CN110196176A - A kind of high-temperature high dust dioxin sampling apparatus - Google Patents

A kind of high-temperature high dust dioxin sampling apparatus Download PDF

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Publication number
CN110196176A
CN110196176A CN201810158964.7A CN201810158964A CN110196176A CN 110196176 A CN110196176 A CN 110196176A CN 201810158964 A CN201810158964 A CN 201810158964A CN 110196176 A CN110196176 A CN 110196176A
Authority
CN
China
Prior art keywords
filter cylinder
deduster
sampling
pressure sensor
gas phase
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810158964.7A
Other languages
Chinese (zh)
Inventor
毛洪钧
乔杰
徐晶
王鹏
李火
王玮
王斌
张长卿
王永亮
张大庆
朱高英
王丕征
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
QINGDAO HENGYUAN TECHNOLOGY DEVELOPMENT Co Ltd
Original Assignee
QINGDAO HENGYUAN TECHNOLOGY DEVELOPMENT Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by QINGDAO HENGYUAN TECHNOLOGY DEVELOPMENT Co Ltd filed Critical QINGDAO HENGYUAN TECHNOLOGY DEVELOPMENT Co Ltd
Priority to CN201810158964.7A priority Critical patent/CN110196176A/en
Publication of CN110196176A publication Critical patent/CN110196176A/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/2202Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling
    • G01N1/2205Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling with filters
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/2202Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling
    • G01N1/2211Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling with cyclones
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/2202Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling
    • G01N1/2214Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling by sorption
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/2247Sampling from a flowing stream of gas
    • G01N1/2258Sampling from a flowing stream of gas in a stack or chimney
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N2001/2282Devices for withdrawing samples in the gaseous state with cooling means

Abstract

The present invention provides a kind of high-temperature high dust dioxin sampling apparatus, including deduster, filter cylinder, Gas Phase Adsorption unit, sampling pump, control device with condensing unit before shell, sampling pipe, thermocouple, Pitot tube, filter cylinder.Structure of the invention is reasonable, pass through deduster before installation filter cylinder, by bulky grain sample collection before filter cylinder in the dust arrester of deduster, reduce the collection capacity of sample in filter cylinder, to guarantee that filter cylinder will not be fully loaded with, filter cylinder obstruction is avoided, so as to smoothly complete continuous sampling, the synchronous detection to deduster removal efficiency can be competent at.

Description

A kind of high-temperature high dust dioxin sampling apparatus
Technical field
The present invention relates to a kind of high-temperature high dust dioxin sampling apparatuses, belong to environment monitoring instrument field.
Background technique
Dioxin is a kind of colorless and odorless, the serious liposoluble substance of toxicity.In environmental monitoring field, to fixed dirty The sampling of dye source dioxin is to carry out all data using flue gas of the stationary source dioxin sampler to soot emissions system Acquisition carries out constant speed tracking sampling.Stationary source dioxin sampler, is divided into dry method sampler by work characteristics and wet process is adopted Sample device, there is many limitations, especially dustiness for stationary source dioxin sampler common at present greatly, flue dust temperature Under conditions of height, humidity are big, filter cylinder blocking can be generated, accessory high-temperature expansion causes poorly sealed, humidity is excessive heat exchange is caused to be imitated The problems such as rate is low, especially in the device for abatement of smoke and dust of exhaust gas dioxin abatement equipment is checked and accepted, according to " state, the People's Republic of China (PRC) Family's environment protectment protection " requirement, the detection of abatement equipment removal efficiency needs to deduster import and export while sampling, And entrance is that (before exhaust gas dioxin abatement equipment) dust concentration and temperature are all very high, and the capacity of quartzy filter cylinder is limited, Under high dirt state, it is easy to cause filter cylinder fully loaded in a short time, so that airway blockage, resistance increases, and causes sampler automatic Protection, sampling are shut down on the way, cannot keep continuous sampling, therefore the prior art cannot be simultaneously to same before deduster and after deduster Step is sampled.
Summary of the invention
In view of the above deficiencies, the present invention provides a kind of high-temperature high dust dioxin sampling apparatus, before installing filter cylinder additional Deduster, by bulky grain sample collection before filter cylinder in the dust arrester of deduster, a small amount of aerosol sample is collected in filter cylinder, To guarantee that filter cylinder will not be fully loaded with, continuous sampling is kept, completes to detect the synchronous of deduster removal efficiency.
The technical scheme adopted by the invention is that a kind of high-temperature high dust dioxin sampling apparatus, including shell, sampling pipe, Deduster, filter cylinder, Gas Phase Adsorption unit, sampling pump, control device with condensing unit before thermocouple, Pitot tube, filter cylinder.
The enclosure interior is fixedly installed control device, Gas Phase Adsorption unit, sampling pump and pipe with condensing unit Road;
The control device includes PLC control system, pressure sensor one, pressure sensor two, temperature sensor, flow sensing Device, flow regulator;The pressure sensor one, pressure sensor two, temperature sensor, flow sensor, flow are adjusted Device is electrically connected with PLC control system respectively;
The thermocouple is fixed at housing forward end, and the thermocouple is electrically connected with PLC control system;
The Pitot tube is fixed at housing forward end, and the Pitot tube is electrically connected with pressure sensor one;
The sampling pipe is fixed at housing forward end, and the sampling pipe back-end sealing is connected with deduster before filter cylinder, the filter Deduster rear end is connected with filter cylinder before cylinder, and the filter cylinder pipeline is tightly connected the Gas Phase Adsorption unit for having condensing unit;
The sampling pump is successively tightly connected flow regulator, flow sensor and the gas phase with condensing unit by pipeline Absorbing unit;
The pipeline is sealedly connected with pressure sensor two, temperature sensor;
Deduster includes body, air inlet, dust arrester one, cyclone dust collectors, dust arrester two, gas outlet before the filter cylinder;
The air inlet is set to body left upper portion, is sealedly connected with dismountable dust arrester one below the air inlet;
The cyclone dust collectors are fixedly installed on body lower right side, are sealedly connected with below the cyclone dust collectors dismountable Dust arrester two;The gas outlet is fixedly installed on body right upper portion.
Implementation process of the invention:
Smoke sample from sampling pipe enter filter cylinder before deduster, by deduster before filter cylinder, bulky grain smoke sample is collected in Before filter cylinder in the dust arrester of deduster, then little particle and a small amount of aerosol sample are delayed in filter cylinder, are collected, synchronous After detection, filter cylinder and dust arrester are sent into chemical examination simultaneously.
The beneficial effects of the present invention are:
Structure of the invention is reasonable, by deduster before installation filter cylinder, by the dust of bulky grain sample collection deduster before filter cylinder In device, reduce the collection capacity of sample in filter cylinder, to guarantee that filter cylinder will not be fully loaded with, filter cylinder obstruction is avoided, so as to smooth Completion continuous sampling, the synchronous detection to deduster removal efficiency can be competent at.
Detailed description of the invention
Below with reference to examples and drawings, the present invention will be described in more detail.
Fig. 1 is structural schematic diagram of the invention.
Fig. 2 is the structural schematic diagram of deduster before filter cylinder of the present invention.
Specific embodiment
Embodiment 1
The scope of the invention is not limited to the present embodiment.
It is removed before a kind of high-temperature high dust dioxin sampling apparatus, including shell 1, sampling pipe 2, thermocouple 3, Pitot tube 4, filter cylinder Dirt device 5, filter cylinder 6, the Gas Phase Adsorption unit 7 with condensing unit, sampling pump 8, control device 9.
Control device 9, the Gas Phase Adsorption unit 7 with condensing unit, sampling pump 8 are fixedly installed inside the shell 1 With pipeline 10;
The control device 9 includes PLC control system 91, pressure sensor 1, pressure sensor 2 93, temperature sensor 94, flow sensor 95, flow regulator 96;The pressure sensor 1, pressure sensor 2 93, temperature sensor 94, flow sensor 95, flow regulator 96 are electrically connected with PLC control system 91 respectively;
The thermocouple 3 is fixed at 1 front end of shell, and the thermocouple is electrically connected with PLC control system;
The Pitot tube 4 is fixed at 1 front end of shell, and the Pitot tube is electrically connected with pressure sensor one;
The sampling pipe 2 is fixed at 1 front end of shell, and 2 back-end sealing of sampling pipe is connected with deduster 5 before filter cylinder, institute 5 rear end of deduster is connected with filter cylinder 6 before stating filter cylinder, and the filter cylinder 6 is tightly connected the Gas Phase Adsorption unit 7 for having condensing unit;
The sampling pump 8 is successively tightly connected flow regulator 96, flow sensor 95 by pipeline and has condensing unit Gas Phase Adsorption unit 7;
Pressure sensor 2 93, temperature sensor 94 are sealedly connected on the pipeline 10;
Before the filter cylinder deduster 5 include body 51, air inlet 52, dust arrester 1, cyclone dust collectors 54, dust arrester 2 55, Gas outlet 56;
The air inlet 52 is set to 51 left upper portion of body, is sealedly connected with dismountable dust arrester below the air inlet 52 One 53;
The cyclone dust collectors 54 are fixedly installed on 51 lower right side of body, and being sealedly connected with below the cyclone dust collectors 54 can The dust arrester 2 55 of disassembly;The gas outlet 56 is fixedly installed on 51 right upper portion of body;
Implementation process of the invention:
Smoke sample from sampling pipe enter filter cylinder before deduster, by deduster before filter cylinder, bulky grain smoke sample is collected in Before filter cylinder in the dust arrester of deduster, subsequently into filter cylinder, synchronizing after detecting, by filter cylinder and dust arrester while sending to It tests.
The beneficial effects of the present invention are:
Structure of the invention is reasonable, by deduster before installation filter cylinder, by the dust of bulky grain sample collection deduster before filter cylinder In device, to guarantee that filter cylinder will not be fully loaded with, continuous sampling is kept, completes to detect the synchronous of deduster removal efficiency.
The present invention is described for way of example above, but the present invention is not limited to above-mentioned specific implementation case, all bases It is all belonged to the scope of protection of the present invention in any changes or modifications that the present invention is done.

Claims (1)

1. a kind of high-temperature high dust dioxin sampling apparatus, it is characterised in that: including shell, sampling pipe, thermocouple, Pitot tube, filter Deduster, filter cylinder, Gas Phase Adsorption unit, sampling pump, control device with condensing unit before cylinder;
The enclosure interior is fixedly installed control device, Gas Phase Adsorption unit, sampling pump and pipeline with condensing unit;
The control device includes PLC control system, pressure sensor one, pressure sensor two, temperature sensor, flow sensing Device, flow regulator;The pressure sensor one, pressure sensor two, temperature sensor, flow sensor, flow are adjusted Device is electrically connected with PLC control system respectively;
The thermocouple is fixed at housing forward end, and the thermocouple is electrically connected with PLC control system;
The Pitot tube is fixed at housing forward end, and the Pitot tube is electrically connected with pressure sensor one;
The sampling pipe is fixed at housing forward end, and the sampling pipe back-end sealing is connected with deduster before filter cylinder, the filter Deduster rear end is connected with filter cylinder before cylinder, and the filter cylinder pipeline is tightly connected the Gas Phase Adsorption unit for having condensing unit;
The sampling pump is successively tightly connected flow regulator, flow sensor and the gas phase with condensing unit by pipeline Absorbing unit;
The pipeline is sealedly connected with pressure sensor two, temperature sensor;
Deduster includes body, air inlet, dust arrester one, cyclone dust collectors, dust arrester two, gas outlet before the filter cylinder;
The air inlet is set to body left upper portion, is sealedly connected with dismountable dust arrester one below the air inlet;
The cyclone dust collectors are fixedly installed on body lower right side, are sealedly connected with below the cyclone dust collectors dismountable Dust arrester two;The gas outlet is fixedly installed on body right upper portion.
CN201810158964.7A 2018-02-26 2018-02-26 A kind of high-temperature high dust dioxin sampling apparatus Pending CN110196176A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810158964.7A CN110196176A (en) 2018-02-26 2018-02-26 A kind of high-temperature high dust dioxin sampling apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810158964.7A CN110196176A (en) 2018-02-26 2018-02-26 A kind of high-temperature high dust dioxin sampling apparatus

Publications (1)

Publication Number Publication Date
CN110196176A true CN110196176A (en) 2019-09-03

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810158964.7A Pending CN110196176A (en) 2018-02-26 2018-02-26 A kind of high-temperature high dust dioxin sampling apparatus

Country Status (1)

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CN (1) CN110196176A (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202013287U (en) * 2011-03-09 2011-10-19 江苏省优联检测技术服务有限公司 Sampling system used for dioxins detection in stationary source exhaust
CN105181402A (en) * 2015-09-23 2015-12-23 广东电网有限责任公司电力科学研究院 Low-concentration smoke dust sampling device and method
CN205067163U (en) * 2015-08-26 2016-03-02 泰州市环境监测中心站 Multi -functional smoke and dust flue gas sampling rifle
CN107560900A (en) * 2017-08-29 2018-01-09 中国环境科学研究院 A kind of particulate matter zero loses collection system
CN208026517U (en) * 2018-02-26 2018-10-30 青岛恒远科技发展有限公司 A kind of high-temperature high dust bioxin sampling apparatus

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202013287U (en) * 2011-03-09 2011-10-19 江苏省优联检测技术服务有限公司 Sampling system used for dioxins detection in stationary source exhaust
CN205067163U (en) * 2015-08-26 2016-03-02 泰州市环境监测中心站 Multi -functional smoke and dust flue gas sampling rifle
CN105181402A (en) * 2015-09-23 2015-12-23 广东电网有限责任公司电力科学研究院 Low-concentration smoke dust sampling device and method
CN107560900A (en) * 2017-08-29 2018-01-09 中国环境科学研究院 A kind of particulate matter zero loses collection system
CN208026517U (en) * 2018-02-26 2018-10-30 青岛恒远科技发展有限公司 A kind of high-temperature high dust bioxin sampling apparatus

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