CN110218352A - A kind of production technology of graphene Electric radiant Heating Film - Google Patents
A kind of production technology of graphene Electric radiant Heating Film Download PDFInfo
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- CN110218352A CN110218352A CN201910385587.5A CN201910385587A CN110218352A CN 110218352 A CN110218352 A CN 110218352A CN 201910385587 A CN201910385587 A CN 201910385587A CN 110218352 A CN110218352 A CN 110218352A
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Abstract
The invention discloses a kind of production technologies of graphene Electric radiant Heating Film, include the following steps: that the preparation of graphene slurry, substrate are chosen, are coated with, drying, detection, pressing current-carrying item, detected resistance, coding, cutting obtained Electric radiant Heating Film, the heat generating pastes of this Electric radiant Heating Film have many advantages, such as that film-formation result is good, bonding force is strong, flexible, coating is not easy to break, and it is dried using being formed and drying two stages, first the slurry after coating is carried out shaping, then by the way of hot air circulation drying, make slurry drying more evenly, and surface thickness is uniform, improves product quality.
Description
Technical field
The present invention relates to graphene electrothermal film technology field more particularly to a kind of production technologies of graphene Electric radiant Heating Film.
Background technique
Graphene have excellent optics, electricity, mechanical characteristic, materialogy, micro-nano technology, the energy, biomedicine and
Drug delivery etc. is with important application prospects, it is considered to be a kind of future revolutionary material.Electric radiant Heating Film be divided into high temperature,
Low temperature electric heating film.High-temperature electric heating membrane is generally used for electronic apparatus, military affairs etc., the Electric radiant Heating Film of nowadays science and technology production.Electric heat membrane heating
System is to be different from using radiator, air-conditioning, radiator as the point heating system of representative, supply using heating cable as the wire type of representative
Heating system, low-carbon heating high-tech product of the formula heating field using modern aerospace flight technology research and development, graphene Electric radiant Heating Film tool in face
The advantages that some environmental protection, energy conservation, high cost performance, has obtained universal popularization, but there are one for the preparation of traditional graphene Electric radiant Heating Film
Problem is determined, such as the problems such as heat generating pastes are not perfect, and coating drying is uneven, for this purpose, it is proposed that a kind of graphene Electric radiant Heating Film
Production technology.
Summary of the invention
The invention proposes a kind of production technologies of graphene Electric radiant Heating Film, to solve mentioned above in the background art ask
Topic.
The invention proposes a kind of production technologies of graphene Electric radiant Heating Film, include the following steps:
S1: the preparation of graphene slurry is chosen according to weight ratio are as follows: 40-60 parts of graphene, 20-30 parts of conductive carbon powder, metal
10-16 parts of mixture, 30-40 parts of far infrared inorganic nanometer powder, 40-50 parts of resin, helps 30-40 parts of nano-macromolecule material
30-50 parts of agent, 20-30 parts of deionized water raw material, after raw material is ground, dispersed, filtered and is mixed be made fever slurry
Expect spare;
S2: substrate is chosen, and chooses environmentally friendly polyester base material, the surface of polyester base material is first carried out cleaning treatment, then use and remove
Electro static instrument carries out elimination electrostatic treatment to the surface of polyester base material, finally carries out corona to polyester base material surface using corona machine
It is spare after processing;
S3: polyester base material made from S2 is placed on automatic, high precision coating machine and fixes polyester base material by coating, drying
Then heat generating pastes made from S1 are uniformly coated on polyester base material surface by edge, by being moved to for the polyester base material after coating
In drying mechanism, drying mechanism is divided into sizing stage and drying stage, and sizing stage drying tunnel temperature is 70-90 DEG C and is not provided with leading to
Wind, the drying tunnel temperature of drying stage are 110-130 DEG C and ventilation are arranged;
S4: detection: by treated in S3, environmentally friendly polyester base material carries out elimination electrostatic treatment again, to coating mixture
Environmentally friendly polyester base material judges whether to comply with standard using its thickness of infrared detection, then detects environmentally friendly polyester base material again
Whether resistance value complies with standard and its surface is with the presence or absence of flaw, then rejects defective products, retains qualified environmentally friendly polyester base material;
S5: the environmentally friendly polyester base material surface of qualification made from S4 is coated with graphene conductive glue by pressing current-carrying item, and coating is completed
Afterwards, the two sides of polyester base material press current-carrying item, are carried out being moved to drying mechanism and be dried, the baking in drying mechanism and S3
Dry mechanism structure is identical;
S6: polyester base material made from S5 is carried out resistance value detection, rejects defective products, retains qualified polyester by detected resistance
Substrate;
S7: the polyester base material surface of S6 qualification is carried out coding by coding, cutting, and the polyester base material after coding carries out again
Then drying cuts into respective shape after drying as desired, obtains graphene Electric radiant Heating Film.
Preferably, auxiliary agent includes: 1-3 parts of dispersing agent, adjusts 10-20 parts of oil, 10-20 parts of diluent, crosslinking coupling in S1
3-5 parts of agent, 3-5 parts of defoaming agent, 1-3 parts of levelling agent, 1-3 parts of adhesion promoter.
Preferably, graphene, conductive carbon powder and metal mixture are added in grinder and are ground, will ground in S1
Powder afterwards, which is added in dispersion machine, carries out high speed dispersion, and gained powder is added in filter mechanism and is filtered, then will be after filtering
Powder be added in container and add resin, auxiliary agent and deionized water and carry out being sufficiently mixed obtained heat generating pastes.
Preferably, heat generating pastes obtained need to carry out proportion detection before use in S1, and retain detection sample.
Preferably, polyester base material needed on automatic, high precision coating machine carry out edge fix, after coating polyester base material with put
Set the load carrier integral translation of polyester base material.
Compared with prior art, the advantageous effect of present invention is that: the heat generating pastes of this Electric radiant Heating Film have film forming effect
The advantages that fruit is good, bonding force is strong, flexible, coating is not easy to break, and dried using being formed and drying two stages, first to painting
Slurry after cloth carries out shaping, and then by the way of hot air circulation drying, makes slurry drying more evenly, and surface thickness is equal
It is even, improve product quality.
Specific embodiment
It is next combined with specific embodiments below that the present invention will be further described.
Embodiment 1
The invention proposes a kind of production technologies of graphene Electric radiant Heating Film, include the following steps:
S1: the preparation of graphene slurry is chosen according to weight ratio are as follows: 45 parts of graphene, 22 parts of conductive carbon powder, metal mixture
12 parts, 38 parts of nano-macromolecule material, 36 parts of far infrared inorganic nanometer powder, 45 parts of resin, 40 parts of auxiliary agent, 22 parts of deionized water
Raw material graphene, conductive carbon powder and metal mixture are added in grinder and are ground, the powder after grinding is added
High speed dispersion is carried out in dispersion machine, gained powder is added in filter mechanism and is filtered, is then added to filtered powder
Resin, auxiliary agent and deionized water are added in container be sufficiently mixed that obtained heat generating pastes are spare, and auxiliary agent includes: dispersing agent 1
Part adjusts 12 parts of oil, 14 parts of diluent, crosslinking 4 parts of coupling agent, 5 parts of defoaming agent, 2 parts of levelling agent, 2 parts of adhesion promoter, hair
Hot slurry needs to carry out proportion detection before use, and retains detection sample;
S2: substrate is chosen, and chooses environmentally friendly polyester base material, the surface of polyester base material is first carried out cleaning treatment, then use and remove
Electro static instrument carries out elimination electrostatic treatment to the surface of polyester base material, finally carries out corona to polyester base material surface using corona machine
It is spare after processing;
S3: polyester base material made from S2 is placed on automatic, high precision coating machine, polyester base material is automatic by coating, drying
It needs progress edge to fix on high-precision coating machine, heat generating pastes made from S1 is then uniformly coated on polyester base material surface, it will
After cloth in the load carrier integral translation to drying mechanism of polyester base material and placement polyester base material, drying mechanism is divided into the sizing stage
And drying stage, sizing stage drying tunnel temperature are 80 DEG C and are not provided with divulging information, the drying tunnel temperature of drying stage is 120 DEG C and is arranged
Ventilation;
S4: detection: by treated in S3, environmentally friendly polyester base material carries out elimination electrostatic treatment again, to coating mixture
Environmentally friendly polyester base material judges whether to comply with standard using its thickness of infrared detection, then detects environmentally friendly polyester base material again
Whether resistance value complies with standard and its surface is with the presence or absence of flaw, then rejects defective products, retains qualified environmentally friendly polyester base material;
S5: the environmentally friendly polyester base material surface of qualification made from S4 is coated with graphene conductive glue by pressing current-carrying item, and coating is completed
Afterwards, the two sides of polyester base material press current-carrying item, are carried out being moved to drying mechanism and be dried, the baking in drying mechanism and S3
Dry mechanism structure is identical;
S6: polyester base material made from S5 is carried out resistance value detection, rejects defective products, retains qualified polyester by detected resistance
Substrate;
S7: the polyester base material surface of S6 qualification is carried out coding by coding, cutting, and the polyester base material after coding carries out again
Then drying cuts into respective shape after drying as desired, obtains graphene Electric radiant Heating Film.
Embodiment 2
S1: the preparation of graphene slurry is chosen according to weight ratio are as follows: 50 parts of graphene, 25 parts of conductive carbon powder, metal mixture
10 parts, 32 parts of nano-macromolecule material, 35 parts of far infrared inorganic nanometer powder, 46 parts of resin, 45 parts of auxiliary agent, 28 parts of deionized water
Raw material graphene, conductive carbon powder and metal mixture are added in grinder and are ground, the powder after grinding is added
High speed dispersion is carried out in dispersion machine, gained powder is added in filter mechanism and is filtered, is then added to filtered powder
Resin, auxiliary agent and deionized water are added in container be sufficiently mixed that obtained heat generating pastes are spare, and auxiliary agent includes: dispersing agent 1
Part adjusts 15 parts of oil, 18 parts of diluent, crosslinking 3 parts of coupling agent, 3 parts of defoaming agent, 3 parts of levelling agent, 3 parts of adhesion promoter, hair
Hot slurry needs to carry out proportion detection before use, and retains detection sample;
S2: substrate is chosen, and chooses environmentally friendly polyester base material, the surface of polyester base material is first carried out cleaning treatment, then use and remove
Electro static instrument carries out elimination electrostatic treatment to the surface of polyester base material, finally carries out corona to polyester base material surface using corona machine
It is spare after processing;
S3: polyester base material made from S2 is placed on automatic, high precision coating machine, polyester base material is automatic by coating, drying
It needs progress edge to fix on high-precision coating machine, heat generating pastes made from S1 is then uniformly coated on polyester base material surface, it will
After cloth in the load carrier integral translation to drying mechanism of polyester base material and placement polyester base material, drying mechanism is divided into the sizing stage
And drying stage, sizing stage drying tunnel temperature are 75 DEG C and are not provided with divulging information, the drying tunnel temperature of drying stage is 125 DEG C and is arranged
Ventilation;
S4: detection: by treated in S3, environmentally friendly polyester base material carries out elimination electrostatic treatment again, to coating mixture
Environmentally friendly polyester base material judges whether to comply with standard using its thickness of infrared detection, then detects environmentally friendly polyester base material again
Whether resistance value complies with standard and its surface is with the presence or absence of flaw, then rejects defective products, retains qualified environmentally friendly polyester base material;
S5: the environmentally friendly polyester base material surface of qualification made from S4 is coated with graphene conductive glue by pressing current-carrying item, and coating is completed
Afterwards, the two sides of polyester base material press current-carrying item, are carried out being moved to drying mechanism and be dried, the baking in drying mechanism and S3
Dry mechanism structure is identical;
S6: polyester base material made from S5 is carried out resistance value detection, rejects defective products, retains qualified polyester by detected resistance
Substrate;
S7: the polyester base material surface of S6 qualification is carried out coding by coding, cutting, and the polyester base material after coding carries out again
Then drying cuts into respective shape after drying as desired, obtains graphene Electric radiant Heating Film.
Embodiment 4
S1: the preparation of graphene slurry is chosen according to weight ratio are as follows: 55 parts of graphene, 20 parts of conductive carbon powder, metal mixture
15 parts, 35 parts of nano-macromolecule material, 35 parts of far infrared inorganic nanometer powder, 55 parts of resin, 35 parts of auxiliary agent, 30 parts of deionized water
Raw material graphene, conductive carbon powder and metal mixture are added in grinder and are ground, the powder after grinding is added
High speed dispersion is carried out in dispersion machine, gained powder is added in filter mechanism and is filtered, is then added to filtered powder
Resin, auxiliary agent and deionized water are added in container be sufficiently mixed that obtained heat generating pastes are spare, and auxiliary agent includes: dispersing agent 3
Part adjusts 18 parts of oil, 15 parts of diluent, crosslinking 3 parts of coupling agent, 4 parts of defoaming agent, 2 parts of levelling agent, 1 part of adhesion promoter, hair
Hot slurry needs to carry out proportion detection before use, and retains detection sample;
S2: substrate is chosen, and chooses environmentally friendly polyester base material, the surface of polyester base material is first carried out cleaning treatment, then use and remove
Electro static instrument carries out elimination electrostatic treatment to the surface of polyester base material, finally carries out corona to polyester base material surface using corona machine
It is spare after processing;
S3: polyester base material made from S2 is placed on automatic, high precision coating machine, polyester base material is automatic by coating, drying
It needs progress edge to fix on high-precision coating machine, heat generating pastes made from S1 is then uniformly coated on polyester base material surface, it will
After cloth in the load carrier integral translation to drying mechanism of polyester base material and placement polyester base material, drying mechanism is divided into the sizing stage
And drying stage, sizing stage drying tunnel temperature are 75 DEG C and are not provided with divulging information, the drying tunnel temperature of drying stage is 120 DEG C and is arranged
Ventilation;
S4: detection: by treated in S3, environmentally friendly polyester base material carries out elimination electrostatic treatment again, to coating mixture
Environmentally friendly polyester base material judges whether to comply with standard using its thickness of infrared detection, then detects environmentally friendly polyester base material again
Whether resistance value complies with standard and its surface is with the presence or absence of flaw, then rejects defective products, retains qualified environmentally friendly polyester base material;
S5: the environmentally friendly polyester base material surface of qualification made from S4 is coated with graphene conductive glue by pressing current-carrying item, and coating is completed
Afterwards, the two sides of polyester base material press current-carrying item, are carried out being moved to drying mechanism and be dried, the baking in drying mechanism and S3
Dry mechanism structure is identical;
S6: polyester base material made from S5 is carried out resistance value detection, rejects defective products, retains qualified polyester by detected resistance
Substrate;
S7: the polyester base material surface of S6 qualification is carried out coding by coding, cutting, and the polyester base material after coding carries out again
Then drying cuts into respective shape after drying as desired, obtains graphene Electric radiant Heating Film.
The heat generating pastes of this Electric radiant Heating Film have many advantages, such as that film-formation result is good, bonding force is strong, flexible, coating is not easy to break,
And dried using being formed and drying two stages, first the slurry after coating is carried out shaping, is then dried using hot air circulation
Mode, make slurry drying more evenly, and surface thickness is uniform, improves product quality.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (5)
1. a kind of production technology of graphene Electric radiant Heating Film, which comprises the steps of:
S1: the preparation of graphene slurry is chosen according to weight ratio are as follows: 40-60 parts of graphene, 20-30 parts of conductive carbon powder, metal mixed
10-16 parts of object, 30-40 parts of nano-macromolecule material, 30-40 parts of far infrared inorganic nanometer powder, 40-50 parts of resin, auxiliary agent 30-
It is standby that heat generating pastes are made in 50 parts, 20-30 parts of deionized water of raw material after being ground, dispersed, filtered and being mixed by raw material
With;
S2: substrate is chosen, and chooses environmentally friendly polyester base material, the surface of polyester base material is first carried out cleaning treatment, then use and destatic
Instrument carries out elimination electrostatic treatment to the surface of polyester base material, finally carries out sided corona treatment to polyester base material surface using corona machine
It is spare afterwards;
S3: polyester base material made from S2 is placed in the side on automatic, high precision coating machine and fixing polyester base material by coating, drying
Then heat generating pastes made from S1 are uniformly coated on polyester base material surface by edge, the polyester base material after coating is moved to baking
In dry mechanism, drying mechanism is divided into sizing stage and drying stage, and sizing stage drying tunnel temperature is 70-90 DEG C and is not provided with leading to
Wind, the drying tunnel temperature of drying stage are 110-130 DEG C and ventilation are arranged;
S4: detection: by treated in S3, environmentally friendly polyester base material carries out elimination electrostatic treatment again, the environmental protection to coating mixture
Polyester base material judges whether to comply with standard using its thickness of infrared detection, then detects environmentally friendly polyester base material resistance value again
Whether comply with standard and its surface is with the presence or absence of flaw, then rejects defective products, retain qualified environmentally friendly polyester base material;
S5: the environmentally friendly polyester base material surface of qualification made from S4 is coated with graphene conductive glue by pressing current-carrying item, after the completion of coating,
The two sides of polyester base material press current-carrying item, are carried out being moved to drying mechanism and be dried, the drying in drying mechanism and S3
Mechanism structure is identical;
S6: polyester base material made from S5 is carried out resistance value detection, rejects defective products, retains qualified polyester base material by detected resistance;
S7: the polyester base material surface of S6 qualification is carried out coding by coding, cutting, and the polyester base material after coding is dried again,
Respective shape is then cut into as desired after drying, obtains graphene Electric radiant Heating Film.
2. according to claim 1 be used for graphene far infrared planar heat producing body aqueous slurry, which is characterized in that helped in S1
Agent includes: 1-3 parts of dispersing agent, adjusts 10-20 parts of oil, 10-20 parts of diluent, coupling agent 3-5 parts of crosslinking, 3-5 parts of defoaming agent, stream
Flat agent 1-3 parts, 1-3 parts of adhesion promoter.
3. according to claim 1 be used for graphene far infrared planar heat producing body aqueous slurry, which is characterized in that will in S1
Graphene, conductive carbon powder and metal mixture, be added grinder in ground, by after grinding powder be added dispersion machine in into
Row high speed dispersion, gained powder are added in filter mechanism and are filtered, and then filtered powder is added in container and adds again
Enter resin, auxiliary agent and deionized water to carry out being sufficiently mixed obtained heat generating pastes.
4. according to claim 1 be used for graphene far infrared planar heat producing body aqueous slurry, which is characterized in that made in S1
The heat generating pastes obtained need to carry out proportion detection before use, and retain detection sample.
5. according to claim 1 be used for graphene far infrared planar heat producing body aqueous slurry, which is characterized in that polyester base
Material needs progress edge to fix on automatic, high precision coating machine, and the load carrier of polyester base material and placement polyester base material is whole after coating
Body translation.
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CN110904725A (en) * | 2019-12-06 | 2020-03-24 | 浙江万家暖智能科技有限公司 | Heating film and preparation method thereof, and equipment adopting heating film and preparation method thereof |
CN111436168A (en) * | 2020-01-14 | 2020-07-21 | 北京服装学院 | Graphene electrical heating slurry, graphene electrical heating film and preparation method and application thereof |
CN112691832A (en) * | 2020-12-22 | 2021-04-23 | 乐福之家纳米材料有限责任公司 | Graphene electrothermal film production system |
CN113492562A (en) * | 2020-03-19 | 2021-10-12 | 上海康天新能源科技有限公司 | Processing technology for preparing water-based graphene electrothermal film by die cutting and laminating method |
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CN108156676A (en) * | 2017-12-21 | 2018-06-12 | 湖北西控同创石墨烯应用科技有限公司 | A kind of fire-retardant graphene is modified the production method of far-infrared electrothermal film |
CN109688644A (en) * | 2019-02-18 | 2019-04-26 | 中山市君泽科技有限公司 | One kind being used for graphene far infrared planar heat producing body aqueous slurry |
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CN107182140A (en) * | 2016-03-11 | 2017-09-19 | 江苏同创节能科技有限公司 | A kind of graphene is modified the preparation method of far-infrared electrothermal film |
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CN110904725A (en) * | 2019-12-06 | 2020-03-24 | 浙江万家暖智能科技有限公司 | Heating film and preparation method thereof, and equipment adopting heating film and preparation method thereof |
CN111436168A (en) * | 2020-01-14 | 2020-07-21 | 北京服装学院 | Graphene electrical heating slurry, graphene electrical heating film and preparation method and application thereof |
CN113492562A (en) * | 2020-03-19 | 2021-10-12 | 上海康天新能源科技有限公司 | Processing technology for preparing water-based graphene electrothermal film by die cutting and laminating method |
CN113492562B (en) * | 2020-03-19 | 2022-10-14 | 上海康天新能源科技有限公司 | Processing technology for preparing water-based graphene electrothermal film by die cutting and laminating method |
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Application publication date: 20190910 |