CN110172374A - A kind of agalloch eaglewood solid spice and its preparation method and application - Google Patents
A kind of agalloch eaglewood solid spice and its preparation method and application Download PDFInfo
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- CN110172374A CN110172374A CN201910380496.2A CN201910380496A CN110172374A CN 110172374 A CN110172374 A CN 110172374A CN 201910380496 A CN201910380496 A CN 201910380496A CN 110172374 A CN110172374 A CN 110172374A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
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- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention provides a kind of agalloch eaglewood solid spice and its preparation method and application, is related to field of perfumery.Solid spice preparation method of the invention, comprising the following steps: emulsion reaction: agilawood essential oil is mixed with normal heptane, and emulsifier, mixing is added；Polyethylene dissolving alcohol: polyvinyl alcohol is mixed with water, is heated, dissolution；Polymerization reaction: poly-vinyl alcohol solution is mixed with the mixture after emulsion reaction, and inorganic acid and pentanediol is added in heating, and pH adjusting agent is added, obtains agilawood essential oil spice solution；It is dry: the agilawood essential oil spice solution being stood, supernatant is removed, surplus solution is dried, obtain agalloch eaglewood solid spice.Agalloch eaglewood solid spice of the invention has the function of sustained release, is applied to fabric treating, can achieve the effect that lasting lasting and water-fastness.
Description
Technical field
The present invention relates to washing fields, more particularly to a kind of agalloch eaglewood solid spice and its preparation method and application.
Background technique
Have a long history in the use of essence in people's daily life, since ancient times people just have using sachet,
The custom of the personal effects such as sachet is also indispensable one in the modern various articles containing essence in people's daily life
Part.According to scientific research, there are many benefits to human body for essence, such as promote blood circulation of human body, adjust nerve system of human body,
To human body play tranquilizing soporific, releive fatigue effect, and have the function of centainly have antibacterial, sterilizing, Anti-moth-eating etc..It is existing
Make clothing keep fragrance mode be mostly be surface-treated, still, since essence is generally volatile component, perfume substantiation
It is short, and intolerant to washing, improve the use cost of essence.
Summary of the invention
Based on this, it is necessary to for not lasting enough the technical problem of existing clothing processing lasting, it is solid to provide a kind of agalloch eaglewood
The preparation method of body note material.
A kind of preparation method of agalloch eaglewood solid spice, comprising the following steps:
Emulsion reaction: agilawood essential oil is mixed with normal heptane, and emulsifier, mixing is added；
Polyethylene dissolving alcohol: polyvinyl alcohol is mixed with water, is heated, and dissolution obtains poly-vinyl alcohol solution；
Polymerization reaction: above-mentioned poly-vinyl alcohol solution is mixed with the mixture after emulsion reaction, heating, be added inorganic acid and
Pentanediol is added pH adjusting agent, obtains agilawood essential oil spice solution；
It is dry: the agilawood essential oil spice solution being stood, supernatant is removed, surplus solution is dried, sunk
Fragrant solid spice.
Agilawood essential oil is rolled into microcapsules, utricule using polyvinyl alcohol by the agalloch eaglewood solid spice that the preparation method obtains
In agilawood essential oil can have the function of sustained release by the aperture on micro-capsule with time slow release, be applied to fabric weaving,
It can achieve the effect that lasting lasting and water-fastness.
The inorganic acid is hydrochloric acid, nitric acid or sulfuric acid in one of the embodiments,；The pH adjusting agent is sodium hydroxide
Solution or potassium hydroxide solution.
The emulsifier is selected from one of the embodiments: Sorbitan Oleate (sorbester p17), single glycerine fatty acid rouge,
One of triglycerin fatty acid ester and polysorbate (Tween 80) are a variety of, preferably sorbester p17, and sorbester p17 is safe and efficient
Advanced lipophilic emulsifier, and have good smoothing effect to fiber, there is fabric softener of the invention good
Antistatic effect.
The emulsion reaction step in one of the embodiments, specifically: by 8~12 parts by weight agilawood essential oils with 10~
The mixing of 15 parts by weight normal heptanes is added 3~5 parts by weight Emulsifier, stirs 2~4 hours at 20~30 DEG C；
The polyethylene dissolving alcohol step specifically: 12~18 weight account polyethylene alcohol are mixed with water, are heated, stirring,
Dissolution obtains the poly-vinyl alcohol solution that mass fraction is 3.5%~4.0%；
The polymerization procedure specifically: being heated to temperature is 45~50 DEG C, and above-mentioned poly-vinyl alcohol solution is added to
In mixture after emulsion reaction, 13~17min is stirred, 3~8 parts by weight of inorganic acid and 10~15 parts by weight pentanediols are added dropwise,
After reacting 25~35min, stop heating, it is 6~7 to get agilawood essential oil spice solution that pH adjusting agent to pH value, which is added dropwise,.
The drying steps in one of the embodiments, specifically: agilawood essential oil spice solution is stood into 10~14h,
Supernatant is removed, agalloch eaglewood solid spice is made by spray drying in surplus solution.
One aspect of the present invention further includes a kind of agalloch eaglewood solid spice that above-mentioned preparation method obtains.
The agalloch eaglewood solid spice is applied to fabric treating, has the function of being sustained, can reach lasting lasting and water-fastness
Effect.
One aspect of the present invention further includes a kind of preparation method of cotton fabric, is located in advance using above-mentioned agalloch eaglewood solid spice
Reason.
The preparation method of the cotton fabric is pre-processed using agalloch eaglewood solid spice of the invention, obtained cotton fabric tool
There are lasting lasting, water-fastness effect.
It is described in one of the embodiments, that pretreated step is carried out using agalloch eaglewood solid spice specifically: by agalloch eaglewood
Solid spice and water are mixed with the mass ratio of 1:750~850, and the dissolution of agalloch eaglewood solid spice obtains agalloch eaglewood spice solution, will be described
Agalloch eaglewood spice solution sprays on cotton fiber, squirt pretreatment, and environment temperature is 45~50 DEG C, spray time for 45~
50h, keeping the regain of cotton fiber is 12%~14.5%.
In one of the embodiments, before carrying out spraying pretreatment using agalloch eaglewood solid spice, alkali is carried out to cotton fiber
Processing, alkali treatment specifically: the sodium hydroxide solution of 4~5g/L is added into cotton fiber, bath raio is 1:18~22, processing
Temperature is 55~65 DEG C, and the processing time is 170~190min, cleans, dries.Wherein, bath raio refers to sodium hydroxide solution volume
With the ratio of fabric weight.
Opening picking, cotton carding, combed cotton, drafting, thick is additionally provided with after the pre-treatment step in one of the embodiments,
The step of yarn, spun yarn and winder；
In the opening picking step, the equipment used is A003B automatic plucker, A052 type condenser and FA001A roller
Dredge needle opener；
In the cotton carding step, the equipment used is A199G type carding machine；
In the combed cotton step, the equipment used is A209D type combing machine；
In the drafting step, the equipment used is FA003A type drawing frame；
In the rove step, the equipment used is that THF004A type hangs ingot coarse sand maker；
In the spun yarn step, the equipment used is FA602 type compact spinning frame；
In the winder step, the equipment used is LT3200 type bobbin-winding machine.
One aspect of the present invention further includes the cotton fabric that the preparation method of above-mentioned cotton fabric obtains.
The cotton fabric has the effect of lasting lasting, water-fastness, antibacterial.
Compared with prior art, the invention has the following advantages:
Agilawood essential oil is rolled into microcapsules using polyvinyl alcohol, the agalloch eaglewood in utricule by agalloch eaglewood solid spice of the invention
Essential oil can have the function of sustained release, be applied to fabric treating, can reach by the aperture on micro-capsule with time slow release
Lasting lasting, water-fastness and antibacterial effect.
Specific embodiment
It to facilitate the understanding of the present invention, below will be to invention is more fully described.Following present of the invention
Preferred embodiment.But the invention can be realized in many different forms, however it is not limited to embodiment described herein.
It is made the disclosure of the present invention more thorough and comprehensive on the contrary, purpose of providing these embodiments is.
Unless otherwise defined, all technical and scientific terms used herein and belong to technical field of the invention
The normally understood meaning of technical staff is identical.Term as used herein in the specification of the present invention is intended merely to description tool
The purpose of the embodiment of body, it is not intended that in the limitation present invention.
Embodiment 1
A kind of agalloch eaglewood solid spice, is prepared by the following preparation method:
Emulsion reaction: 10g agilawood essential oil is added in the flask equipped with 12.5g normal heptane, 3g emulsifier span is added
80, the mechanical stirring 3 hours in 25 DEG C of water-baths；
Polyethylene dissolving alcohol: weighing 15g polyvinylalcohol solids, is added in beaker, adds water, be heated under agitation molten
Solution, is made into the poly-vinyl alcohol solution that mass fraction is 3.8%, and poly-vinyl alcohol solution is transparence liquid；
Polymerization reaction: under the conditions of 48 DEG C, above-mentioned poly-vinyl alcohol solution being added in the flask after emulsion reaction occurs,
Hydrochloric acid solution and 5ml pentanediol that 9ml concentration is 36% is slowly added dropwise after stirring 15min, after making solution be in acid, stops adding
Enter hydrochloric acid, continue to be slowly added dropwise 10ml pentanediol, after reacting 30min, stop heating, then with sodium hydroxide solution adjust pH value to
7.0 to get.
It is dry: agilawood essential oil spice solution being stood into 12h, removes supernatant, it is heavy that surplus solution is made up of spray drying
Fragrant solid spice.
Embodiment 2
A kind of cotton fabric, is prepared by the following preparation method:
(1) pre-process: the sodium hydroxide solution of 4.5g/L, bath raio 1:20, processing are added into cotton fiber for taking cotton fiber
Temperature is 60 DEG C, and the processing time is 180min, is washed, and dehydration is dried；Agalloch eaglewood solid spice and water are mixed with the mass ratio of 1:800
It closes, the dissolution of agalloch eaglewood solid spice obtains agalloch eaglewood spice solution, agalloch eaglewood spice solution is sprayed in the cotton fiber Jing Guo alkali process
On, squirt pretreatment, environment temperature is 50 DEG C, spray time 50h, keep the regain of cotton fiber be 12%~
14.5%；It will be dried by the pretreated cotton fiber of agalloch eaglewood solid spice solution；
(2) opening picking: needle opener opening or cleaning is dredged using A003B automatic plucker, A052 type condenser and FA001A roller
Cotton；
(3) cotton carding: cotton carding is carried out using A199G type carding machine；
(4) combed cotton: combed cotton is carried out using A209D type combing machine；
(5) drafting: drafting is carried out using FA003A type drawing frame；
(6) rove: ingot coarse sand maker is hanged using THF004A type and carries out rove；
(7) spun yarn: spun yarn is carried out using FA602 type compact spinning frame；
(8) winder: using LT3200 type bobbin-winding machine carry out winder to get.
Embodiment 3
A kind of cotton fabric, the difference from example 2 is that, the mass ratio of agalloch eaglewood solid spice and water is in pre-treatment step
1:750。
Embodiment 4
A kind of agalloch eaglewood solid is fragrant, the difference from embodiment 1 is that, preparation method are as follows:
Emulsion reaction: 8g agilawood essential oil being added in the flask equipped with 10g normal heptane, 3g emulsifier span 80 is added,
The mechanical stirring 4 hours in 30 DEG C of water-baths；
Polyethylene dissolving alcohol: weighing 12g polyvinylalcohol solids, is added in beaker, adds water, be heated under agitation molten
Solution, is made into the poly-vinyl alcohol solution that mass fraction is 3.5%, and poly-vinyl alcohol solution is transparence liquid；
Polymerization reaction: under the conditions of 48 DEG C, above-mentioned poly-vinyl alcohol solution being added in the flask after emulsion reaction occurs,
Hydrochloric acid solution and 4ml pentanediol that 9ml concentration is 36% is slowly added dropwise after stirring 15min, after making solution be in acid, stops adding
Enter hydrochloric acid, continue to be slowly added dropwise 10ml pentanediol, after reacting 30min, stop heating, then with sodium hydroxide solution adjust pH value to
7.0 to get.
It is dry: agilawood essential oil spice solution being stood into 12h, removes supernatant, it is heavy that surplus solution is made up of spray drying
Fragrant solid spice.
Embodiment 5
A kind of agalloch eaglewood solid is fragrant, the difference from embodiment 1 is that, preparation method are as follows:
Emulsion reaction: 12g agilawood essential oil being added in the flask equipped with 15g normal heptane, 5g emulsifier span 80 is added,
The mechanical stirring 4 hours in 30 DEG C of water-baths；
Polyethylene dissolving alcohol: weighing 18g polyvinylalcohol solids, is added in beaker, adds water, be heated under agitation molten
Solution, is made into the poly-vinyl alcohol solution that mass fraction is 4.0%, and poly-vinyl alcohol solution is transparence liquid；
Polymerization reaction: under the conditions of 48 DEG C, above-mentioned poly-vinyl alcohol solution being added in the flask after emulsion reaction occurs,
Hydrochloric acid solution and 5ml pentanediol that 9ml concentration is 36% is slowly added dropwise after stirring 15min, after making solution be in acid, stops adding
Enter hydrochloric acid, continue to be slowly added dropwise 10ml pentanediol, after reacting 30min, stop heating, then with sodium hydroxide solution adjust pH value to
6.0 to get.
It is dry: agilawood essential oil spice solution being stood into 14h, removes supernatant, it is heavy that surplus solution is made up of spray drying
Fragrant solid spice.
Comparative example 1
A kind of commercially available agalloch eaglewood essence surface printing cotton fabric.
Comparative example 2
A kind of cotton fabric, the difference from example 2 is that, agalloch eaglewood solid spice solution is not added in pretreatment, and add
Agilawood essential oil dilution, the agilawood essential oil dilution are that agilawood essential oil and water are obtained with mass ratio 1:800 mixed diluting.
Experimental example 1 (long lasting quality test)
Using the long lasting quality of natural exposing method test cotton fabric, by the cotton fabric of embodiment 2, comparative example 1 and comparative example 2
It, will be pure after nature is placed 0 day, 15 days, 30 days, 45 days, 60 days, 75 days, 90 days, 105 days, 120 days, 135 days, 150 days respectively
Cotton fabric shreds, and accurate weighing 1g is placed it in sealable container, and 100ml absolute alcohol is then added, using water-bath plus
Heat after fulling shake and stands 24 hours, using UV detector, sets wavelength 284nm, measures the content of essence
(mg), test result is as shown in table 1:
1 long lasting quality test result of table
As it can be seen from table 1 the cotton fabric that the present invention implements 2 passes through 135 days, essence content reaches basicly stable, passes through
Organoleptic method, agalloch eaglewood solid spice cotton fabric reach substantially tasteless state in 145 talentes, and lasting is lasting.Comparative example 1 and comparative example 2
It is released into substantially in 15 days or so fragrance, reaches stationary value, sustained release performance is poor, and lasting amount is few.
Experimental example 2 (wash durability test)
Using the wash durability of machine washing method test cotton fabric.By the cotton fabric of embodiment 2, comparative example 1 and comparative example 2 point
It is not put into washing machine, detergent is added, bath raio (detergent volume and cotton fabric weight ratio) is 1:25, is impregnated 5 minutes, washing
5 minutes, dehydration was dried, if remaining fragrance on cotton fabric, the step of repeating above-mentioned immersion, washing, be dehydrated, dry, until
Until fabric substantially tasteless, washing times are recorded.Test result is as shown in table 2:
2 wash durability test result of table (unit: secondary)
| Embodiment 2 | Comparative example 1 | Comparative example 2 | |
| Washing times | 16 | 3 | 5 |
It is known from Table 2 that the water-fastness number of the embodiment of the present invention 2 be 16 times, the 3~5 of the comparative example that compares 1 and comparative example 2
Secondary, wash durability of the invention has greatly improved.
Experimental example 3 (anti-microbial property test)
The cotton fabric of testing example 2 is placed 0 day and after placement 45 days to staphylococcus aureus, Candida albicans, copper
The inhibitory activity of green pseudomonad and Escherichia coli, test method are colorimetric method: test strain be inoculated on agar medium,
It is separately added into the sample to be tested of embodiment 2, comparative example 1 and comparative example 2, is cultivated 24 hours under the conditions of 37 DEG C, with frost physiology
Salt water cleans culture dish, obtains eluate, and a certain amount of TNT reagent is added, and is measured with spectrophotometer in 525nm after stablizing
The light absorption value at place, the viable count after recording the effect of initial and softener, calculates bacteriostasis rate.Antibacterial test result is as shown in table 3:
The test of 3 antibacterial activity of table
From table 3 it can be seen that the cotton fabric of the embodiment of the present invention 2 has preferable fungistatic effect, and place a period of time
It is still able to maintain preferable antibiotic property afterwards.
Each technical characteristic of embodiment described above can be combined arbitrarily, for simplicity of description, not to above-mentioned reality
It applies all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, all should be considered as described in this specification.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention
Range.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.
The present invention provides a kind of agalloch eaglewood solid spice and its preparation method and application, is related to field of perfumery.Of the invention consolidates
Body note preparation method for material, comprising the following steps: emulsion reaction: agilawood essential oil is mixed with normal heptane, and emulsifier, mixing is added；
Polyethylene dissolving alcohol: polyvinyl alcohol is mixed with water, is heated, dissolution；Polymerization reaction: after poly-vinyl alcohol solution and emulsion reaction
Mixture mixing, heating is added inorganic acid and pentanediol, pH adjusting agent is added, obtains agilawood essential oil spice solution；It is dry:
The agilawood essential oil spice solution is stood, supernatant is removed, surplus solution is dried, obtain agalloch eaglewood solid spice.This
The agalloch eaglewood solid spice of invention has the function of sustained release, is applied to fabric treating, can reach lasting lasting and water-fastness effect
Fruit.
Claims (10)
1. a kind of preparation method of agalloch eaglewood solid spice, which comprises the following steps:
Emulsion reaction: agilawood essential oil is mixed with normal heptane, and emulsifier, mixing is added；
Polyethylene dissolving alcohol: polyvinyl alcohol is mixed with water, is heated, and dissolution obtains poly-vinyl alcohol solution；
Polymerization reaction: above-mentioned poly-vinyl alcohol solution is mixed with the mixture after emulsion reaction, and inorganic acid and penta 2 is added in heating
Alcohol is added pH adjusting agent, obtains agilawood essential oil spice solution；
It is dry: the agilawood essential oil spice solution being stood, supernatant is removed, surplus solution is dried, it is solid to obtain agalloch eaglewood
Body note material.
2. the preparation method of agalloch eaglewood solid spice according to claim 1, which is characterized in that the emulsifier is sapn
80；The inorganic acid is hydrochloric acid, nitric acid or sulfuric acid；The pH adjusting agent is sodium hydroxide solution or potassium hydroxide solution.
3. the preparation method of agalloch eaglewood solid spice according to claim 1 or 2, which is characterized in that the emulsion reaction step
Suddenly specifically: 8~12 parts by weight agilawood essential oils are mixed with 10~15 parts by weight normal heptanes, 3~5 parts by weight Emulsifier are added,
It is stirred 2~4 hours at 20~30 DEG C；
The polyethylene dissolving alcohol step specifically: 12~18 weight account polyethylene alcohol are mixed with water, are heated, are stirred, dissolution,
Obtain the poly-vinyl alcohol solution that mass fraction is 3.5%~4.0%；
The polymerization procedure specifically: being heated to temperature is 45~50 DEG C, and above-mentioned poly-vinyl alcohol solution is added to emulsification
In mixture after reaction, 13~17min is stirred, 3~8 parts by weight of inorganic acid and 10~15 parts by weight pentanediols, reaction is added dropwise
After 25~35min, stop heating, it is 6~7 to get agilawood essential oil spice solution that pH adjusting agent to pH value, which is added dropwise,.
4. the preparation method of agalloch eaglewood solid spice according to claim 3, which is characterized in that the drying steps are specific
Are as follows: agilawood essential oil spice solution is stood into 10~14h, removes supernatant, agalloch eaglewood solid is made by spray drying in surplus solution
Fragrance.
5. a kind of agalloch eaglewood solid spice obtained using the described in any item preparation methods of Claims 1 to 4.
6. a kind of preparation method of cotton fabric, which is characterized in that located in advance using the agalloch eaglewood solid spice described in claim 5
Reason.
7. the preparation method of cotton fabric according to claim 6, which is characterized in that described to be carried out using agalloch eaglewood solid spice
Pretreated step specifically: mix agalloch eaglewood solid spice and water with the mass ratio of 1:750~850, agalloch eaglewood solid spice is molten
Solution, obtains agalloch eaglewood spice solution, by agalloch eaglewood spice solution spray on cotton fiber, carries out squirting pretreatment, environment temperature
It is 45~50 DEG C, spray time is 45~50h, and keeping the regain of cotton fiber is 12%~14.5%.
8. the preparation method of cotton fabric according to claim 7, which is characterized in that sprayed using agalloch eaglewood solid spice
Before applying pretreatment, alkali process, alkali treatment are carried out to cotton fiber specifically: the hydroxide of 4~5g/L is added into cotton fiber
Sodium solution, bath raio are 1:18~22, and treatment temperature is 55~65 DEG C, and the processing time is 170~190min, cleans, dries.
9. according to the preparation method of the described in any item cotton fabrics of claim 6~8, which is characterized in that the pre-treatment step
After be additionally provided with opening picking, cotton carding, combed cotton, drafting, rove, spun yarn and winder step；
In the opening picking step, the equipment used is that A003B automatic plucker, A052 type condenser and FA001A roller dredge needle
Opener；
In the cotton carding step, the equipment used is A199G type carding machine；
In the combed cotton step, the equipment used is A209D type combing machine；
In the drafting step, the equipment used is FA003A type drawing frame；
In the rove step, the equipment used is that THF004A type hangs ingot coarse sand maker；
In the spun yarn step, the equipment used is FA602 type compact spinning frame；
In the winder step, the equipment used is LT3200 type bobbin-winding machine.
10. a kind of cotton fabric obtained using the described in any item preparation methods of claim 6~9.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111321589A (en) * | 2020-03-03 | 2020-06-23 | 刘志强 | Cloth processing technology containing Kyara lignum aquilariae resinatum component |
| CN113046883A (en) * | 2021-03-05 | 2021-06-29 | 李庆生 | Color yarn containing agarol and preparation method thereof |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103266375A (en) * | 2013-06-05 | 2013-08-28 | 南通纺织职业技术学院 | Method for processing kapok fiber yarns |
| CN103898649A (en) * | 2014-04-21 | 2014-07-02 | 爱谱诗（苏州）服装有限公司 | Fragrant yarn and manufacturing method thereof |
| CN104278408A (en) * | 2013-07-13 | 2015-01-14 | 江苏悦达纺织集团有限公司 | China-hemp shirt fabric and preparation method thereof |
| CN104830532A (en) * | 2015-05-12 | 2015-08-12 | 天津春发生物科技集团有限公司 | Preparation method of slow release microcapsule ginger oil essence |
| CN104878610A (en) * | 2015-06-18 | 2015-09-02 | 中山大学惠州研究院 | Preparing method for aroma-releasing type baffeta |
| CN205072082U (en) * | 2015-10-28 | 2016-03-09 | 郑培力 | Antibiotic women's pants |
| CN107090355A (en) * | 2017-03-16 | 2017-08-25 | 天津工业大学 | It is sustained the synthetic technology of essence microcapsule |
-
2019
- 2019-05-08 CN CN201910380496.2A patent/CN110172374B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103266375A (en) * | 2013-06-05 | 2013-08-28 | 南通纺织职业技术学院 | Method for processing kapok fiber yarns |
| CN104278408A (en) * | 2013-07-13 | 2015-01-14 | 江苏悦达纺织集团有限公司 | China-hemp shirt fabric and preparation method thereof |
| CN103898649A (en) * | 2014-04-21 | 2014-07-02 | 爱谱诗（苏州）服装有限公司 | Fragrant yarn and manufacturing method thereof |
| CN104830532A (en) * | 2015-05-12 | 2015-08-12 | 天津春发生物科技集团有限公司 | Preparation method of slow release microcapsule ginger oil essence |
| CN104878610A (en) * | 2015-06-18 | 2015-09-02 | 中山大学惠州研究院 | Preparing method for aroma-releasing type baffeta |
| CN205072082U (en) * | 2015-10-28 | 2016-03-09 | 郑培力 | Antibiotic women's pants |
| CN107090355A (en) * | 2017-03-16 | 2017-08-25 | 天津工业大学 | It is sustained the synthetic technology of essence microcapsule |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111321589A (en) * | 2020-03-03 | 2020-06-23 | 刘志强 | Cloth processing technology containing Kyara lignum aquilariae resinatum component |
| CN113046883A (en) * | 2021-03-05 | 2021-06-29 | 李庆生 | Color yarn containing agarol and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN110172374B (en) | 2022-12-30 |
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