CN110317479A - A kind of preparation process of mineral composite energy-saving material - Google Patents

A kind of preparation process of mineral composite energy-saving material Download PDF

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Publication number
CN110317479A
CN110317479A CN201910692225.0A CN201910692225A CN110317479A CN 110317479 A CN110317479 A CN 110317479A CN 201910692225 A CN201910692225 A CN 201910692225A CN 110317479 A CN110317479 A CN 110317479A
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CN
China
Prior art keywords
parts
preparation process
casting
composite energy
mineral composite
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Pending
Application number
CN201910692225.0A
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Chinese (zh)
Inventor
梅力
胡冬云
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Nantong Mengding New Materials Co Ltd
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Nantong Mengding New Materials Co Ltd
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Priority to CN201910692225.0A priority Critical patent/CN110317479A/en
Publication of CN110317479A publication Critical patent/CN110317479A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D1/00Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/08Anti-corrosive paints
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/70Additives characterised by shape, e.g. fibres, flakes or microspheres

Abstract

The invention discloses a kind of preparation processes of mineral composite energy-saving material, it is made in parts by mass by following raw material: 45-65 parts of quartz sand, 10-20 parts of epoxy resin, 4-8 parts of clay, 4-8 parts of borax, 3-6 parts of graphene, 3-5 parts of carbon fiber, 10-15 parts of curing agent, 4-8 parts of defoaming agent, 1-2 parts of diluent, 0.2-0.5 parts of mill base, casting made from the invention is than casting hardness performance made from conventional method, damping capacity and corrosion resistance are more preferable, pyroconductivity is lower, it is slow to the variation reflection of external temperature, save energy consumption, the material of use has good chemical inertness, easily stored and recycling and reusing.

Description

A kind of preparation process of mineral composite energy-saving material
Technical field
The present invention relates to mineral composite energy-saving field of material technology, specially a kind of preparation work of mineral composite energy-saving material Skill.
Background technique
Casting made from conventional mineral composite material is not up to maximum performance, and heat transfer on hardness, damping capacity Performance is excessively high, and energy consumption is caused to increase, it would therefore be highly desirable to a kind of improved technology come solve in the presence of the prior art this ask Topic.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation processes of mineral composite energy-saving material, to solve above-mentioned background technique The problem of middle proposition.
To achieve the above object, the invention provides the following technical scheme: a kind of preparation process of mineral composite energy-saving material, It is made in parts by mass by following raw material: 45-65 parts of quartz sand, 10-20 parts of epoxy resin, 4-8 parts of clay, 4-8 parts of borax, stone Black alkene 3-6 parts, 3-5 parts of carbon fiber, 10-15 parts of curing agent, 4-8 parts of defoaming agent, 1-2 parts of diluent, 0.2-0.5 parts of mill base.
Preferably, it is made in parts by mass by following raw material: 55 parts of quartz sand, 15 parts of epoxy resin, 6 parts of clay, borax 6 Part, 5 parts of graphene, 4 parts of carbon fiber, 12 parts of curing agent, 6 parts of defoaming agent, 1 part of diluent, 0.2 part of mill base.
Preferably, the partial size of the quartz sand is 0.1-3.35mm.
Preferably, the curing agent is that aliphatic amine, aromatic amines, amide groups amine, latent solidification amine, urea replace It is one such or a variety of for object.
Preferably, comprising the following steps:
Step 1: raw material being introduced in mixing machine in proportion and is stirred, and the revolving speed of mixing machine is set as 100-150r/min, is obtained To mixture;
Step 2: selecting suitable vacuum mold, inject a mixture into vacuum mold, spontaneous curing 12-15 hours, takes off Mould obtains casting;
Step 3: finally casting is finished using finishing machinery.
Compared with prior art, the beneficial effects of the present invention are:
(1) casting made from is more preferable than casting hardness performance, damping capacity and corrosion resistance made from conventional method, heat transfer Rate is lower, and slow, saving energy consumption is reflected to the variation of external temperature.
(2) material that the present invention uses has good chemical inertness, easily stored and recycling and reusing.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field Art personnel every other embodiment obtained without making creative work belongs to the model that the present invention protects It encloses.
The present invention provides a kind of technical solution: a kind of preparation process of mineral composite energy-saving material, presses matter by following raw material It measures part meter to be made: 45-65 parts of quartz sand, 10-20 parts of epoxy resin, 4-8 parts of clay, 4-8 parts of borax, 3-6 parts of graphene, carbon fiber Tie up 3-5 parts, 10-15 parts of curing agent, 4-8 parts of defoaming agent, 1-2 parts of diluent, 0.2-0.5 parts of mill base.
Wherein, the partial size of quartz sand is 0.1-3.35mm;Curing agent be aliphatic amine, aromatic amines, amide groups amine, Latent solidification amine, urea substitute are one such or a variety of.
A kind of preparation process of mineral composite energy-saving material, comprising the following steps:
Step 1: raw material being introduced in mixing machine in proportion and is stirred, and the revolving speed of mixing machine is set as 100-150r/min, is obtained To mixture;
Step 2: selecting suitable vacuum mold, inject a mixture into vacuum mold, spontaneous curing 12-15 hours, takes off Mould obtains casting;
Step 3: finally casting is finished using finishing machinery.
Embodiment one:
A kind of preparation process of mineral composite energy-saving material, is made in parts by mass by following raw material: 45 parts of quartz sand, asphalt mixtures modified by epoxy resin 10 parts of rouge, 4 parts of clay, 4 parts of borax, 3 parts of graphene, 3 parts of carbon fiber, 10 parts of curing agent, 4 parts of defoaming agent, 1 part of diluent, color 0.2 part of slurry.
The preparation process of the present embodiment the following steps are included:
Step 1: raw material being introduced in mixing machine in proportion and is stirred, and the revolving speed of mixing machine is set as 100r/min, is mixed Close material;
Step 2: selecting suitable vacuum mold, inject a mixture into vacuum mold, and spontaneous curing 15 hours, demoulding obtained To casting;
Step 3: finally casting is finished using finishing machinery.
Casting made from the present embodiment is subjected to hardness performance, damping capacity, heat-conductive characteristic and corrosion resistance experiment.
Embodiment two:
A kind of preparation process of mineral composite energy-saving material, is made in parts by mass by following raw material: 50 parts of quartz sand, asphalt mixtures modified by epoxy resin 12 parts of rouge, 5 parts of clay, 5 parts of borax, 4 parts of graphene, 3 parts of carbon fiber, 12 parts of curing agent, 5 parts of defoaming agent, 1 part of diluent, color 0.2 part of slurry.
The preparation process of the present embodiment the following steps are included:
Step 1: raw material being introduced in mixing machine in proportion and is stirred, and the revolving speed of mixing machine is set as 100r/min, is mixed Close material;
Step 2: selecting suitable vacuum mold, inject a mixture into vacuum mold, and spontaneous curing 15 hours, demoulding obtained To casting;
Step 3: finally casting is finished using finishing machinery.
Casting made from the present embodiment is subjected to hardness performance, damping capacity, heat-conductive characteristic and corrosion resistance experiment, Casting made from the present embodiment is more preferable than casting hardness performance, damping capacity and corrosion resistance made from embodiment one, and heat passes Conductance is lower.
Embodiment three:
A kind of preparation process of mineral composite energy-saving material, is made in parts by mass by following raw material: 55 parts of quartz sand, asphalt mixtures modified by epoxy resin 15 parts of rouge, 6 parts of clay, 6 parts of borax, 5 parts of graphene, 4 parts of carbon fiber, 12 parts of curing agent, 6 parts of defoaming agent, 1 part of diluent, color 0.2 part of slurry.
The preparation process of the present embodiment the following steps are included:
Step 1: raw material being introduced in mixing machine in proportion and is stirred, and the revolving speed of mixing machine is set as 100r/min, is mixed Close material;
Step 2: selecting suitable vacuum mold, inject a mixture into vacuum mold, and spontaneous curing 15 hours, demoulding obtained To casting;
Step 3: finally casting is finished using finishing machinery.
Casting made from the present embodiment is subjected to hardness performance, damping capacity, heat-conductive characteristic and corrosion resistance experiment, Casting made from the present embodiment is more preferable than casting hardness performance, damping capacity and corrosion resistance made from embodiment two, and heat passes Conductance is lower.
Example IV:
A kind of preparation process of mineral composite energy-saving material, is made in parts by mass by following raw material: 60 parts of quartz sand, asphalt mixtures modified by epoxy resin 17 parts of rouge, 7 parts of clay, 7 parts of borax, 6 parts of graphene, 5 parts of carbon fiber, 14 parts of curing agent, 7 parts of defoaming agent, 2 parts of diluent, color 0.2 part of slurry.
The preparation process of the present embodiment the following steps are included:
Step 1: raw material being introduced in mixing machine in proportion and is stirred, and the revolving speed of mixing machine is set as 100r/min, is mixed Close material;
Step 2: selecting suitable vacuum mold, inject a mixture into vacuum mold, and spontaneous curing 15 hours, demoulding obtained To casting;
Step 3: finally casting is finished using finishing machinery.
Casting made from the present embodiment is subjected to hardness performance, damping capacity, heat-conductive characteristic and corrosion resistance experiment, Casting made from the present embodiment is poorer than casting hardness performance, damping capacity and corrosion resistance made from embodiment one, heat transfer Rate is higher.
Embodiment five:
A kind of preparation process of mineral composite energy-saving material, is made in parts by mass by following raw material: 65 parts of quartz sand, asphalt mixtures modified by epoxy resin 20 parts of rouge, 8 parts of clay, 8 parts of borax, 6 parts of graphene, 5 parts of carbon fiber, 15 parts of curing agent, 8 parts of defoaming agent, 2 parts of diluent, color 0.2 part of slurry.
The preparation process of the present embodiment the following steps are included:
Step 1: raw material being introduced in mixing machine in proportion and is stirred, and the revolving speed of mixing machine is set as 100r/min, is mixed Close material;
Step 2: selecting suitable vacuum mold, inject a mixture into vacuum mold, and spontaneous curing 15 hours, demoulding obtained To casting;
Step 3: finally casting is finished using finishing machinery.
Casting made from the present embodiment is subjected to hardness performance, damping capacity, heat-conductive characteristic and corrosion resistance experiment, Casting made from the present embodiment is poorer than casting hardness performance, damping capacity and corrosion resistance made from embodiment one, heat transfer Rate is higher.
Embodiment six:
A kind of preparation process of mineral composite energy-saving material, is made in parts by mass by following raw material: 55 parts of quartz sand, asphalt mixtures modified by epoxy resin 10 parts of rouge, 4 parts of clay, 4 parts of borax, 3 parts of graphene, 3 parts of carbon fiber, 12 parts of curing agent, 6 parts of defoaming agent, 1 part of diluent, color 0.2 part of slurry.
The preparation process of the present embodiment the following steps are included:
Step 1: raw material being introduced in mixing machine in proportion and is stirred, and the revolving speed of mixing machine is set as 100r/min, is mixed Close material;
Step 2: selecting suitable vacuum mold, inject a mixture into vacuum mold, and spontaneous curing 15 hours, demoulding obtained To casting;
Step 3: finally casting is finished using finishing machinery.
Casting made from the present embodiment is subjected to hardness performance, damping capacity, heat-conductive characteristic and corrosion resistance experiment, Casting made from the present embodiment is poorer than casting hardness performance, damping capacity and corrosion resistance made from embodiment one, heat transfer Rate is higher.
Embodiment seven:
A kind of preparation process of mineral composite energy-saving material, is made in parts by mass by following raw material: 55 parts of quartz sand, asphalt mixtures modified by epoxy resin 20 parts of rouge, 8 parts of clay, 8 parts of borax, 6 parts of graphene, 5 parts of carbon fiber, 15 parts of curing agent, 6 parts of defoaming agent, 1 part of diluent, color 0.2 part of slurry.
The preparation process of the present embodiment the following steps are included:
Step 1: raw material being introduced in mixing machine in proportion and is stirred, and the revolving speed of mixing machine is set as 100r/min, is mixed Close material;
Step 2: selecting suitable vacuum mold, inject a mixture into vacuum mold, and spontaneous curing 15 hours, demoulding obtained To casting;
Step 3: finally casting is finished using finishing machinery.
Casting made from the present embodiment is subjected to hardness performance, damping capacity, heat-conductive characteristic and corrosion resistance experiment, Casting made from the present embodiment is poorer than casting hardness performance, damping capacity and corrosion resistance made from embodiment one, heat transfer Rate is higher.
Casting made from various embodiments of the present invention is carried out to hardness performance, damping capacity, heat-conductive characteristic and anticorrosive Performance test show that casting made from embodiment three can reach optimum performance after comparison.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (5)

1. a kind of preparation process of mineral composite energy-saving material, it is characterised in that: be made in parts by mass by following raw material: quartz 45-65 parts of sand, 10-20 parts of epoxy resin, 4-8 parts of clay, 4-8 parts of borax, 3-6 parts of graphene, 3-5 parts of carbon fiber, curing agent 10-15 parts, 4-8 parts of defoaming agent, 1-2 parts of diluent, 0.2-0.5 parts of mill base.
2. a kind of preparation process of mineral composite energy-saving material according to claim 1, it is characterised in that: by following raw material Be made in parts by mass: 55 parts of quartz sand, 6 parts of clay, 6 parts of borax, 5 parts of graphene, 4 parts of carbon fiber, is consolidated 15 parts of epoxy resin 12 parts of agent, 6 parts of defoaming agent, 1 part of diluent, 0.2 part of mill base.
3. a kind of preparation process of mineral composite energy-saving material according to claim 1, it is characterised in that: the quartz sand Partial size be 0.1-3.35mm.
4. a kind of preparation process of mineral composite energy-saving material according to claim 1, it is characterised in that: the curing agent It is one such or a variety of for aliphatic amine, aromatic amines, amide groups amine, latent solidification amine, urea substitute.
5. a kind of preparation process of mineral composite energy-saving material according to claim 1, it is characterised in that: including following step It is rapid:
Step 1: raw material being introduced in mixing machine in proportion and is stirred, and the revolving speed of mixing machine is set as 100-150r/min, is obtained To mixture;
Step 2: selecting suitable vacuum mold, inject a mixture into vacuum mold, spontaneous curing 12-15 hours, takes off Mould obtains casting;
Step 3: finally casting is finished using finishing machinery.
CN201910692225.0A 2019-07-30 2019-07-30 A kind of preparation process of mineral composite energy-saving material Pending CN110317479A (en)

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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110776275A (en) * 2019-12-02 2020-02-11 山东纳诺新材料科技有限公司 Quartz sand mechanical accessory and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105566856A (en) * 2016-02-01 2016-05-11 福建省正丰数控科技有限公司 Composite-material machine-tool-body mineral casting and preparing method thereof
CN105776949A (en) * 2016-02-01 2016-07-20 福建省正丰数控科技有限公司 Composite machine tool bed mineral casting based on cobblestone and preparation method thereof
CN106077428A (en) * 2016-07-29 2016-11-09 无锡市三峰仪器设备有限公司 A kind of resin sand of instrument casting
CN107868255A (en) * 2017-11-17 2018-04-03 厦门大学 The preparation method and applications of POSS DOPO triazine derivative flame retardants with self assembly humidification
CN109852007A (en) * 2019-02-27 2019-06-07 武汉本邦复合材料科技有限公司 A kind of CF/GF hybrid buildup epoxy resin drawing and extruding section bar and production method

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105566856A (en) * 2016-02-01 2016-05-11 福建省正丰数控科技有限公司 Composite-material machine-tool-body mineral casting and preparing method thereof
CN105776949A (en) * 2016-02-01 2016-07-20 福建省正丰数控科技有限公司 Composite machine tool bed mineral casting based on cobblestone and preparation method thereof
CN106077428A (en) * 2016-07-29 2016-11-09 无锡市三峰仪器设备有限公司 A kind of resin sand of instrument casting
CN107868255A (en) * 2017-11-17 2018-04-03 厦门大学 The preparation method and applications of POSS DOPO triazine derivative flame retardants with self assembly humidification
CN109852007A (en) * 2019-02-27 2019-06-07 武汉本邦复合材料科技有限公司 A kind of CF/GF hybrid buildup epoxy resin drawing and extruding section bar and production method

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110776275A (en) * 2019-12-02 2020-02-11 山东纳诺新材料科技有限公司 Quartz sand mechanical accessory and preparation method thereof

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Application publication date: 20191011