CN110182898A - A kind of water-oil separating experimental provision - Google Patents
A kind of water-oil separating experimental provision Download PDFInfo
- Publication number
- CN110182898A CN110182898A CN201910593813.9A CN201910593813A CN110182898A CN 110182898 A CN110182898 A CN 110182898A CN 201910593813 A CN201910593813 A CN 201910593813A CN 110182898 A CN110182898 A CN 110182898A
- Authority
- CN
- China
- Prior art keywords
- water
- glass
- oil separating
- oil
- silica gel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000011521 glass Substances 0.000 claims abstract description 69
- 239000000741 silica gel Substances 0.000 claims abstract description 23
- 229910002027 silica gel Inorganic materials 0.000 claims abstract description 23
- 239000000463 material Substances 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000004744 fabric Substances 0.000 claims abstract description 4
- 239000006260 foam Substances 0.000 claims abstract description 4
- 230000002209 hydrophobic effect Effects 0.000 claims abstract description 4
- 239000002184 metal Substances 0.000 claims abstract description 4
- 235000019198 oils Nutrition 0.000 claims description 18
- 235000019476 oil-water mixture Nutrition 0.000 claims description 3
- 238000004381 surface treatment Methods 0.000 claims description 3
- 239000004519 grease Substances 0.000 claims description 2
- 230000001276 controlling effect Effects 0.000 claims 2
- 230000001105 regulatory effect Effects 0.000 claims 2
- 239000003921 oil Substances 0.000 description 44
- 238000000926 separation method Methods 0.000 description 6
- 239000002351 wastewater Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- 230000003075 superhydrophobic effect Effects 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 238000005452 bending Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000013505 freshwater Substances 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/40—Devices for separating or removing fatty or oily substances or similar floating material
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The invention discloses a kind of water-oil separating experimental provision, which includes Buchner funnel, water-oil separating material, blender, two mouth flask, rubber stopper, curved glass pipe, silica gel catheter, glass straight hole section door, glass bottle,suction, right-angled glass pipe, vacuum pump using circulatory water, digital low vacuum measuring cell and Y shape glass three-way；Water-oil separating material is fixed on the Buchner funnel being connect by rubber stopper with two mouth flask；Glass bottle,suction with glass straight hole section door and right-angled glass pipe is connect by right-angled glass pipe, silica gel catheter and curved glass pipe with two mouth flask；Y shape glass three-way is connected to vacuum pump using circulatory water, digital low vacuum measuring cell and glass bottle,suction by silica gel catheter；The water-oil separating material is by being surface-treated one of the foam metal with hydrophobic oleophilic oil property, ultra-hydrophobic cloth.Water-oil separating can be fast implemented using the present apparatus, and can accurately test draft required for water-oil separating.
Description
Technical field
The present invention relates to a kind of water-oil separating experimental provisions, belong to oily water separation technique field.
Background technique
A large amount of organic solvents and all kinds of oil product class compounds not soluble in water can be generated in modern industrial production, these are not
Dissolubility oils can serious contaminated soil resource and water resource, wherein oil field generate waste water oil concentration 5000-10000ppm, and
Oil refinery waste water oil content may be up to 1000ppm or more, according to statistics, oil field, oil plant and petrochemical plant, the oil-containing discharged every year
Waste water is up to 300,000 tons, if these oily waste waters can cause World Freshwater Resources very big without the processing of science
Pollution.Therefore, it is extremely urgent to research and develop new and effective oily water separation technique, furthermore, it is also desirable to a kind of new water-oil separating
Method improves oil recovery rate.In order to solve oily waste water destruction caused by environment, various be suitable for is had developed at present
The technology of water-oil separating and new and effective water-oil separating material.Wherein, super-hydrophobic separation membrane technology is water-oil separating field
The popular research direction emerged.Super-hydrophobic seperation film have special surface wettability, with super-hydrophobic and super oleophylic the two
With the characteristics of extreme nature.But current water-oil separating belongs to intermittent operation mostly, process is more and therefore inefficiency has
Necessity invents new oily-water seperating equipment, and to realize continuous separation in situ, oil product is directly continuously recycled from oil water mixture.
In order to realize that above-mentioned target, the present invention propose that a kind of novel water-oil separating experimental provision, Buchner funnel pass through
Rubber stopper and two mouth flask link together, and water-oil separating material is placed in Buchner funnel；Curved glass pipe and two mouth flask
It is fixed together by rubber stopper；Glass straight hole section door and right-angled glass pipe are fixed on one by rubber stopper and glass bottle,suction
It rises；The other end of right-angled glass pipe connects silica gel catheter, and silica gel catheter end is fastened on the bending glass in two mouth flask
Glass pipe；Glass three-way is connected to vacuum pump using circulatory water, digital low vacuum measuring cell and glass bottle,suction by silica gel catheter；It follows
Ring water vacuum pump provides the draft of water-oil separating, regulates and controls the draft being applied on oil transportation material by glass straight hole section door, and lead to
Cross the draft that digital low vacuum measuring cell accurately shows water-oil separating.Water-oil separating can efficiently be realized using the present apparatus, and
Draft needed for water-oil separating capable of accurately being tested.
Summary of the invention
It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of water-oil separating experimental provisions.
The present invention solves its technical problem and is achieved through the following technical solutions: the device includes Buchner funnel, grease
Separation material, two mouth flask, curved glass pipe, blender, rubber stopper, silica gel catheter, glass bottle,suction, right-angled glass pipe, Y shape
Glass three-way, glass straight hole section door, vacuum pump using circulatory water, digital low vacuum measuring cell；Buchner funnel passes through rubber stopper and two
Mouth flask is fixed together, and water-oil separating material is placed inside Buchner funnel；Two mouth flask and curved glass pipe pass through rubber stopper
It is fixed together；Glass straight hole section door and right-angled glass pipe are fixed together by rubber stopper and glass bottle,suction；Right-angled glass
The other end of pipe connects silica gel catheter, and the silica gel catheter other end is fastened on the curved glass pipe of two mouth flask；Y shape glass
Glass threeway is connected to vacuum pump using circulatory water, digital low vacuum measuring cell and glass bottle,suction by silica gel catheter；The oil
Water separation material is one kind by the foam metal with hydrophobic oleophilic oil property of surface treatment, ultra-hydrophobic cloth.Using this
Device can fast implement water-oil separating, and can accurately test draft required for water-oil separating.
The invention has the benefit that the device applicability is extensive, mild condition, simple process；It can be widely applied to not
It is dissolved in the organic solvent of water and the water-oil separating experimental study of the multiple uses such as all kinds of oil product class compounds, there is good popularization
Application prospect.
Detailed description of the invention
The present invention is described further with reference to the accompanying drawings and examples.
Fig. 1 is outside drawing of the invention.
In figure: 1- water-oil separating material, 2- rubber stopper, 3- two mouth flask, 4- blender, 5- Buchner funnel, 6-
Rubber stopper, 7- curved glass pipe, 8- silica gel catheter, 9- right-angled glass pipe, 10- glass straight hole section door, 11- rubber stopper,
The digital low vacuum of 12- glass bottle,suction, 13- silica gel catheter, 14-Y shape glass three-way, 15- silica gel catheter, 16- surveys pressure
Instrument, 17- vacuum pump using circulatory water.
Specific embodiment
The present invention is further described below by specific embodiment, it is not to limit that following instance, which is descriptive,
Property, this does not limit the scope of protection of the present invention.
A kind of water-oil separating experimental provision characterized by comprising 1- water-oil separating material, 2- rubber stopper, 3- two
Mouth flask, 4- blender, 5- Buchner funnel, 6- rubber stopper, 7- curved glass pipe, 8- silica gel catheter, 9- right-angled glass
Pipe, 10- glass straight hole section door, 11- rubber stopper, 12- glass bottle,suction, 13- silica gel catheter, 14-Y shape glass three-way,
The digital low vacuum measuring cell of 15- silica gel catheter, 16-, 17- vacuum pump using circulatory water.Wherein, Buchner funnel passes through rubber stopper
It is fixed together with two mouth flask, water-oil separating material is placed inside Buchner funnel；Two mouth flask and curved glass pipe pass through rubber
Rubber plug is fixed together；Glass straight hole section door and right-angled glass pipe are fixed together by rubber stopper and glass bottle,suction；Right angle
The other end of glass tube connects silica gel catheter, and the silica gel catheter other end is fastened on the curved glass pipe of two mouth flask；Y
Shape glass three-way is connected to vacuum pump using circulatory water, digital low vacuum measuring cell and glass bottle,suction by silica gel catheter；It is described
Water-oil separating material be by one of the foam metal with hydrophobic oleophilic oil property of surface treatment, ultra-hydrophobic cloth.
Start vacuum pump using circulatory water, generate draft, by adjusting the opening degree of glass straight hole section door, regulation is applied to water-oil separating material
Draft on material, oil can be entered in bottle,suction by water-oil separating material in oil water mixture, realize water-oil separating, and can be with
Draft required for water-oil separating is accurately tested by digital low vacuum measuring cell.
Claims (4)
1. a kind of water-oil separating experimental provision, it is characterised in that: including a Buchner funnel, a water-oil separating material, one
Two mouth flask, a curved glass pipe, a blender, three rubber stoppers, four silica gel catheters, a glass bottle,suction, one
A right-angled glass pipe, a Y shape glass three-way, a glass straight hole section door, a vacuum pump using circulatory water, one digital low true
Empty measuring cell；Buchner funnel is fixed together by rubber stopper and two mouth flask, and water-oil separating material is placed in the bottom of Buchner funnel
Material；Two mouth flask and curved glass pipe are fixed together by rubber stopper；Glass straight hole section door and right-angled glass pipe pass through rubber
Plug and glass bottle,suction are fixed together；The other end of right-angled glass pipe connects silica gel catheter, the connection of the silica gel catheter other end
It is fixed on the curved glass pipe of two mouth flask；Y shape glass three-way is connected to vacuum pump using circulatory water, digital by silica gel catheter
Low vacuum measuring cell and glass bottle,suction.
2. a kind of water-oil separating experimental provision according to claim 1, it is characterised in that: the water-oil separating material is
Pass through one of the foam metal with hydrophobic oleophilic oil property of surface treatment, ultra-hydrophobic cloth.
3. a kind of water-oil separating experimental provision according to claim 1, it is characterised in that: the blender provides grease
The power of mixability, by the rotation speed regulating and controlling oil water mixture mixability for controlling blender.
4. a kind of water-oil separating experimental provision according to claim 1, it is characterised in that: the vacuum pump using circulatory water mentions
For the draft of water-oil separating, the draft being applied in water-oil separationg film is regulated and controled by glass straight hole section door, by digital low true
Empty measuring cell accurately shows the draft of water-oil separating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910593813.9A CN110182898A (en) | 2019-07-03 | 2019-07-03 | A kind of water-oil separating experimental provision |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910593813.9A CN110182898A (en) | 2019-07-03 | 2019-07-03 | A kind of water-oil separating experimental provision |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110182898A true CN110182898A (en) | 2019-08-30 |
Family
ID=67724772
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910593813.9A Pending CN110182898A (en) | 2019-07-03 | 2019-07-03 | A kind of water-oil separating experimental provision |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110182898A (en) |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201240886Y (en) * | 2008-08-18 | 2009-05-20 | 曾金华 | Full-automatic |
| RU2449267C1 (en) * | 2010-08-26 | 2012-04-27 | Сергей Геннадьевич Юзов | Vacuum capillary device for determining amount of weakly bound moisture in food products |
| CN103801274A (en) * | 2014-02-28 | 2014-05-21 | 天津工业大学 | Preparation method of oil-absorbing hollow fiber porous membrane |
| CN105002721A (en) * | 2015-06-16 | 2015-10-28 | 西北师范大学 | Preparation of abrasion-resisting super-hydrophobic cotton cloth and application of cotton cloth in oil-water separation |
| CN105442514A (en) * | 2015-12-08 | 2016-03-30 | 中国科学院新疆理化技术研究所 | Oil slick collection method |
| CN105858930A (en) * | 2016-04-20 | 2016-08-17 | 中国科学院新疆理化技术研究所 | Method for treating oil-containing sewage by utilizing oil-water separator |
| CN109307649A (en) * | 2017-09-01 | 2019-02-05 | 中国石油化工股份有限公司 | A kind of skid-mounted type water surface oil absorption material test device |
| CN210214874U (en) * | 2019-07-03 | 2020-03-31 | 青岛科技大学 | Oil-water separation experimental device |
-
2019
- 2019-07-03 CN CN201910593813.9A patent/CN110182898A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201240886Y (en) * | 2008-08-18 | 2009-05-20 | 曾金华 | Full-automatic |
| RU2449267C1 (en) * | 2010-08-26 | 2012-04-27 | Сергей Геннадьевич Юзов | Vacuum capillary device for determining amount of weakly bound moisture in food products |
| CN103801274A (en) * | 2014-02-28 | 2014-05-21 | 天津工业大学 | Preparation method of oil-absorbing hollow fiber porous membrane |
| CN105002721A (en) * | 2015-06-16 | 2015-10-28 | 西北师范大学 | Preparation of abrasion-resisting super-hydrophobic cotton cloth and application of cotton cloth in oil-water separation |
| CN105442514A (en) * | 2015-12-08 | 2016-03-30 | 中国科学院新疆理化技术研究所 | Oil slick collection method |
| CN105858930A (en) * | 2016-04-20 | 2016-08-17 | 中国科学院新疆理化技术研究所 | Method for treating oil-containing sewage by utilizing oil-water separator |
| CN109307649A (en) * | 2017-09-01 | 2019-02-05 | 中国石油化工股份有限公司 | A kind of skid-mounted type water surface oil absorption material test device |
| CN210214874U (en) * | 2019-07-03 | 2020-03-31 | 青岛科技大学 | Oil-water separation experimental device |
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|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20190830 |