CN110250221A - A kind of new material and preparation method thereof of environment-friendly type pest control - Google Patents

A kind of new material and preparation method thereof of environment-friendly type pest control Download PDF

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Publication number
CN110250221A
CN110250221A CN201910601424.6A CN201910601424A CN110250221A CN 110250221 A CN110250221 A CN 110250221A CN 201910601424 A CN201910601424 A CN 201910601424A CN 110250221 A CN110250221 A CN 110250221A
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China
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parts
pest control
extract
environment
new material
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CN201910601424.6A
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Chinese (zh)
Inventor
刘佳妮
余磊
陈泽斌
苏源
张瑜瑜
徐胜光
钟宇
魏薇
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Kunming University
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Kunming University
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/08Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing solids as carriers or diluents
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/12Powders or granules
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N31/00Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
    • A01N31/06Oxygen or sulfur directly attached to a cycloaliphatic ring system
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/18Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/12Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/28Myrtaceae [Myrtle family], e.g. teatree or clove
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Abstract

The present invention provides a kind of new material and preparation method thereof of environment-friendly type pest control, which includes the raw material of following parts by weight: 2-3.2 parts of pyrethrum extract, 0.4-0.8 parts of houttuynia extract, 0.3-0.6 parts of menthol, 1-1.6 parts of capsaicine, 0.3-0.6 parts of eucalyptus oil, 16-23 parts of plant fiber powder, active 20-28 parts of powdered carbon, 5-10 parts of montmorillonite, 26-35 parts of vermiculite power;The new material for the prevention and treatment insect that the present invention is prepared its not only can the short time to contact the material pest effectively be killed, its smell can effectively disinfest, pest control effect is good, had good sustained release effect simultaneously, and it is permanently effective, each substance is easily obtained and not can cause environmental pollution, environmentally protective.

Description

A kind of new material and preparation method thereof of environment-friendly type pest control
Technical field
The present invention relates to technical field of pest control, and in particular to a kind of new material of environment-friendly type pest control and its preparation Method.
Background technique
Caste is various, comes in every shape, and belongs to the arthropod in invertebrate, and being that quantity is most on the earth moves Object group accounts in all biological species (including bacterium, fungi, virus) more than 50%, their trace almost spreads over generation Each corner on boundary.At the beginning of 21 century, insect known to the mankind has more than 100 ten thousand kinds, but still waits to find there are many type. Insect most species in the animal kingdom, quantity is maximum, causes significant impact to agricultural production and human health.
In agricultural production, can have an adverse effect to the production of crop there are many insect, for example, locust, aphid, aleyrodid, Thrips, snout moth's larva, diamond-back moth etc..
Dalmatian chrysanthemum with efficient, less toxic, low-residual characteristic be considered as in the world most safe, most effective natural plants kill Worm agent.Having 9 kinds in 12 kinds of biological insecticides that related organization, the United Nations in 1992 is recommended is pyrethrins or quasi- pyrethroids class chemical combination Object, but since quasi- pyrethrin pesticide pollutes in production, moral, Fa Dengguo have been prohibited in its domestic production.Chinese agriculture In industry portion " green food " standard promulgated in 2000, natural insecticide pyrethrins comes the first place for requiring to use pesticide.
Pyrethrum insecticide pharmacological property is strong, quick, lasting medicine, will not cause drug resistance, is ant fly, bee dung beetle, aphid etc. The deadly enemy of numerous software pests, while being also the jinx of a variety of virus and bacterias.The insecticide made of pyrethrins can be used extensively In farmland, silo, food processing factory, hospital and family, in addition to this Dalmatian chrysanthemum can be also used for war industry, timber, industry, The fields such as container, transport service, construction industry.Mainly there are three classes in the case where pyrethrins insecticide makes insect be poisoned to death: weight The generation for leading to a kind of neurotoxin is put after multiple;Comprehensive destruction of nervous system, conduction block;Other lesion tissues, such as dehydration And tissue necrosis etc..
Application No. is the Chinese patents of CN 201510590146.0 to disclose a kind of diatomaceous earth and preparation method thereof And purposes, the diatomaceous earth include following component by mass percentage: diatomite in powder 80-91%;Perian insect powder 1.5- 3.5%;Sepiolite powder 7.5-16.5%.The insecticide ingredient is simple, insecticide efficiency is high, safety and low toxicity, low-residual, is a kind of ring Border friendly natural botanical insecticide, the insecticide have extremely strong lethality to soft-bodied insects, can be widely used for grain and kind The prevention and control of plant diseases, pest control in terms of the storage of son, crops melon and fruit, vegetables and food production, and the insecticide preparation method is simple, It is suitable for industrialized production.But its persistence of the insecticide is short of, and is unable to long term in the prevention and treatment of pest.
Summary of the invention
The purpose of the present invention is to provide a kind of new materials and preparation method thereof of environment-friendly type pest control, are prepared It not only can effectively kill the pest for contacting the material in the short time new material of prevention and treatment insect, and smell can effectively drive It gets rid of insects, pest control effect is good, while had good sustained release effect, and permanently effective, and each substance is easily obtained and will not make to environment It is environmentally protective at pollution.
In order to achieve the above object, the present invention is achieved by the following technical programs:
A kind of new material of environment-friendly type pest control, the raw material including following parts by weight: 2-3.2 parts of pyrethrum extract, 0.4-0.8 parts of houttuynia extract, 0.3-0.6 parts of menthol, 1-1.6 parts of capsaicine, 0.3-0.6 parts of eucalyptus oil, plant fiber powder 16-23 parts last, active 20-28 parts of powdered carbon, 5-10 parts of montmorillonite, 26-35 parts of vermiculite power.
Preferably, the new material of the environment-friendly type pest control includes the raw material of following parts by weight: pyrethrum extract 2.8 Part, 0.5 part of houttuynia extract, 0.4 part of menthol, 1.3 parts of capsaicine, 0.5 part of eucalyptus oil, 20 parts of plant fiber powder, activity 25 parts of powdered carbon, 8 parts of montmorillonite, 31 parts of vermiculite power.
Preferably, the pyrethrum extract the preparation method comprises the following steps: dry perian insect powder is broken to 30-50 mesh, then carry out two Carbonoxide supercritical extract, extracting pressure 15-20Mpa, extraction temperature are 40-50 DEG C, and extraction time is 2-3 hours, separation Extract is collected, pyrethrum extract is obtained.
Preferably, the houttuynia extract the preparation method comprises the following steps: dry herba houttuyniae powder is broken to 50-80 mesh, then carry out two Carbonoxide supercritical extract, extracting pressure 25-30Mpa, extraction temperature are 40-50 DEG C, and extraction time is 1.5-2 hours, point From extract is collected, houttuynia extract is obtained.
Preferably, the plant fiber powder is bamboo fibre powder, stalk fibre powder, ramee powder, sisal hemp fibre Tie up one or more of powder, wood fibre powder.
Preferably, the active powdered carbon be one of rice hull active carbon powder, coconut activated powdered carbon, straw-stem active charcoal powder or It is several.
The preparation method of the new material of environment-friendly type pest control of the present invention, comprising the following steps:
(1) each raw material is weighed by formula;
(2) houttuynia extract, menthol, capsaicine, eucalyptus oil, active powdered carbon, montmorillonite are mixed Material;The adhesive for adding mixture total mass 5-6%, is granulated in pelletizer after mixing, then through cooling, drying, mistake Sieve, obtains core material;
(3) pyrethrum extract, plant fiber powder, vermiculite power are uniformly mixed, and must coat material;
(4) core material made from and cladding material are added in fluidized bed, while spraying into binder solution, and cladding material is coated on core Expect surface, then through drying, whole grain, the new material particle of environment-friendly type pest control is made.
Preferably, the diameter of the new material particle of the environment-friendly type pest control is 3-8mm.
Preferably, in step (2), adhesive therefor is sodium carboxymethylcellulose or hydroxypropyl methyl cellulose;Step (4) In, binder solution is sodium carboxymethyl cellulose solution.
The beneficial effects of the present invention are:
1, the effective component of pest control please on this basis, is matched using pyrethrum extract as main matter in the present invention On the one hand proper amount of houttuynia extract, menthol, capsaicine can make insecticidal effect more preferable, while these four substance smells It is comprehensive, the significant effect to disinfest is promoted.And suitable eucalyptus oil is added, and on the one hand it itself can drive away insect, it is another Aspect can make each ingredient respectively and be better absorption houttuynia extract, menthol, capsaicine preferably with active carbon, montmorillonite into Row absorption to increase the stability of core material, and is allowed to its term of validity extension for preventing and treating insect.
2, the present invention uses the material of pyrethrum extract, plant fiber, vermiculite power as clad, and wherein Dalmatian chrysanthemum mentions It takes object to can be done directly on pest, has preferable effect for killing pest, vermiculite power adsorption effect is strong, can extract to Dalmatian chrysanthemum Object is adsorbed, and the later period is sustained, and the plant fiber of addition can then increase the toughness of clad, makes the impact resistance of particle It can increase, be not easy to crash, keep more complete particle, the new material particle for being good for the environment type pest control plays work for a long time With.
3, pyrethrum extract, houttuynia extract are prepared using carbon dioxide supercritical extraction method, can be obtained desinsection and The more effective component of expelling parasite, to keep the effect of pest control more preferable.
Specific embodiment
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention, Technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is the present invention one Divide embodiment, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making Every other embodiment obtained, shall fall within the protection scope of the present invention under the premise of creative work.
Embodiment 1:
A kind of new material of environment-friendly type pest control, the raw material including following parts by weight: 3 parts of pyrethrum extract, fish raw meat 0.5 part of careless extract, 0.5 part of menthol, 1.3 parts of capsaicine, 0.5 part of eucalyptus oil, 20 parts of bamboo fibre powder, rice hull active carbon powder 28 Part, 8 parts of montmorillonite, 26 parts of vermiculite power.
Pyrethrum extract the preparation method comprises the following steps: dry perian insect powder is broken to 30-50 mesh, then carry out CO 2 supercritical Extraction, extracting pressure 18Mpa, extraction temperature are 50 DEG C, and extraction time is 2.5 hours, separate and collect extract, obtain Dalmatian chrysanthemum Extract.
Houttuynia extract the preparation method comprises the following steps: dry herba houttuyniae powder is broken to 50-80 mesh, then carry out CO 2 supercritical Extraction, extracting pressure 30Mpa, extraction temperature are 50 DEG C, and extraction time is 1.5 hours, separate and collect extract, obtain cordate houttuynia Extract.
The preparation method of the new material of above-mentioned environment-friendly type pest control, comprising the following steps:
(1) each raw material is weighed by formula;
(2) houttuynia extract, menthol, capsaicine, eucalyptus oil, rice hull active carbon, montmorillonite are mixed Close material;The sodium carboxymethylcellulose for adding mixture total mass 5.56%, is granulated in pelletizer after mixing, then through cold But, dry, sieving, obtains core material;
(3) pyrethrum extract, bamboo fibre powder, vermiculite power are uniformly mixed, and must coat material;
(4) core material made from and cladding material are added in fluidized bed, while spraying into methylcellulose sodium water solution, and cladding is expected It is coated on core material surface, then through drying, whole grain, the new material particle of environment-friendly type pest control is made;The diameter of new material particle For 4 ± 0.5mm.
Embodiment 2:
A kind of new material of environment-friendly type pest control, the raw material including following parts by weight: 2 parts of pyrethrum extract, fish raw meat 0.4 part of careless extract, 0.6 part of menthol, 1.6 parts of capsaicine, 0.4 part of eucalyptus oil, 20 parts of bamboo fibre powder, rice hull active carbon powder 25 Part, 10 parts of montmorillonite, 30 parts of vermiculite power.
Pyrethrum extract the preparation method comprises the following steps: dry perian insect powder is broken to 30-50 mesh, then carry out CO 2 supercritical Extraction, extracting pressure 20Mpa, extraction temperature are 40 DEG C, and extraction time is 2 hours, separate and collect extract, obtain Dalmatian chrysanthemum and mention Take object.
Houttuynia extract the preparation method comprises the following steps: dry herba houttuyniae powder is broken to 50-80 mesh, then carry out CO 2 supercritical Extraction, extracting pressure 30Mpa, extraction temperature are 50 DEG C, and extraction time is 1.5 hours, separate and collect extract, obtain cordate houttuynia Extract.
The preparation method of the new material of above-mentioned environment-friendly type pest control, comprising the following steps:
(1) each raw material is weighed by formula;
(2) houttuynia extract, menthol, capsaicine, eucalyptus oil, rice hull active carbon powder, montmorillonite are uniformly mixed and are obtained Mixture;The sodium carboxymethylcellulose for adding mixture total mass 6%, is granulated in pelletizer after mixing, then through cold But, dry, sieving, obtains core material;
(3) pyrethrum extract, bamboo fibre powder, vermiculite power are uniformly mixed, and must coat material;
(4) core material made from and cladding material are added in fluidized bed, while spraying into methylcellulose sodium water solution, and cladding is expected It is coated on core material surface, then through drying, whole grain, the new material particle of environment-friendly type pest control is made;The diameter of new material particle For 7.5 ± 0.5mm.
Embodiment 3:
A kind of new material of environment-friendly type pest control, the raw material including following parts by weight: 3.2 parts of pyrethrum extract, fish 0.4 part of raw meat grass extract, 0.3 part of menthol, 1 part of capsaicine, 0.3 part of eucalyptus oil, 23 parts of stalk fibre powder, coconut activated powdered carbon 28 parts, 8 parts of montmorillonite, 26 parts of vermiculite power.
Pyrethrum extract the preparation method comprises the following steps: dry perian insect powder is broken to 30-50 mesh, then carry out CO 2 supercritical Extraction, extracting pressure 15Mpa, extraction temperature are 50 DEG C, and extraction time is 2.5 hours, separate and collect extract, obtain Dalmatian chrysanthemum Extract.
Houttuynia extract the preparation method comprises the following steps: dry herba houttuyniae powder is broken to 50-80 mesh, then carry out CO 2 supercritical Extraction, extracting pressure 25Mpa, extraction temperature are 40 DEG C, and extraction time is 2 hours, separate and collect extract, obtain cordate houttuynia and mention Take object.
The preparation method of the new material of above-mentioned environment-friendly type pest control, comprising the following steps:
(1) each raw material is weighed by formula;
(2) houttuynia extract, menthol, capsaicine, eucalyptus oil, coconut activated powdered carbon, montmorillonite are uniformly mixed and are obtained Mixture;The sodium carboxymethylcellulose for adding mixture total mass 5%, is granulated in pelletizer after mixing, then through cold But, dry, sieving, obtains core material;
(3) pyrethrum extract, stalk fibre powder, vermiculite power are uniformly mixed, and must coat material;
(4) core material made from and cladding material are added in fluidized bed, while spraying into methylcellulose sodium water solution, and cladding is expected It is coated on core material surface, then through drying, whole grain, the new material particle of environment-friendly type pest control is made;The diameter of new material particle For 3.5 ± 0.5mm.
Embodiment 5:
A kind of new material of environment-friendly type pest control, the raw material including following parts by weight: 2.5 parts of pyrethrum extract, fish 0.8 part of raw meat grass extract, 0.5 part of menthol, 1.3 parts of capsaicine, 0.6 part of eucalyptus oil, 16 parts of wood fibre powder, straw-stem active charcoal 20 parts of powder, 5 parts of montmorillonite, 35 parts of vermiculite power.
Pyrethrum extract the preparation method comprises the following steps: dry perian insect powder is broken to 30-50 mesh, then carry out CO 2 supercritical Extraction, extracting pressure 18Mpa, extraction temperature are 45 DEG C, and extraction time is 3 hours, separate and collect extract, obtain Dalmatian chrysanthemum and mention Take object.
Houttuynia extract the preparation method comprises the following steps: dry herba houttuyniae powder is broken to 50-80 mesh, then carry out CO 2 supercritical Extraction, extracting pressure 28Mpa, extraction temperature are 50 DEG C, and extraction time is 2 hours, separate and collect extract, obtain cordate houttuynia and mention Take object.
The preparation method of the new material of above-mentioned environment-friendly type pest control, comprising the following steps:
(1) each raw material is weighed by formula;
(2) houttuynia extract, menthol, capsaicine, eucalyptus oil, straw-stem active charcoal powder, montmorillonite are uniformly mixed and are obtained Mixture;The hydroxypropyl methyl cellulose for adding mixture total mass 5.5%, is granulated in pelletizer after mixing, then Through cooling, drying, sieving, core material is obtained;
(3) pyrethrum extract, wood fibre powder, vermiculite power are uniformly mixed, and must coat material;
(4) core material made from and cladding material are added in fluidized bed, while spraying into methylcellulose sodium water solution, and cladding is expected It is coated on core material surface, then through drying, whole grain, the new material particle of environment-friendly type pest control is made;The diameter of new material particle For 5.5 ± 0.5mm.
Embodiment 5:
A kind of new material of environment-friendly type pest control, the raw material including following parts by weight: 2.8 parts of pyrethrum extract, fish 0.5 part of raw meat grass extract, 0.4 part of menthol, 1.3 parts of capsaicine, 0.5 part of eucalyptus oil, 20 parts of bamboo fibre powder, coconut activated powdered carbon 25 parts, 8 parts of montmorillonite, 31 parts of vermiculite power.
The preparation method is the same as that of Example 1 for the preparation method of pyrethrum extract, houttuynia extract.
The preparation method is the same as that of Example 1 for the new material of environment-friendly type pest control.
Embodiment 6:
A kind of new material of environment-friendly type pest control, the raw material including following parts by weight: 2.5 parts of pyrethrum extract, fish 0.5 part of raw meat grass extract, 0.5 part of menthol, 1.3 parts of capsaicine, 0.5 part of eucalyptus oil, 20 parts of stalk fibre powder, rice hull active carbon 25 parts of powder, 8 parts of montmorillonite, 31 parts of vermiculite power.
The preparation method is the same as that of Example 1 for the preparation method of pyrethrum extract, houttuynia extract.
The preparation method is the same as that of Example 1 for the new material of environment-friendly type pest control.
The preparation method of the new material of above-mentioned environment-friendly type pest control, comprising the following steps:
(1) each raw material is weighed by formula;
(2) houttuynia extract, menthol, capsaicine, eucalyptus oil, active carbon, montmorillonite are uniformly mixed and obtain mixture; The hydroxypropyl methyl cellulose for adding mixture total mass 5.5%, is granulated in pelletizer after mixing, then through cooling, Dry, sieving, obtains core material;
(3) pyrethrum extract, plant fiber powder, vermiculite power are uniformly mixed, and must coat material;
(4) core material made from and cladding material are added in fluidized bed, while spraying into methylcellulose sodium water solution, and cladding is expected It is coated on core material surface, then through drying, whole grain, the new material particle of environment-friendly type pest control is made;The diameter of new material particle For 5 ± 0.5mm.
Comparative example 1:
A kind of new material of environment-friendly type pest control extracts in raw material without containing cordate houttuynia unlike the first embodiment Object, capsaicine, it is other same as Example 1.
Comparative example 2:
A kind of new material of environment-friendly type pest control, unlike the first embodiment, pyrethrum extract, fish in raw material Raw meat grass extract is that water extracts;It is other same as Example 1.
Prevent and treat insect effect test:
8 vials are taken, and are put into 300g Rice Leaf into each vial, are then put into the 8th vial 100 snout moth's larvas, be then put into the 1-6 vial the new material 4 of the pest control that embodiment 1-6 is prepared ± 0.2g is put into the 4 ± 0.2g of new material for the pest control that comparative example 1-2 is prepared in the 7-8 vial.
The first day and second day death rate of snout moth's larva is detected, testing result is as shown in table 1.
Table 1:
As shown in Table 1, the new material of pest control of the present invention has good killing effect for snout moth's larva, quick. Wherein houttuynia extract, capsaicine and pyrethrum extract have certain synergy, can dramatically increase the death rate of pest.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations;Although with reference to the foregoing embodiments Invention is explained in detail, those skilled in the art should understand that: it still can be to aforementioned each implementation Technical solution documented by example is modified or equivalent replacement of some of the technical features;And these modification or Replacement, the spirit and scope for technical solution of various embodiments of the present invention that it does not separate the essence of the corresponding technical solution.

Claims (9)

1. a kind of new material of environment-friendly type pest control, which is characterized in that the raw material including following parts by weight: pyrethrum extract 2-3.2 parts, 0.4-0.8 parts of houttuynia extract, 0.3-0.6 parts of menthol, 1-1.6 parts of capsaicine, 0.3-0.6 parts of eucalyptus oil, plant 16-23 parts of fibres powder, active 20-28 parts of powdered carbon, 5-10 parts of montmorillonite, 26-35 parts of vermiculite power.
2. the new material of environment-friendly type pest control according to claim 1, which is characterized in that the original including following parts by weight Material: 2.8 parts of pyrethrum extract, 0.5 part of houttuynia extract, 0.4 part of menthol, 1.3 parts of capsaicine, 0.5 part of eucalyptus oil, plant 20 parts of fiber dust, active 25 parts of powdered carbon, 8 parts of montmorillonite, 31 parts of vermiculite power.
3. the new material of environment-friendly type pest control according to claim 1, which is characterized in that the pyrethrum extract The preparation method comprises the following steps: dry perian insect powder is broken to 30-50 mesh, then carbon dioxide supercritical extraction is carried out, extracting pressure 15- 20Mpa, extraction temperature are 40-50 DEG C, and extraction time is 2-3 hours, separate and collect extract, obtain pyrethrum extract.
4. the new material of environment-friendly type pest control according to claim 1, which is characterized in that the houttuynia extract The preparation method comprises the following steps: dry herba houttuyniae powder is broken to 50-80 mesh, then carbon dioxide supercritical extraction is carried out, extracting pressure 25- 30Mpa, extraction temperature are 40-50 DEG C, and extraction time is 1.5-2 hours, separate and collect extract, obtain houttuynia extract.
5. the new material of environment-friendly type pest control according to claim 1, which is characterized in that the plant fiber powder is One or more of bamboo fibre powder, stalk fibre powder, ramee powder, sisal fiber powder, wood fibre powder.
6. the new material of environment-friendly type pest control according to claim 1, which is characterized in that the active carbon is living for rice husk One or more of property powdered carbon, coconut activated powdered carbon, straw-stem active charcoal powder.
7. the preparation method of the new material of environment-friendly type pest control according to claim 1 to 6, feature exist In, comprising the following steps:
(1) each raw material is weighed by formula;
(2) houttuynia extract, menthol, capsaicine, eucalyptus oil, active powdered carbon, montmorillonite are uniformly mixed and obtain mixture;Again The adhesive of mixture total mass 5-6% is added, is granulated in pelletizer after mixing, then through cooling, drying, sieving, obtain Core material;
(3) pyrethrum extract, plant fiber powder, vermiculite power are uniformly mixed, and must coat material;
(4) core material made from and cladding material are added in fluidized bed, while spraying into binder solution, and cladding material is coated on core material table Face, then through drying, whole grain, the new material particle of environment-friendly type pest control is made.
8. the preparation method of the new material of environment-friendly type pest control according to claim 7, which is characterized in that the environmental protection The diameter of the new material particle of type pest control is 3-8mm.
9. the preparation method of the new material of environment-friendly type pest control according to claim 7, which is characterized in that step (2) In, adhesive therefor is sodium carboxymethylcellulose or hydroxypropyl methyl cellulose;In step (4), binder solution is carboxymethyl Sodium cellulosate aqueous solution.
CN201910601424.6A 2019-07-04 2019-07-04 A kind of new material and preparation method thereof of environment-friendly type pest control Pending CN110250221A (en)

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CN106171684A (en) * 2016-06-30 2016-12-07 桐城市华猫软膜有限公司 A kind of insect-repelling mulching film and processing technology thereof
CN107242258A (en) * 2016-11-25 2017-10-13 芜湖国苑苗木服务有限公司 A kind of environment protecting plant flower planting insecticide and preparation method thereof
CN108294058A (en) * 2018-03-29 2018-07-20 合肥卓畅农业科技有限公司 A kind of safety and environmental protection effective, harmless slow-release pesticidal particle and preparation method thereof

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CN106171684A (en) * 2016-06-30 2016-12-07 桐城市华猫软膜有限公司 A kind of insect-repelling mulching film and processing technology thereof
CN107242258A (en) * 2016-11-25 2017-10-13 芜湖国苑苗木服务有限公司 A kind of environment protecting plant flower planting insecticide and preparation method thereof
CN108294058A (en) * 2018-03-29 2018-07-20 合肥卓畅农业科技有限公司 A kind of safety and environmental protection effective, harmless slow-release pesticidal particle and preparation method thereof

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Application publication date: 20190920