好的苹果用清水清洗干净,晾干,去除果核,带皮,将苹果切成5cm大的苹果块。Step 1: Select fresh, non-polluted, non-damaged, mature and high-quality Fuji apples as raw materials for wine making, wash the selected apples with clean water, dry them, remove the core, remove the skin, and cut the apples into 5cm-large apple pieces .
步骤二:配制复合护色液,所述的复合护色液含有0.2wt%抗坏血酸、0.07wt%半胱氨酸和0.125wt%焦亚硫酸钾,通过将抗坏血酸、半胱氨酸和焦亚硫酸钾溶解于蒸馏水中配制得到,复合护色液中游离SO2的含量为60mg/L,将苹果块浸泡于复合护色液中15min,捞出,破碎机榨汁,不添加水,获得100%质量浓度的苹果果浆。Step 2: prepare compound color-protecting solution, described compound color-protecting solution contains 0.2wt% ascorbic acid, 0.07wt% cysteine and 0.125wt% potassium pyrosulfite, by ascorbic acid, cysteine and pyrosulfite Prepared by dissolving potassium in distilled water. The content of free SO2 in the composite color protection solution is 60mg/L. Soak the apple pieces in the composite color protection solution for 15 minutes, remove them, squeeze the juice with a crusher, and obtain 100% without adding water. Mass concentration of apple pulp.
步骤三:将50mg/L纤维素酶和60mg/L果胶酶加入到步骤二所得的苹果果浆中,置于恒温水浴锅中在60℃下恒温酶解1h,静置澄清,用四层纱布过滤后,用低温冷冻离心机4℃离心8min,分离得到的苹果清汁,颜色浅黄,澄清无杂质。Step 3: Add 50mg/L cellulase and 60mg/L pectinase to the apple pulp obtained in Step 2, place it in a constant temperature water bath at 60°C for 1 hour, let it stand for clarification, and use four layers of After filtering with gauze, use a low-temperature refrigerated centrifuge to centrifuge at 4°C for 8 minutes to separate the clear apple juice, which is light yellow in color and clear without impurities.
步骤四:将步骤三得到的苹果清汁进行巴氏杀菌,所述的巴氏杀菌为:将苹果清汁加热到70℃,保持温度30min;急速冷却到4℃。Step 4: Pasteurize the clear apple juice obtained in Step 3. The pasteurization is as follows: heating the clear apple juice to 70° C. and keeping the temperature for 30 minutes; rapidly cooling to 4° C.
步骤五:在步骤四所得苹果清汁中加入蔗糖调整总糖含量,用手持折光仪测得可溶性固形物含量为20°Brix。糖度确定好以后在此基础上加入柠檬酸调整总酸含量,在柠檬酸的添加过程中检测苹果汁pH的变化,最终测得苹果汁pH值在3.40,进而保证苹果酒的发酵基质环境。Step 5: Add sucrose to the clear apple juice obtained in Step 4 to adjust the total sugar content, and measure the soluble solids content to be 20°Brix with a hand-held refractometer. After the sugar content is determined, citric acid is added on this basis to adjust the total acid content, and the pH change of the apple juice is detected during the addition of citric acid. Finally, the pH value of the apple juice is measured at 3.40, thereby ensuring the fermentation substrate environment of the cider.
步骤六:将帝伯仕酵母用10倍体积的35℃、2wt%蔗糖水进20min的活化,再将活化后的酵母液按比例加入步骤五得到的苹果汁,帝伯仕酵母(干酵母)的添加量为0.09g/L。苹果汁放入22℃的生化培养箱开始为期7天的发酵,第二天要加入10wt%帝伯仕发酵助剂。发酵前期(第1天到第3天)要每隔4h倒罐一次,搅拌10min,提供酵母生长繁殖所需充足的氧气,发酵中期(第4天到第5天)密闭发酵罐,酵母在缺氧、无氧的条件下进行酒精发酵。发酵后期(第6天到第7天),当酒精度在3%vol,降温至0℃,4℃低温冷藏,终止发酵,得到苹果酒。Step 6: Use 10 times the volume of 35°C, 2wt% sucrose water to activate Diboshi yeast for 20 minutes, and then add the activated yeast liquid in proportion to the apple juice obtained in Step 5, Diboshi yeast (dry yeast) The amount added is 0.09g/L. The apple juice is put into a biochemical incubator at 22° C. to start fermentation for 7 days, and 10 wt % Diboshi fermentation aid will be added the next day. In the early stage of fermentation (from day 1 to day 3), the tank should be poured every 4 hours and stirred for 10 minutes to provide sufficient oxygen for the growth and reproduction of the yeast. Alcoholic fermentation is carried out under oxygen and anaerobic conditions. In the later stage of fermentation (6th day to 7th day), when the alcohol content is 3% vol, the temperature is lowered to 0° C., and the fermentation is terminated at 4° C. to obtain cider.
步骤七:将帝伯仕皂土和壳聚糖按照1:1.2的重量比例加入到蒸馏水中,搅拌均匀后封口,静置36h。将所得混合液按照1:10的体积比(混合液:苹果酒)添加到步骤六所得到的苹果酒中进行下胶澄清处理,皂土和壳聚糖在苹果酒中的总添加量为0.1g/L,静置澄清5天后,过滤分离。Step 7: Add Diboshi bentonite and chitosan into distilled water at a weight ratio of 1:1.2, stir evenly, seal, and let stand for 36 hours. The resulting mixed solution is added to the cider obtained in step 6 according to a volume ratio of 1:10 (mixed solution: apple cider) to carry out the clarification process, and the total amount of bentonite and chitosan in the cider is 0.1 g/L, after standing for clarification for 5 days, filter and separate.
步骤八:将步骤七过滤分离后的苹果酒4℃冷藏3天后,过滤,罐装,即得低酒精度苹果酒成品。Step 8: Refrigerate the cider separated by filtration in Step 7 at 4°C for 3 days, filter, and pack in cans to obtain a low-alcohol cider product.
本实施例产品的感官评定平均得分为96分(满分100分)。参照表1中详细的苹果酒的感官评分标准,邀请了30名男女各半,经过感官评价专业知识培训的群众来进行打分,其中处在小孩,青年,中年三个年龄阶段的群众各10人。本实施例的感官评价具有一定的依据性。The average sensory evaluation score of the product of this embodiment is 96 points (out of 100 points). Referring to the detailed sensory evaluation criteria for cider in Table 1, 30 people, half male and half male, who have been trained in sensory evaluation expertise were invited to score the scores. people. The sensory evaluation of this embodiment has certain basis.
表1苹果酒感官评分表:Table 1 Apple cider sensory evaluation table:
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