CN110170365A - A kind of dispersing method of powder class cosmetics - Google Patents
A kind of dispersing method of powder class cosmetics Download PDFInfo
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- CN110170365A CN110170365A CN201910349658.6A CN201910349658A CN110170365A CN 110170365 A CN110170365 A CN 110170365A CN 201910349658 A CN201910349658 A CN 201910349658A CN 110170365 A CN110170365 A CN 110170365A
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- Prior art keywords
- powder
- class cosmetics
- dispersing method
- powder class
- blush
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/08—Preparations containing skin colorants, e.g. pigments for cheeks, e.g. rouge
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/12—Face or body powders for grooming, adorning or absorbing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C19/00—Other disintegrating devices or methods
- B02C19/06—Jet mills
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Inorganic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Food Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to cosmetic field, in particular to a kind of dispersing method of powder class cosmetics.This method includes acceptable raw material mixing in taking adhesive and other powder class cosmetics, and air-flow dispersion is carried out in airslide disintegrating mill；The pressure of the air-flow dispersion is 0.7Mpa.The present invention solves adhesive and the non-uniform situation of other feed distributions in powder class cosmetics using the air-flow dispersing method of specified pressure, it effectively improves drop test and not easily passs through problem, simultaneously effective avoid transportational process powder class cosmetics problem easy to break.
Description
Technical field
The present invention relates to cosmetic technical field more particularly to a kind of dispersing methods of powder class cosmetics.
Background technique
With the fast development of color make-up industry, powder agglomates class color make-up product is also rapidly developing, in the fast development of this industry
While, there is also many problems.There is the broken of larger proportion when wherein powder agglomates transports in consumer's hand, causes to disappear
The person of expense complains.The production method that powder agglomates class product uses at present is to carry out dispersion completion with blender and pulverizer, is produced in part
Product are easy dispersion unevenly, and causing to fall can't pass；Distribute the bright dispersing method used different from blender and pulverizer, has
The help product of effect improves anti-drop, reduces the broken ratio of powder agglomates.
In color make-up powder agglomates cosmetic field, due to the Sheng Xing of e-commerce, the distance of logistics farther out, express transportation risk
The phenomenon that uncertainty, powder class product is frequently present of fragmentation, receive the complaint of consumer；Show for complaining to research and develop: makeup
It is most important reason that being unevenly distributed of product dusty raw materials and adhesive, which causes powder agglomates broken,.
Summary of the invention
In view of this, the purpose of the present invention is to provide a kind of dispersing methods of powder class cosmetics, so that using this method
Powder class cosmetics are made
In order to achieve the object of the present invention, the present invention adopts the following technical scheme:
The present invention provides a kind of dispersing methods of powder class cosmetics, comprising: in taking adhesive and other powder class cosmetics
Acceptable raw material mixing, carries out air-flow dispersion in airslide disintegrating mill；
The pressure of the air-flow dispersion is 0.7Mpa.
The present invention solves cosmetics powder class raw material by air-flow good pressure distribution principle, using specific air-flow dispersion pressure
With the non-uniform situation of adhesive distribution, the problem of drop test not easily passs through is effectively improved.Air-flow dispersion passes through air-flow powder
Broken machine equipment is completed, its working principle is that the effects of mutual collision of high pressure draught and material, friction, keeps the material dispersion uniform,
Under the powerful centrifugal force effect that high-speed rotating stage turbine generates, makes thickness feed separation, meet thin of granularity requirements
Grain enters cyclone separator and deduster is collected, and coarse granule, which drops to disintegrating area, to be continued to crush.Through air-flow crushing treated object
Material, partial size is smaller and disperses more evenly, and effectively dusty raw materials and bonding can be more evenly distributed.
The working principle of airslide disintegrating mill is negative pressure caused by the high-speed jet that high compressed air passes through feed injector
So that powder material is sucked mixing chamber, and pulverizing chamber is ejected by high-speed jet.Several crushing nozzles are with outside pulverizing chamber, there is direction
Property to pulverizing chamber high speed spray, crush powder in pulverizing chamber, high-speed jet forms strong eddy flow in crushing chamber, by
Powerful centrifugal force caused by eddy flow makes powder particle crush high-speed motion near chamber interior walls.When powder particle is crushed to point
When below grade diameter, it is detached from classification eddy flow by centripetal airflow function, trapping system is entered by central outlet pipe and is collected.
3.1 feed injector
A. the air-flow HI high impact that the raw material that feed opening gets off is come out by feed injector.Accelerate particle constantly, due to
Particle plucked.Cause flow velocity in air-flow different.Thus make particle generate collision in mixing chamber and front particle to cause to crush
This part mainly crushes larger particles.
B. the raw material high speed that feed opening gets off is injected into pulverizing chamber by the high-speed jet of feed injector, with height in pulverizing chamber
The particle encounter of speed movement generates crushing.
3.2 pulverizing chambers are most important crushing positions in entire airslide disintegrating mill:
A. jet port --- since air-flow is sprayed with velocity of sound or ultrasonic flow velocity into pulverizing chamber in jet port, make jet stream
The collision of particle fierceness, friction in region cause to crush.
B. two beam high velocity stream infall --- impact comminution is formed to powder in two injection stream infalls.
C. in turbulent flow --- low-pressure area is generated around each high velocity stream, forms very strong turbulent flow, powder particle is in turbulent flow
Middle movement velocity is very big, and mutually fierce friction causes to crush.
In some embodiments, described adhesive is selected from sad certain herbaceous plants with big flowers acid glyceride, dimethyl silicone polymer, benzene oxygen second
One of alcohol, zinc stearate, ethylhexanoic acid glyceride are a variety of.
In certain embodiments, the binder includes sad certain herbaceous plants with big flowers acid glyceride, dimethyl silicone polymer, benzene oxygen second
Pure and mild zinc stearate；In other specific embodiments, described adhesive includes ethylhexanoic acid glyceride, dimethyl silicone polymer
And Phenoxyethanol.
In some embodiments, acceptable raw material is selected from filler, colorant, prevents in other described powder class cosmetics
One of rotten agent is a variety of.
Wherein, filler is selected from talcum powder, mica powder, silicon powder, nylon powder, magnesium silicate, boron nitride, kaolin, dimethyl
In silylated silica, one of aluminium oxide, aluminium hydroxide, bentonite or a variety of.
Colorant be selected from red CI15850, CI77891, CI77007, CI45380, CI45410, CI77491,
One of CI77492.CI77499, CI77718, CI15985 or a variety of.
In the present invention, the oil content or water content of the powder class cosmetics are no more than 10%.
In a specific embodiment, the powder class cosmetics are muffin, wherein adhesive includes sad certain herbaceous plants with big flowers acid glycerol
Ester, dimethyl silicone polymer, Phenoxyethanol and zinc stearate；Acceptable raw material includes talcum in other described powder class cosmetics
Powder, mica powder, silicon powder, nylon powder, CI77491, CI77492 and CI77499.
In another specific embodiment, the powder class cosmetics are blush, wherein adhesive includes thylhexoic acid glycerol
Ester, dimethyl silicone polymer, Phenoxyethanol；In other described powder class cosmetics acceptable raw material include talcum powder, mica powder,
Magnesium silicate, boron nitride, titanium dioxide, CI77491, CI15850 and CI77492.
The present invention also provides powder class cosmetics made from the dispersing method.
Product made of dispersing method of the present invention is the common powder class cosmetics in this field, as the preferred powder class
Cosmetics are powder agglomates class product, such as blush, finishing powder, muffin, eye shadow powder or brow powder,.
The present invention provides a kind of dispersing method of powder class cosmetics, comprising: can in taking adhesive and other powder class cosmetics
The raw material of receiving mixes, and air-flow dispersion is carried out in airslide disintegrating mill；The pressure of the air-flow dispersion is 0.7Mpa.The present invention point
It dissipates method and solves adhesive and the non-uniform situation of other feed distributions in powder class cosmetics using the air-flow of specified pressure, have
Effect improves drop test and not easily passs through problem, simultaneously effective avoids that transportational process powder class cosmetics are easy to break to ask
Topic.
Detailed description of the invention
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below
There is attached drawing needed in technical description to be briefly described.
Fig. 1 is drop test block diagram in embodiment 4；
Fig. 2 is muffin drop testing results figure in embodiment 4, wherein Fig. 2A shows the test result of muffin 1, and Fig. 2 B is powder
Cake 2, Fig. 2 C are muffin 3, and Fig. 2 D is muffin 4；
Fig. 3 is blush drop testing results figure in embodiment 4, wherein Fig. 3 A is blush 1, and Fig. 3 B is blush 2, and Fig. 3 C is
Blush 3, Fig. 3 D are blush 4；
Fig. 4 is muffin simulation transport test result figure in embodiment 4, wherein Fig. 4 A is muffin 1, and Fig. 4 B is muffin 2, figure
4C is muffin 3, and Fig. 4 D is muffin 4；
Fig. 5 is blush simulation transport test result figure in embodiment 4, wherein Fig. 5 A is blush 1, and Fig. 5 B is blush 2, figure
5C is blush 3, and Fig. 5 D is blush 4.
Specific embodiment
The invention discloses a kind of dispersing method of powder class cosmetics, those skilled in the art can use for reference present disclosure,
It is suitably modified realization of process parameters.In particular, it should be pointed out that all similar substitutions and modifications carry out those skilled in the art
Say it is it will be apparent that they are considered as being included in the present invention.Method and application of the invention has passed through preferred embodiment
It is described, related personnel can obviously not depart from the content of present invention, in spirit and scope to method described herein and answer
With being modified or appropriate changes and combinations, carry out implementation and application the technology of the present invention.
To the explanation of the disclosed embodiments, enable those skilled in the art to implement or use the present invention.To this
A variety of modifications of a little embodiments will be readily apparent to those skilled in the art, as defined herein general
Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, the present invention will not
It can be intended to be limited to the embodiments shown herein, and be to fit to consistent with the principles and novel features disclosed in this article
Widest scope.
The test material that the present invention uses is all common commercially available product, can all be bought in market.The cosmetic material of use meets
Cosmetics supervise relevant regulations, all meet the requirement of " cosmetics safety technical specification (version in 2015) ".
Below with reference to embodiment, the present invention is further explained:
The dispersing method of the present invention of embodiment 1
Acceptable raw material mixing, carries out air-flow point in airslide disintegrating mill in taking adhesive and other powder class cosmetics
It dissipates, the pressure of air-flow dispersion is 0.7Mpa.
The preparation of 2 muffin of embodiment
(1) muffin is prepared in formula as below ratio
1 muffin formula table of table
(2) preparation process
1. muffin production technology: 2kg Material is prepared by above-mentioned formula table, with small machines (8 liang of dress pulverizers) toner
It is pre-dispersed in advance；Base-material and pre-dispersed toner are added blender and mix 2 times, each incorporation time 5S, adhesive and preservative
Oil spout bucket is added, turn on agitator stirs 3 minutes, while oil has been sprayed；After machine stops stirring, open machine by lid and
The powder chipping of machine inner wall is clean, and locking cover is stirred for 1 minute, takes out Material.
The preparation of muffin 1: deserving to be called to state 1kg Material and cross traditional grinding machine and crushed, and takes out smashed Material and is pressed into
Type obtains muffin 1.
The preparation of muffin 2: taking above-mentioned 1Kg Material to carry out high pressure draught dispersion according to the method for embodiment 1, (pressure is
0.7Mpa), by the Material compression moulding after dispersion, muffin 2 is obtained.
The preparation of muffin 3: taking above-mentioned 1Kg Material to carry out high pressure draught dispersion in airslide disintegrating mill, (pressure is
0.6Mpa), by the Material compression moulding after dispersion, muffin 3 is obtained.
The preparation of muffin 4: taking above-mentioned 1Kg Material to carry out high pressure draught dispersion in airslide disintegrating mill, (pressure is
0.8Mpa), by the Material compression moulding after dispersion, muffin 4 is obtained.
Muffin is respectively suppressed when suppressing using the aluminium dish of same model, uniform pressure, identical dwell time, identical pressure maintaining number
6 powder agglomates out.
The preparation of 3 blush of embodiment
Blush is prepared in formula as below ratio
2 blush formula table of table
(2) blush production technology: 2kg Material is prepared by above-mentioned formula table, with small machines (8 liang of dress pulverizers) toner
It is pre-dispersed；Base-material and pre-dispersed toner are added blender and mix 2 times, each incorporation time 5S, and adhesive and preservative are added
Oil spout bucket, turn on agitator stir 5 minutes, while oil has been sprayed；After machine stops stirring, opening machine will be in lid and machine
The powder chipping of wall is clean, and locking cover is stirred for 1 minute, takes out Material.
The preparation of blush 1: deserving to be called to state 1kg Material and cross traditional grinding machine and crushed, and takes out smashed Material and is pressed into
Type obtains blush 1.
The preparation of blush 2: taking above-mentioned 1Kg Material to carry out high pressure draught dispersion according to the method for embodiment 1, (pressure is
0.7Mpa), by the Material compression moulding after dispersion, blush 2 is obtained.
The preparation of blush 3: taking above-mentioned 1Kg Material to carry out high pressure draught dispersion in airslide disintegrating mill, (pressure is
0.6Mpa), by the Material compression moulding after dispersion, blush 3 is obtained.
The preparation of blush 4: taking above-mentioned 1Kg Material to carry out high pressure draught dispersion in airslide disintegrating mill, (pressure is
0.8Mpa), by the Material compression moulding after dispersion, blush 4 is obtained.
Blush is respectively suppressed when suppressing using the aluminium dish of same model, uniform pressure, identical dwell time, identical pressure maintaining number
6 powder agglomates out.
4 drop test of embodiment and transport testing experiment
The present embodiment is to the muffin prepared of embodiment 2 and the blush of the preparation of embodiment 3 carries out drop test, transport is tested.
(1) test method
1) drop test
1. small articles drop machine model is shown in Table 3.
3 small articles drop machine parameter list of table
2. test method
A connects control cabinet power supply with electric power connection line, turns on the power switch, and connect air pressure.
B adjusts frame object plate to required test height and adjusts in horizontal position b.
C is placed on powder agglomates on frame object plate, moves drop test button, and powder agglomates is freely fallen, and completes drop test.
D is completed, and is cut off the power, and air pressure is fastened.
2) simulation transport test
1. transport simulating shake table model is shown in Table 4.
4 transport simulating shake table parameter list of table
| Model | KJ-7030 |
| Power supply | 220V50Hz is single-phase |
| Power of motor | 1HP |
| Speed (rev/min) | 100-300RPM |
| Maximum load (pound) | 100 |
| Working time range (hour) | 0.~99.99 |
| Mode of vibration | It is reciprocating |
2. test method
A simulation transport bumper connects power supply, turns on the power switch.
The powder agglomates of compression moulding is carried out assembling packing, vanning by manner of packing by b, need to be with filling out if casing discontented FCL
It fills object and is filled solid product, shake product not in the case.
C is upward placed on carton erection on transport simulating shake table, need to use the fixture secure carton on shake table, simulation
Transport Vibration platform parameter is set as 240 revs/min, 2 hours.
After d is tested the case where unpacking observation built-in product.
3) partial size is tested
1. laser fineness gage model is shown in Table 5.
Table 5
2. test method
A test prepares: the preparation of sampling and suspension.
B testing procedure: booting and starting → document → test parameter → routine test
(2) experimental result
1. drop testing results
A small articles falling tester connects power supply, turns on the power switch, and connect air pressure, such as Figure 1A；
B adjusts frame object plate to 50cm height and adjusts in horizontal position, powder agglomates 1 is placed on frame object plate, such as Figure 1B.
C moves drop test button, and powder agglomates is freely fallen, and drop test is completed, such as Fig. 1 C.
The muffin 1~4 prepared respectively to embodiment 2 with falling tester, blush 1~4 prepared by embodiment 3, which is done, falls survey
Examination, is as a result shown in Fig. 2~3, table 6~7.
6 muffin drop testing results of table
7 blush drop testing results of table
| Group | Blush 1 | Blush 2 of the present invention | Blush 3 | Blush 4 |
| Fall number | 6 | 6 | 6 | 6 |
| Rupture | 2 | 0 | 0 | 0 |
| Alice | 0 | 0 | 1 | 2 |
| Fraction defective | 33% | 0 | 16.67% | 33% |
2. simulation transport test result
To muffin 1~4 prepared by embodiment 2, blush 1~4 prepared by embodiment 3 carries out simulation transport test, as a result sees
Fig. 4~5, table 8~9.
Test data is transported in the simulation of 8 four kinds of muffin products of table
| Group | Muffin 1 | Muffin 2 of the present invention | Muffin 3 | Muffin 4 |
| Simulation transport number | 6 | 6 | 6 | 6 |
| Rupture | 1 | 0 | 0 | 0 |
| Alice | 0 | 0 | 1 | 1 |
| Fraction defective | 16.67% | 0 | 16.67% | 16.67% |
Test data is transported in the simulation of 9 four kinds of Blush products of table
| Group | Blush 1 | Blush 2 of the present invention | Blush 3 | Blush 4 |
| Simulation transport number | 6 | 6 | 6 | 6 |
| Rupture | 1 | 0 | 0 | 0 |
| Alice | 0 | 0 | 1 | 1 |
| Fraction defective | 16.67% | 0 | 16.67% | 16.67% |
By the result of table 6~9 and Fig. 2~5 it is found that compared with traditional grinding machine crushes the blush 1 prepared, muffin 1, Material
By blush 2~4 made from air-flow crushing and muffin 2~4, rupture number is 0 in drop test and simulation transport test, bright
It is aobvious to be better than blush 1.It is muffin 2 and blush 2 made from 0.7Mpa when air-flow powder machine crushes pressure, in drop test and simulation transport
Crack-free and alice situation, fraction defective are 0 in test；And air-flow powder machine crush pressure be 0.6Mpa or 0.8Mpa when it is obtained
Blush 3~4 and muffin 3~4, after falling and simulating transport, there are alice situation and/or rupture event in corner.Result above table
Bright, the present invention solves adhesive and other feed distributions unevenness in powder class cosmetics using the air-flow dispersing method of specified pressure
Even situation effectively improves drop test and not easily passs through problem, simultaneously effective avoids transportational process powder class cosmetics appearance
The problem of easy fragmentation, the qualification rate of product is up to 100%.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered
It is considered as protection scope of the present invention.
Claims (10)
1. a kind of dispersing method of powder class cosmetics, which is characterized in that acceptable in taking adhesive and other powder class cosmetics
Raw material mixing, carries out air-flow dispersion in airslide disintegrating mill；
The pressure of the air-flow dispersion is 0.7Mpa.
2. dispersing method according to claim 1, which is characterized in that described adhesive is selected from sad certain herbaceous plants with big flowers acid glyceride, gathers
One of dimethyl siloxane, Phenoxyethanol, zinc stearate, ethylhexanoic acid glyceride are a variety of.
3. dispersing method according to claim 1, which is characterized in that acceptable raw material in other described powder class cosmetics
Selected from one of filler, colorant, preservative or a variety of.
4. dispersing method according to claim 3, which is characterized in that the filler is selected from talcum powder, mica powder, silicon
Powder, nylon powder, magnesium silicate, boron nitride, kaolin, in dimetylsilyl SiClx stone, aluminium oxide, aluminium hydroxide, bentonite
It is one or more.
5. dispersing method according to claim 3, which is characterized in that the colorant be selected from CI 15850, CI 77891,
CI 77007, CI 45380, CI 45410, CI 77491, CI 77492.CI 77499, CI 77718, one in CI 15985
Kind is a variety of.
6. dispersing method according to claim 1, which is characterized in that the oil content or water content of the powder class cosmetics are not
More than 10%.
7. dispersing method according to claim 1, which is characterized in that the powder class cosmetics are muffin, described adhesive
Including sad certain herbaceous plants with big flowers acid glyceride, dimethyl silicone polymer, Phenoxyethanol and zinc stearate；It can be connect in other described powder class cosmetics
The raw material received includes talcum powder, mica powder, silicon powder, nylon powder, iron oxide yellow, iron oxide red and iron oxide black.
8. dispersing method according to claim 1, which is characterized in that the powder class cosmetics are blush, described adhesive
Including ethylhexanoic acid glyceride, dimethyl silicone polymer, Phenoxyethanol；Acceptable raw material packet in other described powder class cosmetics
Include talcum powder, mica powder, magnesium silicate, boron nitride, titanium dioxide, iron oxide red, red 6 color lake and iron oxide yellow.
9. powder class cosmetics made from dispersing method according to any one of claims 1 to 8.
10. powder class cosmetics according to claim 9, which is characterized in that the powder class cosmetics be blush, finishing powder,
Muffin, eye shadow powder or brow powder,.
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| CN201910349658.6A CN110170365A (en) | 2019-04-28 | 2019-04-28 | A kind of dispersing method of powder class cosmetics |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112999113A (en) * | 2021-01-29 | 2021-06-22 | 广州卡迪莲化妆品科技有限公司 | Anti-fading toner and preparation method thereof |
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| CN103239367A (en) * | 2012-02-02 | 2013-08-14 | 上海露凡西化妆品有限公司 | Baking powder and preparation method thereof |
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| CN112999113A (en) * | 2021-01-29 | 2021-06-22 | 广州卡迪莲化妆品科技有限公司 | Anti-fading toner and preparation method thereof |
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Address after: 510000 2-3, Huasheng South Road, Donghua, Baiyun District, Guangzhou City, Guangdong Province Applicant after: Guangzhou cadillan cosmetics technology Co.,Ltd. Address before: 510470, No. 2, No. 3, South Sheng Road, Donghua Town, people's and town, Baiyun District, Guangdong, Guangzhou Applicant before: GUANGZHOU CADLIN COSMETICS Co.,Ltd. |
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Application publication date: 20190827 |