CN110157491A - A kind of dismountable condenser pipe for being used for biomass collection thermal cracking oil - Google Patents
A kind of dismountable condenser pipe for being used for biomass collection thermal cracking oil Download PDFInfo
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- CN110157491A CN110157491A CN201910592975.0A CN201910592975A CN110157491A CN 110157491 A CN110157491 A CN 110157491A CN 201910592975 A CN201910592975 A CN 201910592975A CN 110157491 A CN110157491 A CN 110157491A
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- 239000002028 Biomass Substances 0.000 title claims abstract description 51
- 238000004227 thermal cracking Methods 0.000 title claims abstract description 38
- 239000011521 glass Substances 0.000 claims abstract description 206
- 239000002355 dual-layer Substances 0.000 claims abstract description 64
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000005337 ground glass Substances 0.000 claims description 32
- 238000009833 condensation Methods 0.000 claims description 26
- 230000005494 condensation Effects 0.000 claims description 26
- 239000007787 solid Substances 0.000 claims description 26
- 239000011232 storage material Substances 0.000 claims description 13
- 238000009434 installation Methods 0.000 claims description 6
- 239000004579 marble Substances 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 4
- 239000010410 layer Substances 0.000 claims description 3
- 239000000741 silica gel Substances 0.000 claims description 3
- 229910002027 silica gel Inorganic materials 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 2
- 239000004576 sand Substances 0.000 claims 1
- 239000003921 oil Substances 0.000 description 28
- 239000007789 gas Substances 0.000 description 21
- 238000000197 pyrolysis Methods 0.000 description 15
- 239000000203 mixture Substances 0.000 description 9
- 238000009835 boiling Methods 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- 238000013461 design Methods 0.000 description 4
- 238000003032 molecular docking Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000001125 extrusion Methods 0.000 description 2
- 239000005338 frosted glass Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000003780 insertion Methods 0.000 description 2
- 230000037431 insertion Effects 0.000 description 2
- 238000002679 ablation Methods 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000012075 bio-oil Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 229910021538 borax Inorganic materials 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000004328 sodium tetraborate Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0003—Condensation of vapours; Recovering volatile solvents by condensation by using heat-exchange surfaces for indirect contact between gases or vapours and the cooling medium
- B01D5/0006—Coils or serpentines
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0003—Condensation of vapours; Recovering volatile solvents by condensation by using heat-exchange surfaces for indirect contact between gases or vapours and the cooling medium
- B01D5/0012—Vertical tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0078—Condensation of vapours; Recovering volatile solvents by condensation characterised by auxiliary systems or arrangements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0078—Condensation of vapours; Recovering volatile solvents by condensation characterised by auxiliary systems or arrangements
- B01D5/009—Collecting, removing and/or treatment of the condensate
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10K—PURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
- C10K1/00—Purifying combustible gases containing carbon monoxide
- C10K1/04—Purifying combustible gases containing carbon monoxide by cooling to condense non-gaseous materials
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a kind of condenser pipes for being removably used for biomass collection thermal cracking oil, to overcome the problems, such as to need to consume, a large amount of water sources and electric energy, cold energy use rate is not high, piping connection is complicated, installs and using cumbersome comprising the fixed bracket of threaded cap, barb, inner tube, dual-layer vacuum glass outer tube, spherical glass inner tube, glass three-way and receiving flask；Spherical glass inner tube is fitted into dual-layer vacuum glass outer tube, spherical glass inner tube lower end and the outer pipe end of dual-layer vacuum glass connect, the fixed support casing of inner tube is mounted in the junction of first inner tube ball bubble and exhaust outlet of spherical glass inner tube, the fixed bracket T shape part of the support bracket fastened inner tube of inner tube is connect with the barb on dual-layer vacuum glass outer tube wall, threaded cap is sleeved in spherical glass inner tube and connect with dual-layer vacuum glass external pipe thread, the inner wall of the interior interface tube of pipe end outer wall and glass three-way connects in spherical glass, the vial interface of glass three-way and the bottleneck of receiving flask upper end connect.
Description
Technical field
The present invention relates to a kind of devices for belonging to technical field of experiment equipment, it more particularly relates to which one kind can
The condenser pipe for laboratory biomass collection thermal cracking oil of disassembly.
Background technique
The collection of laboratory biological matter thermal cracking oil generally uses condenser pipe or the cooling recycling of multi-stage condensing pipe, tests at present
On the one hand the condenser pipe that room generally uses needs the water source largely continuously flowed or pump working to recycle water, erroneous for installation,
It occupies limited lab space and energy consumption is higher, there are problems that the waste of great lot of water resources；Another aspect biomass hot tearing
The condensable gases generated in solution preocess can start at 110 DEG C or less condensation collect, it is common to use condenser pipe there are cold
High situation can be lost using insufficient；There are also be on the one hand that laboratory conventional condensation pipe is made of inner and outer tubes and is linked to be one
Body is non-dismountable, according to the difference of different condensed materials, it is also necessary to replace different types of condenser pipe, and conventional condensation pipe range
Phase, which uses, can also make to stockpile scale in inner and outer pipes cavity, reduce working efficiency；Since original biomass thermal cracking gas temperature is normal
Often reach several hundred degrees Celsius, so the collection of laboratory biological matter thermal cracking oil at present generally requires the cooling (air setting of two steps
And circulating water condensing) or the mode of multi-stage condensing pipe arrangement carry out, so complicated condensing plant being built and excessively collecting
The use of vessel causes the problems such as biomass thermal cracking oil collects difficult and inefficiency.
Summary of the invention
The technical problem to be solved by the present invention is to overcome biomass thermal cracking oil condenser pipe of the existing technology to exist
Need to consume when use a large amount of water sources and electric energy, cold energy use rate is not high, piping connection is complicated, installation and using it is cumbersome, tie up
Lab space, inner tube cleaning be difficult, condensation chamber use for a long time between outer tube and inner tube cause scale build-up cannot clean and
Non-dismountable problem provides a kind of disassembling cleaning without external flowing water source or electric pump driving for laboratory biological
The condenser pipe that the condensation of matter thermal cracking oil is collected.
In order to solve the above technical problems, the present invention is achieved by the following technical scheme: described one kind is dismountable
Condenser pipe for biomass collection thermal cracking oil include threaded cap, barb, the fixed bracket of inner tube, dual-layer vacuum glass outer tube,
Cold-storage material, spherical glass inner tube, glass three-way and receiving flask；
The spherical glass inner tube is packed into wherein from the top of dual-layer vacuum glass outer tube, the lower end of spherical glass inner tube
The inner wall at end of conical outer wall and dual-layer vacuum glass outer tube connects, and the fixed bracket of inner tube passes through the fixed bracket inner ring of inner tube
It is sleeved on the junction of first inner tube ball bubble and exhaust outlet of spherical glass inner tube, the fixed bracket of the support bracket fastened inner tube of inner tube
T shape part is connect with the barb on dual-layer vacuum glass outer tube wall, and cold-storage material is packed into spherical glass inner tube and double-layer vacuum glass
It is formed by condensation chamber between glass outer tube, threaded cap is sleeved on the air inlet of spherical glass inner tube and and dual-layer vacuum glass
The top of outer tube is threadedly coupled, and spherical glass inner tube end cone outer wall is contacted with the inner wall of the interior interface tube of glass three-way upper end
Connection, the vial interface of glass three-way lower end and the bottleneck of receiving flask upper end connect.
Dual-layer vacuum glass outer tube described in technical solution include tube body, the identical barb of 3 structures, discharge outlet and
Solid wedge ground glass interface；The tube body is formed by connecting by the cylinder of upper end and the conical shell of lower end, cylinder
With the rotation conllinear of conical shell, the upper end of tube body is provided with external screw thread identical with threaded cap structure；Inboard wall of tube body is equal
It is identical with groove for fixing what bracket T shape part connected with the support bracket fastened inner tube of inner tube that it is provided with 3 structures evenly
Barb, the height of barb is lower than horizontal plane where after the fixed bracket inner ring installation of the support bracket fastened inner tube of inner tube, on conical shell
It is provided with the discharge outlet for discharging extra water in condensation chamber；Outer pipe end, that is, conical shell the end of dual-layer vacuum glass is to arranging
It is provided with solid wedge ground glass interface in the mouth of a river between branch pipe root, solid wedge ground glass interface and conical shell
Rotation conllinear.
Solid wedge ground glass interface described in technical solution is hollow glass cone part, is outside dual-layer vacuum glass
In a part of conical shell in pipe, the taper of the outer conical surface of solid wedge ground glass interface and dual-layer vacuum glass outer tube
The taper of conical shell is equal, and a tapered centre through-hole, center cone are provided at the center of solid wedge ground glass interface
The rotation conllinear of shape through-hole and outer conical surface, the taper of tapered centre through-hole and the taper of spherical glass inner tube lower end cone
Equal, the top surface of solid wedge ground glass interface is spherical surface, the corresponding centre of sphere of the spherical surface and the outer tube hub of dual-layer vacuum glass
Axis collinear, and with where discharge outlet branch and dual-layer vacuum glass outer tube intersection connect, where spherical surface and discharge outlet
The bottom surface of branch is tangent.
The identical barb of 3 structures described in technical solution are set on the inner wall of dual-layer vacuum glass outer tube, and three
The identical barb of structure is in the same plane vertical with dual-layer vacuum glass outer tube axis of rotation；Barb global shape uses
Tri-prismoid structure, three sides of barb are respectively horizontal plane, vertical plane and inclined surface, and inclined surface and horizontal plane intersect institute
The seamed edge of formation is connected with the inner wall of dual-layer vacuum glass outer tube, is provided on vertical plane for fixing bracket T shape with inner tube
The horizontal groove that part links.
Spherical glass inner tube described in technical solution includes exhaust outlet, 3~6 ball bubbles and wedge-shaped ground glass interface；
The spherical glass inner tube is single-glass inner tube, and the exhaust outlet of straight tube-like is provided at the top of spherical glass inner tube, spherical
The middle part of glass inner tube is joined end to end by 3~6 glass sky balls and is connect, and the axis of rotation of 3~6 glass sky balls and exhaust outlet is total
The sphere center position for first glass marble that line is connected with exhaust outlet is higher than the plane where the identical barb of 3 structures, finally
The terminal position of one glass marble is higher than the plane where dual-layer vacuum glass outer tube conical shell upper end；Spherical glass inner tube end
The wedge-shaped ground glass interface at end is divided into two sections, wherein the taper of upper end be less than lower end taper and with solid wedge frosted
The taper of the central through hole of glass interface matches, and the taper of the interior interface tube of the taper and glass three-way of lower end matches.
The fixed bracket of inner tube described in technical solution is to use circular ring structure part made of flexible silica gel material,
The fixed bracket of inner tube is made of the fixed bracket inner ring of inner tube, the fixed bracket outer ring of inner tube connecting rod identical with 3 root knot structures, inner tube
The internal diameter of fixed bracket inner ring is equal to the outer diameter of exhaust outlet in spherical glass inner tube and is sleeved on first inner tube ball bubble and exhaust
The junction of mouth；The fixed bracket race diameter of inner tube is equal to the inner diameter of dual-layer vacuum glass outer tube, the identical company of 3 root knot structures
Extension bar uniformly distributed, identical connecting rod of 3 root knot structures in the circumferencial direction of the fixed bracket inner ring of inner tube and the fixed bracket outer ring of inner tube
One end and inner tube fixed bracket inner ring connect, the fixed bracket outer ring company of the other end and inner tube of the identical connecting rod of 3 root knot structures
It connects, the identical connecting rod of 3 root knot structures and inner tube fix the fixed bracket T shape part of inner tube and double-layer vacuum that bracket outer ring connects into
Barb connection on outer glass tube inner wall.
Glass three-way described in technical solution include the interior interface tube of upper end, middle section isodiametric annulus cylinder under
The receiving flask interface at end, interior interface tube and receiving flask interface are all the annulus cone of wedge shape, the interior interface tube of glass three-way upper end
Taper be equal to spherical glass inner tube end taper, receiving flask interface taper be equal to receiving flask bottleneck taper；Interior interface tube
Lower end be connected with the upper end of annulus cylinder, annulus cylinder lower end is connected with the upper end of receiving flask interface；Glass three
The diameter of the interior interface tube of logical upper end is greater than the diameter of the receiving flask interface of lower end, and the diameter of the receiving flask interface of lower end, which is less than, to be received
Collect the bottleneck diameter of bottle, the middle part of the isodiametric annulus cylinder in middle section is obliquely provided with air inlet pipe, while where air inlet
Branch pipe is all made of ground glass face using extension pipe obliquely, the interface surface of interior interface tube, receiving flask interface and receiving flask.
Compared with prior art the beneficial effects of the present invention are:
1. outside the condenser pipe in a kind of condenser pipe for being removably used for biomass collection thermal cracking oil of the present invention
Pipe is designed using dual-layer vacuum glass pipe, thus has good thermal and insulating performance, which can effectively prevent outside heat
Entrance, avoid the loss of cold energy in condensation chamber, substantially increase the utilization efficiency of cold energy；
2. of the present invention a kind of removably for the condenser pipe in the condenser pipe of biomass collection thermal cracking oil
Outer tube and inner tube have dismountable characteristic, outer tube and inner tube using interspersed combined connection type, therefore can be according to condensing gas
The needs of body, flexible choice straight, spherical shape, coiled inner tube achieve the effect that one tube multipurpose, while in the design of detachability makes
The cleaning of pipe and outer tube is more convenient and thorough, improves the applicability and conventional efficient of condenser pipe；
3. the condenser pipe in a kind of condenser pipe for being removably used for biomass collection thermal cracking oil of the present invention is adopted
Cold energy is provided with cold-storage material is launched in the cavity (condensation chamber) formed to outer tube and inner tube, cold-storage material may be reused, be not required to
It wants external flowing water source or the task driven water source of electric pump to recycle, is saved while saving great lot of water resources and electric energy limited
Lab space, make the installation of condenser pipe and using simpler more environmentally-friendly；
4. it is of the present invention it is a kind of removably for the condenser pipe in the condenser pipe of biomass collection thermal cracking oil into
Tracheae is allowed to the effect for the air setting for having certain, is realized sky using lengthening obliquely and the design of cone-shaped collection bottle
The solidifying combination with two kinds of condensing modes of circulating water condensing of air cooling, improves the collection efficiency of biomass thermal cracking oil, while can be effective
It prevents the biomass thermal cracking oil condensed from passing back into air inlet pipe, avoids the blocking of air inlet pipe.
Detailed description of the invention
The present invention will be further described below with reference to the drawings:
Fig. 1 is a kind of removably main view for the condenser pipe of biomass collection thermal cracking oil of the present invention；
Fig. 2 is a kind of removably part for the condenser pipe lower end of biomass collection thermal cracking oil of the present invention
Enlarged view；
Fig. 3 is of the present invention a kind of removably for employed in the condenser pipe of biomass collection thermal cracking oil
The main view that the fixed bracket of inner tube is connected with the barb on dual-layer vacuum glass outer tube wall；
Fig. 4 is of the present invention a kind of removably for employed in the condenser pipe of biomass collection thermal cracking oil
The left view that the fixed bracket of inner tube is connected with the barb on dual-layer vacuum glass outer tube wall；
Fig. 5 is of the present invention a kind of removably for employed in the condenser pipe of biomass collection thermal cracking oil
The top view that the fixed bracket of inner tube is connected with the barb on dual-layer vacuum glass outer tube wall；
Fig. 6 is of the present invention a kind of removably for employed in the condenser pipe of biomass collection thermal cracking oil
Inner tube fixes bracket top view；
Fig. 7 is of the present invention a kind of removably for glass employed in the condenser pipe of biomass collection thermal cracking oil
The main view of glass threeway；
Fig. 8 is of the present invention a kind of removably for glass employed in the condenser pipe of biomass collection thermal cracking oil
Glass threeway right view；
Fig. 9 is of the present invention a kind of removably for glass employed in the condenser pipe of biomass collection thermal cracking oil
The top view of glass threeway；
In figure: 1. exhaust outlets, 2. threaded caps, 3. barbs, the fixed bracket of 4. inner tubes, 5. dual-layer vacuum glass outer tubes, 6. is cold
Solidifying room, 7. spherical glass inner tubes, 8. discharge outlet, 9. wedge-shaped ground glass interfaces, 10. glass three-ways, 11. solid wedge frosted glass
Glass interface, 12. air inlets, 13. receiving flasks, the fixed bracket inner ring of 14. inner tubes, the fixed bracket outer ring of 15. inner tubes, 16. inner tubes are solid
Fixed rack T shape part, interface tube in 17., 18. receiving flask interfaces.
Specific embodiment
The present invention is explained in detail with reference to the accompanying drawing:
Refering to fig. 1, a kind of condenser pipe removably collected for laboratory biological matter thermal cracking oil provided by the invention
Including threaded cap 2, barb 3, inner tube fixed bracket 4, dual-layer vacuum glass outer tube 5, cold-storage material, spherical glass inner tube 7, glass three
Lead to 10 and receiving flask 13.
The threaded cap 2 uses PVC material, is provided with internal screw thread on threaded cap 2, the internal diameter of threaded cap 2 be provided with
The outer diameter of externally threaded 5 upper end of dual-layer vacuum glass outer tube is identical, and a diameter is provided at the center of threaded cap 2 and is equal to spherical shape
The through-hole of the exhaust outlet 1 of glass inner tube 7 keeps threaded cap 2 and the exhaust outlet 1 of spherical glass inner tube 7 light equipped and true with bilayer
Empty 5 threaded upper ends of outer glass tube connection.The function of threaded cap 2 is the closing for condensation chamber 6 and the root in condenser pipe work
According to the convenient supplement for carrying out ice cube in time of the ablation situation of ice cube in condensation chamber, the continuous work of condenser pipe is realized；
Refering to fig. 1 with Fig. 2, the dual-layer vacuum glass outer tube 5 includes tube body, barb 3, discharge outlet 8 and solid wedge
Shape ground glass interface 11.
The tube body is formed by connecting by the cylinder of upper end and the conical shell of lower end, time of cylinder and conical shell
Shaft axis is conllinear, and the upper end of tube body is provided with external screw thread identical with 2 structure of threaded cap；Inboard wall of tube body is equably provided with 3
The identical barb 3 with gap of structure for the connection of the fixed bracket T shape part 16 of inner tube with the fixed bracket 4 of inner tube, and falls
The height of hook 3 fixes bracket inner ring 14 place horizontal plane, purpose (after installation) at work lower than the inner tube of the fixed bracket 4 of inner tube
It is to provide a downward stress to spherical glass inner tube 7 and then improves spherical glass inner tube 7 and dual-layer vacuum glass outer tube 5
The airtightness of lower end；5 lower end of dual-layer vacuum glass outer tube is provided with discharge outlet 8 on conical shell, for more in condensation chamber 6
The discharge of remaining water；5 ends of dual-layer vacuum glass outer tube, that is, conical shell end is provided between branch pipe root into discharge outlet 8
Solid wedge ground glass interface 11, the solid wedge ground glass interface 11 are hollow glass cone part, are double-deck true
A part of conical shell in empty outer glass tube 5, the taper and bilayer of the outer conical surface of solid wedge ground glass interface 11 are true
The taper of conical shell is equal in empty outer glass tube 5, and a center is provided at the center of solid wedge ground glass interface 11
Conical through-hole, the rotation conllinear of tapered centre through-hole and outer conical surface, in the taper and spherical glass of tapered centre through-hole
The taper of 7 lower end centrum of pipe is equal, and the top surface of solid wedge ground glass interface 11 is spherical structure, the corresponding centre of sphere of the spherical surface
It is conllinear with 5 central axis of dual-layer vacuum glass outer tube, and handed over the branch at 8 place of discharge outlet and dual-layer vacuum glass outer tube 5
It is connected at remittance, the bottom surface of spherical surface and 8 place branch of discharge outlet is tangent.Use solid wedge ground glass interface 11 for spherical glass
Glass inner tube 7 and 5 end of dual-layer vacuum glass outer tube provide bigger contact area and then improve airtightness, while convenient for cleaning
When condensation chamber 6 in residual amount whole outflows；
Refering to fig. 1 with Fig. 2, the spherical glass inner tube 7 includes exhaust outlet 1, ball bubble and wedge-shaped ground glass interface 9.
The spherical glass inner tube 7 is single-glass inner tube, and the top of spherical glass inner tube 7 is provided with the row of straight tube-like
Port 1, the discharge for uncondensable Pyrolysis Gas From Biomass body；The middle part of spherical glass inner tube 7 is by 3~6 glass skies
Ball, which joins end to end, to be connect, and plays the role of effectively condensing, the rotation conllinear of 3~6 glass sky balls and exhaust outlet 1, and row
The sphere center position for first glass sky ball that port 1 is connected is higher than the plane where the identical barb 3 of 3 structures, last
The terminal position of a glass marble is higher than plane where 5 conical shell upper end of dual-layer vacuum glass outer tube；7 end of spherical glass inner tube
Wedge-shaped ground glass interface be divided into two sections, wherein the taper of upper end be less than lower end taper and with solid wedge frosted glass
The taper of the central through hole of glass interface 11 matches, and realizes friction docking, the taper of lower end and the interior interface tube of glass three-way 10
17 taper matches, realize friction docking and it is closed.
Refering to fig. 1 with Fig. 6, the fixed bracket 4 of the inner tube is using annulus knot made of flexible silica gel material
Component, the fixed bracket 4 of inner tube is by the identical connection of the fixed bracket inner ring 14 of inner tube, the fixed root knot structure of bracket outer ring 15 and 3 of inner tube
Bar composition, fixed 14 diameter of bracket inner ring of inner tube are equal to the diameter of 7 exhaust outlet 1 of spherical glass inner tube and are sleeved on first inner tube
The junction of ball bubble and exhaust outlet 1；Fixed 15 diameter of bracket outer ring of inner tube is equal to the inner diameter of dual-layer vacuum glass outer tube 5, and 3
The identical connecting rod of root knot structure is uniformly distributed in the fixed bracket inner ring 14 of inner tube with fixed 15 circumferencial direction of bracket outer ring of inner tube, and 3
The fixed bracket inner ring 14 of one end of the identical connecting rod of structure and inner tube connects, the other end of the identical connecting rod of 3 root knot structures and
The fixed bracket outer ring 15 of inner tube connects, and the inner tube of the identical connecting rod of 3 root knot structures and the fixed connection of bracket outer ring 15 of inner tube is fixed
16 hook of bracket T shape part is at the barb 3 on 5 inner wall of dual-layer vacuum glass outer tube；
Refering to Fig. 3, Fig. 4 and Fig. 5, the identical barb 3 of 3 structures is set to the interior of dual-layer vacuum glass outer tube 5
On wall, three barbs 3 are in same plane, and the plane is vertical with 5 axis of rotation of dual-layer vacuum glass outer tube；Barb 3 is whole
Shape uses tri-prismoid structure, and three sides of composition barb 3 are respectively horizontal plane, vertical plane and inclined surface, inclined surface
Seamed edge is formed by with horizontal plane intersection to be connected with the inner wall of dual-layer vacuum glass outer tube 5, is provided on vertical plane horizontal recessed
Slot, horizontal groove are used to mutually link with the fixed bracket T shape part 16 of inner tube.
Refering to fig. 1, Fig. 7 to Fig. 9, the interior interface tube 17 of the glass three-way 10 including upper end, middle section it is isodiametric
The receiving flask interface 18 of annulus cylinder and lower end, interior interface tube 17 are all wedge-shaped annulus cone, glass with receiving flask interface 18
The taper of the interior interface tube 17 of 10 upper end of threeway is equal to the end taper of spherical glass inner tube 7, and 18 taper of receiving flask interface is equal to
The taper of 13 bottleneck of receiving flask；The lower end of interior interface tube 17 is connected with the upper end of annulus cylinder, annulus cylinder lower end and receipts
The upper end of collection bottle interface 18 is connected；The diameter of the interior interface tube 17 of 10 upper end of glass three-way is greater than the receiving flask interface of lower end
The middle part of 18 diameter, the isodiametric annulus cylinder in middle section is obliquely provided with air inlet pipe 12 upwards, and the receiving flask of lower end connects
The diameter of mouth 18 is less than the bottleneck diameter of receiving flask 13, and interior interface tube 17, receiving flask interface 18 and the interface surface of receiving flask 13 are equal
Using wedge-shaped ground glass face, each interface is closed by the extruding realization of interface top condenser pipe weight in connection, while glass
The 12 place branch pipe of air inlet at 10 middle part of threeway makes high boiling biomass high-temperature cracked gas first using extension pipe obliquely
It is condensed out by air cooled mode, avoids excessive temperature gas while improving biomass thermal cracking oil collection efficiency
Condenser pipe is burst into spherical glass inner tube 7；
The receiving flask 13 uses glass frosted prostomum shape bottle structure, and receiving flask 13 is supporting entire condenser pipe weight
Make the Pyrolysis Gas From Biomass body to have cooled down further cool down simultaneously to be collected condensable part, prevent in spherical glass
Pipe 7 is burst because of excessive temperature differentials.
The condensation chamber 6 is that spherical glass inner tube 7 is fitted into the space after dual-layer vacuum glass outer tube 5 therebetween
It launches cold-storage material and is formed by condensation chamber, provide cold energy for the work of condenser pipe；Reach the cold-storage material of heat absorption saturation from condensation chamber 6
After discharge, it can be recycled.The cold-storage material used in the present invention is mixture of ice and water, water, Polyvinyl alcohol-borax cold-storage material etc.
Fluid cold-storage material.
The end (insertion end) of spherical glass inner tube 7 is inserted into from the top (insertion end) of dual-layer vacuum glass outer tube 5；Inner tube
Fixed bracket inner ring 14 is sleeved on the junction of first inner tube ball bubble and exhaust outlet 1 of spherical glass inner tube 7, and inner tube is consolidated
Fixed rack T shape part 16 is buckled on barb 3；By threaded cap 2 be sleeved on the air inlet 1 of spherical glass inner tube 7 and with bilayer
The top of vacuum glass outer tube 5 screws up connection by screw thread；Outside the spherical glass inner tube 7 that fits together, dual-layer vacuum glass
The inner tube of 7 end of spherical glass inner tube and 10 upper end of glass three-way that the fixed bracket inner ring 14 of pipe 5, inner tube passes through with threaded cap 2
Interface 17 is equipped, and the vial interface 18 of 10 lower end of glass three-way and the bottleneck of 13 upper end of receiving flask are equipped with and each component can be completed
Connection.
A kind of working principle of dismountable condenser pipe collected for biomass thermal cracking oil:
A kind of condenser pipe removably collected for biomass thermal cracking oil of the present invention (hereinafter referred to as condenses
Pipe) it is plugged together, outside 7 end of spherical glass inner tube in 5 inner wall at end of dual-layer vacuum glass outer tube and 7 lower end outer wall of spherical glass inner tube
In wall and glass three-way 10 17 inner wall of interface tube plug together, the bottleneck of receiving flask interface 18 outer wall and receiving flask 13 of glass three-way 10
The inserting position of inner wall has used ground glass interface to will form the design feature in excellent sealing face by squeezing, and then realizes this
Closed docking in invention between each component.Wherein 5 inner wall at end of dual-layer vacuum glass outer tube and 7 lower end outer wall of spherical glass inner tube
Barb 3 of the extrusion stress docked that rubs on the fixed bracket 4 of inner tube and 5 inner wall of dual-layer vacuum glass outer tube links generation
Stress；17 inner wall of interface tube in 7 end outer wall of spherical glass inner tube and glass three-way 10, the receiving flask interface of glass three-way 10
Gravity of the extrusion stress from condenser pipe itself that 18 outer walls are docked with wall friction in 13 bottleneck of receiving flask.
The condenser pipe Pyrolysis Gas From Biomass body that biomass through pyrolysis equipment exports at work in the present invention is (condensable
It is not condensable) enter condenser pipe from the air inlet of condenser pipe 12 first, wherein condensable high-temperature biomass hot pyrolysis gas
During passing through 12 place slender glass pipeline of air inlet, high-temperature biomass hot pyrolysis gas is using glass as medium and experiment
The lower cold air of room temperature carries out heat exchange, substantially reduces the heat and temperature of the carrying of original biomass hot pyrolysis gas
It spends, some high boiling compositions take the lead in condensing on the inner wall of the glass piping where air inlet 12 in Pyrolysis Gas From Biomass body
Get off and slides to the collection for completing part higher boiling ingredient in bio oil in receiving flask 13；
Next enter receiving flask 13 by the Pyrolysis Gas From Biomass body for tentatively cooling down and condensing to receive further
The collection of air setting and condensable part, to prevent from causing because Pyrolysis Gas From Biomass body is excessively high spherical glass inner tube 7 fried
It splits；In receiving flask 13 uncooled Pyrolysis Gas From Biomass body under the pressure of subsequent bio matter hot pyrolysis gas entrance, from spherical glass
7 end of glass inner tube enters spherical glass inner tube 7 and moves upwards, under the cold environmental conditions that condensation chamber 6 provides, biomass thermal
The mixture of ice and water in inner wall and condensation chamber 6 that cracked gas passes through spherical glass inner tube 7 carries out heat exchange, makes biomass hot tearing
Remaining condensable ingredient is condensed on the inner wall of spherical glass inner tube 7 and is slid to receiving flask 13 in solution gas, completes biology
The collection of low boiling point composition in oil；
Last uncondensable Pyrolysis Gas From Biomass body is discharged from exhaust outlet 1.Due to the company of Pyrolysis Gas From Biomass body
Continuous to be passed through, (use of cold-storage material is by taking the mixture of ice and water as an example) mixture of ice and water in condensation chamber 6 is absorbing spherical glass inner tube 7
After the heat of endogenous substance hot pyrolysis gas, ice cube starts slowly to melt, when in condensation chamber 6 ice cube close to all melt when
It waits, needs to unscrew threaded cap 2 and add appropriate ice cube into condensation chamber 6, screw up threaded cap 2 after adding ice cube, later the row of opening
Valve in the mouth of a river 8 carries out the lower end that draining makes the water level line in condensation chamber 6 be down to threaded cap 2.According to ice cube in condensation chamber 6
The variation for melting situation and water level line, makes corresponding measure to condenser pipe；The design of dual-layer vacuum glass outer tube 5 is using very
Empty heat-insulated principle minimizes the energy loss of mixture of ice and water in condensation chamber 6, improves the primary use time on the rocks, makes
The work of condenser pipe continuous high-efficient.
Claims (7)
1. a kind of condenser pipe for being removably used for biomass collection thermal cracking oil, which is characterized in that described one kind is detachable
The condenser pipe for biomass collection thermal cracking oil include threaded cap (2), it is barb (3), inner tube fixed bracket (4), double-deck true
Empty outer glass tube (5), cold-storage material, spherical glass inner tube (7), glass three-way (10) and receiving flask (13)；
The spherical glass inner tube (7) is packed into wherein from the top of dual-layer vacuum glass outer tube (5), spherical glass inner tube (7)
Lower end conical outer wall and the inner wall at end of dual-layer vacuum glass outer tube (5) connect, inner tube fixed bracket (4) passes through inner tube
Fixed bracket inner ring (14) are sleeved on the junction of first inner tube ball bubble and exhaust outlet (1) of spherical glass inner tube (7), inner tube
The inner tube of fixed bracket (4) fixed bracket T shape part (16) is connect with the barb (3) on dual-layer vacuum glass outer tube (5) inner wall,
Cold-storage material is fitted between spherical glass inner tube (7) and dual-layer vacuum glass outer tube (5) and is formed by condensation chamber (6), threaded cap
(2) it is sleeved on the air inlet (1) of spherical glass inner tube (7) and is threadedly coupled with the top of dual-layer vacuum glass outer tube (5), ball
The inner wall of shape glass inner tube (7) end cone outer wall and the interior interface tube (17) of glass three-way (10) upper end connects, glass
The vial interface (18) of threeway (10) lower end and the bottleneck of receiving flask (13) upper end connect.
2. a kind of condenser pipe for being removably used for biomass collection thermal cracking oil described in accordance with the claim 1, feature exist
In the dual-layer vacuum glass outer tube (5) includes tube body, the identical barb (3) of 3 structures, discharge outlet (8) and solid wedge
Shape ground glass interface (11)；
The tube body is formed by connecting by the cylinder of upper end and the conical shell of lower end, the rotating shaft of cylinder and conical shell
Line is conllinear, and the upper end of tube body is provided with external screw thread identical with threaded cap (2) structure；Inboard wall of tube body is equably provided with 3 knots
The identical barb (3) with groove for inner tube fixed bracket T shape part (16) connection with inner tube fixed bracket (4) of structure,
The height of barb (3) is lower than place horizontal plane after inner tube fixed bracket inner ring (14) installation of inner tube fixed bracket (4), conical shell
The discharge outlet (8) for discharging extra water in condensation chamber (6) is provided on body；It bores dual-layer vacuum glass outer tube (5) end
Shape shell end is provided with solid wedge ground glass interface (11), solid wedge mill in discharge outlet (8) between branch pipe root
The rotation conllinear of sand glass interface (11) and conical shell.
3. a kind of condenser pipe for being removably used for biomass collection thermal cracking oil, feature exist according to claim 2
In it is taper in dual-layer vacuum glass outer tube (5) that the solid wedge ground glass interface (11), which is hollow glass cone part,
A part of shell, in the taper of the outer conical surface of solid wedge ground glass interface (11) and dual-layer vacuum glass outer tube (5)
The taper of conical shell is equal, and a tapered centre through-hole is provided at the center of solid wedge ground glass interface (11), in
The rotation conllinear of heart conical through-hole and outer conical surface, taper and the end cone under spherical glass inner tube (7) of tapered centre through-hole
The taper of body is equal, and the top surface of solid wedge ground glass interface (11) is spherical surface, the corresponding centre of sphere of the spherical surface and double-layer vacuum
Outer glass tube (5) central axis is conllinear, and with where discharge outlet (8) branch and dual-layer vacuum glass outer tube (5) intersection
The bottom surface of connection, spherical surface and branch where discharge outlet (8) is tangent.
4. a kind of condenser pipe for being removably used for biomass collection thermal cracking oil, feature exist according to claim 2
In the identical barb (3) of 3 structures is set on the inner wall of dual-layer vacuum glass outer tube (5), and three structures are identical
Barb (3) is in the same plane vertical with dual-layer vacuum glass outer tube (5) axis of rotation；Barb (3) global shape uses
Tri-prismoid structure, three sides of barb (3) are respectively horizontal plane, vertical plane and inclined surface, inclined surface and horizontal plane phase
Friendship is formed by seamed edge and is connected with the inner wall of dual-layer vacuum glass outer tube (5), is provided on vertical plane for fixing with inner tube
The horizontal groove that bracket T shape part (16) links.
5. a kind of condenser pipe for being removably used for biomass collection thermal cracking oil described in accordance with the claim 1, feature exist
In the spherical glass inner tube (7) includes exhaust outlet (1), 3~6 ball bubbles and wedge-shaped ground glass interface (9)；
The spherical glass inner tube (7) is single-glass inner tube, and the row of straight tube-like is provided at the top of spherical glass inner tube (7)
Port (1), the middle part of spherical glass inner tube (7) is joined end to end by 3~6 glass sky balls to be connect, 3~6 glass sky balls and exhaust
It is identical that the sphere center position for first glass marble that the rotation conllinear of mouth (1) is connected with exhaust outlet (1) is higher than 3 structures
Barb (3) where plane, the terminal position of the last one glass marble is higher than on dual-layer vacuum glass outer tube (5) conical shell
Plane where holding；The wedge-shaped ground glass interface (9) of spherical glass inner tube (7) end is divided into two sections, wherein upper end
Taper is less than the taper of lower end and matches with the taper of the central through hole of solid wedge ground glass interface (11), the cone of lower end
It spends and matches with the taper of the interior interface tube (17) of glass three-way (10).
6. a kind of condenser pipe for being removably used for biomass collection thermal cracking oil described in accordance with the claim 1, feature exist
In the inner tube fixed bracket (4) is using circular ring structure part made of flexible silica gel material, the fixed bracket of inner tube
(4) it is made of inner tube fixed bracket inner ring (14), inner tube fixed bracket outer ring (15) connecting rod identical with 3 root knot structures, inner tube
The internal diameter of fixed bracket inner ring (14) is equal to the outer diameter of exhaust outlet (1) in spherical glass inner tube (7) and is sleeved on first inner tube
The junction of ball bubble and exhaust outlet (1)；Fixed bracket outer ring (15) diameter of inner tube is equal to the inner wall of dual-layer vacuum glass outer tube (5)
Diameter, the identical connecting rod of 3 root knot structures is in the circumference side of inner tube fixed bracket inner ring (14) and inner tube fixed bracket outer ring (15)
It is inwardly uniformly distributed, one end of the identical connecting rod of 3 root knot structures and inner tube fixed bracket inner ring (14) connection, the identical company of 3 root knot structures
The other end and inner tube of extension bar fixed bracket outer ring (15) connection, the identical connecting rod of 3 root knot structures and the fixed bracket outer ring of inner tube
(15) inner tube fixed bracket T shape part (16) connected into is connect with the barb (3) on dual-layer vacuum glass outer tube (5) inner wall.
7. a kind of condenser pipe for being removably used for biomass collection thermal cracking oil described in accordance with the claim 1, feature exist
In, the glass three-way (10) include the interior interface tube (17) of upper end, middle section isodiametric annulus cylinder and lower end receipts
Collect bottle interface (18), interior interface tube (17) and receiving flask interface (18) are all wedge-shaped annulus cone, glass three-way (10) upper end
Interior interface tube (17) taper be equal to spherical glass inner tube (7) end taper, receiving flask interface (18) taper be equal to collect
The taper of bottle (13) bottleneck；The lower end of interior interface tube (17) is connected with the upper end of annulus cylinder, annulus cylinder lower end and receipts
The upper end of collection bottle interface (18) is connected；The diameter of the interior interface tube (17) of glass three-way (10) upper end is greater than the collection of lower end
The diameter of bottle interface (18), the diameter of the receiving flask interface (18) of lower end are less than the bottleneck diameter of receiving flask (13), middle section etc.
The middle part of the annulus cylinder of diameter is obliquely provided with air inlet pipe (12), while branch pipe uses obliquely where air inlet (12)
The interface surface of extension pipe, interior interface tube (17), receiving flask interface (18) and receiving flask (13) is all made of ground glass face.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910592975.0A CN110157491B (en) | 2019-07-03 | 2019-07-03 | Detachable condenser pipe for collecting biomass thermal cracking oil |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910592975.0A CN110157491B (en) | 2019-07-03 | 2019-07-03 | Detachable condenser pipe for collecting biomass thermal cracking oil |
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| CN110157491A true CN110157491A (en) | 2019-08-23 |
| CN110157491B CN110157491B (en) | 2024-02-09 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114949908A (en) * | 2022-06-17 | 2022-08-30 | 河南工业大学 | Online acquisition system for liquid-phase product in thermal conversion process of organic solid |
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| CN203861952U (en) * | 2014-05-19 | 2014-10-08 | 内蒙古民族大学 | Condensing equipment for extracting casein |
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| CN107643000A (en) * | 2017-10-30 | 2018-01-30 | 叶玉妹 | A kind of self-loopa condenser pipe |
| CN207816021U (en) * | 2018-01-25 | 2018-09-04 | 郑州大学 | Condenser pipe |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000081292A (en) * | 1998-09-07 | 2000-03-21 | Gl Sciences Inc | Condenser in organic solvent collector |
| CN203861952U (en) * | 2014-05-19 | 2014-10-08 | 内蒙古民族大学 | Condensing equipment for extracting casein |
| CN106370552A (en) * | 2016-11-04 | 2017-02-01 | 北京林业大学 | On-line analysis experiment device for biomass microwave pyrolysis refining and method of on-line analysis experiment device |
| CN107643000A (en) * | 2017-10-30 | 2018-01-30 | 叶玉妹 | A kind of self-loopa condenser pipe |
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| CN114949908A (en) * | 2022-06-17 | 2022-08-30 | 河南工业大学 | Online acquisition system for liquid-phase product in thermal conversion process of organic solid |
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| CN110157491B (en) | 2024-02-09 |
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