CN110257176A - A kind of silicon material degumming cleaning agent - Google Patents

A kind of silicon material degumming cleaning agent Download PDF

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Publication number
CN110257176A
CN110257176A CN201910693746.8A CN201910693746A CN110257176A CN 110257176 A CN110257176 A CN 110257176A CN 201910693746 A CN201910693746 A CN 201910693746A CN 110257176 A CN110257176 A CN 110257176A
Authority
CN
China
Prior art keywords
cleaning agent
silicon material
degumming
degumming cleaning
material degumming
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910693746.8A
Other languages
Chinese (zh)
Inventor
孟闯
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jinzhou Zhongertai Industrial Co Ltd
Original Assignee
Jinzhou Zhongertai Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jinzhou Zhongertai Industrial Co Ltd filed Critical Jinzhou Zhongertai Industrial Co Ltd
Priority to CN201910693746.8A priority Critical patent/CN110257176A/en
Publication of CN110257176A publication Critical patent/CN110257176A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02Anionic compounds
    • C11D1/12Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/22Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
    • C11D3/2006Monohydric alcohols
    • C11D3/201Monohydric alcohols linear
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
    • C11D3/2006Monohydric alcohols
    • C11D3/2034Monohydric alcohols aromatic
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
    • C11D3/2041Dihydric alcohols
    • C11D3/2044Dihydric alcohols linear
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2075Carboxylic acids-salts thereof
    • C11D3/2079Monocarboxylic acids-salts thereof
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/24Organic compounds containing halogen

Abstract

The invention discloses a kind of silicon material degumming cleaning agent, specially cleaning agent technical field.The silicon material degumming cleaning agent includes following materials in percentage by mass: ethylene glycol 2%-7%, dehydrated alcohol 2%-7%, formic acid 2%-7%, methylene chloride 70-90%, phenol 2-5%, neopelex 2-4%.Using degumming agent degumming may be implemented high-volume, low consumption, employment it is few, without heating, without external force, the thorough advantage of degumming, to realize the purpose that scouring processes processing cost declines to a great extent.

Description

A kind of silicon material degumming cleaning agent
Technical field
The present invention relates to a kind of silicon material degumming cleaning agent, specially cleaning agent technical field.
Background technique
Sheet is sliced in remained on surface bar glue and resin mass, such impurity is removed and generally uses " high temperature boiling ", " high temperature Fire is roasting " etc. modes.Except the cost is relatively high for glue, degumming, mainly power consumption, gas consumption (acetylene) and cost of labor are higher.And Day processing yield is small, and traditional approach mentions that produce a possibility that big smaller, can not achieve high-volume degumming, except glue a possibility that.And Degumming quality and it is subsequent wash material processing in terms of there is also defective products such as " missing inspections " under pass the problem of.Therefore, in order to realize Batch degumming, remove glue, reduce production cost, completely remove silicon material remained on surface glue impurity, need using degumming agent quickly, batch It measures, completely remove glue impurity.
The shortcomings that existing degumming mode " high temperature boiling ": the big power consumption cost of electricity consumption is high, needs to go using external force after degumming Except surface viscose, and such scouring processes need special messenger's completion, generally require 2-4 completion, and personnel cost increases. Realize that the feasibility produced in enormous quantities is smaller.
The shortcomings that existing degumming mode " high temp fire is roasting ": acetylene or other gases roasting glue repeatedly are used, glue pyrocarbon is made Change, can generate a large amount of flue gases, sucking flue gas is larger to personal injury, and acetylene etc. can hot gas price it is higher, after degumming Fouling can be formed in silicon material surface again, need special messenger to complete the removing to fouling, and such fouling can clean the silicon material in later period The drawbacks of forming rejected product, remaining by mainly impurity, generally requires 2-4 people's completion, and personnel cost increases.Realize high-volume The feasibility of production is smaller.
Summary of the invention
The purpose of the present invention is to provide a kind of silicon material degumming cleaning agent.
To achieve the above object, the invention provides the following technical scheme: a kind of silicon material degumming cleaning agent includes following quality Percentage raw material: ethylene glycol 2%-7%, dehydrated alcohol 2%-7%, formic acid 2%-7%, methylene chloride 70-90%, phenol 2-5%, 12 Sodium alkyl benzene sulfonate 2-4%.
Further preferably, the silicon material degumming cleaning agent includes following materials in percentage by mass: ethylene glycol 5%, anhydrous Ethyl alcohol 5%, formic acid 5%, methylene chloride 76%, phenol 5%, neopelex 4%.
Preferably, the ethylene glycol specific gravity range is 1.111-1.115.
Preferably, ethanol content >=99.7% in the dehydrated alcohol.
Preferably, active matter content >=35.0% in the neopelex.
Compared with prior art, beneficial effects of the present invention are as follows: high-volume may be implemented using degumming agent degumming, low disappear Consumption, employment is few, is not necessarily to heating, is not necessarily to external force, the thorough advantage of degumming, to realize what scouring processes processing cost declined to a great extent Purpose.
Detailed description of the invention
Status diagram after Fig. 1 impregnates resin mass 17 hours for degumming agent in the embodiment of the present invention;
Fig. 2 is that resin is dissolved into fritter status diagram in impregnating in the embodiment of the present invention;
Fig. 3 is the most of separate state diagram of interlayer sheet (having larger gap) in impregnating in the embodiment of the present invention;
Fig. 4 is state after impregnating 24 hours in the embodiment of the present invention, with the undivided separate state diagram in small angle part;
Fig. 5 is that serious interlayer sheet starts fragmentation status diagram in impregnating in the embodiment of the present invention.
Specific embodiment
Technical solution of the present invention is clearly and completely described below in conjunction in the embodiment of the present invention, it is clear that institute The embodiment of description is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, Every other embodiment obtained by those of ordinary skill in the art without making creative efforts, belongs to this hair The range of bright protection.
Embodiment 1
A kind of silicon material degumming cleaning agent includes following materials in percentage by mass: ethylene glycol 7%, dehydrated alcohol 4%, formic acid 7%, dichloro Methane 73%, phenol 5%, neopelex 4%.
Embodiment 2
A kind of silicon material degumming cleaning agent includes following materials in percentage by mass: ethylene glycol 5%, dehydrated alcohol 5%, formic acid 5%, dichloro Methane 76%, phenol 5%, neopelex 4%.
Embodiment 3
A kind of silicon material degumming cleaning agent includes following materials in percentage by mass: ethylene glycol 7%, dehydrated alcohol 7%, formic acid 6%, dichloro Methane 72%, phenol 4%, neopelex 4%.
It adopts degumming agent prepared with embodiment 3 and impregnates resin block, interlayer sheet 5, the shape after recording the time and impregnating State is as follows:
17 hours states: the floating material of a large amount of resins for dissolving, decomposing, sticklac is had already appeared in bucket.State is referring to 1 institute of attached drawing Show,
Resin monolithic has been completely separated, and resin is dissolved into fritter, referring to Fig. 2
Interlayer sheet (having larger gap) largely separates, and having small angle part, there are also adhesions, cracks, referring to Fig. 3
Synusia (serious seamless interlayer sheet) does not separate, but edge has begun dissolution and loosens.
State after impregnating 24 hours has been separated with small angle part is undivided, referring to Fig. 4
Serious interlayer sheet starts fragmentation, and sticklac beginning is decomposed, is detached from, referring to Fig. 5
Be exactly above decomposition of the degumming agent to different sheet stocks, degumming state, in 16 hours, resin, category of glass monolithic can be with It completely disengages, decompose, and can be with mass disposal, within 24 hours -30 hours, not serious interlayer sheet can take off completely From, decompose, can also be with mass disposal.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (5)

1. a kind of silicon material degumming cleaning agent, it is characterised in that: the silicon material degumming cleaning agent includes that following mass percent is former Material: ethylene glycol 2%-7%, dehydrated alcohol 2%-7%, formic acid 2%-7%, methylene chloride 70-90%, phenol 2-5%, detergent alkylate sulphur Sour sodium 2-4%.
2. a kind of silicon material degumming cleaning agent according to claim 1, it is characterised in that: the silicon material degumming cleaning agent packet Containing following materials in percentage by mass: ethylene glycol 5%, dehydrated alcohol 5%, formic acid 5%, methylene chloride 76%, phenol 5%, dodecyl Benzene sulfonic acid sodium salt 4%.
3. a kind of silicon material degumming cleaning agent according to claim 1, it is characterised in that: the ethylene glycol specific gravity range is 1.111-1.115。
4. a kind of silicon material degumming cleaning agent according to claim 1, it is characterised in that: ethyl alcohol contains in the dehydrated alcohol Amount >=99.7%.
5. a kind of silicon material degumming cleaning agent according to claim 1, it is characterised in that: the neopelex Middle active matter content >=35.0%.
CN201910693746.8A 2019-07-30 2019-07-30 A kind of silicon material degumming cleaning agent Pending CN110257176A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910693746.8A CN110257176A (en) 2019-07-30 2019-07-30 A kind of silicon material degumming cleaning agent

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910693746.8A CN110257176A (en) 2019-07-30 2019-07-30 A kind of silicon material degumming cleaning agent

Publications (1)

Publication Number Publication Date
CN110257176A true CN110257176A (en) 2019-09-20

Family

ID=67912274

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910693746.8A Pending CN110257176A (en) 2019-07-30 2019-07-30 A kind of silicon material degumming cleaning agent

Country Status (1)

Country Link
CN (1) CN110257176A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112376060A (en) * 2020-10-26 2021-02-19 中锗科技有限公司 Germanium single crystal slice degumming agent and degumming method thereof
CN112620233A (en) * 2020-12-23 2021-04-09 孟闯 Cleaning method of sheet degumming agent
CN112852564A (en) * 2021-01-08 2021-05-28 孟闯 Silicon material cleaning agent and cleaning method

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101173156A (en) * 2007-09-27 2008-05-07 夏晓军 Conductive adhesive degumming agent and use method of the degumming agent
CN108865463A (en) * 2018-08-14 2018-11-23 上海应用技术大学 A kind of room temperature glue cleaning agent and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101173156A (en) * 2007-09-27 2008-05-07 夏晓军 Conductive adhesive degumming agent and use method of the degumming agent
CN108865463A (en) * 2018-08-14 2018-11-23 上海应用技术大学 A kind of room temperature glue cleaning agent and preparation method thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112376060A (en) * 2020-10-26 2021-02-19 中锗科技有限公司 Germanium single crystal slice degumming agent and degumming method thereof
CN112376060B (en) * 2020-10-26 2022-03-29 中锗科技有限公司 Germanium single crystal slice degumming agent and degumming method thereof
CN112620233A (en) * 2020-12-23 2021-04-09 孟闯 Cleaning method of sheet degumming agent
CN112852564A (en) * 2021-01-08 2021-05-28 孟闯 Silicon material cleaning agent and cleaning method

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Application publication date: 20190920

RJ01 Rejection of invention patent application after publication