CN110326628A - Improving tobacco incense tolerance improves aroma quality preparation and makes and uses - Google Patents
Improving tobacco incense tolerance improves aroma quality preparation and makes and uses Download PDFInfo
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/34—Rosaceae [Rose family], e.g. strawberry, hawthorn, plum, cherry, peach, apricot or almond
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Abstract
The present invention provides a kind of raising tobacco incense tolerance to improve aroma quality preparation and preparation and application.It fresh in full bloom remove the yulan magnolia petal juice after anthocaulus using manually squeezing, remove the rose petal juice after anthocaulus, auxiliary agent calcium carbonate nano material, it is stirred according to 30~50:30 of mass ratio~50:1~15 ratio, 45~90d after cigarette strain transplanting, with 300~1000g/666.7m2Usage amount is added in 30~45kg clean water and is mixed evenly, and carries out foliage-spray when selecting fine day, cloudy day without rain or rain rear blade without dew after the morning 10~12 point perhaps at 4 points in afternoon.Tobacco Glandular Trichome secretion content can be improved in preparation of the invention, increases cured tobacco leaf fragrance object total amount, improves the aroma quality of tobacco leaf, and then improve quality of tobacco.
Description
Technical field:
The invention belongs to tobacco cultivation technical field of cultivation, and in particular to be in the existing tobacco cultivation in China and harvesting
Under baking technology and installations and facilities, based on promoting tobacco leaf glandular secretion object amount to realize, baking tobacco leaves increase perfume quantity and improve aroma quality
Theory, a kind of used raising tabacco fragrance object content improves tobacco aroma quality preparation and its preparation and application.
Background technique:
Tobacco is one of most important industrial crops in current China's agricultural production, to our socio-economic development and country
Tax revenue has important influence.Due to the genetic difference of different tobacco breds, ecological environmental condition in leaf tobacco production
The difference of (soil, illumination, temperature, humidity, height above sea level, topography and geomorphology), cultivation technique measure (fertilising, topping, water management, disease
Pest control measure) it is different with roasting technology is adopted, it is variant that Tobacco Glandular Trichome secretes object amount, and then influences tabacco fragrance object content and perfume (or spice)
Makings, leads to toast that later quality of tobacco is variant, to influence utilization of the cigarette industry to high-grade raw tobacco material.
Under kind, plant cigarette district domain ecological environmental condition unanimous circumstances, the perfume quantity of tobacco leaf how is improved, fragrance is improved
Matter? it produces at present and goes up an effective simple measures not yet, often through water and fertilizer management, disease pest in prior art measure
Evil prevention and treatment is suitable for adopting roasting technology and technique etc., to improve the perfume quantity for drying cured tobacco leaf, improves aroma quality, but existing research
Show that these measures are difficult to obtain ideal effect.Based on this, the present invention is by the way that in production, foliage-spray is added with nano-calcium carbonate
Pure plant yulan magnolia and the rose-juice liquor of calcium experiments have shown that: the present invention has effect good, and raw material sources are extensive,
It is low in cost, it is easy to the advantages that preparing with using.
Summary of the invention:
The purpose of the present invention is to provide a kind of improvement of raising tabacco fragrance object content tobacco aroma quality preparation, Yi Jiqi
Preparation method and application method, effectively solve China's leaf tobacco production in because kind gene, ecological environmental condition (soil,
Illumination, temperature, humidity, height above sea level, topography and geomorphology), cultivation technique measure (fertilising, topping, water management, pest control measure)
With adopt toasted caused by roasting technical measures etc. after tobacco incense tolerance is low, aroma quality is poor etc. influences the problem of tobacco leaf industrial applicability.
A kind of raising tabacco fragrance object content of the invention improves tobacco aroma quality preparation, by natural fresh go anthocaulus with
Yulan magnolia petal and rose petal juicing filtrate and auxiliary agent nanometer calcium carbonate afterwards, it is mixed to be made.
The raising tabacco fragrance object content improves tobacco aroma quality preparation, be bloomed by natural fresh go anthocaulus
Yulan magnolia petal and rose petal juicing filtrate and auxiliary agent nanometer calcium carbonate, according to 30~50:30 of mass ratio~50:1-15
Ratio be stirred.It is preferred that the yulan magnolia petal for going anthocaulus later and the juicing of rose petal that the natural fresh squeezed is in full bloom
Filtrate and auxiliary agent nanometer calcium carbonate are stirred mixed according to the ratio of mass ratio 45:50:5 with the clean water that 35kg is added in container
Solution after closing uniformly to obtain the final product.The raising tabacco fragrance object content improves tobacco aroma quality preparation, the juicing filter of yulan flower
Liquid hold-up >=98%, rose flower juicing filtrate content >=98%, auxiliary agent calcium carbonate nano material content >=98%.
Invention also provides the above-mentioned tabacco fragrance object contents that improves to improve the preparation method of tobacco aroma quality preparation:
First by the fresh yulan magnolia for going anthocaulus and rose petal in full bloom, using the broken machine (Shandong of the Chinese herbal ultra-fine powder with Cryo Equipment
Jinan City, province Jinan sky special equipment Co., Ltd, 8L/1.1KW/380V.50HZ) mashing, then with bilayer medical cotton gauze pressure
Tight filtering is placed in container, and juicing filtrate refrigerates spare under 5~15 DEG C of environment.Then by yulan magnolia petal and rose petal
Juice and auxiliary agent nanometer calcium carbonate, according to the ratio of mass ratio 45:50:5, mixing is added to the container, and the clean water of 35kg is added
Solution after being uniformly mixed is used for crop field cigarette strain foliage-spray.
Preferential application method is that the raising tabacco fragrance object content is improved tobacco aroma quality preparation to add water complete
It is used after being dissolved into 10.0%~15.0% aqueous solution.The raising tabacco fragrance object content is most preferably improved into tobacco incense
Makings preparation uses after adding water to be completely dissolved into 12.5% aqueous solution.With 300~1000g/666.7m2 usage amount, for moving
The tobacco leaf of 45~90d after cultivation, progress foliage-spray is primary, can spray repeatedly.According to existing picking and roasting skill after tobacco leaf is mature
Art measure and technique carry out the baking of tobacco leaf.
In the preferred technical solution of the present invention:
According to reasonable yulan magnolia and rose petal juicing filtrate and the configuration proportion of auxiliary agent nanometer calcium carbonate, mixing
When accomplish to be used while allocating；Unspent juicing filtrate refrigerates spare under 5~15 DEG C of environment.
1. in order to improve the effect used, in the aqueous solution being prepared into, the calcium dodecyl benzene sulfonate of addition, additive amount
For 5g or so/40kg aqueous solution, then to stir, it can not be excessive.
2. field is using foliage-spray is carried out, to select at fine day, cloudy day without rain or rain rear blade without dew, the morning
It is carried out after 10-12 point or at 4 points in afternoon, the front and back of blade is intended to spray application to, such better effect.
3. 45~90d after transplanting is in use, the time interval that can be used for multiple times, but use will be more than 7-10d.
Tobacco Glandular Trichome secretion content can be improved in the present invention.After transplanting 60d, measurement Hunan cigarette No. 4 and Hunan cigarette 5 is roasting
Its middle leaf glandular hairs of tobacco kind point must object Contents of Main Components.Wherein: toluene, butylated hydroxytoluene, decane, dodecane, ten
Four alkane, eicosane, heptacosane, octacosane, nonacosane, hentriacontane, nicotine, octahydro -1 1,2,3,5,6,7,8,8a-,
8a- dimethyl-7- (1- methyl ethylene)-naphthalene, 1,3,5- trioxane, 2- methyl-1-nonene-3- alkynes, 2,2- neopentanoic acid,
4- hexadecane ester and other unknown materials etc. are above control, mentioned component compared with the control, improve ratio 1.08%~
In 8.48% (Hunan cigarette 4) and 5.58%~9.05% (Hunan cigarette 5) amplitude range.
B2F and C3F tobacco leaf can be respectively increased in the present invention, in which: 11.0~11.6% He of ligroin extraction total content
12.0~15.7%, carotenoid aroma substance total content 15.4~16.8% and 15.10~17.1%, catabolite always contains
Amount 18.3~20.1% and 4.6~18.5%, solanone total content 19.3~19.5% and 15.4~18.1%, non-enzymatic milkproduct are anti-
Answer product total content 20.6~23.1% and 17.3~21.2%, aromatic amino acid pyrolysis product total content 21.0~24.8%
With 18.4~21.5%, neophytadiene total content 51.5~54.9% and 41.2~48.5%, Neutral Aroma Constituents total amount 44.7
~46.2% and 43.8~47.9%.
The features of the present invention mainly has:
Vitamin, amino acid and various trace elements rich in the juicing of natural fresh yulan magnolia, yulan magnolia contain
Volatile oil, wherein predominantly citral, cloves oleic acid etc. and magnoflorine, alkaloid, Magnolin, capric acid, rutin, oil
The ingredients such as acid, vitamin A, contain 300 various chemical components in rose, such as alcohol of fragrance, aldehyde, fatty acid, phenol and contain essence
Oil and rouge；Rose (attar of rose) containing volatile oil, predominantly citronellol, nerol, Eugenol, benzyl carbinol, nonyl alcohol, benzene first
The ingredients such as alcohol, linalool, phenethyl acetate and quercitrin, amaroid, tannin, gallic acid, carrotene, haematochrome.On
The fresh petal squeezeding juice contained substance for going anthocaulus and anthocyanidin are stated, is both to promote tobacco leaf and grown with glandular hairs, improves glandular hairs point
Must object amount nutrients and Auto-regulator, and be the nutrients of tabacco fragrance precursor carotenoid, these substances pass through cigarette
Leaf is absorbed and utilized, and can increase tabacco fragrance content of material after baking, improves aroma quality, improves the quality of tobacco leaf；Nano-calcium carbonate
For calcium as a kind of carrier auxiliary agent, main function is to increase suction of the tobacco leaf to yulan and rose juice effective component as diffusant
It receives, followed by plays protective effect, and calcium nutrition enhancing tobacco plant resistance and disease-resistant pest-resistant performance are provided.
Advantage of the invention:
1. it is easy to draw materials and process, it is low in cost.Yulan (Magnolia denudata Desr.) Magnoliaceae fallen leaves are tall
Wood, alias Flos micheliae Albae hope spring, yulan magnolia.Now there is cultivation in middle part each province native to China on the south Beijing and Yellow River basin；Wood
There are plantation in orchid family subgenus Yulania, deciduous tree, all parts of the country, and the yulan each province that especially south is grown in flakes has, every year
Mid-March start to bloom, be continued until June, the florescence 2~3 months；It is bright-coloured that yulan flower is very large, gives off a strong fragrance, and is both
Preferable garden plants are also important fragrance and extract raw material.Yulan magnolia vitamin rich in, amino acid and a variety of
Microelement, yulan magnolia contain volatile oil, wherein predominantly citral, cloves oleic acid etc. and magnoflorine, alkaloid, prestige
The ingredients such as vernalin, capric acid, rutin, oleic acid, vitamin A, contain 300 various chemical components in rose, such as alcohol of fragrance,
Aldehyde, fatty acid, phenol and oil and rouge containing essence have certain medical value.
Rose (scientific name: Rosa rugosa) is rosaceae rose, and it is China that rose, which originates in, and rose belongs to fallen leaves and fills
Wood, branch bar spininess thorn, imparipinnate leaf, 5~9, leaflet, ellipse has side thorn.Petal obovate, polyphyll to half polyphyll,
Flower has an aubergine, white, 8~September of fruiting period, oblate spheroid, branch more it is weak it is soft hang down and how close thorn, the annual florescence only once,
Florescence is longer, and there are cultivation in China various regions；Rose (attar of rose) containing volatile oil, predominantly citronellol, nerol, caryophyllus oil
Phenol, benzyl carbinol, nonyl alcohol, benzyl alcohol, linalool, phenethyl acetate and quercitrin, amaroid, tannin, gallic acid, Hu Luo
The ingredients such as Bu Su, haematochrome.
Yulan magnolia and rose is wild and plantation at this stage, from a wealth of sources, raw material is sufficient, materials convenience.For shredding flower
The orchard shears of valve have sale in flowers market, and 8L/1.1KW/380V.50HZ beater is special by the Jinan City, Shandong Province Jinan sky
It is produced with equipment Co., Ltd, the similar producer in the whole nation has tens.
Yulan magnolia and rose source are wide, it is only necessary to certain artificial picking is processed and both be can get, manually, water power etc. at
This, overall cost is lower than 10 yuan per acre.Auxiliary agent nm-class active calcium carbonate, which is easy to chemical products at home, to be purchased in the market and arrives, city
800 yuan/T of unit price on field or so.
2. formula is unique.The alcohol of yulan magnolia vitamin rich in, amino acid and various trace elements and fragrance,
300 multiple compounds such as aldehyde, fatty acid, phenol and oil containing essence and rouge；Ethereal oil in yulan magnolia, predominantly citral,
The ingredients such as cloves oleic acid and magnoflorine, alkaloid, Magnolin, capric acid, rutin, oleic acid, vitamin A；Rose, which contains, to be waved
Hair oil (attar of rose), predominantly citronellol, nerol, Eugenol, benzyl carbinol, nonyl alcohol, benzyl alcohol, linalool, acetic acid benzene second
The ingredients such as ester and quercitrin, amaroid, tannin, gallic acid, carrotene, haematochrome；In yulan magnolia and rose juicing
Amino acid, alkaloid and the vitamin contained is the bioactive substance of tobacco growing development, there is promotion growth and Tobacco Glandular Trichome
The functions such as secretion generation, Trichome exudates are the vitals for improving tabacco fragrance object content and improving aroma quality.Two kinds of flowers
Anthocyanidin in juicing, is absorbed by tobacco leaf, to tobacco leaf pigment content is improved, there is certain effect effect, and in tobacco leaf pigment
Carotenoid is the precursor of fragrance object.Nanometer calcium carbonate is conducive to improve tobacco leaf to calcium Nutrient Absorption, and calcium is carbon water
The instrumentality of transport compounds is improved the disease resistance of tobacco leaf and the absorption of other substances；Meanwhile nanometer calcium carbonate foliage-spray
Be equivalent to play and diffusant and be stained with agent function, be conducive to the diffusion of the Related Component in mixed liquor and be stained with and absorb, this with
The method and principle that related flavoring substances are added in forefathers' invention have difference substantially.
3. preparation method is easy, it is easy to grasp.As long as yulan magnolia petal and rose petal juicing filtrate and auxiliary agent are received
Rice calcium carbonate, mixes according to certain mass ratio, is placed in plastics, in the container that wooden or clay is fired, is subject to certain mass
Clean water stir.
Specific embodiment:
It is intended to further illustrate the present invention with reference to embodiments, is not intended to limit the present invention.
Embodiment 1:
Improving tobacco incense tolerance improves the preparation of aroma quality preparation:
Improving tobacco incense tolerance improves the preparation method of aroma quality preparation: first in full bloom removing anthocaulus yulan magnolia and rose for fresh
Rare petal is beaten using the broken machine of the Chinese herbal ultra-fine powder with Cryo Equipment, then is compressed filtering with the double-deck medical cotton gauze and be placed in appearance
In device, juicing filtrate refrigerates spare under 5~15 DEG C of environment.Then it by yulan magnolia petal juice and rose petal juice and helps
Agent nanometer calcium carbonate, according to the ratio of mass ratio 45:50:5, mixing is added to the container, and using clean water, it is molten to be configured to 12.5%
Liquid, 45~90d after transplanting, with 300~1000g/666.7m2Usage amount carries out foliage-spray；Repeatedly spray, spray when
Between between be divided into 7d.
2016, for trying flue-cured tobacco cultivars Hunan cigarette 4, spray and not spraying and (compare) two comparative tests handled,
Wherein: processing 1: 45~90d after transplanting using 5000g object+40kg clean water of the present invention, is configured to 12.5% solution, into
Row foliage-spray；Handle 2 (controls): the fresh water spraying of phase homogenous quantities.1. middle part Tobacco Glandular Trichome point must the main type and content of object
Measurement
1.1 tobacco leaf glandular hairs point must object extraction: the 60d after flue-cured tobacco transplanting selects the morning 9 of the fine day blade without dew
~11 points, each processing chooses representational 5 plants of cigarette strain, and every plant takes its maximum leaf blade, is put into the foam thermal insulation with ice cube
Laboratory is taken back in case, as unit of processing, is respectively soaked the methylene chloride that 1000mL is put into per a piece of blade of each processing
It washes, with 2 1000mL graduated cylinders, each graduated cylinder pours into the methylene chloride of 450mL, and every leaf embathes 4 times in first graduated cylinder,
Soaking time is 2S/ time, and above-mentioned process is repeated in two, ground graduated cylinder, then by containing blade face divide must the solvent filter of object pour into
In the beaker of 1L, 50g anhydrous sodium sulfate analytical reagents is uniformly placed on filter paper when filtering, graduated cylinder and filter paper use remainder
100mL tetrachloromethane rinse net, leaching liquor is placed on rotary evaporator under the conditions of 40 DEG C and 0.06MPa and is concentrated to 1~
1.5mL, finally move into 5mL volumetric flask in carry out constant volume, be then placed in black paper wrapper it is spare in 0 DEG C of refrigerating box, it is above-mentioned
Method is referring to (Han Jinfeng wait .1995, Chinese tobacco) such as Han Jinfeng.
1.2 tobacco leaf glandular hairs point must object qualitative, quantitative measurement: it is internal standard that 10 μ L methyl phenylacetates, which are added, in each sample,
(chromatographic column: DB-5MS (30m × 0.25mm.i.d. × 0.25 μm d.f) is measured using internal standard method CG/MS sample introduction qualitative, quantitative；It carries
Gas and flow velocity: He 0.8mL/min；Transmission line temperature: 280 DEG C；Temperature program: 50 DEG C of 12 DEG C/min → 180 DEG C (2min)
(2min)4℃/min→210℃(5min)3℃/min→240℃(30min)；Ionization energy 70eV；250 DEG C of injector temperature；Into
2 μ L of sample amount；Split ratio 1: 10；35~500amu of mass number range).Treated sample by CG/MS qualification result and
NIST02 library searching is qualitative, uses the ingredient and content of efficient gas phase hplc determination Trichome exudates.
2. major grades tobacco leaf key odorant object total amount tests and analyzes detection after roasting
When maturation adopts roasting, each processing is taken singly to adopt and singly be baked, and is classified after roasting, takes two grade tobacco leaf samples of B2F and C3F
Each 0.5kg of product, the analysis detection for carrying out key odorant object total amount (are used using phenethyl acetate as internal standard, with gas-chromatography-matter
Spectrum/Salbutamol Selected Ion Monitoring (GC-MS/SIM) carries out fragrance species qualitative, quantitative and measures total amount), referring to Li Ling swallow and Zhou Jiheng
Deng (Li Ling swallow, waits Chinese Tobacco Science, and 2015；Zhou Jiheng, waits Agricultural University Of Hunan journal, 2005) method is detected.
As known from Table 1, after present invention processing, B2F tobacco leaf key odorant object ligroin extraction total content, carotenoids
Plain aroma substance total content, catabolite total content, solanone total content, non enzymatic browning reacton product total content, aromatic amine
Base acid cleavage product total content, neophytadiene total content and Neutral Aroma Constituents total amount, processing 1 are successively higher than 2 (controls) of processing
0.86%, 3.80 μ g/g, 14.8 μ g/g, 12.0 μ g/g, 11.90 μ g/g, 7.40 μ g/g, 429.0 μ g/g, 446.2 μ g/g.
C3F tobacco leaf key odorant object ligroin extraction total content, carotenoid aroma substance total content, catabolite
Total content, solanone total content, non enzymatic browning reacton product total content, aromatic amino acid pyrolysis product total content, planting two
Alkene total content and Neutral Aroma Constituents total amount, processing 1 than handle 2 (controls) successively high 1.32%, 4.40 μ g/g, 14.9 μ g/g,
10.5μg/g、11.8μg/g、7.00μg/g、429.6μg/g、491.1μg/g。
It is relatively learnt from the fragrance object total content of tobacco leaf major grades, the tobacco leaf handled using object of the present invention, perfume quantity
It is able to larger raising, aroma quality has obtained preferable improvement.
No. 4 B2F and C3F tobacco leaf ligroin extractions of 1 different disposal Hunan cigarette of table, carotenoid fragrance object and degradation produce
Object, solanone, non enzymatic browning reacton product, aromatic amino acid pyrolysis product, Neutral Aroma Constituents total amount
As known from Table 2, mainly divide must object amount for the glandular hairs of the maximum tobacco leaves of the Hunan 90d cigarette 4 after transplanting, in which: toluene, butylation
Hydroxy-methylbenzene, decane, dodecane, the tetradecane, eicosane, heptacosane, octacosane, nonacosane, hentriacontane, nicotine,
1,2,3,5,6,7,8,8a- octahydro-1,8a- dimethyl-7- (1- methyl ethylene)-naphthalene, 1,3,5- trioxane, 2- methyl-1-
Nonene -3- alkynes, 2,2-Dimethylpropionic acid, 4- hexadecane ester and other unknown materials etc. are above control, improve ratio 1.08%
In~8.48% amplitude range.Tobacco leaf glandular hairs point must object content raising, be conducive to tabacco fragrance substance after toasting and contain
The increase of amount and the improvement of aroma quality, the above results show the invention patent be conducive to Tobacco Glandular Trichome point must object content raising.
Mainly divide must species and content for the glandular hairs of the maximum tobacco leaves of the Hunan 90d cigarette 4 after table 2 is transplanted
Test 2:
2017, for trying flue-cured tobacco cultivars Hunan cigarette 5, spray and not spraying and (compare) two comparative tests handled,
Wherein: processing 1: 45~90d after transplanting is configured to 13.3% solution using 6000g object+45kg clean water of the present invention, into
Row foliage-spray；Handle 2 (controls): the fresh water spraying of phase homogenous quantities.
1. middle part Tobacco Glandular Trichome point must the main type and content of object measurement
1.1 tobacco leaf glandular hairs point must object extraction: the 75d after flue-cured tobacco transplanting selects the morning of the fine day blade without dew
9-11 point, each processing choose representational 5 plants of cigarette strain, and every plant takes its maximum leaf blade, are put into the foam thermal insulation with ice cube
Laboratory is taken back in case, as unit of processing, is respectively soaked the methylene chloride that 1000mL is put into per a piece of blade of each processing
It washes, with 2 1000mL graduated cylinders, each graduated cylinder pours into the methylene chloride of 450mL, and every leaf embathes 4 times in first graduated cylinder,
Soaking time is 2S/ time, and above-mentioned process is repeated in two, ground graduated cylinder, then by containing blade face divide must the solvent filter of object pour into
In the beaker of 1L, 50g anhydrous sodium sulfate analytical reagents is uniformly placed on filter paper when filtering, graduated cylinder and filter paper use remainder
100mL tetrachloromethane rinse net, leaching liquor is placed on rotary evaporator under the conditions of 40 DEG C and 0.06MPa and is concentrated to 1~
1.5mL, finally move into 5mL volumetric flask in carry out constant volume, be then placed in black paper wrapper it is spare in 0 DEG C of refrigerating box, it is above-mentioned
Method is referring to (Han Jinfeng wait .1995, Chinese tobacco) such as Han Jinfeng.
2. major grades tobacco leaf key odorant object total amount tests and analyzes detection after roasting
When maturation adopts roasting, each processing is taken singly to adopt and singly be baked, and is classified after roasting, takes two grade tobacco leaf samples of B2F and C3F
Each 0.5kg of product, the analysis detection for carrying out key odorant object total amount (are used using phenethyl acetate as internal standard, with gas-chromatography-matter
Spectrum/Salbutamol Selected Ion Monitoring (GC-MS/SIM) carries out fragrance species qualitative, quantitative and measures total amount), referring to Li Ling swallow and Zhou Jiheng
Deng (Li Ling swallow, waits Chinese Tobacco Science, and 2015；Zhou Jiheng, waits Agricultural University Of Hunan journal, 2005) method is detected.
As known from Table 3, B2F tobacco leaf key odorant object ligroin extraction total content, carotenoid aroma substance always contain
Amount, catabolite total content, solanone total content, non enzymatic browning reacton product total content, aromatic amino acid pyrolysis product are total
Content, neophytadiene total content and Neutral Aroma Constituents total amount, processing 1 is than handling 2 (controls) successively high 0.95%, 4.30 μ g/
g、13.9μg/g、12.1μg/g、11.0μg/g、6.60μg/g、436.8μg/g、457.1μg/g。
C3F tobacco leaf key odorant object ligroin extraction total content, carotenoid aroma substance total content, catabolite
Total content, solanone total content, non enzymatic browning reacton product total content, aromatic amino acid pyrolysis product total content, planting two
Alkene total content and Neutral Aroma Constituents total amount, processing 1 than handle 2 (controls) successively high 1.09%, 4.10 μ g/g, 4.20 μ g/g,
12.2μg/g、10.1μg/g、6.30μg/g、407.1μg/g、545.0μg/g。
Equally, it relatively learns from the fragrance object total content of test tobacco leaf major grades in 2017, is handled using object of the present invention
Tobacco leaf, tabacco fragrance object content has biggish increase, and tobacco aroma quality has obtained preferable improvement.
No. 5 B2F and C3F tobacco leaf ligroin extractions of 3 different disposal Hunan cigarette of table, carotenoid fragrance object and degradation produce
Object, solanone, non enzymatic browning reacton product, aromatic amino acid pyrolysis product, Neutral Aroma Constituents total amount
As known from Table 4, mainly divide must object amount for the glandular hairs of the maximum tobacco leaves of the Hunan 90d cigarette 4 after transplanting, in which: toluene, butylation
Hydroxy-methylbenzene, decane, dodecane, the tetradecane, eicosane, heptacosane, octacosane, nonacosane, hentriacontane, nicotine,
1,2,3,5,6,7,8,8a- octahydro-1,8a- dimethyl-7- (1- methyl ethylene)-naphthalene, 1,3,5- trioxane, 2- methyl-1-
Nonene -3- alkynes, 2,2-Dimethylpropionic acid, 4- hexadecane ester and other unknown materials etc. are above control, improve ratio 5.58%
In~9.05% amplitude range.Tobacco leaf glandular hairs point must object content raising, be conducive to tabacco fragrance substance after toasting and contain
The increase of amount and the improvement of aroma quality, the above results show the invention patent be conducive to Tobacco Glandular Trichome point must object content raising.
Mainly divide must species and content for the glandular hairs of the maximum tobacco leaves of the Hunan 90d cigarette 5 after table 4 is transplanted
Claims (10)
1. a kind of raising tobacco incense tolerance improves aroma quality preparation, which is characterized in that fresh in full bloom gone by what is naturally squeezed
The later yulan flower of anthocaulus and rose flower juice and auxiliary agent calcium carbonate nano material are mixed evenly obtained.
2. a kind of raising tobacco incense tolerance according to claim 1 improves aroma quality preparation, which is characterized in that by naturally squeezing
Fresh the yulan flower for going anthocaulus later and rose flower juice filtrate and auxiliary agent calcium carbonate nano material in full bloom taken, is pressed
It is stirred according to 30~50:30 of mass ratio~50:1~15 ratio obtained.
3. a kind of raising tobacco incense tolerance according to claim 2 improves aroma quality preparation, which is characterized in that according to fresh
The yulan flower for going anthocaulus later and rose flower juicing filtrate and auxiliary agent calcium carbonate nano material, according to mass ratio 45:
The ratio of 50:5 is placed in container and manually stirs 30 minutes or so later mixed solutions to obtain the final product, spare.
4. a kind of raising tobacco incense tolerance according to claim 1 improves aroma quality preparation, which is characterized in that using artificial
Squeeze the rose petal that the fresh yulan magnolia petal for going anthocaulus later in full bloom juicing filtrate content >=98%, goes anthocaulus later
Juicing filtrate content >=98%, auxiliary agent calcium carbonate nano material content >=98%.
5. a kind of tobacco incense tolerance that improves according to any one of claims 1-4 improves the preparation method of aroma quality preparation,
It is characterized in that, yulan magnolia petal juicing filtrate, rose petal juicing filtrate are all made of manual method, first by the fresh of acquisition
The yulan magnolia petal and rose petal for going anthocaulus break into pulpous state using the broken machine of the Chinese herbal ultra-fine powder with Cryo Equipment, then with double
Layer medical cotton gauze compresses filtering and is placed in container, and juicing filtrate refrigerates spare under 5~15 DEG C of environment.
6. a kind of raising tabacco fragrance object content according to any one of claims 1 to 4 improves tobacco aroma quality preparation or power
Benefit requires the application method for the preparation that preparation method is prepared in 5, which is characterized in that by a kind of raising tabacco fragrance
Object content improves tobacco aroma quality preparation and passes through the juice for going anthocaulus, low-temperature grinding mashing, filtering, 45 after tobacco leaf transplanting~
90d carries out foliage-spray.
7. application method according to claim 6, which is characterized in that by the preparation, be added in clean water to mix and stir
It mixes uniformly, is made after 10.0%~15.0% aqueous solution and uses.
8. application method according to claim 7, which is characterized in that by the preparation, be added in clean water to mix and stir
It mixes uniformly, the cigarette after 12.5% aqueous solution is made, with 300~1000g/666.7m2 usage amount, for 45~90d after transplanting
Leaf, progress foliage-spray is one or many, and 7~10d is divided between spraying time.
9. application method according to claim 7 or 8, which is characterized in that add 12 in the aqueous solution being prepared
Alkyl benzene calcium sulfonate, additive amount are 4-6g/40kg aqueous solution, are then stirred.
10. application method according to claim 7 or 8, which is characterized in that when field is using foliage-spray is carried out, to select
It selects and, without dew, is carried out in the morning 10~12 point or after at 4 points in afternoon, blade is just at fine day, cloudy day without rain or rain rear blade
Face and the back side are intended to spray application to.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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