CN110270287B - Reaction kettle device for high-performance polyphenylene sulfide composite material - Google Patents

Reaction kettle device for high-performance polyphenylene sulfide composite material Download PDF

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Publication number
CN110270287B
CN110270287B CN201910534385.2A CN201910534385A CN110270287B CN 110270287 B CN110270287 B CN 110270287B CN 201910534385 A CN201910534385 A CN 201910534385A CN 110270287 B CN110270287 B CN 110270287B
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China
Prior art keywords
reaction kettle
kettle body
annular
stirring
frame
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CN110270287A (en
Inventor
张奇
丁丽娜
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Nanjing Qingyan New Material Research Institute Co ltd
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Nanjing Qingyan New Material Research Institute Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C4/00Crushing or disintegrating by roller mills
    • B02C4/02Crushing or disintegrating by roller mills with two or more rollers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C4/00Crushing or disintegrating by roller mills
    • B02C4/28Details
    • B02C4/42Driving mechanisms; Roller speed control
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B9/00Cleaning hollow articles by methods or apparatus specially adapted thereto
    • B08B9/08Cleaning containers, e.g. tanks
    • B08B9/087Cleaning containers, e.g. tanks by methods involving the use of tools, e.g. brushes, scrapers

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Mechanical Engineering (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

The invention discloses a reaction kettle device for a high-performance polyphenylene sulfide composite material, which comprises a base and a reaction kettle body, wherein a material preparation box body is arranged beside the outer side of the top end of the reaction kettle body, the inner cavity of the material preparation box body is divided into an upper material guiding grinding cavity and a lower stirring drying cavity through a partition layer, a material guiding cylinder and a material collecting bin are arranged in the upper material guiding grinding cavity, a rotating shaft is arranged in the lower stirring drying cavity, stirring rods are uniformly arranged on the rotating shaft, a driving assembly is arranged in the middle of the outer top end of the reaction kettle body, a transmission shaft is vertically arranged on the middle side of the inner top end of the reaction kettle body, the bottom end of the transmission shaft is connected with a cross-shaped rotating frame, a manual stirring paddle regulating mechanism is arranged at the lower end of the cross-shaped rotating frame, an annular rotating frame is movably arranged on the inner side wall of the top inner side of the reaction kettle body, an annular feeding frame is uniformly provided with feeding openings in equal radian, and a scraping plate is uniformly and vertically arranged at the lower end of the annular feeding frame.

Description

Reaction kettle device for high-performance polyphenylene sulfide composite material
Technical Field
The invention relates to the field of production and preparation of polyphenylene sulfide composite materials, in particular to a reaction kettle device for a high-performance polyphenylene sulfide composite material.
Background
The preparation raw materials of the polyphenylene sulfide composite material comprise solid raw materials and liquid raw materials, the particle size of the solid raw materials can directly influence the preparation process of the polyphenylene sulfide composite material, the solid raw materials can be damped in the long-time storage process, the solid raw materials can influence the preparation of the polyphenylene sulfide composite material, the polyphenylene sulfide composite material can be often used in a reaction kettle in the preparation process, the preparation efficiency of the reaction kettle is usually improved in the preparation process of the polyphenylene sulfide composite material by adopting a stirring mode, a stirring shaft and a stirring rod are driven by a motor in the common stirring mode to realize material stirring, the stirring efficiency of the stirring mode is low, the stirring effect is poor, raw material particles are inevitably adhered on the inner side end wall of the reaction kettle body after the reaction kettle is operated, the adhesion of the raw material particles can not only reduce the internal cleanliness of equipment, but also can cause the waste of the raw materials, a solid raw material inlet at the inner end of the reaction kettle body is usually formed in a fixed position, the raw material is led into the reaction kettle body, the raw material can be accumulated, and thus the mixing reaction of various raw materials can be interfered, and therefore the reaction kettle device for the high-performance polyphenylene sulfide composite material is needed.
Disclosure of Invention
In order to solve the problems, the invention discloses a reaction kettle device for a high-performance polyphenylene sulfide composite material, which can grind, stir and dry solid raw materials, avoid the influence on the preparation of the polyphenylene sulfide composite material caused by oversized solid raw material particles and wet raw materials, realize the efficient stirring of materials in a reaction kettle body, realize the manual regulation and control of the position of a stirring paddle, realize the optimal and most efficient stirring effect according to the position of the stirring paddle regulated and controlled according to the amount of the raw materials in the reaction kettle body, realize the cleaning of the inner end wall of the reaction kettle body, reduce the waste of the raw materials while ensuring the cleanliness of the inside of the reaction kettle body, realize the uniform introduction of the solid raw materials and avoid the phenomenon of raw material accumulation.
In order to achieve the above purpose, the present invention provides the following technical solutions: the reaction kettle device for the high-performance polyphenylene sulfide composite material comprises a base seat and a reaction kettle body arranged at the upper end of the base seat, wherein a supporting column is uniformly arranged between the lower end of the reaction kettle body and the upper end of the base seat, the upper end of the reaction kettle body is hollow cylindrical, the lower end of the reaction kettle body is hollow mud bucket-shaped, a material preparation box body is arranged beside the outer side of the top end of the reaction kettle body, an interlayer is horizontally arranged at the middle side of the material preparation box body, the material preparation box body is divided into an upper material guiding grinding cavity and a lower stirring and drying cavity by the interlayer, a material guiding cylinder is uniformly arranged at the bottom of the inner cavity of the upper material guiding grinding cavity, a material collecting bin is arranged in the middle of the upper end of the inner cavity of the upper material guiding grinding cavity, a solid material feeding port is formed in the middle of the top end of the upper material guiding grinding cavity, a rotating shaft is arranged at the middle side of the inner cavity of the lower stirring and drying cavity along the length direction of the lower stirring and a stirring rod is uniformly arranged on the rotating shaft, the top end of the reaction kettle body is provided with a liquid raw material feeding port, the middle part of the outer top end of the reaction kettle body is provided with a driving component, the middle side of the inner top end of the reaction kettle body is vertically provided with a transmission shaft, the top end of the transmission shaft is connected with the driving component, the bottom end of the transmission shaft is connected with a cross rotating frame, the lower end of the cross rotating frame is provided with a manual stirring paddle regulating mechanism, the manual stirring paddle regulating mechanism consists of a strip-shaped groove respectively arranged at the lower end of the four sides of the cross rotating frame, a screw rod respectively arranged in the strip-shaped groove, a sliding seat respectively arranged in the strip-shaped groove, a stirring paddle respectively vertically fixed at the lower end of the sliding seat, a round groove vertically movably arranged at the middle end of the middle part of the cross rotating frame, a driving gear sleeved on the round shaft and a driven gear respectively sleeved at the end part of one side of the length direction of the screw rod, the automatic feeding device is characterized in that an annular rotating frame is movably arranged on the end wall of the inner side of the top of the reaction kettle body, an annular feeding frame is arranged on the inner side of the annular rotating frame, feeding ports are uniformly formed in the annular feeding frame in an equal radian mode, and scraping plates are uniformly and vertically arranged at the lower end of the annular feeding frame in an equal radian mode. The scraping plate is closely attached to the inner side end wall of the reaction kettle body, and the scraping plate is designed along the vertical direction of the inner side end wall of the reaction kettle body, and the first motor and the second motor are rotating motors.
As an improvement of the invention, a supporting installation frame is arranged between the outer bottom end of the material preparation box body and the outer side end wall of the top of the reaction kettle body, the material collection bin is hollow round table-shaped, the upper end opening design and the lower end of the material collection bin are provided with cover plates, the cross section area of the upper end of the material collection bin is larger than that of the lower end of the material collection bin, the bottom end of the inner cavity of the material collection bin is uniformly connected with a material guide pipeline, the discharge end of the material guide pipeline is respectively connected with the upper end opening of the material guide bin, the material guide drums are hollow rectangular, a group of grinding rollers are respectively arranged in the material guide drums at horizontal intervals in parallel, the outer side end walls of the material guide drums are respectively provided with a first motor, the output shafts of the first motors extend into the material guide drums and are connected with the rotating ends of the grinding rollers on one side, the grinding rollers in different positions are mutually spaced, the lower end opening of the material guide drums are communicated with the inner cavity of the top of the lower stirring drying cavity, one end wall in the length direction of the rotation shaft penetrates through the inner end wall of the lower stirring cavity to extend out of the upper end opening of the upper end of the material guide cavity, the motor extends out of the air outlet through the second motor and is connected with the air outlet end of the air heater through the air outlet through the air heater, the air outlet is connected with the air heater through the air outlet end of the air heater, the air heater through the air outlet is connected with the air heater, and the air heater is connected with the air inlet heater through the air heater, and the air heater is connected with the air heater through the air heater, and the air heater. The clearance distance between the grinding rollers in the guide cylinder is unequal, so that grinding of solid raw materials with different degrees can be realized, the air heater realizes air heating, the gas processor realizes treatment of leading-out gas in the lower stirring drying cavity, and the inner sides of the feeding ends of the guide pipelines are respectively provided with an electric switch.
As an improvement of the invention, a discharge opening is arranged in the middle of the bottom end of the reaction kettle body, the inner ends of the solid raw material feed opening and the liquid raw material feed opening are respectively and detachably provided with a cover plate, the bottom inner cavity of the lower stirring and drying cavity is communicated with the top inner cavity of the reaction kettle body through a pipeline, the inner ends of the discharge opening and the inner side of the discharge end of the bottom of the lower stirring and drying cavity are respectively and internally provided with an electric control switch valve, the driving assembly comprises a driving motor, a speed reducer and a magnetic coupler, the end plate at the top end of the reaction kettle body is detachably designed, the adjacent ends of the strip-shaped grooves are respectively communicated with the circular grooves, one ends of the length direction of the lead screw extend into the circular grooves respectively, the end parts of the extending ends of the lead screw are respectively sleeved with driven gears, the driving gears and the driven gears are respectively, the end parts of the lower end part of the circular shaft are sleeved with a manual frame, the lead screw respectively and movably penetrates through the inner cavity of the sliding seat, a connecting assembly is arranged between the outer part of the lead screw and the inner end wall of the sliding seat, and the connecting assembly is uniformly designed by adopting the existing lead screw transmission principle. The driving gear is meshed with the driven gear for transmission, the sliding seat is enabled to reciprocate along the length direction of the strip-shaped groove by the aid of the connecting assembly through rotation of the screw rod, and related components in the driving assembly are in transmission connection through the aid of the prior art.
As an improvement of the invention, an annular groove is formed in the inner side end wall of the top of the reaction kettle body, the annular rotating frame is movably arranged in the annular groove, the annular groove is formed at the position below the solid raw material inlet position of the reaction kettle body, the inner end diameter of the horizontal cross section of the annular rotating frame is larger than the outer end diameter of the horizontal cross section of the annular feeding frame, a first screw hole is uniformly formed in the annular rotating frame in an equal radian mode, a second screw hole is uniformly and horizontally formed in the annular feeding frame in an equal radian mode, screws are respectively screwed into the second screw hole, a detachable design is adopted between the top end of the scraping plate and the lower end of the annular feeding frame, bayonets are uniformly and vertically formed in the equal radian mode in the inner side end wall of the annular feeding frame, clamping blocks are respectively arranged at the four side end parts of the cross-shaped rotating frame, a rectangular through hole is formed in the position corresponding to the top end of the annular feeding frame, a baffle plate is vertically and vertically inserted in the rectangular through hole, and the baffle plate is positioned behind the solid raw material inlet position of the reaction kettle body along the rotation direction of the transmission shaft. The screw rod can run through the second screw and screw into in the first screw, and first screw, second screw quantity are two or more, and the fixture block can just insert in the bayonet socket, and bayonet socket quantity is four, and the striker plate lower extreme collides with annular pay-off frame upper end, and the scraper blade passes through screw, bolt realization position's fastening, and the installation of position is realized through screw, bolt, nut etc. to reation kettle body top tip.
Compared with the prior art, the invention has the following advantages: the device can realize grinding and stirring stoving of solid raw materials, avoid solid raw materials granule too big, the raw materials wets and cause the influence to polyphenylene sulfide combined material's preparation, the clearance distance between the grinding roller is unequal, the operation workman selects corresponding guide cylinder to realize the guide according to the solid raw materials granule size of needs, the grinding roller realizes that solid raw materials grinds the crushing, air heater, gaseous treater and lower stirring stoving chamber realize the cyclic treatment recycling of high-temperature gas, resources are saved, the stirring rake that is equipped with, the scraper blade can realize the high-efficient stirring of the inside material of reation kettle body, manual stirring rake regulation and control mechanism that is equipped with can realize the manual regulation and control of stirring rake position, thereby reach best, most efficient stirring effect according to the inside raw materials's of reation kettle body quantity position regulation stirring rake, the scraper blade that is equipped with still can realize the clearance of reation kettle body inboard end wall when assisting the material stirring, the waste of raw materials has also been reduced in the inside cleanliness of reation kettle body, the annular pay-off frame that is equipped with realizes the even leading-off of solid raw materials, the emergence of phenomenon is piled up to avoid the raw materials.
Drawings
FIG. 1 is a schematic diagram of the overall structure of a reaction kettle device for a high-performance polyphenylene sulfide composite material;
FIG. 2 is a schematic diagram of the internal cavity structure of the stock tank;
FIG. 3 is a schematic view of the inner cavity structure of the guide cylinder;
FIG. 4 is a schematic view of the planar structure of the top cavity of the reactor body;
FIG. 5 is a schematic plan view of the manual paddle control mechanism;
FIG. 6 is a schematic plan view of the striker plate position;
list of reference numerals: 1. a base; 2. a reaction kettle body; 3. a material preparing box body; 4. a material guiding grinding cavity is arranged; 5. a lower stirring and drying cavity; 6. a guide cylinder; 7. a collecting bin; 8. a rotating shaft; 9. a stirring rod; 10. a drive assembly; 11. a transmission shaft; 12. a cross-shaped rotating frame; 13. a manual stirring paddle regulating and controlling mechanism; 14. a strip-shaped groove; 15. a screw rod; 16. a sliding seat; 17. stirring paddles; 18. a circular groove; 19. a circular shaft; 20. a drive gear; 21. a driven gear; 22. an annular rotating frame; 23. an annular feeding frame; 24. a feeding port; 25. a scraper; 26. a second motor; 27. a screw; 28. a bayonet; 29. a clamping block; 30. and a striker plate.
Detailed Description
Example 1: referring to fig. 1, fig. 2, fig. 3, fig. 4, fig. 5, fig. 6, the reaction kettle device for high-performance polyphenylene sulfide composite material provided by the invention is now described, which comprises a base 1 and a reaction kettle body 2 arranged at the upper end of the base 1, support columns are uniformly arranged between the lower end of the reaction kettle body 2 and the upper end of the base 1, the upper end of the reaction kettle body 2 is hollow cylindrical, the lower end is hollow mud bucket-shaped, a material preparation box 3 is arranged beside the outer side of the top end of the reaction kettle body 2, a separation layer is horizontally arranged at the middle side of the inner cavity of the material preparation box 3, the inner cavity of the material preparation box 3 is divided into an upper material guiding grinding cavity 4 and a lower stirring drying cavity 5 by the separation layer, a material guiding cylinder 6 is uniformly arranged at the bottom of the inner cavity of the upper material guiding grinding cavity 4, a material collecting bin 7 is arranged in the middle of the upper end of the inner cavity of the upper material guiding grinding cavity 4, a solid material feeding port is arranged in the middle of the top end of the upper material guiding grinding cavity 4, the inner cavity middle side of the lower stirring and drying cavity 5 is provided with a rotating shaft 8 along the length direction of the rotating shaft 8, stirring rods 9 are uniformly arranged on the rotating shaft 8, a liquid raw material feeding port is formed in the top end of the reaction kettle body 2, a driving assembly 10 is arranged in the middle of the outer top end of the reaction kettle body 2, a transmission shaft 11 is vertically arranged on the middle side of the inner top end of the reaction kettle body 2, the transmission shaft 11 top end is connected with the driving assembly 10, the bottom end is connected with a cross rotating frame 12, a manual stirring paddle regulating mechanism 13 is arranged at the lower end of the cross rotating frame 12, the manual stirring paddle regulating mechanism 13 comprises a strip-shaped groove 14 formed in the lower end of the four side ends of the cross rotating frame 12, a screw rod 15 respectively arranged in the strip-shaped groove 14, a sliding seat 16 respectively arranged in the strip-shaped groove 14, stirring paddles 17 respectively vertically fixed in the lower ends of the sliding seat 16 respectively, circular recess 18 that the lower extreme opened in cross rotating frame 12 middle part is equipped with, circular shaft 19 that the vertical activity of circular recess 18 inner chamber middle side was equipped with, the driving gear 20 that the cover was equipped with on the circular shaft 19 and the driven gear 21 that one side end tip of lead screw 15 length direction was equipped with respectively constitutes, the activity is equipped with annular rotating frame 22 on the inboard end wall in reation kettle body 2 top, annular rotating frame 22 inboard is equipped with annular pay-off frame 23, evenly open with equal radian on annular pay-off frame 23 has pay-off mouth 24, evenly vertically being equipped with scraper blade 25 with equal radian of annular pay-off frame 23 lower extreme.
Example 2: referring to fig. 1, fig. 2, fig. 3, the reaction kettle device for high performance polyphenylene sulfide composite material provided by the invention is now described, a supporting mounting frame is arranged between the outer bottom end of the material preparation box 3 and the outer end wall of the top of the reaction kettle body 2, the material collection bin 7 is hollow round table-shaped, the upper end opening design and the lower end of the material collection bin 7 are provided with cover plates, the cross section area of the upper end of the material collection bin 7 is larger than the cross section area of the lower end of the material collection bin is in inverted trapezoid arrangement, the bottom end of the inner cavity of the material collection bin 7 is uniformly connected with a material guide pipeline, the discharge ends of the material guide pipeline are respectively connected with the upper port of the material guide cylinder 6, the material guide cylinders 6 are hollow rectangular, a group of grinding rollers are respectively arranged in parallel at horizontal intervals in the material guide cylinders 6, a first motor is respectively arranged on the outer end wall of the material guide cylinder 6, the output shaft of the first motor extends into the material guide cylinder 6 to be connected with the rotating ends of the grinding rollers positioned at one side, the clearance distance between the grinding rolls in the guide cylinder 6 at different positions is different, the lower port of the guide cylinder 6 is communicated with the inner cavity at the top of the lower stirring and drying cavity 5, one end of the length direction of the rotating shaft 8 movably penetrates through the inner end wall of the lower stirring and drying cavity 5 and extends out, the extending end of the rotating shaft is connected with a second motor 26 through a coupling, an air heater and a gas processor are arranged on the outer end wall of the material preparation box 3, the air heater air outlet end is communicated with the inner cavity at the bottom of the lower stirring and drying cavity 5 through a pipeline, the top of the side end of the lower stirring and drying cavity 5 is provided with an air outlet, and the air outlet end of the gas processor is communicated with the air inlet end of the air heater through a pipeline.
Example 3: referring to fig. 1, fig. 4 and fig. 5, the reaction kettle device for high-performance polyphenylene sulfide composite materials provided by the invention is now described, a discharge opening is formed in the middle of the bottom end of a reaction kettle body 2, cover plates are respectively and detachably arranged at the inner ends of a solid raw material feeding opening and a liquid raw material feeding opening, the bottom inner cavity of a lower stirring and drying cavity 5 is communicated with the inner cavity of the top end of the reaction kettle body 2 through a pipeline, electric control switch valves are respectively arranged at the inner ends of the discharge opening and the inner side of the discharge end of the bottom of the lower stirring and drying cavity 5, a driving assembly 10 comprises a driving motor, a speed reducer and a magnetic coupler, the end plate at the top end of the reaction kettle body 2 is detachably designed, the adjacent ends of a strip-shaped groove 14 are respectively communicated with a circular groove 18, one end of the length direction of a lead screw 15 is respectively extended into the circular groove 18, driven gears 21 are respectively sleeved at the end parts of the extending ends of the lead screw 15, driving gears 20 and driven gears 21 are respectively bevel gears, a manual frame is sleeved at the end part of the lower end of the circular shaft 19, the lead screw 15 movably penetrates through the inner cavity 16, and a sliding seat 16 is respectively arranged at the end part of the lead screw 16, and the end seat is respectively connected with the end of the lead screw assembly by adopting the prior art, and the principle of the connecting part is respectively.
Example 4: referring to fig. 1, fig. 4, and fig. 6, the reaction kettle device for high-performance polyphenylene sulfide composite material provided by the invention is now described, an annular groove is formed on the inner side end wall of the top of the reaction kettle body 2, the annular rotating frame 22 is movably arranged in the annular groove, the annular groove is arranged below the solid raw material inlet position of the reaction kettle body 2, the diameter of the inner end of the horizontal cross section of the annular rotating frame 22 is larger than the diameter of the outer end of the horizontal cross section of the annular rotating frame 23, a first screw hole is uniformly formed in the annular rotating frame 22 in an equal radian manner, a second screw hole is uniformly and horizontally formed in the annular rotating frame 23 in an equal radian manner, screws 27 are respectively screwed into the second screw holes, a detachable design is adopted between the top end of the scraping plate 25 and the lower end of the annular rotating frame 23, clamping blocks 29 are uniformly and vertically arranged in an equal radian manner on the inner side end wall of the annular rotating frame 23, a rectangular through hole is respectively formed in the four side end of the cross-shaped rotating frame 12, a rectangular through hole is formed in the position of the annular rotating frame 23, a movable through hole is inserted into a movable through hole in the rectangular through hole, a movable through hole is inserted into the rectangular through hole, a baffle plate is inserted into the rectangular through hole in the position of the end 23, and is positioned along the direction of the solid raw material inlet 30, and is positioned along the direction of a material inlet of a transmission shaft 11, and is positioned along the direction of a transmission shaft 30.
The present invention also makes it possible to combine at least one of the technical features described in examples 2, 3, 4 with example 1 to form a new embodiment.
Working principle: the solid raw materials passes through the leading-in material grinding intracavity that goes up of solid raw materials feed inlet, and solid raw materials falls into in the collection silo, and the grinding of raw materials is derived by artifical corresponding guide cylinder of selecting, and the operation of first motor drives the grinding roller that is located one side and rotates, and this grinding roller cooperates the grinding roller that is located the opposite side to operate and realizes the grinding of material and derive, and the clearance distance between the grinding roller is unequal, and the operator can select the grinding roller of corresponding clearance distance to realize the material grinding. The solid raw materials after grinding is led into the lower stirring drying cavity, the operation of the second motor drives the rotation shaft to rotate, the rotation of the rotation shaft drives the stirring rod to rotate, and the stirring rod realizes stirring of materials. The air heater realizes the introduction of high-temperature gas in the lower stirring and drying cavity, the gas processor realizes the treatment of the gas led out from the lower stirring and drying cavity, the recycling treatment and the reutilization of the high-temperature gas are realized, and the resources are saved. The stirred and dried raw materials are led into the reaction kettle body through a pipeline, and a liquid raw material feeding port is used for leading in the liquid raw materials. The detachable design of reation kettle body top end plate, annular pay-off frame runs through the second screw and screws into in the first screw realization and annular rotating frame's connection through the screw, when reation kettle body top end plate installs, the fixture block of cross rotating frame tip inserts in the bayonet socket respectively, drive assembly's operation drives the transmission shaft and rotates, the transmission shaft drives cross rotating frame and rotates, the cross rotating frame inserts in the bayonet socket through the fixture block and drives annular pay-off frame, annular rotating frame rotates, this internal leading-in solid raw materials of reation kettle can drop annular pay-off frame on, annular pay-off frame is its material accessible pay-off mouth drops to reation kettle body bottom when rotating, the striker plate runs through the rectangle through-hole setting, the striker plate is used for the timely clear of material on the annular pay-off frame. The annular feeding frame rotates and drives the scraping plate to rotate, the scraping plate can also clean the inner side end wall of the reaction kettle body when assisting the material stirring and mixing reaction, and the stirring paddles are used for stirring and mixing the raw materials inside the reaction kettle body. Before the reaction kettle body top end plate is installed, the manual frame can be manually operated to rotate so that the round shaft rotates, the round shaft rotates and simultaneously drives the driving gear to rotate, the driving gear is meshed with the driven gear to drive the screw rod to rotate, and the screw rod rotates to drive the sliding seat to reciprocate along the length direction of the strip-shaped groove through the connecting component, so that the position of the stirring paddle can be regulated and controlled. The discharge opening is used for guiding out the materials after the stirring and mixing reaction.
The technical means disclosed by the scheme of the invention is not limited to the technical means disclosed by the embodiment, and also comprises the technical scheme formed by any combination of the technical features. It should be noted that modifications and adaptations to the invention may occur to one skilled in the art without departing from the principles of the present invention and are intended to be within the scope of the present invention.

Claims (1)

1. The utility model provides a high performance is reation kettle device for polyphenylene sulfide combined material, includes reation kettle body (2) that base (1) and base (1) upper end were equipped with, a serial communication port, reation kettle body (2) lower extreme with evenly be equipped with the support post between base (1) upper end, reation kettle body (2) upper end is hollow cylinder, lower tip is cavity mud bucket shape, reation kettle body (2) top outside side is equipped with and prepares workbin (3), prepare workbin (3) inner chamber middle side level be equipped with the interlayer just the interlayer will prepare workbin (3) inner chamber and cut apart into last guide grinding chamber (4) and lower stirring stoving chamber (5), go up guide grinding chamber (4) inner chamber bottom evenly be equipped with guide cylinder (6), go up guide grinding chamber (4) inner chamber upper end middle part and be equipped with collecting vessel (7), go up guide grinding chamber (4) top middle part and open there is solid raw materials feed inlet, lower stirring chamber (5) inner chamber middle side and be equipped with axis of rotation (8) along its length direction, stirring body (2) top (10) are equipped with evenly in the stirring rod (2), stirring kettle (2) top (2) are equipped with top end (10), the automatic feeding device is characterized in that the top end of the transmission shaft (11) is connected with the driving assembly (10), the bottom end of the transmission shaft is connected with the cross-shaped rotating frame (12), a manual stirring paddle regulating mechanism (13) is arranged at the lower end of the cross-shaped rotating frame (12), the manual stirring paddle regulating mechanism (13) consists of a strip-shaped groove (14) respectively arranged at the lower end of the four side ends of the cross-shaped rotating frame (12), a screw rod (15) respectively arranged in the strip-shaped groove (14), a sliding seat (16) respectively arranged in the strip-shaped groove (14), stirring paddles (17) vertically fixed at the lower end of the sliding seat (16) respectively, a circular groove (18) vertically arranged at the middle end of the cross-shaped rotating frame (12), a circular shaft (19) vertically arranged at the middle end of the inner cavity of the circular groove (18), a driving gear (20) sleeved on the circular shaft (19) and a driven gear (21) respectively sleeved at the end part at one side of the length direction of the screw rod (15), an annular rotating frame (22) is movably arranged on the end wall at the inner side of the top of the reaction kettle body (2), an annular rotating frame (23) is arranged at the inner side of the annular rotating frame (22), an annular feeding frame (23) is arranged, an arc-shaped frame (23) is uniformly arranged at the inner side of the annular frame (23), and the annular frame (23) is uniformly provided with an arc-shaped feeding end (25), and the like;
a supporting installation frame is arranged between the outer bottom end of the material preparation box body (3) and the outer end wall of the top of the reaction kettle body (2), the material collection bin (7) is hollow round table-shaped, the upper end of the material collection bin is provided with an opening, the lower end of the material collection bin is provided with a cover plate, the cross section area of the upper end of the material collection bin (7) is larger than that of the lower end of the material collection bin, the cross section area of the upper end of the material collection bin is in an inverted trapezoid shape, the bottom end of the inner cavity of the material collection bin (7) is uniformly connected with a material guide pipeline, the discharge ends of the material guide pipeline are respectively connected with the upper port of the material guide cylinder (6), the material guide cylinders (6) are hollow rectangular, a group of grinding rollers are respectively arranged in parallel at horizontal intervals in the material guide cylinders (6), the utility model discloses a stirring and drying device, which is characterized in that a first motor is respectively arranged on the outer side end wall of a guide cylinder (6), the output shaft of the first motor extends into the guide cylinder (6) and is connected with the rotating end of a grinding roller positioned at one side, the clearance distances between the grinding rollers positioned in the guide cylinders (6) at different positions are different, the lower port of the guide cylinder (6) is communicated with the inner cavity at the top of a lower stirring and drying cavity (5), one end of the length direction of a rotating shaft (8) movably penetrates through the inner end wall of the lower stirring and drying cavity (5) and extends out, the extending end of the rotating shaft is connected with a second motor (26) through a coupling, an air heater and a gas processor are arranged on the outer side end wall of a spare box (3), the air heater outlet end is communicated with the inner cavity at the bottom of the lower stirring and drying cavity (5) through a pipeline, the top of the side end of the lower stirring drying cavity (5) is provided with an exhaust port which is communicated with the air inlet end of the gas processor through a pipeline, and the air outlet end of the gas processor is communicated with the air inlet end of the air heater through a pipeline;
the middle part of the bottom end of the reaction kettle body (2) is provided with a discharge opening, the inner ends of the solid raw material feed opening and the liquid raw material feed opening are respectively and detachably provided with a cover plate, the bottom inner cavity of the lower stirring and drying cavity (5) is communicated with the top inner cavity of the reaction kettle body (2) through a pipeline, the inner ends of the discharge opening and the inner side of the bottom discharge end of the lower stirring and drying cavity (5) are respectively provided with an electric control switch valve, the driving assembly (10) comprises a driving motor, a speed reducer and a magnetic coupler, the end plate of the top end of the reaction kettle body (2) is detachably designed, the adjacent ends of the strip-shaped grooves (14) are respectively communicated with the circular grooves (18), one ends of the length direction of the screw rods (15) are respectively stretched into the circular grooves (18), the end parts of the stretching ends of the screw rods (15) are respectively sleeved with driven gears (21), the driving gears (20) and the driven gears (21) are respectively, the lower end parts of the circular shafts (19) are respectively sleeved with a manual frame, the screw rods (15) movably penetrate through the inner cavities (16) and are respectively provided with a sliding seat (16), and the inner end parts (16) are respectively connected with the sliding seat, and the inner end parts are respectively by adopting the existing sliding seat and the principle;
the novel reaction kettle comprises a reaction kettle body (2), and is characterized in that an annular groove is formed in the inner side end wall of the top of the reaction kettle body (2), an annular rotating frame (22) is movably arranged in the annular groove, the annular groove is formed in the position below the inlet position of solid raw materials in the reaction kettle body (2), the inner end diameter of the horizontal cross section of the annular rotating frame (22) is larger than the outer end diameter of the horizontal cross section of the annular feeding frame (23), a first screw hole is uniformly formed in the upper equal radian of the annular rotating frame (22), a second screw hole is uniformly formed in the upper equal radian of the annular feeding frame (23), screws (27) are respectively screwed into the second screw hole, a bayonet (28) is uniformly and vertically formed in the inner side end wall of the annular feeding frame (23), clamping blocks (29) are uniformly and vertically formed in the end parts of the four sides of the annular rotating frame (12), rectangular through holes are uniformly formed in the positions of the annular feeding frame (22), a movable through hole is vertically inserted into a movable through plate (30) in the rectangular through hole, and a transmission shaft (30) is positioned in the position of the reaction kettle body (2) along the direction of the inlet position of the solid raw materials.
CN201910534385.2A 2019-06-20 2019-06-20 Reaction kettle device for high-performance polyphenylene sulfide composite material Active CN110270287B (en)

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