CN110152579A - A kind of ultrasonic disperse polymerization reaction kettle - Google Patents

A kind of ultrasonic disperse polymerization reaction kettle Download PDF

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Publication number
CN110152579A
CN110152579A CN201910487418.2A CN201910487418A CN110152579A CN 110152579 A CN110152579 A CN 110152579A CN 201910487418 A CN201910487418 A CN 201910487418A CN 110152579 A CN110152579 A CN 110152579A
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CN
China
Prior art keywords
reaction kettle
angular wheel
sleeve column
kettle shell
ultrasonic disperse
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201910487418.2A
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Chinese (zh)
Inventor
徐永江
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Maanshan Spore Mechanics Technology Service Co Ltd
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Maanshan Spore Mechanics Technology Service Co Ltd
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Priority to CN201910487418.2A priority Critical patent/CN110152579A/en
Publication of CN110152579A publication Critical patent/CN110152579A/en
Withdrawn legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/10Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing sonic or ultrasonic vibrations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00054Controlling or regulating the heat exchange system
    • B01J2219/00056Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058Temperature measurement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00092Tubes

Abstract

The invention discloses a kind of ultrasonic disperse polymerization reaction kettles, including reaction kettle shell and motor, the inside of the reaction kettle shell, which is run through, is connected with regulating device, the upper and lower surface of the slide plate offers the first sliding rail, second rotating bar is welded and connected with agitating plate far from one end of slide plate, one end face of the separate slide plate of the agitating plate is welded and connected with fixed link, the outer surface of the slide plate is welded and connected with sliding block, the agitating plate is set in the outer surface of regulating device, the left upper end and bottom righthand side of the reaction kettle shell are threaded with feeding pipe and discharge nozzle respectively, it is bolted to connection between the lower end and regulating device of the Rotational Cylindrical.The ultrasonic disperse polymerization reaction kettle convenient for carrying out adequately uniform stirring to material, while also avoiding the inner wall adhesion of material Yu reaction kettle shell, influence reaction, and conveniently the temperature of the inside of reaction kettle shell is regulated and controled in time, convenient for improving working efficiency, guarantee going on smoothly for reaction.

Description

A kind of ultrasonic disperse polymerization reaction kettle
Technical field
The present invention relates to ultrasonic disperse polymerization reaction kettle technical field, specially a kind of ultrasonic disperse polymerization reaction kettle.
Background technique
Polymer reaction monomer meeting neither endothermic nor exothermic, the selection of the control of temperature to reactive material in polymerization process Property and yield have a great role, and during the reaction, when beginning needs to heat up induced reaction polymer reaction monomer, into anti- It answers again highly exothermic after process, needs quickly to remove heat, and the ultrasonic wave of ultrasonic disperse polymerization reaction kettle, it is poly- convenient for improving Closing object dispersion is in monomer, improves working efficiency.
But general ultrasonic disperse polymerization reaction kettle is at work, there are the following problems:
1, inconvenient that adequately uniform stirring is carried out to material, cause reaction speed low;
2, also inconvenient that the inner wall adhesion situation of material and reaction kettle shell is handled;
3, the temperature of the inconvenient inside to reaction kettle shell carries out control stable in time, influences the problem of reaction uses, is We have proposed a kind of ultrasonic disperse polymerization reaction kettles for this, for solving the above problems.
Summary of the invention
It is mentioned above in the background art to solve the purpose of the present invention is to provide a kind of ultrasonic disperse polymerization reaction kettle General ultrasonic disperse polymerization reaction kettle, it has not been convenient to adequately uniform stirring be carried out to material, cause reaction speed low, together When it is also inconvenient the inner wall adhesion situation of material and reaction kettle shell is handled, and it is inconvenient in reaction kettle shell The temperature in portion carries out control stable in time, influences the problem of reaction uses.
To achieve the above object, the invention provides the following technical scheme: a kind of ultrasonic disperse polymerization reaction kettle, including reaction Kettle shell and motor, the inside of the reaction kettle shell, which is run through, is connected with regulating device, and cunning is arranged in the middle part of regulating device Plate, the upper and lower surface of the slide plate offers the first sliding rail, and the internal slide of the first sliding rail is connected with the second rotating bar, institute It states the second rotating bar and is welded and connected with agitating plate far from one end of slide plate, and the left and right ends of agitating plate are fixedly installed with cleaning One end face of scraper plate, the separate slide plate of the agitating plate is welded and connected with fixed link, and strainer is fixedly installed in fixed link, institute The outer surface for stating slide plate is welded and connected with sliding block, and sliding block is slidably connected on the inner wall of reaction kettle shell, the agitating plate It is set in the outer surface of regulating device, the left upper end and bottom righthand side of the reaction kettle shell are threaded with feeding pipe respectively and go out Expects pipe, and the upper center of reaction kettle shell passes through spiral shell between the lower end and regulating device of the Rotational Cylindrical through there is Rotational Cylindrical Bolt is fixedly connected, and the upper end of Rotational Cylindrical has been bolted to connection motor, and the Rotational Cylindrical is applied in the inside of sleeve, and Sleeve is slidably connected on limit plate by the second sliding rail, and the left and right ends of the limit plate are fixedly connected to electric expansion Bar, and the lower end of electric telescopic rod is fixedly mounted on the upper end face of reaction kettle shell, the upper end of the sleeve is welded and connected with Second angular wheel, and the inside of the second angular wheel is arranged through Rotational Cylindrical, the rear side of second angular wheel is connected with There is support frame, and support frame is fixedly mounted on reaction kettle upper surface of outer cover, the upper end of support frame as described above is equipped with motor, and supports The left and right ends of frame are fixedly connected with stainless steel tube, the second hose are threaded in the middle part of the stainless steel tube, and second is soft It manages and is fitted with adjusting rod close to the side of Rotational Cylindrical, the adjusting rod level is applied in the middle part of support frame, and before support frame Side is rotatably equipped with the first angular wheel, and the lower end of the stainless steel tube is applied in the inside of leakproof block, and stainless steel tube is located at The left and right sides of regulating device, the leakproof block are fixedly mounted on the upper surface of reaction kettle shell, and the left and right sides of leakproof block Threaded rod and gag lever post are extended through, the lower end of the stainless steel tube is fixedly connected with the first hose, and under the first hose End is fixedly connected with screen pipe, and the left and right ends of screen pipe extend through and are connected with threaded rod and gag lever post.
Preferably, the regulating device includes the first sleeve column, the first rotating bar and the second sleeve column, the first sleeve column and second set The inside of column, which is run through, is connected with the first rotating bar, and the upper end of the first rotating bar has been bolted to connection Rotational Cylindrical, and first The lower end of rotating bar is rotatably connected on the inner wall lower end of reaction kettle shell, and the upper end of the first sleeve column is fixed on the upper of reaction kettle shell Inner wall is held, the lower end of the first rotating bar is fixedly connected on the lower end inner wall of reaction kettle shell.
Preferably, the length dimension of first sleeve column and the second sleeve column is equal, and the cross of the first sleeve column and the second sleeve column Cross-sectional sizes size is greater than the cross section size dimension of the first rotating bar, the first sleeve column, the first rotating bar and the second sleeve column it is outer Surface is in thread-like structure, and the spacing dimension of the first sleeve column and the second sleeve column is equal to the length dimension of the first sleeve column.
Preferably, the slide plate and the rounded structure of agitating plate, and slide plate and agitating plate are in Openworks shape structure, and The cross-sectional diameter size of slide plate is greater than the cross-sectional diameter size of agitating plate.
Preferably, the screen pipe and leakproof block are to be threadedly coupled, and screen pipe passes through with the connection type of threaded rod Threaded rod constitutes lifting structure on leakproof block.
Preferably, the T-shaped structure in the longitudinal section of the screen pipe, and the lower end of screen pipe is in Openworks shape spherical junctions Structure.
Preferably, the connection type of the sleeve and Rotational Cylindrical is engagement connection, and sleeve and the second angular wheel are constituted Weldedization structure, and the second angular wheel constitutes rotational structure by sleeve on limit plate.
Preferably, first angular wheel is to engage connection, and the second angular wheel and first with the second angular wheel Angular wheel is vertical setting, and the second angular wheel constitutes lifting structure on limit plate.
Preferably, the connection type of the adjusting rod and the first angular wheel connects for engagement, and adjusting rod and adjusting block Constitute 2 the second hoses that the sum of weldedization structure, and length dimension of adjusting rod and adjusting block are equal to the left and right sides Minimum spacing size.
Preferably, the adjusting block is in half cylindrical structure, and the height dimension of adjusting block is less than the height of the second hose Size.
Compared with prior art, the beneficial effects of the present invention are: the ultrasonic disperse polymerization reaction kettle, is convenient for carrying out material Adequately uniform stirring, while the inner wall adhesion of material Yu reaction kettle shell is also avoided, it influences to react, and conveniently to reaction The temperature of the inside of kettle shell is regulated and controled in time, convenient for improving working efficiency, guarantees going on smoothly for reaction;
1, it is equipped with regulating device, slide plate and agitating plate, drives slide plate to be gone up and down when the first rotating bar rotates, consequently facilitating to stirring It mixes plate to be pushed and pulled, facilitates agitating plate to be rotated on the first sleeve column or the second sleeve column, facilitate full and uniform stirring, mention High reaction speed;
2, it is equipped with agitating plate and scraper cleaner, agitating plate is rotated and gone up and down in the outer surface of the second sleeve column, consequently facilitating clearly Scraper plate is swept adequately to be contacted with the inner wall of reaction kettle shell, it is convenient that the material of the inner wall of reaction kettle shell is purged, Avoid adhesion, influence using;
3, it is equipped with the second angular wheel, the first angular wheel and adjusting rod, the second angular wheel constitutes lifting knot on limit plate Structure, consequently facilitating adjust the second angular wheel height, convenient for control the second angular wheel and the first angular wheel connection or Person is not connected to, consequently facilitating adjusting rod is driven to slide left and right, facilitates the connected state of the second hose of the control left and right sides, It is conveniently discharged into heat or takes heat away.
Detailed description of the invention
Fig. 1 is that the present invention faces the schematic diagram of the section structure;
Fig. 2 is enlarged structure schematic diagram at A in Fig. 1 of the present invention;
Fig. 3 is enlarged structure schematic diagram at B in Fig. 1 of the present invention;
Fig. 4 is the overlooking structure diagram of slide plate of the present invention;
Fig. 5 is the overlooking structure diagram of agitating plate of the present invention;
Fig. 6 connects overlooking structure diagram with limit plate for Rotational Cylindrical of the present invention;
Fig. 7 is adjusting rod overall structure diagram of the present invention;
Fig. 8 is regulating device structural schematic diagram of the present invention;
Fig. 9 is workflow schematic diagram of the present invention.
In figure: 1, reaction kettle shell;2, regulating device;201, the first sleeve column;202, the first rotating bar;203, second set Column;3, slide plate;4, the first sliding rail;5, sliding block;6, agitating plate;7, the second rotating bar;8, scraper cleaner;9, strainer;10, fixed Bar;11, feeding pipe;12, leakproof block;13, stainless steel tube;14, the first hose;15, screen pipe;16, gag lever post;17, threaded rod; 18, the second angular wheel;19, sleeve;20, limit plate;21, electric telescopic rod;22, Rotational Cylindrical;23, the first angular wheel;24, Adjusting rod;25, adjusting block;26, the second hose;27, motor;28, support frame;29, discharge nozzle;30, the second sliding rail.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
Fig. 1-9 is please referred to, the present invention provides a kind of technical solution: a kind of ultrasonic disperse polymerization reaction kettle, including reaction kettle Shell 1, slide plate 3, the first sliding rail 4, sliding block 5, agitating plate 6, the second rotating bar 7, scraper cleaner 8, strainer 9, is consolidated regulating device 2 Fixed pole 10, feeding pipe 11, leakproof block 12, stainless steel tube 13, the first hose 14, screen pipe 15, gag lever post 16, threaded rod 17, Two angular wheels 18, limit plate 20, electric telescopic rod 21, Rotational Cylindrical 22, the first angular wheel 23, adjusting rod 24, are adjusted sleeve 19 Locking nub 25, the second hose 26, motor 27, support frame 28, discharge nozzle 29 and the second sliding rail 30, the inside of reaction kettle shell 1 are run through It is connected with regulating device 2, and the middle part of regulating device 2 is arranged with slide plate 3, the upper and lower surface of slide plate 3 offers the first sliding rail 4, and the internal slide of the first sliding rail 4 is connected with the second rotating bar 7, the second rotating bar 7 is welded and connected with far from one end of slide plate 3 Agitating plate 6, and the left and right ends of agitating plate 6 are fixedly installed with scraper cleaner 8, an end face weld of the separate slide plate 3 of agitating plate 6 It is connected to fixed link 10 in succession, and is fixedly installed with strainer 9 in fixed link 10, the outer surface of slide plate 3 is welded and connected with sliding block 5, and For sliding block 5 to be slidably connected on the inner wall of reaction kettle shell 1, agitating plate 6 is set in the outer surface of regulating device 2, outside reaction kettle The left upper end and bottom righthand side of shell 1 are threaded with feeding pipe 11 and discharge nozzle 29 respectively, and the upper center of reaction kettle shell 1 is passed through It is installed with Rotational Cylindrical 22, is bolted to connection between the lower end and regulating device 2 of Rotational Cylindrical 22, and the upper end of Rotational Cylindrical 22 is logical It crosses bolt and is fixedly connected with motor 27, Rotational Cylindrical 22 is applied in the inside of sleeve 19, and sleeve 19 is being limited by the second sliding rail 30 To be slidably connected on the plate 20 of position, the left and right ends of limit plate 20 are fixedly connected to electric telescopic rod 21, and electric telescopic rod 21 Lower end be fixedly mounted on the upper end face of reaction kettle shell 1, the upper end of sleeve 19 is welded and connected with the second angular wheel 18, and Through Rotational Cylindrical 22 is connected with, the rear side of the second angular wheel 18 is provided with support frame 28 for the inside of second angular wheel 18, and Support frame 28 is fixedly mounted on 1 upper surface of reaction kettle shell, and the upper end of support frame 28 is equipped with motor 27, and a left side for support frame 28 Right both ends are fixedly connected with stainless steel tube 13, and the middle part of stainless steel tube 13 is threaded with the second hose 26, and the second hose 26 Side close to Rotational Cylindrical 22 is fitted with adjusting rod 24, and 24 level of adjusting rod is applied in the middle part of support frame 28, and support frame 28 Front side be rotatably equipped with the first angular wheel 23, the lower end of stainless steel tube 13 is applied in the inside of leakproof block 12, and stainless steel Pipe 13 is located at the left and right sides of regulating device 2, and leakproof block 12 is fixedly mounted on the upper surface of reaction kettle shell 1, and leakproof block 12 The left and right sides extended through threaded rod 17 and gag lever post 16, the lower end of stainless steel tube 13 is fixedly connected with the first hose 14, And first the lower end of hose 14 be fixedly connected with screen pipe 15, and the left and right ends of screen pipe 15 extend through and are connected with screw thread Bar 17 and gag lever post 16.
As in Fig. 1 and Fig. 8 regulating device 2 include the first sleeve column 201, the first rotating bar 202 and the second sleeve column 203, first The inside of sleeve column 201 and the second sleeve column 203, which is run through, is connected with the first rotating bar 202, and the upper end of the first rotating bar 202 passes through spiral shell Bolt is fixedly connected with Rotational Cylindrical 22, and the lower end of the first rotating bar 202 is rotatably connected on the inner wall lower end of reaction kettle shell 1, and first The upper end of sleeve column 201 is fixed on the upper end inner wall of reaction kettle shell 1, and the lower end of the first rotating bar 202 is fixedly connected on reaction kettle The lower end inner wall of shell 1, the first rotating bar 202 rotate when, convenient for drive slide plate 3 gone up and down, consequently facilitating to agitating plate 6 into Row pushes up, and agitating plate 6 and the first sleeve column 201 or the second sleeve column 203 is facilitated to carry out threaded connection rotation, convenient sufficient Stirring improves working efficiency, as the length dimension of the first sleeve column 201 and the second sleeve column 203 is equal in Fig. 1 and Fig. 8, and first set The cross section size dimension of column 201 and the second sleeve column 203 is greater than the cross section size dimension of the first rotating bar 202, the first sleeve column 201, the outer surface of the first rotating bar 202 and the second sleeve column 203 is in thread-like structure, and the first sleeve column 201 and the second sleeve column 203 spacing dimension is equal to the length dimension of the first sleeve column 201, and the convenient path gone up and down to slide plate 3 controls, and avoids strainer The inner wall of 9 extrusion damage reaction kettle shells 1.
Such as Fig. 1, Fig. 4 and Fig. 6 middle slide plate 3 and the rounded structure of agitating plate 6, and slide plate 3 and agitating plate 6 are in Openworks shape Structure, and the cross-sectional diameter size of slide plate 3 is greater than the cross-sectional diameter size of agitating plate 6, it is convenient to reaction kettle shell 1 Internal material is adequately stirred, and convenient connection up and down avoids accumulating, influences to mix, such as screen pipe 15 in Fig. 1 and Fig. 2 It is to be threadedly coupled, and screen pipe 15 passes through threaded rod 17 on leakproof block 12 with the connection type of threaded rod 17 with leakproof block 12 Lifting structure is constituted, facilitates the depth of the material of the inside according to reaction kettle shell 1, the height of regulation filtering tube 15 conveniently makes With.
Such as the T-shaped structure in longitudinal section of screen pipe 15 in Fig. 1 and Fig. 2, and the lower end of screen pipe 15 is in Openworks shape ball Shape structure, it is convenient that material is filtered, avoid material from entering the inside of stainless steel tube 13, such as Fig. 1, Fig. 3 and Fig. 6 middle sleeve 19 and the connection type of Rotational Cylindrical 22 be engagement connection, and sleeve 19 and the second angular wheel 18 constitute weldedization structure, And the second angular wheel 18 constitutes rotational structure on limit plate 20 by sleeve 19, convenient for passing through the rotation band of Rotational Cylindrical 22 Dynamic second angular wheel 18 rotation facilitates the left and right position for adjusting adjusting rod 24 consequently facilitating driving the rotation of the first angular wheel 23 It sets, is easy to use, as the first angular wheel 23 is to engage connection, and second bores with the second angular wheel 18 in Fig. 1, Fig. 3 and Fig. 6 Shape gear 18 and the first angular wheel 23 are vertical setting, and the second angular wheel 18 constitutes lifting knot on limit plate 20 Structure is easy to use convenient for adjusting the rotation and stopping of the first angular wheel 23 of control.
If the connection type of adjusting rod 24 in Fig. 1, Fig. 3 and Fig. 7 and the first angular wheel 23 is engagement connection, and adjusting rod 24 and adjusting block 25 constitute the sum of weldedization structure, and length dimension of adjusting rod 24 and adjusting block 25 be equal to left and right two The minimum spacing size of 2 the second hoses 26 of side, by the position of left and right adjusting adjusting rod 24, consequently facilitating to the second hose 26, which carry out extruding, does not squeeze perhaps convenient for inputting hot water heating or input cold water to the inside of reaction kettle shell 1, convenient for control Equilibrium temperature, if adjusting block 25 is in half cylindrical structure in Fig. 7, and the height dimension of adjusting block 25 is less than the height of the second hose 26 Size is spent, it is convenient that second hose 26 is squeezed, while being also convenient for protecting the second hose 26, it avoids damaging.
Working principle: when using the ultrasonic disperse polymerization reaction kettle, material is drained into instead by feeding pipe 11 first The inside for answering kettle shell 1 needs the depth dimensions of material to be reacted according to the inside of reaction kettle shell 1, to the height of screen pipe 15 The phenomenon that degree size is adjusted, convenient when injecting water to the inside of reaction kettle shell 1, avoids the occurrence of splashing, influences material Reaction, then threaded rod 17 is rotated on leakproof block 12, consequently facilitating regulation filtering tube 15 is upper in gag lever post 16 It sets, easy of rise regulation filtering tube 15, then the power switch of motor 27 is opened, motor 27 drives first turn by Rotational Cylindrical 22 Lever 202 is rotated, and the slide plate 3 being threadedly coupled with the first rotating bar 202 is by sliding block 5 in reaction kettle shell 1 Elevating movement is carried out on wall, to upwardly or downwardly pushed and pulled to agitating plate 6 by the second rotating bar 7, agitating plate 6 and the The connection type of one sleeve column 201 or the second sleeve column 203 is to be threadedly coupled, consequently facilitating agitating plate 6 is revolved on slide plate 3 Turn, it is convenient that the material of the inside of reaction kettle shell 1 is adequately stirred, it is easy to use;
Temperature sensor is monitored the temperature of the inside of reaction kettle shell 1 simultaneously, when temperature exceeds defined temperature, temperature Degree sensor transmits a signal to central processing unit, and central processing unit is opened the power switch of just electric telescopic rod 21, closed simultaneously The switch of motor 27 is closed, consequently facilitating having upwards thrust to limit plate 20, facilitates the second angular wheel 18 and the first angular wheel 23 are engaged connection, then the power switch of motor 27 is opened, and drive adjusting rod 24 to carry out when the first angular wheel 23 rotates Sliding, consequently facilitating pushing to adjusting block 25, facilitates adjusting block 25 to squeeze the second hose 26 of side, convenient another Second hose 26 of side keeps the state of connection, opens the switch of the external aspiration pump of stainless steel tube 13, convenient for taking heat away, side Just the temperature for adjusting the inside of reaction kettle shell 1, when the temperature of the inside of reaction kettle shell 1 is lower, same method is adjusted Motor 27 rotates backward, and the convenient stainless steel tube 13 by the other side injects heat, is easy to use, after temperature is adjusted, electricity Dynamic telescopic rod 21 is shunk, and is avoided the first angular wheel 23 from contacting with the second angular wheel 18, is continued the inside to reaction kettle shell 1 Carry out uniform stirring reaction;
Scraper cleaner 8 is bonded with the inner wall of reaction kettle shell 1, convenient to be purged to the inner wall of reaction kettle shell 1, avoids gluing Even, influence using, after the completion of final reaction, reactor product be discharged from discharge nozzle 29 collect and electricity used above The model XD-60KTYZ of machine 27, facilitates adjusting positive and negative rotation, and here it is the whole process that ultrasonic disperse polymerization reaction kettle uses.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (10)

1. a kind of ultrasonic disperse polymerization reaction kettle, including reaction kettle shell (1) and motor (27), it is characterised in that: the reaction The inside of kettle shell (1), which is run through, to be connected with regulating device (2), and slide plate (3), the cunning are arranged in the middle part of regulating device (2) The upper and lower surface of plate (3) offers the first sliding rail (4), and the internal slide of the first sliding rail (4) is connected with the second rotating bar (7), second rotating bar (7) is welded and connected with agitating plate (6) far from the one end of slide plate (3), and the left and right two of agitating plate (6) End is fixedly installed with scraper cleaner (8), and an end face of the separate slide plate (3) of the agitating plate (6) is welded and connected with fixed link (10), it and in fixed link (10) being fixedly installed with strainer (9), the outer surface of the slide plate (3) is welded and connected with sliding block (5), and Sliding block (5) is slidably connected on the inner wall of reaction kettle shell (1), and the agitating plate (6) is set in the appearance of regulating device (2) Face;
The left upper end and bottom righthand side of the reaction kettle shell (1) are threaded with feeding pipe (11) and discharge nozzle (29) respectively, and The upper center of reaction kettle shell (1), which runs through, to be had Rotational Cylindrical (22), between the lower end and regulating device (2) of the Rotational Cylindrical (22) It is bolted to connection, and the upper end of Rotational Cylindrical (22) has been bolted to connection motor (27), the Rotational Cylindrical (22) It is applied in the inside of sleeve (19), and sleeve (19) is slidably connected on limit plate (20) by the second sliding rail (30), it is described The left and right ends of limit plate (20) are fixedly connected to electric telescopic rod (21), and the lower end of electric telescopic rod (21) is fixedly mounted The upper end of upper end face in reaction kettle shell (1), the sleeve (19) is welded and connected with the second angular wheel (18), and second The inside of angular wheel (18) is provided with support frame on rear side of second angular wheel (18) through being connected with Rotational Cylindrical (22) (28), and support frame (28) is fixedly mounted on reaction kettle shell (1) upper surface, and the upper end of support frame as described above (28) is equipped with motor (27), and the left and right ends of support frame (28) are fixedly connected with stainless steel tube (13);
It is threaded with the second hose (26) in the middle part of the stainless steel tube (13), and the second hose (26) is close to Rotational Cylindrical (22) Side be fitted with adjusting rod (24), adjusting rod (24) level is applied in the middle part of support frame (28), and support frame (28) Front side be rotatably equipped with the first angular wheel (23), the lower end of the stainless steel tube (13) is applied in the interior of leakproof block (12) Portion, and stainless steel tube (13) is located at the left and right sides of regulating device (2), the leakproof block (12) is fixedly mounted on reaction kettle shell (1) upper surface, and threaded rod (17) and gag lever post (16), the stainless steel have been extended through at left and right sides of leakproof block (12) The lower end of pipe (13) is fixedly connected with the first hose (14), and the lower end of the first hose (14) is fixedly connected with screen pipe (15), And the left and right ends of screen pipe (15), which extend through, is connected with threaded rod (17) and gag lever post (16).
2. a kind of ultrasonic disperse polymerization reaction kettle according to claim 1, it is characterised in that: regulating device (2) packet Include the first sleeve column (201), the first rotating bar (202) and the second sleeve column (203), the first sleeve column (201) and the second sleeve column (203) Through being connected with the first rotating bar (202), the upper end of the first rotating bar (202) has been bolted to connection Rotational Cylindrical for inside (22), the lower end of the first rotating bar (202) is rotatably connected on the inner wall lower end of reaction kettle shell (1), the first sleeve column (201) it is upper End is fixed on the upper end inner wall of reaction kettle shell (1), and the lower end of the first rotating bar (202) is fixedly connected on reaction kettle shell (1) Lower end inner wall.
3. a kind of ultrasonic disperse polymerization reaction kettle according to claim 2, it is characterised in that: first sleeve column (201) It is equal with the length dimension of the second sleeve column (203), and the cross section size dimension of the first sleeve column (201) and the second sleeve column (203) Greater than the cross section size dimension of the first rotating bar (202), the first sleeve column (201), the first rotating bar (202) and the second sleeve column (203) outer surface is in thread-like structure, and the spacing dimension of the first sleeve column (201) and the second sleeve column (203) is equal to first The length dimension of sleeve column (201).
4. a kind of ultrasonic disperse polymerization reaction kettle according to claim 1, it is characterised in that: the slide plate (3) and stirring The rounded structure of plate (6), and slide plate (3) and agitating plate (6) they are in Openworks shape structure, and the cross-sectional diameter of slide plate (3) Size is greater than the cross-sectional diameter size of agitating plate (6).
5. a kind of ultrasonic disperse polymerization reaction kettle according to claim 1, it is characterised in that: the screen pipe (15) and anti- Leakage block (12) is to be threadedly coupled, and screen pipe (15) passes through threaded rod (17) in leakproof block with the connection type of threaded rod (17) (12) lifting structure is constituted on.
6. a kind of ultrasonic disperse polymerization reaction kettle according to claim 1, it is characterised in that: the screen pipe (15) is indulged The T-shaped structure in section, and the lower end of screen pipe (15) is in Openworks shape spherical structure.
7. a kind of ultrasonic disperse polymerization reaction kettle according to claim 1, it is characterised in that: the sleeve (19) and rotation The connection type of column (22) is engagement connection, and sleeve (19) and the second angular wheel (18) constitute weldedization structure, and And second angular wheel (18) constitute rotational structure on limit plate (20) by sleeve (19).
8. a kind of ultrasonic disperse polymerization reaction kettle according to claim 1, it is characterised in that: first angular wheel It (23) is to engage connection with the second angular wheel (18), and the second angular wheel (18) and the first angular wheel (23) is perpendicular sets It sets, and the second angular wheel (18) constitutes lifting structure on limit plate (20).
9. a kind of ultrasonic disperse polymerization reaction kettle according to claim 1, it is characterised in that: the adjusting rod (24) and The connection type of one angular wheel (23) is engagement connection, and adjusting rod (24) and adjusting block (25) constitute weldedization knot Structure, and the sum of length dimension of adjusting rod (24) and adjusting block (25) is equal to 2 the second hoses (26) of the left and right sides most Small spacing dimension.
10. a kind of ultrasonic disperse polymerization reaction kettle according to claim 9, it is characterised in that: the adjusting block (25) is in Half cylindrical structure, and the height dimension of adjusting block (25) is less than the height dimension of the second hose (26).
CN201910487418.2A 2019-06-05 2019-06-05 A kind of ultrasonic disperse polymerization reaction kettle Withdrawn CN110152579A (en)

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