CN110270287A - A kind of high-performance polyphenylene sulfide composite material reaction kettle device - Google Patents

A kind of high-performance polyphenylene sulfide composite material reaction kettle device Download PDF

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Publication number
CN110270287A
CN110270287A CN201910534385.2A CN201910534385A CN110270287A CN 110270287 A CN110270287 A CN 110270287A CN 201910534385 A CN201910534385 A CN 201910534385A CN 110270287 A CN110270287 A CN 110270287A
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CN
China
Prior art keywords
reaction kettle
kettle ontology
annular
rotating turret
inner cavity
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Granted
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CN201910534385.2A
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Chinese (zh)
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CN110270287B (en
Inventor
张奇
丁丽娜
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Nanjing Qingyan New Materials Research Institute Co Ltd
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Nanjing Qingyan New Materials Research Institute Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C4/00Crushing or disintegrating by roller mills
    • B02C4/02Crushing or disintegrating by roller mills with two or more rollers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C4/00Crushing or disintegrating by roller mills
    • B02C4/28Details
    • B02C4/42Driving mechanisms; Roller speed control
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B9/00Cleaning hollow articles by methods or apparatus specially adapted thereto 
    • B08B9/08Cleaning containers, e.g. tanks
    • B08B9/087Cleaning containers, e.g. tanks by methods involving the use of tools, e.g. brushes, scrapers

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Mechanical Engineering (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

The invention discloses a kind of high-performance polyphenylene sulfide composite material reaction kettle devices, including sole plate and reaction kettle ontology, stock cabinet is equipped with by the reaction kettle ontology apical lateral, the stock cabinets cavity is divided into upper guide grinding chamber and lower stirring and drying chamber by interlayer, feed tube is equipped in the upper guide grinding chamber, collecting bin, the lower stirring and drying is intracavitary to be equipped with rotation axis, stirring rod is uniformly provided in the rotation axis, driving assembly is equipped in the middle part of the reaction kettle ontology outer top, side is equipped with transmission shaft vertically in top in the reaction kettle ontology, the transmission shaft bottom end is connected with cross rotating turret, cross rotating turret lower end is equipped with hand operated mixing paddle regulating and controlling mechanism, annular rotating turret is movably equipped on the reaction kettle bodies top inward bottom wall, annular cradle is equipped on the inside of the annular rotating turret, it is described Equal radians are uniformly provided with feeding port on annular cradle, and the radians homogeneous vertical such as described annular cradle lower end is equipped with scraper plate.

Description

A kind of high-performance polyphenylene sulfide composite material reaction kettle device
Technical field
The present invention relates to polyphenyl thioether composite materials to produce preparation field, and in particular to a kind of high-performance polyphenylene sulfide is compound Material reaction kettle device.
Background technique
The raw material for preparing of polyphenyl thioether composite material includes solid material and liquid charging stock, the granular size of solid material Can the preparation process of direct poly-p-phenylene sulfide ether composite material impact, solid material may be by long-time storing process Tide, solid material dampness may the preparation of poly-p-phenylene sulfide ether composite material impact, it is prepared by polyphenyl thioether composite material Reaction kettle is often used in the process, and reaction kettle generallys use stirring side in realizing polyphenyl thioether composite material preparation process Formula improves preparation efficiency, and common agitating mode is motor driven agitating shaft, stirring rod realization material stirring, this kind of agitating mode Stirring efficiency is low, and mixing effect is bad, and reaction kettle ontology is inevitably stained with raw material on its inward bottom wall after work Grain, the adherency of feed particles can not only make the reduction of equipment cleaning inside degree, but also will cause the waste of raw material, reaction kettle sheet End solid material import in vivo is usually that fixed position opens up, and raw material imports in reaction kettle ontology it is possible that raw material accumulation is existing The generation of elephant to can interfere to the hybrid reaction of plurality of raw materials, therefore needs a kind of high-performance polyphenylene sulfide multiple now Condensation material reaction kettle device.
Summary of the invention
To solve the above problems, the invention discloses a kind of high-performance polyphenylene sulfide composite material reaction kettle device, it should Grinding and the stirring and drying of solid material may be implemented in device, avoids that solid material particle is excessive, raw material dampness and poly-p-phenylene sulfide The preparation of ether composite material impacts, and realizes the high-efficiency stirring of reaction kettle body interior material, realizes the hand of agitating paddle position How much dynamic regulation regulates and controls the position of agitating paddle according to reaction kettle body interior material quantity to reach best, most efficient stirring Effect realizes that the cleaning of reaction kettle ontology inward bottom wall also reduces original while ensureing reaction kettle body interior cleannes Uniformly introducing for solid material is realized in the waste of material, avoids the generation of raw material packing phenomenon.
In order to reach the goals above, the invention provides the following technical scheme: a kind of high-performance polyphenylene sulfide composite material is used Reaction kettle device, including the reaction kettle ontology that sole plate and sole plate upper end are equipped with, reaction kettle ontology lower end and institute It states and is uniformly provided with support post between sole plate upper end, the reaction kettle body upper end is hollow cylindrical, lower end is Hollow bucket shape, the reaction kettle ontology apical lateral side are equipped with stock cabinet, and side level is equipped in the stock cabinets cavity The stock cabinets cavity is divided into upper guide grinding chamber and lower stirring and drying chamber by interlayer and the interlayer, and the upper guide is ground Mill chamber intracavity bottom is uniformly provided with feed tube, and the upper guide grinding chamber inner cavity upper center is equipped with collecting bin, the upper guide Grinding chamber top middle portion is provided with solid material feeding port, in the lower intracavitary chamber of stirring and drying side and be provided along its length turn Moving axis is uniformly provided with stirring rod in the rotation axis, and reaction kettle ontology top is provided with liquid charging stock feeding port, the reaction Driving assembly is equipped in the middle part of kettle ontology outer top, side is equipped with transmission shaft, the transmission vertically in top in the reaction kettle ontology Axis top is connected with the driving component, bottom end is connected with cross rotating turret, and cross rotating turret lower end is equipped with hand Dynamic agitating paddle regulating and controlling mechanism, the hand operated mixing paddle regulating and controlling mechanism is had by the four side lower part of cross rotating turret Strip groove, be respectively equipped in strip groove screw rod, be respectively equipped in strip groove sliding seat, sliding seat lower end difference Side in lower end is provided in the middle part of the agitating paddle that is fixed with vertically, the cross rotating turret circular groove, circular groove inner cavity The driving gear and one side end part of screw rod length direction being cased on the circular shaft that is movably equipped with vertically, circular shaft are not cased with driven Gear forms, and annular rotating turret is movably equipped on the reaction kettle bodies top inward bottom wall, is set on the inside of the annular rotating turret There is annular cradle, radians is waited uniformly to be provided with feeding port on the annular cradle, the radians such as described annular cradle lower end are equal It is even to be equipped with scraper plate vertically.Scraper plate abutting reaction kettle ontology inward bottom wall is arranged and it is along reaction kettle ontology inward bottom wall vertical direction Shape design, first motor, the second motor are rotating electric machine.
As an improvement of the present invention, the external bottom end of the material-supplying box and the reaction kettle bodies top outer end wall it Between be equipped with support mounting rack, the collecting bin be hollow round table shape and thereon end opening design, lower end be equipped with cover board, it is described to gather materials Storehouse upper end cross-sectional area is greater than its lower end cross-sectional area and is arranged in inverted trapezoidal, and collecting bin inner cavity bottom end is uniformly connected with Guide pipeline and passage way discharging device end is connected with the feed tube upper port respectively, the feed tube is hollow square Shape, horizontal interval is equipped with one group of mixing roll in parallel respectively in the feed tube, distinguishes in the feed tube outer end wall Equipped with first motor and the first motor output shaft puts in the feed tube and is connected with the mixing roll round end for being located at side Connect, the mutual clearance distance of the mixing roll in the feed tube at different location differs, the feed tube lower port with The lower stirring and drying top of chamber inner cavity is connected, and rotation axis length direction one end activity runs through the lower stirring and drying chamber Inner end wall is stretched out and its extension end by shaft coupling is connected with the second motor, and the material-supplying box body outer end wall adds equipped with air Hot device and gas processer, the air heater outlet side are connected by pipeline with the lower stirring and drying bottom of chamber portion inner cavity It is logical, it is provided with exhaust outlet at the top of the lower stirring and drying chamber side and the exhaust outlet passes through pipeline and the gas processer air inlet End is connected, and the gas processer outlet side is connected by pipeline with the air heater inlet end.In feed tube Clearance distance between mixing roll differs, and different degrees of volume solid material grinding may be implemented, and air heater realizes that air adds Heat, gas processer realize the processing of the lower intracavitary export gas of stirring and drying, are respectively equipped with electricity on the inside of guide pipeline feed end Dynamic switch.
As an improvement of the present invention, the reaction kettle ontology center bottom is provided with discharge port, and the solid material is thrown Material mouth, liquid charging stock feeding port inner end are detachable respectively to be equipped with covering plate, and the lower stirring and drying bottom of chamber portion inner cavity passes through Pipeline is connected with reaction kettle ontology top inner cavity, on the inside of the discharge port inner end, lower stirring and drying bottom of chamber portion discharge end It is respectively equipped with electric-controlled switch valve, the driving component includes driving motor, gear reducer and magnetic coupling, the reaction kettle sheet The detachable design of body top end plate, the strip groove mutually lean on proximal end not to be connected with the circular groove respectively, the silk Pole length direction one end is put in the circular groove respectively, and the screw rod puts in end end and is cased with driven gear respectively, The driving gear, driven gear are bevel gear, and the circular shaft lower end is cased with manual frame, the screw rod activity respectively It is arranged through the sliding seat inner cavity, is respectively equipped with connection between the sliding seat through part inner end wall outside the screw rod Component, the connection component are all made of existing screw rod transmission principle art and are designed.Driving gear engages biography with driven gear Dynamic, the rotation of screw rod makes phase of the sliding seat in strip groove length direction back and forth movement, driving assembly by connection component It closes component and transmission connection is realized using the prior art.
As an improvement of the present invention, annular groove, the annular are provided on the reaction kettle bodies top inward bottom wall Rotating turret is movably arranged in the annular groove, and the annular groove opens up position and is located at the reaction kettle bulk solid material inlet position Lower section is set, the annular rotating turret level cross-sectionn inner end diameter is greater than annular cradle level cross-sectionn outer diameter, Radians are waited uniformly to be provided with the first screw hole on the annular rotating turret, equal radians even level is provided with second on the annular cradle Screw rod is screwed in screw hole and second screw hole respectively, it is removable between the scraper plate top and the annular cradle lower end It designs, equal radians homogeneous vertical opens up bayonet, the four side end of cross rotating turret on the annular cradle inward bottom wall It is respectively equipped with fixture block in portion, the reaction kettle ontology top and corresponding annular feeding rack position is provided with rectangle impenetrating mouth, Vertically through inserted with striker plate, the striker plate is located at institute along the transmission rotational axis direction for activity in the rectangle impenetrating mouth State reaction kettle bulk solid material inlet position rear.Screw rod can be screwed into the first screw hole through the second screw hole, the first screw hole, the Two screw hole quantity are two or two or more, and fixture block can be just inserted into bayonet, and bayonet quantity is four, striker plate lower end and annular feeding Frame upper end is mutually touched, scraper plate by screw hole, bolt realize position fastening, reaction kettle ontology top end by screw hole, bolt, The installation of the realization such as nut position.
Compared with the existing technology, the present invention has the advantage that the grinding and stirring of solid material may be implemented in the device Drying, avoid solid material particle is excessive, raw material dampness and the preparation of poly-p-phenylene sulfide ether composite material impacts, mixing roll it Between clearance distance differ, operator's solid material granular size as needed selects corresponding feed tube to realize guide, Mixing roll realizes that solid material is ground, and air heater, gas processer and lower stirring and drying chamber realize hot gas Circular treatment recycles, and economizes on resources, the high efficiency stirring of reaction kettle body interior material may be implemented in the agitating paddle, the scraper plate that are equipped with It mixes, the manual regulation of agitating paddle position may be implemented in the hand operated mixing paddle regulating and controlling mechanism being equipped with, former according to reaction kettle body interior The position of how much regulation agitating paddles of doses is to reach best, most efficient mixing effect, and the scraper plate being equipped with is in supplies The cleaning that reaction kettle ontology inward bottom wall can also be realized while stirring is ensureing the same of reaction kettle body interior cleannes When, the waste of raw material is also reduced, the annular cradle being equipped with realizes uniformly introducing for solid material, avoids raw material packing phenomenon Generation.
Detailed description of the invention
Fig. 1 is a kind of high-performance polyphenylene sulfide composite material reaction kettle device overall structure diagram of the present invention;
Fig. 2 is the stock cabinets cavity structural schematic diagram;
Fig. 3 is the feed tube inner-cavity structure schematic diagram;
Fig. 4 is reaction kettle bodies top inner cavity planar structure schematic diagram;
Fig. 5 is the hand operated mixing paddle regulating and controlling mechanism planar structure schematic diagram;
Fig. 6 is the striker plate position plane schematic diagram;
Reference signs list: 1, sole plate;2, reaction kettle ontology;3, stock cabinet;4, upper guide grinding chamber;5, lower stirring is dried Dry chamber;6, feed tube;7, collecting bin;8, rotation axis;9, stirring rod;10, driving assembly;11, transmission shaft;12, cross rotates Frame;13, hand operated mixing paddle regulating and controlling mechanism;14, strip groove;15, screw rod;16, sliding seat;17, agitating paddle;18, circular groove; 19, circular shaft;20, driving gear;21, driven gear;22, annular rotating turret;23, annular cradle;24, feeding port;25, it scrapes Plate;26, the second motor;27, screw rod;28, bayonet;29, fixture block;30, striker plate.
Specific embodiment
Embodiment 1: referring to Fig. 1, Fig. 2, Fig. 3, Fig. 4, Fig. 5, Fig. 6, now to a kind of high-performance polyphenylene sulfide provided by the invention Ether composite material is illustrated with reaction kettle device, including the reaction kettle ontology 2 that sole plate 1 and 1 upper end of sole plate are equipped with, Support post is uniformly provided between 1 upper end of 2 lower end of reaction kettle ontology and the sole plate, on the reaction kettle ontology 2 End is hollow cylindrical, lower end is hollow bucket shape, and stock cabinet 3, institute are equipped with by 2 apical lateral of reaction kettle ontology It states side level in stock 3 inner cavity of cabinet and is equipped with interlayer and the interlayer and 3 inner cavity of stock cabinet is divided into upper guide grinding Chamber 4 and lower stirring and drying chamber 5, upper 4 intracavity bottom of guide grinding chamber are uniformly provided with feed tube 6, the upper guide grinding chamber 4 Inner cavity upper center is equipped with collecting bin 7, and upper 4 top middle portion of guide grinding chamber is provided with solid material feeding port, stirs under described It mixes side in 5 inner cavity of drying cavity and is provided along its length rotation axis 8, stirring rod 9 is uniformly provided in the rotation axis 8, it is described 2 top of reaction kettle ontology is provided with liquid charging stock feeding port, is equipped with driving assembly 10, institute in the middle part of 2 outer top of reaction kettle ontology State in reaction kettle ontology 2 that side is equipped with transmission shaft 11 vertically in top, 11 top of transmission shaft is connected with the driving component 10 Connect, bottom end is connected with cross rotating turret 12,12 lower end of cross rotating turret be equipped with hand operated mixing paddle regulating and controlling mechanism 13, institute Stating hand operated mixing paddle regulating and controlling mechanism 13 is strip groove 14, the item being had by the 12 4 side lower part of cross rotating turret The sliding seat 16 that is respectively equipped in the screw rod 15 that is respectively equipped in connected in star 14, strip groove 14,16 lower end of sliding seat are erected respectively In circular groove 18 that the agitating paddle 17 that is directly fixed with, 12 middle part lower end of the cross rotating turret are provided with, circular groove 18 The one side end of driving gear 20 and 15 length direction of screw rod being cased on side is movably equipped with vertically in chamber circular shaft 19, circular shaft 19 The driven gear 21 being cased with respectively forms, and is movably equipped with annular rotating turret 22, institute on the 2 inside top end wall of reaction kettle ontology It states and is equipped with annular cradle 23 on the inside of annular rotating turret 22, wait radians to be uniformly provided with feeding port 24 on the annular cradle 23, The radians homogeneous verticals such as 23 lower end of the annular cradle are equipped with scraper plate 25.
Embodiment 2: referring to Fig. 1, Fig. 2, Fig. 3, now to a kind of high-performance polyphenylene sulfide composite material use provided by the invention Reaction kettle device is illustrated, and branch is equipped between 2 top outer end wall of the outer bottom end of the stock cabinet 3 and the reaction kettle ontology Mounting rack is supportted, the collecting bin 7 is hollow round table shape and end opening design thereon, lower end are equipped with cover board, 7 upper end of collecting bin Cross-sectional area is greater than its lower end cross-sectional area and is arranged in inverted trapezoidal, and the 7 inner cavity bottom end of collecting bin is uniformly connected with guide Pipeline and passage way discharging device end is connected with 6 upper port of feed tube respectively, the feed tube 6 is hollow, rectangular Shape, horizontal interval is equipped with one group of mixing roll in parallel respectively in the feed tube 6, distinguishes in 6 outer end wall of feed tube Equipped with first motor and the first motor output shaft puts in the feed tube 6 and is connected with the mixing roll round end for being located at side It connects, the mutual clearance distance of the mixing roll in feed tube 6 at different location differs, 6 lower port of feed tube It is connected with the lower 5 top inner cavity of stirring and drying chamber, 8 length direction one end activity of rotation axis is dried through the lower stirring Dry 5 inner end wall of chamber is stretched out and its extension end by shaft coupling is connected with the second motor 26, is set in 3 outer end wall of stock cabinet There is the gentle body processor of air heater, the air heater outlet side passes through pipeline and lower 5 bottom of stirring and drying chamber Inner cavity is connected, and is provided with exhaust outlet at the top of lower 5 side of stirring and drying chamber and the exhaust outlet passes through pipeline and the gas Processor inlet end is connected, and the gas processer outlet side is connected by pipeline with the air heater inlet end.
Embodiment 3: referring to Fig. 1, Fig. 4, Fig. 5, now to a kind of high-performance polyphenylene sulfide composite material use provided by the invention Reaction kettle device is illustrated, and 2 center bottom of reaction kettle ontology is provided with discharge port, the solid material feeding port, liquid Raw material feeding port inner end is detachable respectively to be equipped with covering plate, and the lower 5 bottom inner cavity of stirring and drying chamber passes through pipeline and institute It states 2 top inner cavity of reaction kettle ontology to be connected, distinguish on the inside of the discharge port inner end, 5 bottom discharge end of lower stirring and drying chamber Equipped with electric-controlled switch valve, the driving component 10 includes driving motor, gear reducer and magnetic coupling, the reaction kettle ontology 2 The detachable design of top end plate, 14 phase of strip groove divides equally by proximal end and is not connected with the circular groove 18, described 15 length direction one end of screw rod is put in respectively in the circular groove 18, the screw rod 15 put in end end be cased with respectively from Moving gear 21, the driving gear 20, driven gear 21 are bevel gear, and 19 lower end of circular shaft is cased with manual frame, institute Stating screw rod 15, activity is arranged through 16 inner cavity of sliding seat respectively, 15 outside of screw rod and 16 through part of sliding seat Connection component is respectively equipped between inner end wall, the connection component is all made of existing screw rod transmission principle art and is designed.
Embodiment 4: referring to Fig. 1, Fig. 4, Fig. 6, now to a kind of high-performance polyphenylene sulfide composite material use provided by the invention Reaction kettle device is illustrated, and annular groove is provided on the 2 inside top end wall of reaction kettle ontology, and the annular rotating turret 22 is living Dynamic to be set in the annular groove, the annular groove opens up position and is located at below the 2 solid material entrance location of reaction kettle ontology, The annular 22 level cross-sectionn inner end diameter of rotating turret is greater than 23 level cross-sectionn outer diameter of the annular cradle, described Equal radians are uniformly provided with the first screw hole on annular rotating turret 22, wait radians even level to be provided with second on the annular cradle 23 Screw rod 27 is screwed in screw hole and second screw hole respectively, between 23 lower end of 25 top of scraper plate and the annular cradle Removable design, equal radians homogeneous vertical opens up bayonet 28, the cross rotation on annular cradle 23 inward bottom wall Fixture block 29,2 top of reaction kettle ontology and the corresponding annular cradle 23 are respectively equipped on 12 4 side end of frame It sets and is provided with rectangle impenetrating mouth, activity is vertically through inserted with striker plate 30 in the rectangle impenetrating mouth, and the striker plate 30 is along institute It states 11 rotation direction of transmission shaft and is located at the 2 solid material entrance location rear of reaction kettle ontology.
The present invention can also be formed in combination with example 1 at least one of described technical characteristic of embodiment 2,3,4 newly Embodiment.
Working principle: solid material is imported in upper guide grinding chamber by solid material feeding port, and solid material falls into collection In feed bin, the corresponding feed tube of artificial selection realizes the grinding export of raw material, and the running of first motor, which drives, is located at grinding for side Grinding roller rotation, which realizes that the grinding of material exports with the mixing roll cooperation running for being located at the other side, between mixing roll Clearance distances etc., the mixing roll that respective clearance distance may be selected in operator realize material grinding.Solid material after grinding It is intracavitary to import lower stirring and drying, the running of the second motor drives rotation axis rotation, and the rotation of rotation axis drives stirring rod rotation, stirs Mix the stirring that bar realizes material.Air heater realizes the importing of the lower intracavitary hot gas of stirring and drying, and gas processer is realized The processing of the lower intracavitary export gas of stirring and drying, realizes that the circular treatment of hot gas recycles, economizes on resources.After stirring and drying Raw material by pipeline import reaction kettle ontology in, liquid charging stock feeding port be used for liquid charging stock importing.Reaction kettle ontology top The detachable design of end plate is held, annular cradle is screwed into realization and annular in the first screw hole through the second screw hole by screw rod and rotates The connection of frame, when reaction kettle ontology top end plate is installed, the fixture block of cross rotating turret end is inserted into bayonet respectively, driving group The running of part drives transmission shaft rotation, and transmission shaft drives the rotation of cross rotating turret, and cross rotating turret is inserted by fixture block to be blocked Annular cradle, annular rotating turret rotation are driven in mouthful, the solid material imported in reaction kettle ontology can fall to annular feeding On frame, material of the annular cradle in rotation thereon can fall to reaction kettle body bottom portion by feeding port, and striker plate runs through The setting of rectangle impenetrating mouth, striker plate are used for the timely removing of material on annular cradle.Annular cradle drives while rotation Scraper plate rotation, scraper plate can also realize the cleaning of reaction kettle ontology inward bottom wall while supplies are stirred reaction, The agitating paddle being equipped with is stirred reaction for reaction kettle body interior raw material.It, can hand before reaction kettle ontology headboard is installation Dynamic manipulator's moving frame rotates so that circular shaft rotation, drives driving gear rotation, driving gear and driven tooth while circular shaft rotates Wheel engaged transmission, so that screw rod be driven to rotate, the rotation of screw rod drives sliding seat along strip groove length side by connection component To back and forth movement, so as to realize the regulation of agitating paddle position.The discharge port being equipped with is used to be stirred the material after reaction Export.
The technical means disclosed in the embodiments of the present invention is not limited only to technological means disclosed in above embodiment, further includes Technical solution consisting of any combination of the above technical features.It should be pointed out that for those skilled in the art For, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also considered as Protection scope of the present invention.

Claims (4)

1. a kind of high-performance polyphenylene sulfide composite material reaction kettle device, including sole plate (1) and sole plate (1) upper end The reaction kettle ontology (2) being equipped with, which is characterized in that between reaction kettle ontology (2) lower end and the sole plate (1) upper end It is uniformly provided with support post, reaction kettle ontology (2) upper end is hollow cylindrical, lower end is hollow bucket shape, described Stock cabinet (3) is equipped with by reaction kettle ontology (2) apical lateral, in stock cabinet (3) inner cavity side level equipped with interlayer and Stock cabinet (3) inner cavity is divided into upper guide grinding chamber (4) and lower stirring and drying chamber (5) by the interlayer, it is described on lead Abrasive lapping chamber (4) intracavity bottom is uniformly provided with feed tube (6), and upper guide grinding chamber (4) the inner cavity upper center, which is equipped with, gathers materials Storehouse (7), upper guide grinding chamber (4) top middle portion are provided with solid material feeding port, in lower stirring and drying chamber (5) inner cavity It side and is provided along its length rotation axis (8), is uniformly provided with stirring rod (9) on the rotation axis (8), the reaction kettle ontology (2) top is provided with liquid charging stock feeding port, is equipped with driving assembly (10) in the middle part of reaction kettle ontology (2) outer top, described anti- Side in kettle ontology (2) interior top is answered to be equipped with vertically transmission shaft (11), transmission shaft (11) top and the driving component (10) Be connected, bottom end is connected with cross rotating turret (12), cross rotating turret (12) lower end equipped with hand operated mixing paddle regulate and control Mechanism (13), the hand operated mixing paddle regulating and controlling mechanism (13) are had by (12) the four side lower part of cross rotating turret Strip groove (14), the screw rod (15) being respectively equipped in strip groove (14), the sliding that is respectively equipped in strip groove (14) Under in the middle part of agitating paddle (17) that seat (16), sliding seat (16) lower end are fixed with vertically respectively, the cross rotating turret (12) The circular groove (18) being provided with, circular shaft (19), the circular shaft that side is movably equipped with vertically in circular groove (18) inner cavity is held to cover on (19) By the driven gear (21) that is not cased with of driving gear (20) and one side end part of screw rod (15) length direction form, it is described anti- It answers and is movably equipped with annular rotating turret (22) on kettle ontology (2) inside top end wall, be equipped with ring on the inside of the annular rotating turret (22) Shape cradle (23), described annular cradle (23) first-class radian are uniformly provided with feeding port (24), the annular cradle (23) The radians homogeneous vertical such as lower end is equipped with scraper plate (25).
2. a kind of high-performance polyphenylene sulfide composite material reaction kettle device according to claim 1, which is characterized in that institute It states and is equipped with support mounting rack between the outer bottom end of stock cabinet (3) and the reaction kettle ontology (2) top outer end wall, it is described to gather materials Storehouse (7) is hollow round table shape and end opening design thereon, lower end are equipped with cover board, and collecting bin (7) upper end cross-sectional area is big It is arranged in its lower end cross-sectional area in inverted trapezoidal, collecting bin (7) the inner cavity bottom end is uniformly connected with guide pipeline and described Passage way discharging device end is connected with the feed tube (6) upper port respectively, and the feed tube (6) is hollow, rectangular shape, institute It states in feed tube (6) that horizontal interval is equipped with one group of mixing roll in parallel respectively, is set respectively in feed tube (6) outer end wall There is first motor and the first motor output shaft puts in the feed tube (6) and is connected with the mixing roll round end for being located at side It connects, the mutual clearance distance of the mixing roll in feed tube (6) at different location differs, under the feed tube (6) Port is connected with inner cavity at the top of the lower stirring and drying chamber (5), and rotation axis (8) length direction one end activity is through described Lower stirring and drying chamber (5) inner end wall is stretched out and its extension end is connected with the second motor (26) by shaft coupling, the stock cabinet (3) outer end wall be equipped with air heater and gas processer, the air heater outlet side by pipeline and it is described under Stirring and drying chamber (5) bottom inner cavity is connected, and is provided with exhaust outlet and the exhaust outlet at the top of lower stirring and drying chamber (5) side It is connected by pipeline with the gas processer inlet end, the gas processer outlet side is added by pipeline and the air Hot device inlet end is connected.
3. a kind of high-performance polyphenylene sulfide composite material reaction kettle device according to claim 1, which is characterized in that institute It states reaction kettle ontology (2) center bottom and is provided with discharge port, the solid material feeding port, liquid charging stock feeding port inner end are distinguished Detachable to be equipped with covering plate, lower stirring and drying chamber (5) the bottom inner cavity passes through pipeline and reaction kettle ontology (2) top Inner cavity is connected, and is respectively equipped with electric-controlled switch valve on the inside of the discharge port inner end, lower stirring and drying chamber (5) bottom discharge end, The driving component (10) includes driving motor, gear reducer and magnetic coupling, and reaction kettle ontology (2) top end plate is removable Formula design is unloaded, the strip groove (14) mutually divides equally by proximal end and is not connected with the circular groove (18), the screw rod (15) Length direction one end is put in respectively in the circular groove (18), the screw rod (15) put in end end be cased with respectively it is driven Gear (21), the driving gear (20), driven gear (21) are bevel gear, and circular shaft (19) lower end is cased with manually Frame, activity is arranged the screw rod (15) through the sliding seat (16) inner cavity respectively, screw rod (15) outside and the cunning It is respectively equipped with connection component between dynamic seat (16) through part inner end wall, the connection component is all made of existing screw rod transmission principle Technology is designed.
4. a kind of high-performance polyphenylene sulfide composite material reaction kettle device according to claim 3, which is characterized in that institute It states and is provided with annular groove on reaction kettle ontology (2) inside top end wall, the annular rotating turret (22) is movably arranged at the annular groove Interior, the annular groove opens up position and is located at below reaction kettle ontology (2) the solid material entrance location, the annular rotating turret (22) level cross-sectionn inner end diameter is greater than annular cradle (23) level cross-sectionn outer diameter, the annular rotating turret (22) first-class radian is uniformly provided with the first screw hole, described annular cradle (23) first-class radian even level be provided with the second screw hole and It is screwed with respectively in second screw hole screw rod (27), between scraper plate (25) top and described annular cradle (23) lower end Removable design, equal radians homogeneous vertical opens up bayonet (28) on described annular cradle (23) inward bottom wall, the cross Rotating turret is respectively equipped with fixture block (29) on (12) four side end, reaction kettle ontology (2) top and the corresponding annular Cradle (23) position is provided with rectangle impenetrating mouth, and activity is vertically through inserted with striker plate (30), institute in the rectangle impenetrating mouth It states after striker plate (30) is located at reaction kettle ontology (2) the solid material entrance location along the transmission shaft (11) rotation direction Side.
CN201910534385.2A 2019-06-20 2019-06-20 Reaction kettle device for high-performance polyphenylene sulfide composite material Active CN110270287B (en)

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