CN110283665A - A kind of extraction equipment and extracting process of cosmetics plants essential oil - Google Patents
A kind of extraction equipment and extracting process of cosmetics plants essential oil Download PDFInfo
- Publication number
- CN110283665A CN110283665A CN201910606776.0A CN201910606776A CN110283665A CN 110283665 A CN110283665 A CN 110283665A CN 201910606776 A CN201910606776 A CN 201910606776A CN 110283665 A CN110283665 A CN 110283665A
- Authority
- CN
- China
- Prior art keywords
- outer layer
- layer
- internal layer
- gap
- extraction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000605 extraction Methods 0.000 title claims abstract description 73
- 239000002537 cosmetic Substances 0.000 title claims abstract description 17
- 239000000341 volatile oil Substances 0.000 title claims abstract description 16
- 238000000034 method Methods 0.000 title claims abstract description 10
- 239000007788 liquid Substances 0.000 claims abstract description 55
- 241001411320 Eriogonum inflatum Species 0.000 claims abstract description 36
- 239000002904 solvent Substances 0.000 claims abstract description 36
- 241000196324 Embryophyta Species 0.000 claims abstract description 12
- 238000001514 detection method Methods 0.000 claims abstract description 8
- 238000003756 stirring Methods 0.000 claims description 15
- 239000000463 material Substances 0.000 claims description 9
- 238000007789 sealing Methods 0.000 claims description 7
- 230000005611 electricity Effects 0.000 claims description 6
- 239000011521 glass Substances 0.000 claims description 6
- 239000012046 mixed solvent Substances 0.000 claims description 6
- 239000007779 soft material Substances 0.000 claims description 6
- 239000012530 fluid Substances 0.000 claims description 5
- 239000004033 plastic Substances 0.000 claims description 5
- 229920003023 plastic Polymers 0.000 claims description 5
- 229940099259 vaseline Drugs 0.000 claims description 4
- 238000009434 installation Methods 0.000 claims description 3
- 239000012188 paraffin wax Substances 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 229910001220 stainless steel Inorganic materials 0.000 claims description 3
- 239000010935 stainless steel Substances 0.000 claims description 3
- 239000011259 mixed solution Substances 0.000 abstract description 2
- 238000010186 staining Methods 0.000 abstract description 2
- 238000005070 sampling Methods 0.000 abstract 1
- 238000013517 stratification Methods 0.000 abstract 1
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 12
- 239000000243 solution Substances 0.000 description 7
- 241000220317 Rosa Species 0.000 description 5
- 238000013461 design Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 238000011109 contamination Methods 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 238000005096 rolling process Methods 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000011435 rock Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000116 mitigating effect Effects 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000011897 real-time detection Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000012780 transparent material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The present invention relates to the extraction equipments and extracting process of a kind of cosmetics plants essential oil, the extraction equipment includes extraction container, bottle stopper, blender and bracket, wherein extraction container includes internal layer and outer layer, internal layer side is provided with perpendicular gap, outer layer side is provided with horizontal gap, when perpendicular gap and horizontal gap are overlapped, the upper layer solvent in extraction container can be flowed out from the overlapping position of perpendicular gap and horizontal gap.The device application method is as follows: S1, closing lower end liquid outlet, outer layer is moved up, is overlapped horizontal gap and perpendicular gap not；S2, extraction container is added in the solvent containing solute and extractant；S3, mixed solution is stirred；S4, stratification can release appropriate lower layer's solvent detection from the liquid outlet of lower end；S5, outer layer is moved down, upper layer solvent is flowed out from lateral liquid outlet, and lower layer's solvent brings out liquid stream from down and goes out.The extraction equipment avoids that staining apparatus when upper layer solvent is poured out, effect of extracting are more preferable, save manpower, facilitate sampling.
Description
Technical field
The present invention relates to chemical fields, and in particular to a kind of extraction equipment and extracting process of cosmetics plants essential oil.
Background technique
Extraction is that a common unit in the fields such as cosmetics preparation, food processing, medical processing, biology operates, one
As complete this step using separatory funnel.Separatory funnel is divided into funnel plug and funnel, and the upper end of funnel is inlet, middle-end
It is liquid outlet for mixing vessel, lower end, the centre of lower end is provided with rotating piston, controls the outflow of liquid.
It when using separatory funnel, generally first hunts leak, turns off rotation match, be then added from inlet containing molten
The solvent and extractant of matter, funnel plug, then rocks and mixes different solvents, manually during mixing beyond the Great Wall
Solute is shifted in two kinds of solvents, realizes extraction process, is finally stood until two kinds of different solvents layerings, lower layer's solvent
It is released from the liquid outlet of lower end, upper layer solvent is poured out from upper end inlet.
There are the following problems during above-mentioned extraction:
1, upper layer solvent is poured out from the inlet of upper end, and inlet can be stained with to upper layer solvent, and solvent can flow to funnel
Elsewhere, cause funnel by solvent contamination, be unfavorable for reusing for funnel.
2, conventional separatory funnel is manual operation in extraction process, and need to constantly rock mixes solvent and extractant,
Be inconvenient to be manually operated when liquid volume is larger.
3, conventional extraction operation realizes that primary complete extraction process needs that extraction is repeated several times, and can not learn molten
Whether matter is transferred in extractant from solvent.
This invention address that a kind of extraction equipment of cosmetics flower class essential oil is developed, it is molten in above-mentioned extraction process to solve
Agent be infected with funnel, manual operation it is inconvenient, can not real-time monitoring the problem of.
Summary of the invention
The present invention provides a kind of extraction equipment of cosmetics flower class essential oil, which is in cylindrical
Shape, including extraction container, bottle stopper, blender and bracket, the extraction container upper end neck and lower end base are fixed on bracket
On, at the upper end opening of extraction container and the fitting of the sealing-plug of blender is close.
The extraction container is inside and outside double-layer structure, and the outer diameter of internal layer is equal to the internal diameter of outer layer, and inside and outside layer fitting is tight
Close, contact surface is coated with sealing fluid, and outer layer can be moved along the upper and lower vertical direction of internal layer.
The internal layer is cylinder cup-shaped structure, and the lower end of internal layer is provided with liquid outlet, setting one on the right side of internal layer middle-end
Perpendicular gap, erecting gap is vertical direction, and the width for erecting gap is 1-2mm, erects the 1/3-1/2 that gap length is interior layer height, the outside of internal layer
Face is provided with three ball orbits, is located at left end, the front-end and back-end of internal layer, three ball orbits of internal layer are perpendicular
Histogram is to internal layer ball orbit length is the 1/2-2/3 of interior layer height, and internal layer ball orbit depth is the radius of ball.
The outer layer is bottomless cylinder cup-shaped structure, is provided with lateral liquid outlet, the right side of outer layer on the right side of the middle-end of outer layer
Side is provided with horizontal gap, and horizontal gap is horizontal direction, and the height of horizontal gap is 1-2mm, and the width of horizontal gap is 3-4mm, the medial surface of outer layer
Three ball orbits are provided with, are located at left end, the front-end and back-end of outer layer, three ball orbits of outer layer are vertical
Direction, outer layer ball orbit length are the 4/5-5/6 of outer layer height, and outer layer ball orbit depth is the radius of ball.
The perpendicular gap and horizontal gap are overlapped, and the intersection of perpendicular gap and horizontal gap is liquid flowing outlet；The internal layer rolling
Pearl track and the fitting of outer layer ball orbit, and internal layer, outer layer ball orbit are formed by channel cross-section for circle, including ball
Layer, outer layer ball orbit are formed by channel.
The bottle stopper upper end be cake shape, bottle stopper lower end is tapered from top to bottom, and cross section be circle, bottle stopper and
Internal layer inlet is mutually matched, and there is motor in the inside of bottle stopper, and the rotary shaft of vertical direction, the left end of bottle stopper are equipped on motor
It is provided with electricity jack, electricity jack is connected with motor by conducting wire.
For the blender in the lower end of bottle stopper, motor gives blender to provide rotary power by rotary shaft, in rotary shaft
It is provided with agitating paddle, agitating paddle is fixed on the two sides of rotary shaft, and is symmetrical structure, and agitating paddle and rotary shaft are assembling structure,
The installation number of agitating paddle is adjustable, and mountable 2-6 pairs, rotary shaft rotating speed size changes the opening angle of agitating paddle, and revolving speed is got over
Greatly, opening angle is bigger, and stirring region is bigger.
The bracket is stainless steel stent, and the upper end neck and lower end base of extraction container are fixed by bracket, and extraction is held
The contact area of device and bracket is provided with soft material.
Further, the internal layer, outer layer are glass material, and the lower end of bottle stopper is glass material, the upper end of bottle stopper
For plastic material, the soft material between extraction container and bracket is EVA plastics.
Further, the sealing fluid is at least one of vaseline and paraffin or two kinds.
Further, the liquid outlet of the internal layer lower end is branched structure, and left side liquid outlet is interim sample detection use
Liquid outlet, right side liquid outlet connect the conduit of 1-2m, and right side liquid outlet is the outlet of lower liquid at the end of extracting.
Further, there is a circle tag line at the outer layer liquid outlet, tag line is in red, yellow and blue
It is a kind of.
Further, the motor speed is adjustable, and revolving speed has 3-5 grades of either variable speed, the range of speeds are as follows:
120-800r/min。
Further, the agitating paddle and rotary shaft are assembling structure, and one end of agitating paddle is hook solid, rotary shaft
On be equidistantly positioned groove, lateral hanging column is provided in groove, the crotch of agitating paddle one end is hung on hanging column, and curved
The tonicity of hook opening is small, and crotch has certain elasticity, and crook and hanging column just cooperate in crotch.
Further, the extracting process of the extraction equipment has the following steps:
S1, bottle stopper is opened, closes the liquid outlet valve of bottom, outer layer is moved up, make the horizontal gap and internal layer of outer layer
Perpendicular gap is not overlapped；
S2, the solvent containing solute and extractant are added in extraction container, and stopper bottle stopper, open motor, stirring
Device stirs mixed solvent；
S3, stirring 10-15min, close motor and stop stirring, stand 5-10min, be layered to solvent and extractant；
S4, outer layer is slowly moved down, tag line is in above solution line of demarcation at 1-2mm, while in lateral solution
Outlet contains the solution of outflow with container；
After S5, upper solution outflow, lower layer's solution is released from the bottom of extraction container, while being contained with container, and two layers
The mixed solvent of boundary, which omits, not to be collected.
It wherein, present invention is characterized in that the extraction equipment is divided into inside and outside double-layer structure, and is transparent material
Matter has the ball orbit of three vertical directions, is filled with ball in ball orbit, outer layer jacket is in internal layer between outer layer and internal layer
On, and can be moved up and down along internal layer, the right side of internal layer is provided with a perpendicular gap, and the right side of outer layer is provided with a cross
Gap, outer layer and internal layer fitting it is close and between be coated with vaseline, the horizontal gap of outer layer can be moved up and down along perpendicular gap, when horizontal gap and
When perpendicular gap is not overlapped, internal layer and outer layer are sealing state, and the solute inside extraction equipment can not flow out, when horizontal gap and perpendicular gap weight
When conjunction, solvent can be flowed out from the intersection of horizontal gap and perpendicular gap, then be flowed out by the lateral liquid outlet of outer layer right end, be used simultaneously
Container contains, and avoiding separatory funnel, solvent needs are poured out from upper end inlet at the middle and upper levels, therefore avoid solvent staining apparatus
Outer wall.
The agitating device is connected on motor by rotary shaft, and motor rotation drives rotary shaft, and rotary shaft drive is stirred
Mix paddle, agitating paddle and rotary shaft are assembling structure, and one end of agitating paddle is hook structure, and the opening of hook is less than normal, hook it is curved
Match at hook with the hanging column of rotary shaft, and crotch has certain elasticity, after agitating paddle is fixed on rotary shaft, agitating paddle can be with
It is swung up and down around fixed point, when the revolving speed of rotary shaft increases, the angle that agitating paddle opens becomes larger, and the region of stirring becomes larger, and mixes
The ability enhancing for closing solution, when the revolving speed of rotary shaft reduces, the angle that agitating paddle opens reduces, and the ability of mixed solution subtracts
It is small.The quantity of agitating paddle can be installed as needed, when solvent volume is larger, can suitably increase the quantity of agitating paddle.Agitating paddle
With the cooperation of motor, the inconvenience of extraction manual operation is avoided.
The liquid outlet of the extraction equipment lower end is branched structure, and left side liquid outlet is interim sample detection liquid out
Mouthful, right side liquid outlet is connected with conduit, for extraction at the end of lower liquid outlet, when solvent and extractant mixing are stood point
After layer, a little lower layer's solvent can be released from left side liquid outlet, be used for gas chromatographic detection, when testing result shows solute from molten
After shifting completely in agent, extracting operation can be terminated, upper layer solvent is released from lateral liquid outlet, and lower layer's solvent is on the right side of lower end
Liquid outlet is released.
Beneficial effect
1. the present invention devises the extraction equipment and extracting process of a kind of cosmetics plants essential oil, which can be certainly
Dynamic stirring, the workload for mitigating extraction, upper layer solvent can directly liquid outlet releases, avoids contamination extraction equipment from the side of the transverse,
Lower end liquid outlet is branched structure, facilitates real-time detection.
2. agitating paddle and motor be used cooperatively and the design of the structure of agitating paddle, different solvents can be stirred
It mixes, reduces the inconvenience for manually rocking extraction equipment.
3. the double layer design of extraction equipment makes upper layer solvent not need to pour out from upper end inlet, solvent contamination is avoided
Device.
4. the embranchment Design of lower end liquid outlet facilitates real time sample, the detection of lower layer's solvent composition, enhancing are carried out
The accurate assurance of extraction work.
Detailed description of the invention
Fig. 1 is the schematic diagram of the section structure of the invention；
Fig. 2 is the horizontal section schematic diagram of extraction container of the invention；
Fig. 3 is rotary shaft and agitating paddle assembling structure front view of the invention；
Fig. 4 is rotary shaft and agitating paddle assembling structure side view of the invention；
Fig. 5 is outer layer schematic diagram of the invention.
Specific embodiment
It is described in further detail referring to Fig. 1-5 pairs of design features and operating procedure of the invention.
A kind of extraction equipment of cosmetics flower class essential oil, the extraction equipment monnolithic case are in cylindrical shape, including extraction
Container 1, bottle stopper 2, blender 3 and bracket 4, the 1 upper end neck of extraction container and lower end base are fixed on 4 on bracket, extraction
It is bonded closely at the upper end opening of extracting container 1 with bottle stopper 2；
The extraction container 1 is inside and outside double-layer structure, and the outer diameter of internal layer 5 is equal to the internal diameter of outer layer 6, inside and outside layer patch
It closes closely, contact surface is coated with sealing fluid, and outer layer 6 can be moved along the upper and lower vertical direction of internal layer 5；
The internal layer 5 is cylinder cup-shaped structure, and the lower end of internal layer 5 is provided with liquid outlet 7, setting on the right side of 5 middle-end of internal layer
One perpendicular gap 8, erecting gap 8 is vertical direction, and the width for erecting gap 8 is 1-2mm, erects the 1/3-1/2 that 8 length of gap is 5 height of internal layer,
The lateral surface of internal layer 5 is provided with three ball orbits, is located at left end, the front-end and back-end of internal layer 5, three rollings of internal layer 5
Pearl track is vertical direction, and internal layer ball orbit length is the 1/2-2/3 of 5 height of internal layer, and internal layer ball orbit depth is rolling
The radius of pearl 9；
The outer layer 6 is bottomless cylinder cup-shaped structure, is provided with lateral liquid outlet 10, outer layer on the right side of the middle-end of outer layer 6
6 right side is provided with horizontal gap 11, and horizontal gap 11 is horizontal direction, and the height of horizontal gap 11 is 1-2mm, and the width of horizontal gap 11 is 3-
4mm, the medial surface of outer layer 6 are provided with three ball orbits, are located at left end, the front-end and back-end of outer layer 6, and the three of outer layer 6
Ball orbit is vertical direction, and outer layer ball orbit length is the 4/5-5/6 of 6 height of outer layer, outer layer ball orbit depth
For the radius of ball 9；
The perpendicular gap 8 and horizontal gap 11 are overlapped, and the intersection of perpendicular gap 8 and horizontal gap 11 is liquid flowing outlet；Described
Internal layer ball orbit and the fitting of outer layer ball orbit, and internal layer, outer layer ball orbit are formed by channel cross-section as circle, roll
Pearl 9 is formed by channel in internal layer, outer layer ball orbit；
2 upper end of bottle stopper is cake shape, and 2 lower end of bottle stopper is tapered from top to bottom, and cross section is circle, bottle stopper 2
It being mutually matched with 5 inlet of internal layer, there is motor 12 in the inside of bottle stopper 2, the rotary shaft 13 of vertical direction is installed on motor 12,
The left end of bottle stopper 2 is provided with electricity jack 14, and electricity jack 14 is connected with motor 12 by conducting wire；
The blender 3 provides rotary power to blender 3 by rotary shaft 13 in the lower end of bottle stopper 2, motor 12,
Agitating paddle 15 is provided in rotary shaft 13, agitating paddle 15 is fixed on the two sides of rotary shaft 13, and is symmetrical structure, agitating paddle 15
It is assembling structure with rotary shaft 13, the installation number of agitating paddle 15 is adjustable, and mountable 2-6 pairs, 13 revolving speed size of rotary shaft changes
Become the opening angle of agitating paddle 15, revolving speed is bigger, and opening angle is bigger, and stirring region is bigger；
The bracket 4 is stainless steel stent, and the upper end neck and lower end base of extraction container 1 are fixed by bracket 4, is extracted
The contact area of extracting container 1 and bracket 4 is provided with soft material.
The internal layer 5, outer layer 6 are glass material, and the lower end of bottle stopper 2 is glass material, and the upper end of bottle stopper 2 is modeling
Expect material, the soft material between extraction container 1 and bracket 4 is EVA plastics.
The sealing fluid is at least one of vaseline and paraffin or two kinds.
The liquid outlet 7 of 5 lower end of internal layer is branched structure, and left side liquid outlet is interim sample detection liquid outlet,
Right side liquid outlet connects the conduit of 1-2m, and right side liquid outlet is the outlet of lower liquid at the end of extracting.
There is a circle tag line 16 at the outer layer transverse direction liquid outlet 10, tag line 16 is in red, yellow and blue
It is a kind of.
12 revolving speed of motor is adjustable, and revolving speed has 3-5 grades of either variable speed, the range of speeds are as follows: 120-800r/
min。
The agitating paddle 15 and rotary shaft 13 is assembling structure, and one end of agitating paddle 15 is hook solid, in rotary shaft 13
It is equidistantly positioned groove, lateral hanging column 17 is provided in groove, the crotch of 15 one end of agitating paddle is hung on hanging column 17,
And the tonicity of crotch opening is small, crotch has certain elasticity, and crook and hanging column 17 just cooperate in crotch.
For extracting rose dissolved matter, the extraction step of extraction equipment is as follows:
S1, open bottle stopper 2, close 7 valve of liquid outlet of bottom, outer layer 6 is moved up, make the horizontal gap 11 of outer layer 6 with
The perpendicular gap 8 of internal layer 5 is not overlapped；
S2, it will be added in extraction container 1 containing the aqueous solution of rose dissolved matter, add extractant ethyl acetate, and fill in
Tight bottle stopper 2, opens motor 12, and blender 3 stirs mixed solvent；
S3, stirring 10-15min, close motor 12 and stop stirring, stand 5-10min, be layered to solvent and extractant, can
Liquid outlet releases a small amount of water layer solution on the left of from lower end, with gas chromatographic detection, analyzes the content of rose dissolved matter in water layer,
If rose dissolves the content of substance nearly close to zero, do not need to extract again, if the content of rose dissolved matter is larger,
It needs to extract again；
S4, outer layer is slowly moved down, tag line 16 is in above water layer and ethyl acetate line of demarcation at 1-2mm, together
When lateral taphole 10 with container contain outflow acetate extractant；
After S5, the outflow of upper layer ethyl acetate, lower aqueous solution is released from the bottom of extraction container 1, while being contained with container
Dress, and the mixed solvent of water layer and ethyl acetate boundary is omitted and is not collected.
The basic principles, main features and advantages of the invention have been shown and described above.The technical staff of the industry should
Understand, the present invention is not limited to the above embodiments, and only illustrating for the description in above embodiments and description is of the invention
Principle, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these variation and
Improvement all fall within the protetion scope of the claimed invention.
Claims (8)
1. a kind of extraction equipment of cosmetics plants essential oil, including extraction container (1), bottle stopper (2), blender (3) and bracket
(4), it is characterised in that: extraction container (1) the upper end neck and lower end base are fixed on bracket (4), extraction container (1)
Upper end opening at and bottle stopper (2) fitting it is close；
The extraction container (1) is inside and outside double-layer structure, and the contact surface of internal layer (5) outer diameter and outer layer (6) internal diameter is coated with sealing
Liquid, and outer layer (6) can be mobile along the upper and lower vertical direction of internal layer (5)；
The internal layer (5) is cylinder cup-shaped structure, and the lower end of internal layer (5) is provided with liquid outlet (7), on the right side of internal layer (5) middle-end
One perpendicular gap (8) is set, and erecting gap (8) is vertical direction, and the width for erecting gap (8) is 1-2mm, and erecting gap (8) length is that internal layer (5) are high
The 1/3-1/2 of degree, the lateral surface of internal layer (5) are provided with three ball orbits, and three ball orbits are located at a left side for internal layer (5)
End, front-end and back-end, three ball orbits of internal layer (5) are vertical direction, and internal layer ball orbit length is internal layer (5) height
1/2-2/3；
The outer layer (6) is bottomless cylinder cup-shaped structure, is provided with lateral liquid outlet (10) on the right side of the middle-end of outer layer (6), outside
It is provided with horizontal gap (11) on the right side of layer (6), horizontal gap (11) is horizontal direction, and the height of horizontal gap (11) is 1-2mm, horizontal gap (11)
Width is 3-4mm, and the medial surface of outer layer (6) is provided with three ball orbits, be located at the left ends of outer layer (6), front end and after
End, three ball orbits of outer layer (6) are vertical direction, and outer layer ball orbit length is the 4/5-5/6 of outer layer (6) height；
The perpendicular gap (8) and horizontal gap (11) are overlapped, and the intersection of perpendicular gap (8) and horizontal gap (11) is liquid flowing outlet；Institute
Internal layer ball orbit and outer layer the ball orbit fitting stated, and it is circle that internal layer, outer layer ball orbit, which are formed by channel cross-section,
Ball (9) is formed by channel in internal layer, outer layer ball orbit；
Bottle stopper (2) upper end is cake shape, and bottle stopper (2) lower end is tapered from top to bottom, and cross section is circle, bottle stopper
(2) it is mutually matched with internal layer (5) inlet, the inside of bottle stopper (2) has motor (12), and motor is equipped with vertical direction on (12)
Rotary shaft (13), the left end of bottle stopper (2) are provided with electricity jack (14), and electricity jack (14) is connected with motor (12) by conducting wire；
The blender (3) provides rotation to blender (3) by rotary shaft (13) in the lower end of bottle stopper (2), motor (12)
Power is provided with agitating paddle (15) in rotary shaft (13), and agitating paddle (15) is fixed on the two sides of rotary shaft (13), and is symmetrical junction
Structure, agitating paddle (15) and rotary shaft (13) they are assembling structure, and the installation number of agitating paddle (15) is adjustable, mountable 2-6 pairs, rotation
Shaft (13) revolving speed size changes the opening angle of agitating paddle (15), and revolving speed is bigger, and opening angle is bigger, and stirring region is bigger；
The bracket (4) is stainless steel stent, and the upper end neck and lower end base of extraction container (1) are fixed by bracket (4), extraction
The contact area of extracting container (1) and bracket (4) is provided with soft material.
2. a kind of extraction equipment of cosmetics plants essential oil as described in claim 1, it is characterised in that: the internal layer (5),
Outer layer (6) is glass material, and the lower end of bottle stopper (2) is glass material, and the upper end of bottle stopper (2) is plastic material, extraction container
(1) soft material between bracket (4) is EVA plastics.
3. a kind of extraction equipment of cosmetics plants essential oil as described in claim 1, it is characterised in that: the sealing fluid is
At least one of vaseline and paraffin or two kinds.
4. a kind of extraction equipment of cosmetics plants essential oil as described in claim 1, it is characterised in that: the internal layer (5)
The liquid outlet (7) of lower end is branched structure, and left side liquid outlet is interim sample detection liquid outlet, and right side liquid outlet connects 1-2m
Conduit, right side liquid outlet be extraction at the end of lower liquid outlet.
5. a kind of extraction equipment and extracting process of cosmetics plants essential oil as described in claim 1, it is characterised in that: described
Outer layer transverse direction liquid outlet (10) at have a circle tag line (16), tag line (16) is one of red, yellow and blue.
6. a kind of extraction equipment of cosmetics plants essential oil as described in claim 1, it is characterised in that: the motor (12)
Revolving speed is adjustable, and revolving speed has 3-5 grades or variable speed, the range of speeds are as follows: 120-800r/min.
7. a kind of extraction equipment of cosmetics plants essential oil as described in claim 1, it is characterised in that: the agitating paddle
(15) and rotary shaft (13) is assembling structure, and one end of agitating paddle (15) is hook solid, is equidistantly positioned in rotary shaft (13) recessed
Slot is provided with lateral hanging column (17) in groove, and the crotch of agitating paddle (15) one end is hung on hanging column (17), and crotch is opened
Tonicity at mouthful is small, and crotch has certain elasticity, and crook and hanging column (17) just cooperate in crotch.
8. a kind of extraction equipment of cosmetics plants essential oil as described in claim 1, it is characterised in that: the extraction equipment
Extracting process has the following steps:
S1, bottle stopper (2) are opened, closes liquid outlet (7) valve of bottom, outer layer (6) is moved up, the horizontal gap of outer layer (6) is made
(11) it is not overlapped with the perpendicular gap (8) of internal layer (5)；
S2, the solvent containing solute and extractant are added in extraction container (1), and stopper bottle stopper (2), open motor
(12), blender (3) stirs mixed solvent；
S3, stirring 10-15min, close motor (12) and stop stirring, stand 5-10min, be layered to solvent and extractant；
S4, outer layer is slowly moved down, tag line (16) is in above solution line of demarcation at 1-2mm, while in lateral solution
Export the solution that (10) contain outflow with container；
After S5, upper solution outflow, lower layer's solution is released from the bottom of extraction container (1), while being contained with container, and two layers point
Mixed solvent at boundary, which omits, not to be collected.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910606776.0A CN110283665B (en) | 2019-07-06 | 2019-07-06 | Extraction device and extraction method for cosmetic plant essential oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910606776.0A CN110283665B (en) | 2019-07-06 | 2019-07-06 | Extraction device and extraction method for cosmetic plant essential oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN110283665A true CN110283665A (en) | 2019-09-27 |
| CN110283665B CN110283665B (en) | 2020-05-12 |
Family
ID=68020763
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910606776.0A Active CN110283665B (en) | 2019-07-06 | 2019-07-06 | Extraction device and extraction method for cosmetic plant essential oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110283665B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112403019A (en) * | 2020-10-14 | 2021-02-26 | 王倩 | Supercritical extraction process for effective components of Chinese herbal medicine |
| CN113671089A (en) * | 2021-09-18 | 2021-11-19 | 云南中烟工业有限责任公司 | Tobacco essence extraction, separation and concentration device with sample feeding bottle and method |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105312098A (en) * | 2015-11-30 | 2016-02-10 | 河南师范大学 | Separating funnel used in extraction process |
| CN205435054U (en) * | 2015-09-06 | 2016-08-10 | 山东康美乐医药科技有限公司 | Extraction device is used in laboratory of simulation production |
| CN207680090U (en) * | 2017-12-19 | 2018-08-03 | 南开大学 | A kind of automanual magnetic agitation liquid liquid extraction plant |
-
2019
- 2019-07-06 CN CN201910606776.0A patent/CN110283665B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN205435054U (en) * | 2015-09-06 | 2016-08-10 | 山东康美乐医药科技有限公司 | Extraction device is used in laboratory of simulation production |
| CN105312098A (en) * | 2015-11-30 | 2016-02-10 | 河南师范大学 | Separating funnel used in extraction process |
| CN207680090U (en) * | 2017-12-19 | 2018-08-03 | 南开大学 | A kind of automanual magnetic agitation liquid liquid extraction plant |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112403019A (en) * | 2020-10-14 | 2021-02-26 | 王倩 | Supercritical extraction process for effective components of Chinese herbal medicine |
| CN113671089A (en) * | 2021-09-18 | 2021-11-19 | 云南中烟工业有限责任公司 | Tobacco essence extraction, separation and concentration device with sample feeding bottle and method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN110283665B (en) | 2020-05-12 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN110283665A (en) | A kind of extraction equipment and extracting process of cosmetics plants essential oil | |
| CN107080979A (en) | Slurries bubble elimination device and method | |
| CN103889582A (en) | Centrifugal rotary disk | |
| CN109453544A (en) | Efficient automatic liquid liquid extracter | |
| CN204177625U (en) | A kind of sampler measuring grain size of sediment | |
| CN110237563A (en) | Multi-connection automatic liquid-liquid extraction device | |
| CN212236887U (en) | Animal remedy production is with joining in marriage liquid device | |
| CN203824993U (en) | Improved dissolubility testing device | |
| CN206138792U (en) | Separator and adopt this separator from dynamic testing oil appearance | |
| CN210596003U (en) | Blending tank for blueberry wine production | |
| CN206881210U (en) | Slurries bubble elimination device | |
| CN207318513U (en) | A kind of automatic textile quantitative chemical analysis instrument | |
| CN206910868U (en) | A kind of extraction separation device for activated thioester of cefixime side chain post processing | |
| CN206881205U (en) | A kind of constant temperature stirring-type separatory funnel | |
| CN209423018U (en) | Efficient automatic liquid liquid extracter | |
| CN208212581U (en) | A kind of new and effective centrifugal extraction apparatus | |
| CN209222138U (en) | A kind of rotary shaker for batch samples simultaneous reactions | |
| CN208043489U (en) | Full-automatic water quality divides sampling device | |
| CN110812884B (en) | Traditional Chinese medicine alcohol precipitation tank and alcohol precipitation method | |
| CN206661243U (en) | A kind of double-deck separatory funnel | |
| CN209656508U (en) | Material resource feedway based on deposition physical simulation experiment | |
| CN110079439A (en) | A kind of cell isolation method based on two-freedom continuous centrifuge | |
| CN110314588A (en) | A kind of polyurethane grouting material dilution device | |
| CN206435148U (en) | A kind of coating material agitator | |
| CN207203866U (en) | One kind dissolving mixer |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20200119 Address after: 046000 No. 188 Taihang North Road, Changzhi City, Shanxi Province, Accelerator No. 8 Workshop of Science and Technology Enterprise Applicant after: Quzhican Address before: 312500 Room 242, 132 Gushan New Village, Nanming Street, Xinchang County, Shaoxing City, Zhejiang Province Applicant before: Chen Hanyuan |
|
| GR01 | Patent grant | ||
| GR01 | Patent grant |