CN110251992A - A kind of sand core chromatographic column - Google Patents

A kind of sand core chromatographic column Download PDF

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Publication number
CN110251992A
CN110251992A CN201910451948.1A CN201910451948A CN110251992A CN 110251992 A CN110251992 A CN 110251992A CN 201910451948 A CN201910451948 A CN 201910451948A CN 110251992 A CN110251992 A CN 110251992A
Authority
CN
China
Prior art keywords
shell
inner tube
tube
sand core
outlet
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910451948.1A
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Chinese (zh)
Inventor
刘青
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jianhu Zhiyue Glass Instrument Co Ltd
Original Assignee
Jianhu Zhiyue Glass Instrument Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jianhu Zhiyue Glass Instrument Co Ltd filed Critical Jianhu Zhiyue Glass Instrument Co Ltd
Priority to CN201910451948.1A priority Critical patent/CN110251992A/en
Publication of CN110251992A publication Critical patent/CN110251992A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/10Selective adsorption, e.g. chromatography characterised by constructional or operational features

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  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)

Abstract

The present invention relates to experiment equipment technical fields, and disclose a kind of sand core chromatographic column, including tube body, screen pipe, outlet end and the outlet tube set gradually from top to bottom, the tube body includes the shell one of transparent plastic and the inner tube one inside shell one and for glass, the outlet end includes the shell two of transparent plastic and the inner tube two inside shell two and for glass, said inner tube two is connected to outlet tube, the screen pipe is disposed in proximity at outlet end, and the outlet end is connected with tube body by screen pipe, is connect below the outlet end with outlet tube.When sand core damage, or when needing to change sand core according to experiment demand, it is not necessary to which integral replacing only needs to change screen pipe;Gasket prevents internal liquid to overflow outward, ensure that leakproofness;Screen pipe and tube body, outlet end outer ring maintain an equal level, not lofty, improve globality and aesthetics.

Description

A kind of sand core chromatographic column
Technical field
The present invention relates to experiment equipment technical field, specially a kind of sand core chromatographic column.
Background technique
Existing sand core chromatographic column, generally use by glass sand plate sintering on glass tube, the filter hole of glass sand plate it is big It is small, before sintering it has been determined that just can not change after being sintered into finished product, when tube body damage, need to change entire chromatography Column, or when the blocking of glass sand plate, not easy cleaning.
In the prior art, there is a kind of sand core changeable type glass chromatography column, by upper and lower flange by filter device When connecting, but connecting by the method, upper and lower flange need to be bolted, process is relatively complicated, while flange is outside Protrusion, also affects the overall beautiful of chromatographic column.
Summary of the invention
(1) the technical issues of solving
In view of the deficiencies of the prior art, the present invention provides a kind of sand core chromatographic columns, to realize that sand core is replaceable, cleans, And globality, the function of good airproof performance.
(2) technical solution
To achieve the above object, the invention provides the following technical scheme: a kind of sand core chromatographic column, including from top to bottom according to Tube body, screen pipe, outlet end and the outlet tube of secondary setting, the tube body include transparent plastic shell one and be located at shell One inside and be glass inner tube one, the outlet end includes the shell two of transparent plastic and positioned at the inside of shell two and is The inner tube two of glass, said inner tube two are connected to outlet tube, and the screen pipe is disposed in proximity at outlet end, and the liquid out End is connected with tube body by screen pipe, is connect below the outlet end with outlet tube.
Preferably, the shell one and the top of inner tube one maintain an equal level, and the lower end of said inner tube one extends downwardly and is located at outer The upper end of the downside of shell one, said inner tube two upwardly extends and is located at the upside of shell two, said inner tube one, said inner tube two Elongated end periphery be arranged with plastic sheath, the plastic sheath is externally provided with external screw thread.
Preferably, the screen pipe includes the shell three of transparent plastic, be arranged in shell three and transparent sealing Pad, the glass collar being connect with gasket and the sand core being arranged in glass collar;The gasket is integrally formed comprising one Vertical pad and two lateral pads that are perpendicular and extending to the center of circle, the outside vertically padded and shell three bond, the glass Glass circle is fastened between two lateral pads.
Preferably, the vertical pad inside of the gasket is equipped with the matched internal screw thread of external screw thread with plastic sheath, the glass The wall thickness of glass circle be said inner tube one, the plastic sheath wall thickness summation, while being also the wall thickness of inner tube two and plastic sheath Summation, the tube body, the outlet end are realized by the internal screw thread on the external screw thread and gasket on plastic sheath and screen pipe Connection, and be fully connected the bottom end of rear said inner tube one, the top of said inner tube two press up against glass collar up and down Side.
Preferably, the upper end of the outlet tube is S-type, the laterally setting and to extension of the middle part of the outlet tube S type part Stretch to form cock chamber, be connected with cock on the cock chamber, the cock control outlet end, outlet tube closure be connected to.
Preferably, the tube body upper end is inserted with bottle cap.
(3) beneficial effect
Compared with prior art, the present invention provides a kind of sand core chromatographic column, beneficial effect is:
1, when sand core damages, or when needing to change sand core according to experiment demand, it is not necessary to which integral replacing only needed to change Chimney filter.
2, the shell one of tube body, inner tube one, the shell two of outlet end, inner tube two, shell three, the gasket of screen pipe are equal For transparence, it is easy to observe internal chromatography situation.
3, by being arranged plastic sheath in the outside of inner tube one, inner tube two, external screw thread is equipped on the outside of plastic sheath, in shell three Equipped with gasket, gasket inside is equipped with internal screw thread, it can be achieved that the connection of tube body, screen pipe, outlet end, installation and removal are more Add conveniently, and inner tube one, glass collar, inner tube two abut after connection, realizes the connection of glass tube, while gasket prevents Internal liquid overflows outward, ensure that leakproofness.
4, screen pipe and tube body, outlet end outer ring maintain an equal level, not lofty, improve globality and aesthetics.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention;
Fig. 2 is the broken away view of Fig. 1;
Fig. 3 is the enlarged drawing at the A of Fig. 2;
Fig. 4 is the cross-sectional view of Fig. 1;
Fig. 5 is the cross-sectional view of screen pipe of the invention;
Fig. 6 is the broken away view of Fig. 5;
In figure: 1- tube body, 11- shell one, 12- inner tube one, 2- screen pipe, 21- shell three, 22- gasket, 221- are perpendicular To pad, 222- lateral pad, 223- internal screw thread, 23- glass collar, 24- sand core, 3- outlet end, 31- shell two, 32- inner tube two, 4- Outlet tube, 41- cock chamber, 5- plastic sheath, 51- external screw thread, 6- cock.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts it is all its His embodiment, shall fall within the protection scope of the present invention.
Please refer to Fig. 1-6, a kind of sand core chromatographic column, including tube body 1, screen pipe 2, the out liquid set gradually from top to bottom End 3 and outlet tube 4, tube body 1 include the shell 1 of transparent plastic and the inner tube one inside shell 1 and for glass 12, outlet end 3 includes the shell 2 31 of transparent plastic and the inner tube 2 32 inside shell 2 31 and for glass, inner tube 2 32 are connected to outlet tube 4, and screen pipe 2 is disposed in proximity at outlet end 3, and outlet end 3 and tube body 1 are connected by screen pipe 2 It connects, 3 lower section of outlet end is connect with outlet tube 4;The upper end of outlet tube 4 is S-type, and the middle part of the S type part of outlet tube 4 is laterally set Cock chamber 41 is set and extended outward to form, is connected with cock 6 on cock chamber 41, cock 6 controls outlet end 3, outlet tube 4 closes It closes and is connected to.
The top of shell 1 and inner tube 1 maintains an equal level, and the lower end of inner tube 1 extends downwardly and is located at shell 1 The upper end of downside, inner tube 2 32 upwardly extends and is located at the upside of shell 2 31, inner tube 1, inner tube 2 32 elongated end outside It encloses and is arranged with plastic sheath 5, plastic sheath 5 is externally provided with external screw thread 51.
The shell 3 21 of screen pipe 2 including transparent plastic, be arranged in shell 3 21 and transparent gasket 22, with The glass collar 23 and the sand core 24 being arranged in glass collar 23 that gasket 22 connects;Gasket 22 is integrally formed comprising one Vertical pad 221 and two lateral pads 222 that are perpendicular and extending to the center of circle, the outside of vertical pad 221 and shell 3 21 are viscous Knot, glass collar 23 are fastened between two lateral pads 222.The outer spiral shell with plastic sheath is equipped on the inside of the vertical pad 221 of gasket 22 The matched internal screw thread 223 of line 51, the wall thickness of glass collar 23 be said inner tube 1, plastic sheath 5 wall thickness summation, while For the summation of inner tube 2 32 and the wall thickness of plastic sheath 5, tube body 1, outlet end 3 by the external screw thread 51 on plastic sheath 5 and are sealed Internal screw thread 223 on pad 22 realizes the connection with screen pipe 2, and is fully connected the top of the bottom end of rear inner tube 1, inner tube 2 32 End presses up against the upper and lower sides of glass collar 23.
Above-mentioned sand core chromatographic column, by being arranged plastic sheath 5, plastics in the outside of one 12 lower end of inner tube, 2 32 upper end of inner tube 5 outside of set is equipped with external screw thread 51, and gasket 22 is equipped in shell 3 21, be equipped with internal screw thread 223 on the inside of gasket 22, it can be achieved that The connection of tube body 1, screen pipe 2, outlet end 3, installation and removal are more convenient, and inner tube 1, glass collar, inner tube after connection 2 32 abut, and realize the connection of glass tube, while gasket 22 prevents internal liquid to overflow outward, ensure that leakproofness. During actual experiment, acid solution can be encountered, the material of acid-alkali-corrosive-resisting can be used in gasket 22, since vitreum connects It is logical, in addition the setting of gasket 22, can prevent corrosion external shell and other equipment.
When sand core 24 damages, or when needing to change sand core according to experiment demand, it is not necessary to which integral replacing only needed to change Chimney filter 2.In manufacturer's production, various types of screen pipes can be produced according to the different size in sand core aperture, with Adapt to different experiment demands.
In the present invention, the shell 1 of tube body 1, inner tube 1, the shell 2 31 of outlet end 3, inner tube 2 32, filtering Shell 3 21, the gasket 22 of pipe 2 are transparence, are easy to observe internal chromatography situation.And screen pipe 2 and tube body 1, go out 3 outer ring of liquid end maintains an equal level, not lofty, improves globality and aesthetics.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality Body or operation are distinguished with another entity or operation, without necessarily requiring or implying between these entities or operation There are any actual relationship or orders.Moreover, the terms "include", "comprise" or its any other variant are intended to Cover non-exclusive inclusion, so that the process, method, article or equipment for including a series of elements not only includes that A little elements, but also including other elements that are not explicitly listed, or further include for this process, method, article or The intrinsic element of equipment.In the absence of more restrictions, the element limited by sentence "including a ...", not There is also other identical elements in the process, method, article or apparatus that includes the element for exclusion.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (6)

1. a kind of sand core chromatographic column, it is characterised in that: including tube body (1), screen pipe (2), the out liquid set gradually from top to bottom Hold (3) and outlet tube (4), the tube body (1) include the shell one (11) of transparent plastic and be located inside shell one (11) and For the inner tube one (12) of glass, the outlet end (3) includes the shell two (31) of transparent plastic and is located in shell two (31) Portion and be glass inner tube two (32), said inner tube two (32) is connected to outlet tube (4), and the screen pipe (2) is disposed in proximity to At outlet end (3), and the outlet end (3) and tube body (1) are connected by screen pipe (2), outlet end (3) lower section and liquid out Manage (4) connection.
2. a kind of sand core chromatographic column according to claim 1, it is characterised in that: the shell one (11) and inner tube one (12) Top maintain an equal level, the lower end of said inner tube one (12) extends downwardly and is located at the downside of shell one (11), said inner tube two (32) Upper end upwardly extend and be located at the upside of shell two (31), said inner tube one (12), said inner tube two (32) elongated end outside It encloses and is arranged with plastic sheath (5), the plastic sheath (5) is externally provided with external screw thread (51).
3. a kind of sand core chromatographic column according to claim 2, it is characterised in that: the screen pipe (2) includes transparent plastic Shell three (21), glass collar setting in shell three (21) and transparent gasket (22), connect with gasket (22) (23) and sand core (24) in glass collar (23) is set;The gasket (22) is integrally formed comprising a vertical pad (221) and it is perpendicular and to the center of circle extend two laterally pad (222), it is described it is vertical pad (221) outside and shell three (21) it bonds, the glass collar (23) is fastened on two and laterally pads between (222).
4. a kind of sand core chromatographic column according to claim 3, it is characterised in that: the vertical pad of the gasket (22) (221) inside is equipped with external screw thread (51) matched internal screw thread (223) with plastic sheath, and the wall thickness of the glass collar (23) is described Inner tube one (12), the plastic sheath (5) wall thickness summation, while also for inner tube two (32) and plastic sheath (5) wall thickness it is total With the tube body (1), the outlet end (3) pass through the interior spiral shell on the external screw thread (51) and gasket (22) on plastic sheath (5) Line (223) realizes the connection with screen pipe (2), and is fully connected the bottom end of rear said inner tube one (12), said inner tube two (32) Top press up against the upper and lower sides of glass collar (23).
5. a kind of sand core chromatographic column according to claim 1, it is characterised in that: the upper end of the outlet tube (4) is S-type, The middle part of outlet tube (4) S type part is laterally arranged and extends outward to form cock chamber (41), connects on the cock chamber (41) Be connected to cock (6), the cock (6) control outlet end (3), outlet tube (4) closure be connected to.
6. a kind of sand core chromatographic column according to claim 1, it is characterised in that: tube body (1) upper end is inserted with bottle cap.
CN201910451948.1A 2019-05-28 2019-05-28 A kind of sand core chromatographic column Pending CN110251992A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910451948.1A CN110251992A (en) 2019-05-28 2019-05-28 A kind of sand core chromatographic column

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910451948.1A CN110251992A (en) 2019-05-28 2019-05-28 A kind of sand core chromatographic column

Publications (1)

Publication Number Publication Date
CN110251992A true CN110251992A (en) 2019-09-20

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Application Number Title Priority Date Filing Date
CN201910451948.1A Pending CN110251992A (en) 2019-05-28 2019-05-28 A kind of sand core chromatographic column

Country Status (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112630355A (en) * 2020-11-23 2021-04-09 江苏同济分析仪器有限公司 Enrichment column of liquid chromatograph

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN206444245U (en) * 2016-12-27 2017-08-29 杜马司仪器(上海)有限公司 A kind of core changeable type glass chromatography column

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN206444245U (en) * 2016-12-27 2017-08-29 杜马司仪器(上海)有限公司 A kind of core changeable type glass chromatography column

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112630355A (en) * 2020-11-23 2021-04-09 江苏同济分析仪器有限公司 Enrichment column of liquid chromatograph

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Application publication date: 20190920