CN110281337A - A kind of extracting method of archeological site high humidity state fragility wooden cultural relic - Google Patents

A kind of extracting method of archeological site high humidity state fragility wooden cultural relic Download PDF

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Publication number
CN110281337A
CN110281337A CN201910707979.9A CN201910707979A CN110281337A CN 110281337 A CN110281337 A CN 110281337A CN 201910707979 A CN201910707979 A CN 201910707979A CN 110281337 A CN110281337 A CN 110281337A
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CN
China
Prior art keywords
cultural relic
wooden cultural
wooden
high humidity
extracting method
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CN201910707979.9A
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Chinese (zh)
Inventor
陈家昌
张良帅
贺思予
武志江
陈晓琳
唐静
崔新战
迟铭
刘欣
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Henan Institute Of Cultural Relics And Archaeology
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Henan Institute Of Cultural Relics And Archaeology
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Priority to CN201910707979.9A priority Critical patent/CN110281337A/en
Publication of CN110281337A publication Critical patent/CN110281337A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/34Organic impregnating agents
    • B27K3/36Aliphatic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/34Organic impregnating agents
    • B27K3/50Mixtures of different organic impregnating agents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/0005Cryogenic treatment
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27MWORKING OF WOOD NOT PROVIDED FOR IN SUBCLASSES B27B - B27L; MANUFACTURE OF SPECIFIC WOODEN ARTICLES
    • B27M3/00Manufacture or reconditioning of specific semi-finished or finished articles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K2240/00Purpose of the treatment
    • B27K2240/20Removing fungi, molds or insects

Abstract

The present invention provides a kind of extracting method of archeological site high humidity state fragility wooden cultural relic.Including using glycol water, glycerin solution or both mixture to carry out pre-treatment step to the fragile waterlogged wooden culture relics in high humidity environment, ethylene glycol solution, glycerin solution or both mixture is made to penetrate into wooden cultural relic;It further include that fast freezing 30s-2min is carried out to pretreated wooden cultural relic, the wooden cultural relic after then taking out freezing.Preprocessing process can slow down destruction of the liquid nitrogen frozen process to fragile wooden cultural relic, and have positive acting to the subsequent dehydration of waterlogged wooden culture relics setting.The material that this method uses is environmentally protective, nontoxic, cheap and easily-available, will not cause significantly to adversely affect to being further processed for wooden cultural relic.

Description

A kind of extracting method of archeological site high humidity state fragility wooden cultural relic
Technical field
The invention discloses a kind of extracting methods of high humidity state fragility wooden cultural relic.
Background technique
The historical relic's protection of archaeological excavation scene is to carry out the important link of historical relic's protection work, and the purpose is to go out in cultural relic excavation The first time of soil, fragile historical relic ontology and its Conservation environment to environmental resistance difference implement intervening measure, by the object of historical relic The load informations such as matter entity, traces form and related microenvironment situation more completely preserve.So-called fragility historical relic refers to that Material serious deterioration, performance big portion loses traces, the trace of various unearthed relics etc. in buring environment a bit.From substance From the aspect of body existence form and structural constituent, these fragile matter historical relics have the spy of vulnerability, mutability and irreversibility Point.Specific manifestation are as follows: degradation speed is fast after excavation is unearthed, and cultural relic entity morphs or even damages completely in the short time.Pass through Protection practice in recent years for the protection key of fragile historical relic as can be seen that be to unearthed environment and historical relic ontology implementation section It learns and intervenes.Under usual conditions, since the condition of archeological site is complex, the protection for not being well positioned to meet fragile historical relic is needed It asks.Therefore, fragility historical relic extracted, be transported to laboratory progress allopatric protection processing, obtained historical relic's protection worker It is more and more to pay attention to.
Summary of the invention
To solve the above problems, the present invention provides a kind of extracting method of archeological site high humidity state fragility wooden cultural relic.
The object of the present invention is achieved in the following manner: a kind of extraction of archeological site high humidity state fragility wooden cultural relic Method, including using glycol water, glycerin solution or both mixture to the fragile waterlogged wooden in high humidity environment Historical relic carries out pre-treatment step, and ethylene glycol solution, glycerin solution or both mixture is made to penetrate into wooden cultural relic;It further include to pre- Treated, and wooden cultural relic carries out fast freezing 30s-2min, the wooden cultural relic after then taking out freezing.Preprocessing process can Slow down destruction of the liquid nitrogen frozen process to fragile wooden cultural relic, and has positive work to the subsequent dehydration of waterlogged wooden culture relics setting With.
The volumetric concentration of glycol water is 50%-60%, and the volumetric concentration of glycerin solution is 50%-60%.
Pretreated mode is at least one of to impregnate, instil or spray, and pretreatment time is 1-3 hours.Guarantee molten Liquid effectively penetrates into historical relic.
After pre-treatment step is completed, 2~5 layers of degreasing cotton gauze are covered on wooden cultural relic surface, degreasing cotton gauze uses The alcohol compound aqueous solution of 10%-20% volumetric concentration is sufficiently impregnated, and is worked and is to pour when spilling liquid nitrogen, avoids to wooden cultural relic Direct impact, and the integral strength of fragile wooden cultural relic after liquid nitrogen frozen can be effectively improved.Alcohol compound is ethylene glycol, third The mixture of glycol or both.
The mode for being rapidly frozen processing is that liquid nitrogen frozen handles 30s-2min, continuously pours on wooden cultural relic and spills liquid nitrogen to wood Matter historical relic entirety fully charge.
Between wooden cultural relic bottom and its supporting body, insertion bamboo stick is separated and forms interactive support.
The freezing wooden cultural relic of taking-up is placed in the acid and alkali-resistance equipped with deionized water or distilled water, in corrosion resistant container, water Amount there was not wooden cultural relic completely, prevented its quick dehydration shrinkage after defrosting.Acid and alkali-resistance, corrosion resistant container are organic glass Container.
Wooden cultural relic after extraction is complete, should be transported to as early as possible in the specialized laboratory with preferable protective condition, and The vibration facter in transportational process should be fully considered during this.
Be directed under high humidity state, water content is higher and the fragile wooden cultural relic of serious deterioration, located in advance using alcohols Reason is extracted historical relic to the profession with more preferable protective condition from complicated archeological site using liquid nitrogen under certain ancillary measure Subsequent protection processing is carried out in laboratory.The material that this method uses is environmentally protective, nontoxic, cheap and easily-available, will not be to wood Being further processed for matter historical relic causes significantly to adversely affect, and is a kind of fragile wooden for high humidity state in complicated archeological site Matter historical relic safely and effectively extracting method.
Compared with the existing technology, method provided by the invention is under the premise of carrying out pretreated, liquid nitrogen frozen treatment process Slight to the negative effect of full water fragility wooden cultural relic, the historical relic color difference after freezing changes < 0.01%, deformation quantity < 0.1%, historical relic The strength of materials is without being decreased obviously.Method provided by the invention avoids chemical material curable type and extracts to wooden cultural relic bring dirt Dye mainly takes the intensity of liquid nitrogen flash freezer enhancing historical relic;The material previously treated of use and cold source material are environmentally protective, to environment with Human body is without side-effects, and method provided by the invention is highly suitable in high humidity environment or the large-scale wood of the fragility of thorough impregnation Yu Shuizhong Matter historical relic, fragile bamboo matter historical relic under water-saturated state same for same environment also have certain be applicable in by the lacquerware of tire of bamboo and wood Property.
Detailed description of the invention
Fig. 1 is that the colored paint bamboo mat that archeological site extracts in case extracts preceding schematic diagram.
Fig. 2 is the schematic diagram for the colored paint bamboo mat insertion bamboo stick that archeological site extracts in case.
Fig. 3 is that the hydrophilic glycol water of colored paint bamboo mat sprinkling, glycerine that archeological site extracts in case are water-soluble The schematic diagram of liquid or both mixture.
Fig. 4 is the schematic diagram for the colored paint bamboo mat covering degreasing cotton gauze that archeological site extracts in case.
Fig. 5 is that archeological site extracts the schematic diagram after the colored paint bamboo mat in case freezes.
Fig. 6 is that archeological site extracts the schematic diagram that laboratory is transported to after the colored paint bamboo mat in case extracts.
Specific embodiment
A kind of extracting method of archeological site high humidity state fragility wooden cultural relic, including use glycol water, the third three Alcohol solution or both mixture carries out pre-treatment step to the fragile waterlogged wooden culture relics in high humidity environment, keeps ethylene glycol molten Liquid, glycerin solution or both mixture penetrate into wooden cultural relic;It further include being rapidly frozen to pretreated wooden cultural relic 30s-2min, the wooden cultural relic after then taking out freezing.Preprocessing process can slow down liquid nitrogen frozen process to fragile wooden text The destruction of object, and have positive acting to the subsequent dehydration of waterlogged wooden culture relics setting, fast freezing makes historical relic not dehydration as far as possible Freezing, it can increase fragile wooden cultural relic intensity, fragile wooden cultural relic facilitated to extract and transhipment, but can portion's damage as far as possible it is crisp Weak wooden cultural relic.
The volumetric concentration of glycol water is 50%-60%, and the volumetric concentration of glycerin solution is 50%-60%.
Pretreated mode is at least one of to impregnate, instil or spray, and pretreatment time is 1-3 hours.Guarantee molten Liquid effectively penetrates into historical relic.
After pre-treatment step is completed, 2~5 layers of degreasing cotton gauze are covered on wooden cultural relic surface, degreasing cotton gauze uses The alcohol compound aqueous solution of 10%-20% volumetric concentration is sufficiently impregnated, and is worked and is to pour when spilling liquid nitrogen, avoids to wooden cultural relic Direct impact, and the integral strength of fragile wooden cultural relic after liquid nitrogen frozen can be effectively improved.Alcohol compound is ethylene glycol, third The mixture of glycol or both.
The mode for being rapidly frozen processing is that liquid nitrogen frozen handles 30s-2min, continuously pours on wooden cultural relic and spills liquid nitrogen to wood Matter historical relic entirety fully charge.
Between wooden cultural relic bottom and its supporting body, insertion bamboo stick is separated and forms interactive support.
The freezing wooden cultural relic of taking-up is placed in the acid and alkali-resistance equipped with deionized water or distilled water, in corrosion resistant container, water Amount there was not wooden cultural relic completely, prevented its quick dehydration shrinkage after defrosting.Acid and alkali-resistance, corrosion resistant container are organic glass Container.
Embodiment 1
A kind of extracting method of archeological site high humidity state fragility wooden cultural relic, (1) wooden cultural relic bottom and its supporting body it Between, insertion bamboo stick is separated and forms interactive support;(2) the fragile waterlogged wooden culture relics in high humidity environment are located in advance Reason: wooden cultural relic is penetrated by way of immersion using the glycol water that volumetric concentration is 50%, pretreatment time is 2 small When;(3) it is then continuously poured on wooden cultural relic and spills liquid nitrogen to wooden cultural relic entirety fully charge, time 30s then takes out cold Wooden cultural relic after jelly.
Embodiment 2
A kind of extracting method of archeological site high humidity state fragility wooden cultural relic, (1) wooden cultural relic bottom and its supporting body it Between, insertion bamboo stick is separated and forms interactive support;(2) the fragile waterlogged wooden culture relics in high humidity environment are located in advance Reason: wooden cultural relic is penetrated by way of instillation using the glycol water that volumetric concentration is 60%, pretreatment time is 1 small When;(3) after pre-treatment step is completed, 2 layers of degreasing cotton gauze are covered on wooden cultural relic surface, degreasing cotton gauze uses 10% body The glycol water of product concentration is sufficiently impregnated;(4) then continuously pour that spill liquid nitrogen integrally complete to wooden cultural relic on wooden cultural relic Freeze entirely, time 2min, the wooden cultural relic after then taking out freezing.
Embodiment 3
A kind of extracting method of archeological site high humidity state fragility wooden cultural relic, (1) wooden cultural relic bottom and its supporting body it Between, insertion bamboo stick is separated and forms interactive support;(2) the fragile waterlogged wooden culture relics in high humidity environment are located in advance Reason: wooden cultural relic, pretreatment time 2.2 are penetrated by way of immersion using the glycerin solution that volumetric concentration is 50% Hour;(3) after pre-treatment step is completed, 3 layers of degreasing cotton gauze are covered on wooden cultural relic surface, degreasing cotton gauze uses 20% The glycol water of volumetric concentration is sufficiently impregnated;(4) it is then continuously poured on wooden cultural relic and spills liquid nitrogen to wooden cultural relic entirety Fully charge, time 1.5min, the wooden cultural relic after then taking out freezing;(5) the freezing wooden cultural relic of taking-up is placed in dress In the plexiglass box for having deionized water or distilled water, water there was not wooden cultural relic completely, prevented it quick after defrosting Dehydration shrinkage.
Embodiment 4
A kind of extracting method of archeological site high humidity state fragility wooden cultural relic, (1) wooden cultural relic bottom and its supporting body it Between, insertion bamboo stick is separated and forms interactive support;(2) the fragile waterlogged wooden culture relics in high humidity environment are located in advance Reason: wooden cultural relic is penetrated by way of sprinkling using the glycerin solution that volumetric concentration is 60%, pretreatment time is 3 small When;(3) after pre-treatment step is completed, 4 layers of degreasing cotton gauze are covered on wooden cultural relic surface, degreasing cotton gauze uses 10% body The glycerin solution of product concentration is sufficiently impregnated;(4) then continuously pour that spill liquid nitrogen integrally complete to wooden cultural relic on wooden cultural relic Freeze entirely, time 1min, the wooden cultural relic after then taking out freezing;(5) the freezing wooden cultural relic of taking-up is placed in be equipped with and is gone In the plexiglass box of ionized water or distilled water, water there was not wooden cultural relic completely, prevented its quick dehydration after defrosting It shrinks.
Embodiment 5
A kind of extracting method of archeological site high humidity state fragility wooden cultural relic, (1) wooden cultural relic bottom and its supporting body it Between, insertion bamboo stick is separated and forms interactive support;(2) the fragile waterlogged wooden culture relics in high humidity environment are located in advance Reason: the mixed liquor for the glycerin solution that the glycol water and volumetric concentration for the use of volumetric concentration being 50% are 60% passes through leaching The mode of bubble penetrates into wooden cultural relic, and pretreatment time is 1.5 hours;(3) after pre-treatment step is completed, on wooden cultural relic surface 5 layers of degreasing cotton gauze are covered, degreasing cotton gauze is sufficiently impregnated 5 hours using the glycerin solution of 20% volumetric concentration;(4) so It is continuously poured on wooden cultural relic afterwards and spills liquid nitrogen to wooden cultural relic entirety fully charge, time 40s, the wood after then taking out freezing Matter historical relic;(5) the freezing wooden cultural relic of taking-up is placed in the plexiglass box equipped with deionized water or distilled water, water is complete Do not had wooden cultural relic entirely, and prevented its quick dehydration shrinkage after defrosting.
Embodiment 6
A kind of extracting method of archeological site high humidity state fragility wooden cultural relic, (1) wooden cultural relic bottom and its supporting body it Between, insertion bamboo stick is separated and forms interactive support;(2) the fragile waterlogged wooden culture relics in high humidity environment are located in advance Reason: the mixed liquor for the glycerin solution that the glycol water and volumetric concentration for the use of volumetric concentration being 55% are 60% passes through drop The mode of note penetrates into wooden cultural relic, and pretreatment time is 1.2 hours;(3) it is then continuously poured on wooden cultural relic and spills liquid nitrogen to wood Matter historical relic entirety fully charge, time 60s, the wooden cultural relic after then taking out freezing;(4) the freezing wooden cultural relic of taking-up It is placed in the plexiglass box equipped with deionized water or distilled water, water there was not wooden cultural relic completely, prevented it in defrosting Quick dehydration shrinkage afterwards.
Embodiment 7
A kind of extracting method of archeological site high humidity state fragility wooden cultural relic, (1) wooden cultural relic bottom and its supporting body it Between, insertion bamboo stick is separated and forms interactive support;(2) the fragile waterlogged wooden culture relics in high humidity environment are located in advance Reason: the mixed liquor for the glycerin solution that the glycol water and volumetric concentration for the use of volumetric concentration being 50% are 55% passes through spray The mode spilt penetrates into wooden cultural relic, and pretreatment time is 3 hours;(3) it after pre-treatment step is completed, is covered on wooden cultural relic surface 3 layers of degreasing cotton gauze of lid, degreasing cotton gauze is using the glycol water of 10% volumetric concentration and the glycerine of 20% volumetric concentration The mixed liquor of aqueous solution is sufficiently impregnated 4.5 hours;(4) then continuously pour that spill liquid nitrogen integrally complete to wooden cultural relic on wooden cultural relic Freeze entirely, time 1.5min, the wooden cultural relic after then taking out freezing;(5) the freezing wooden cultural relic of taking-up is placed in and is equipped with In the plexiglass box of deionized water or distilled water, water there was not wooden cultural relic completely, prevented it from quickly losing after defrosting Water is shunk.
Embodiment 8
A kind of extracting method of archeological site high humidity state fragility wooden cultural relic, (1) wooden cultural relic bottom and its supporting body it Between, insertion bamboo stick is separated and forms interactive support;(2) the fragile waterlogged wooden culture relics in high humidity environment are located in advance Reason: wooden cultural relic is penetrated by way of sprinkling using the glycol water that volumetric concentration is 55%, pretreatment time is 3 small When;(3) after pre-treatment step is completed, 4 layers of degreasing cotton gauze are covered on wooden cultural relic surface, degreasing cotton gauze uses 15% body The mixed liquor of the glycerin solution of the glycol water and 15% volumetric concentration of product concentration is sufficiently impregnated 4 hours;(4) then It is continuously poured on wooden cultural relic and spills liquid nitrogen to wooden cultural relic entirety fully charge, time 2min is then whole to extract, and integrally mentions It takes and refers to historical relic, bamboo stick, degreasing cotton gauze and archeological site environment separation, Oscillation Amplitude should be reduced in whole extraction process, It prevents from cracking;(5) the freezing wooden cultural relic of taking-up is placed in the plexiglass box equipped with deionized water or distilled water, water Do not had wooden cultural relic completely, and prevented its quick dehydration shrinkage after defrosting;(6) historical relic after the completion of extraction is transported into laboratory Carry out subsequent protection processing.
Archeological site extracts case (Chu Mu of Chengyang city ruins eight be buried with the dead colored paint bamboo mat):
There are 4 more complete colored paint bamboo mats and several relics overlapped together for extraction, wherein 3 to coat with lacquer red paint Thin bamboo strip is ground, is formed with the thin bamboo strip weave pattern for coating with lacquer pitch-dark, and in addition 1 is compiled using primary colors thin bamboo strips used for weaving the bottom of as, with coating with lacquer pitch-dark thin bamboo strip It damasks.It is about 0.25-0.3 centimetres wide, about 0.05-0.06 centimetres thick that colored paint bamboo mat is all made of thin bamboo strip, and coat with lacquer respectively it is red, After pitch-dark, various floral designs are formed by different weavings.Wherein, size maximum one is about 2.5 meters, and width is 1.8 meters or so, be the maximum colored paint bamboo mat being unearthed so far in Chu, the Warring states, China tomb.
Concrete operations process are as follows: after the sposh and sundries of bamboo mat surrounding profile are cleaned out using clear water first, to bamboo Seat carries out the information extractions such as 3-D scanning, drawing, photograph work;Secondly according to the size of bamboo mat, using the bamboo wood that elasticity is good, system The bamboo stick that standby length and width, thickness out respectively may be about 80 × 5 × 0.5cm is spare.When starting extraction operation, first bamboo mat is selected with coffin chamber Face is combined there are the position in gap, is close to coffin chamber ground with bamboo stick and is carefully inserted into bamboo mat bottom, after first bamboo stick insertion Several bamboo sticks are sequentially inserted into the bamboo stick or so, until bamboo mat is completely disengaged with coffin chamber ground.In addition it is being mentioned to reduce liquid nitrogen It directly impacts caused by bamboo mat during taking, is first carried out in the glycol water that bamboo mat surface sprinkling volumetric concentration is 30% Pretreatment, makes glycol water penetrate into wooden cultural relic by way of immersion, instillation or sprinkling, and pretreatment time is that 1-3 is small When, and be covered each by 2,3,4,5 layers of degreasing cotton gauze soaked with 20% glycol water in the covering of bamboo mat surface or do not cover Lid degreasing cotton gauze.It splashes processing etc. liquid nitrogen can be carried out after the completion of above-mentioned work, liquid nitrogen of splashing carries out 3-5 times back and forth, the time Finally connected bamboo stick until bamboo mat is an entirety together with surrounding medium and degreasing cotton gauze fully charge for 30s-2min Bottom liner takes out together.The bamboo mat extracted is placed in the organic glass cylinder equipped with deionized water, it is subsequent to transport laboratory progress back Protection processing.Schematic diagram is as shown in figs 1 to 6.
What has been described above is only a preferred embodiment of the present invention, it is noted that for those skilled in the art, Without depart from that overall concept of the invention, several changes and improvements can also be made, these also should be considered as of the invention Protection scope.

Claims (9)

1. a kind of extracting method of archeological site high humidity state fragility wooden cultural relic, it is characterised in that: including using ethylene glycol water Solution, glycerin solution or both mixture carry out pre-treatment step to the fragile waterlogged wooden culture relics in high humidity environment, make Ethylene glycol solution, glycerin solution or both mixture penetrate into wooden cultural relic;It further include being carried out to pretreated wooden cultural relic It is rapidly frozen 30s-2min, the wooden cultural relic after then taking out freezing.
2. the extracting method of archeological site high humidity state fragility wooden cultural relic according to claim 1, it is characterised in that: second The volumetric concentration of two alcohol solutions is 50%-60%, and the volumetric concentration of glycerin solution is 50%-60%.
3. the extracting method of archeological site high humidity state fragility wooden cultural relic according to claim 1, it is characterised in that: pre- The mode of processing is at least one of to impregnate, instil or spray, and pretreatment time is 1-3 hours.
4. the extracting method of archeological site high humidity state fragility wooden cultural relic according to claim 1, it is characterised in that: pre- After processing step is completed, 2~5 layers of degreasing cotton gauze are covered on wooden cultural relic surface, degreasing cotton gauze uses 10%-20% volume Concentration alcohol compound aqueous solution is sufficiently impregnated.
5. the extracting method of archeological site high humidity state fragility wooden cultural relic according to claim 4, it is characterised in that: alcohol Class compound is the mixture of ethylene glycol, propylene glycol or both.
6. the extracting method of archeological site high humidity state fragility wooden cultural relic according to claim 1, it is characterised in that: fast The mode of fast freezing processing is liquid nitrogen frozen processing, continuously pours on wooden cultural relic and spills liquid nitrogen 30s-2min.
7. the extracting method of archeological site high humidity state fragility wooden cultural relic according to claim 1, it is characterised in that: Between wooden cultural relic bottom and its supporting body, insertion bamboo stick is separated and forms interactive support.
8. the extracting method of archeological site high humidity state fragility wooden cultural relic according to claim 1, it is characterised in that: take Freezing wooden cultural relic out is placed in the acid and alkali-resistance equipped with deionized water or distilled water, in corrosion resistant container, and water did not had completely Wooden cultural relic.
9. the extracting method of archeological site high humidity state fragility wooden cultural relic according to claim 8, it is characterised in that: resistance to Soda acid, corrosion resistant container are plexiglass box.
CN201910707979.9A 2019-08-01 2019-08-01 A kind of extracting method of archeological site high humidity state fragility wooden cultural relic Pending CN110281337A (en)

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CN112812544A (en) * 2021-02-04 2021-05-18 浙江大学 In-situ solid multi-coated extraction material and extraction recovery method for underwater fragile cultural relics

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CN106799781A (en) * 2017-02-21 2017-06-06 中国林业科学研究院木材工业研究所 A kind of waterlogged wooden culture relics reinforcement means of utilization nano-cellulose
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CN112812544A (en) * 2021-02-04 2021-05-18 浙江大学 In-situ solid multi-coated extraction material and extraction recovery method for underwater fragile cultural relics
CN112812544B (en) * 2021-02-04 2021-11-12 浙江大学 In-situ solid multi-coated extraction material and extraction recovery method for underwater fragile cultural relics

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