CN110157499A - A kind of high heating value synthol oil and preparation method thereof - Google Patents

A kind of high heating value synthol oil and preparation method thereof Download PDF

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Publication number
CN110157499A
CN110157499A CN201910433635.3A CN201910433635A CN110157499A CN 110157499 A CN110157499 A CN 110157499A CN 201910433635 A CN201910433635 A CN 201910433635A CN 110157499 A CN110157499 A CN 110157499A
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synthol
oil
heating value
emulsion machine
high heating
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唐定北
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Guizhou Dingbei Technology Co Ltd
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Guizhou Dingbei Technology Co Ltd
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    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
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    • C10L1/00—Liquid carbonaceous fuels
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    • C10L1/00—Liquid carbonaceous fuels
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    • C10L1/00—Liquid carbonaceous fuels
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    • C10L1/14—Organic compounds
    • C10L1/18—Organic compounds containing oxygen
    • C10L1/182—Organic compounds containing oxygen containing hydroxy groups; Salts thereof
    • C10L1/1822—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms
    • C10L1/1824—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms mono-hydroxy
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    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10L1/00—Liquid carbonaceous fuels
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    • C10L1/14—Organic compounds
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    • C10L1/182—Organic compounds containing oxygen containing hydroxy groups; Salts thereof
    • C10L1/1822—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms
    • C10L1/1826—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms poly-hydroxy
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
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    • C10L1/14—Organic compounds
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    • C10L1/185—Ethers; Acetals; Ketals; Aldehydes; Ketones
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    • C10L1/00—Liquid carbonaceous fuels
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    • C10L1/19—Esters ester radical containing compounds; ester ethers; carbonic acid esters
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    • C10L1/00—Liquid carbonaceous fuels
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    • C10L1/14—Organic compounds
    • C10L1/30—Organic compounds compounds not mentioned before (complexes)
    • C10L1/305—Organic compounds compounds not mentioned before (complexes) organo-metallic compounds (containing a metal to carbon bond)
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    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10L10/00—Use of additives to fuels or fires for particular purposes
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    • C10L10/00—Use of additives to fuels or fires for particular purposes
    • C10L10/02—Use of additives to fuels or fires for particular purposes for reducing smoke development
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    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2230/00—Function and purpose of a components of a fuel or the composition as a whole
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    • C10L2270/00—Specifically adapted fuels
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    • C10L2270/00—Specifically adapted fuels
    • C10L2270/02—Specifically adapted fuels for internal combustion engines
    • C10L2270/026—Specifically adapted fuels for internal combustion engines for diesel engines, e.g. automobiles, stationary, marine

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  • Chemical & Material Sciences (AREA)
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  • General Chemical & Material Sciences (AREA)
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Abstract

The invention discloses a kind of high heating value synthol oil and preparation method thereof, belong to synthol oil field, a kind of high heating value synthol oil, including following component: basic material, stabilizer and combustion adjuvant；A kind of high heating value synthol oil preparation method, comprising the following steps: S1: according to the proportion weigh up raw material；S2: allotment stabilizer；S3: stabilizer obtained is added in methanol；S4: acetone is added；S5: glycerol is added；S6: ferrocene and heavy oil is added；S7: high heating value synthol oil is obtained, in the step C of S2, high-shear emulsion machine running speed is 500rpn, runing time is 10 minutes, in the step B of S2, potassium hydroxide and sodium hydroxide are put into sequence in no particular order, and in the step D and step E of S2, high-shear emulsion machine running speed is 500rpn.The high heating value synthol oil and preparation method thereof is more scientific and reasonable, and the synthol oil produced has high efficiency low cost and clean effect.

Description

A kind of high heating value synthol oil and preparation method thereof
Technical field
The present invention relates to synthol oil field, specially a kind of high heating value synthol oil.
The present invention relates to synthol oil field, specially a kind of high heating value synthol oil preparation method.
Background technique
The world today is faced with serious petroleum-based energy crisis and problem of environmental pollution.And boiler, kiln, vehicle exhaust row Putting is exactly a kind of severe contamination source.
When making raw material with coal and refined oil, contain oxycarbide in emission, carbon chlorine compound oxysulfide and A variety of carcinogens for containing in coal stone oil, caused by the harmfulness that contaminates of air river, threatened the normal life of people It is living.
For active response government current environment protective policy, the practical contradiction mitigated in efforts at environmental protection solves related enterprise not Cheap pollution power sources, the contradiction of " can not afford " other clean energy resourcies can be used.The development of current environmental protection work and enterprise A kind of all clean energy resourcies of high efficiency low cost of urgent need.
The existing energy is divided into high price clean energy resource and cheap pollution power sources, does not have high efficiency low cost and clean effect Fruit.
It is therefore proposed that a kind of high heating value synthol oil and preparation method thereof.
Summary of the invention
(1) the technical issues of solving
In view of the deficiencies of the prior art, the present invention provides a kind of high heating value synthol oil and preparation method thereof, the high fevers Value synthol oil and preparation method thereof is more scientific and reasonable, and the synthol oil produced has high efficiency low cost and clean effect, with Solve the problems mentioned above in the background art.
(2) technical solution
In order to achieve the above object, the present invention is achieved by the following technical programs: a kind of high heating value synthol oil, including Following component: basic material, stabilizer and combustion adjuvant；
Basic material be 99.9% methanol, account for always than 70%；
Stabilizer is made of water, potassium hydroxide, sodium hydroxide, ethyl acetate and dehydrated alcohol, and these ingredients account for respectively Always than 10%, 0.01%, 0.01%, 3.96% and 4%；
Combustion adjuvant is made of acetone, glycerol, ferrocene and heavy oil, and these ingredients account for respectively always than 4%, 4%, 0.02% and 4%.
A kind of high heating value synthol oil preparation method, comprising the following steps:
S1: raw material are weighed up according to the proportion；
S2: allotment stabilizer, comprising the following steps:
A: water, potassium hydroxide, sodium hydroxide, ethyl acetate and dehydrated alcohol are weighed up according to the ratio；
B: being put into potassium hydroxide, sodium hydroxide in rustless steel container, then slowly adds water；
C: starting high-shear emulsion machine, shutdown when solid melts entirely；
D: being cooled to room temperature, and ethyl acetate is added, and starting high-shear emulsion machine is run 20 minutes；
E: being added dehydrated alcohol, and starting high-shear emulsion machine is run 20 minutes；
F: stabilizer is made, and is placed on dark ventilation；
S3: stabilizer obtained is added in methanol, starting high-shear emulsion machine operation stirring 15 minutes；
S4: acetone, starting high-shear emulsion machine operation stirring 15 minutes is added；
S5: glycerol, starting high-shear emulsion machine operation stirring 20 minutes is added；
S6: being added ferrocene and heavy oil, and starting high-shear emulsion machine operation is put in storage after stirring 30 minutes；
S7: wait for quietly obtaining within 12 hours high heating value synthol oil.
Preferably, in the step C of S2, high-shear emulsion machine running speed is 500rpn, and runing time is 10 minutes, In the step B of S2, potassium hydroxide and sodium hydroxide are put into sequence in no particular order.
Preferably, in the step D of S2 and step E, high-shear emulsion machine running speed is 500rpn.
Preferably, in S3, high-shear emulsion machine running speed is 1000rpn.
Preferably, in S4, high-shear emulsion machine running speed is 1000rpn.
Preferably, in S5, high-shear emulsion machine running speed is 1500rpn.
Preferably, in S6, high-shear emulsion machine running speed is 2000rpn.
(3) beneficial effect
The present invention provides a kind of high heating value synthol oil and preparation method thereof, have it is following the utility model has the advantages that
The high heating value synthol oil and preparation method thereof is more scientific and reasonable, the synthol oil produced have high efficiency low cost and Clean effect, due to this high heating value synthol oil for being mainly used for Industrial Boiler, kiln, automobile, the outlet of burning after funnel Maximal ground concentration indices are far below standard limitation, therefore will mitigate to overall situation air pollution, use this high fever It is worth synthol oil and replaces other pollution power sources, the pollution to environment can be reduced, save huge environmental fund, that is, improves environment again It increases economic efficiency, the mode that boosts economic growth is changed from extensive style to intensive style, realizes most optimum distribution of resources and sustainability Development has great importance, this synthol oil calorific value is higher than diesel oil, and cost is 70% of diesel oil or so, and it is urgent that here it is people The cheap energy of the cleaning needed has good social benefit, has positive facilitation to the development of new energy.
Detailed description of the invention
Fig. 1 is overall flow figure of the invention.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
Referring to Fig. 1, the present invention provides a kind of technical solution: a kind of high heating value synthol oil, including following component: basis Material, stabilizer and combustion adjuvant；
Basic material be 99.9% methanol, account for always than 70%；
Stabilizer is made of water, potassium hydroxide, sodium hydroxide, ethyl acetate and dehydrated alcohol, and these ingredients account for respectively Always than 10%, 0.01%, 0.01%, 3.96% and 4%；
Combustion adjuvant is made of acetone, glycerol, ferrocene and heavy oil, and these ingredients account for respectively always than 4%, 4%, 0.02% and 4%.
A kind of high heating value synthol oil preparation method, comprising the following steps:
S1: raw material are weighed up according to the proportion；
S2: allotment stabilizer, comprising the following steps:
A: water, potassium hydroxide, sodium hydroxide, ethyl acetate and dehydrated alcohol are weighed up according to the ratio；
B: being put into potassium hydroxide, sodium hydroxide in rustless steel container, then slowly adds water, potassium hydroxide and sodium hydroxide Be put into sequence in no particular order；
C: starting high-shear emulsion machine, shutdown when solid melts entirely, high-shear emulsion machine running speed is 500rpn, when operation Between be 10 minutes；
D: being cooled to room temperature, and ethyl acetate is added, and starting high-shear emulsion machine is run 20 minutes, high-shear emulsion machine operation Revolving speed is 500rpn；
E: being added dehydrated alcohol, and starting high-shear emulsion machine is run 20 minutes, and high-shear emulsion machine running speed is 500rpn；
F: stabilizer is made, and is placed on dark ventilation；
S3: stabilizer obtained is added in methanol, starting high-shear emulsion machine operation stirring 15 minutes, high-shear emulsifying Machine running speed is 1000rpn；
S4: being added acetone, starting high-shear emulsion machine operation stirring 15 minutes, and high-shear emulsion machine running speed is 1000rpn；
S5: being added glycerol, starting high-shear emulsion machine operation stirring 20 minutes, and high-shear emulsion machine running speed is 1500rpn；
S6: being added ferrocene and heavy oil, and starting high-shear emulsion machine operation is put in storage after stirring 30 minutes, high-shear emulsion machine Running speed is 2000rpn；
S7: wait for quietly obtaining within 12 hours high heating value synthol oil.
The present invention provides high heating value synthol oil and preparation method thereof it is more scientific and reasonable, the synthol oil tool produced Standby high efficiency low cost and clean effect, due to this high heating value synthol oil for being mainly used for Industrial Boiler, kiln, automobile, combustion It burns after funnel outlet maximal ground concentration indices and is far below standard limitation, therefore will mitigate to overall situation air pollution, Other pollution power sources are replaced using this high heating value synthol oil, the pollution to environment can be reduced, save huge environmental fund, Improve environment to increase economic efficiency again, the mode that boosts economic growth is changed from extensive style to intensive style, realizes that resource optimization is matched It sets and has great importance with sustainable development, this synthol oil calorific value is higher than diesel oil, and cost is 70% of diesel oil or so, this Be exactly people there is an urgent need to the cheap energy of cleaning, there is good social benefit, have positive rush to the development of new energy Into effect.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment Intrinsic element.In the absence of more restrictions.By sentence " element limited including one ..., it is not excluded that There is also other identical elements in the process, method, article or apparatus that includes the element ".
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (8)

1. a kind of high heating value synthol oil, which is characterized in that including following component: basic material, stabilizer and combustion adjuvant；
Basic material be 99.9% methanol, account for always than 70%；
Stabilizer is made of water, potassium hydroxide, sodium hydroxide, ethyl acetate and dehydrated alcohol, and these ingredients account for respectively always than 10%, 0.01%, 0.01%, 3.96% and 4%；
Combustion adjuvant is made of acetone, glycerol, ferrocene and heavy oil, and these ingredients account for respectively always than 4%, 4%, 0.02% with 4%.
2. a kind of high heating value synthol oil preparation method according to claim 1, which comprises the following steps:
S1: raw material are weighed up according to the proportion；
S2: allotment stabilizer, comprising the following steps:
A: water, potassium hydroxide, sodium hydroxide, ethyl acetate and dehydrated alcohol are weighed up according to the ratio；
B: being put into potassium hydroxide, sodium hydroxide in rustless steel container, then slowly adds water；
C: starting high-shear emulsion machine, shutdown when solid melts entirely；
D: being cooled to room temperature, and ethyl acetate is added, and starting high-shear emulsion machine is run 20 minutes；
E: being added dehydrated alcohol, and starting high-shear emulsion machine is run 20 minutes；
F: stabilizer is made, and is placed on dark ventilation；
S3: stabilizer obtained is added in methanol, starting high-shear emulsion machine operation stirring 15 minutes；
S4: acetone, starting high-shear emulsion machine operation stirring 15 minutes is added；
S5: glycerol, starting high-shear emulsion machine operation stirring 20 minutes is added；
S6: being added ferrocene and heavy oil, and starting high-shear emulsion machine operation is put in storage after stirring 30 minutes；
S7: wait for quietly obtaining within 12 hours high heating value synthol oil.
3. a kind of high heating value synthol oil preparation method according to claim 2, it is characterised in that: in the step C of S2, High-shear emulsion machine running speed is 500rpn, and runing time is 10 minutes, in the step B of S2, potassium hydroxide and hydroxide Sodium is put into sequence in no particular order.
4. a kind of high heating value synthol oil preparation method according to claim 2, it is characterised in that: S2 step D with In step E, high-shear emulsion machine running speed is 500rpn.
5. a kind of high heating value synthol oil preparation method according to claim 2, it is characterised in that: in S3, high shear Mulser running speed is 1000rpn.
6. a kind of high heating value synthol oil preparation method according to claim 2, it is characterised in that: in S4, high shear Mulser running speed is 1000rpn.
7. a kind of high heating value synthol oil preparation method according to claim 2, it is characterised in that: in S5, high shear Mulser running speed is 1500rpn.
8. a kind of high heating value synthol oil preparation method according to claim 2, it is characterised in that: in S6, high shear Mulser running speed is 2000rpn.
CN201910433635.3A 2019-05-23 2019-05-23 A kind of high heating value synthol oil and preparation method thereof Pending CN110157499A (en)

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Citations (9)

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Publication number Priority date Publication date Assignee Title
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CN102653690A (en) * 2011-03-04 2012-09-05 徐海野 Environmentally-friendly, efficient and low-cost alcohol-oil synthetic fuel
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CN102653690A (en) * 2011-03-04 2012-09-05 徐海野 Environmentally-friendly, efficient and low-cost alcohol-oil synthetic fuel
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Application publication date: 20190823